WO2012145802A3 - Reactor system and method for thermally activating minerals - Google Patents

Reactor system and method for thermally activating minerals Download PDF

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Publication number
WO2012145802A3
WO2012145802A3 PCT/AU2012/000464 AU2012000464W WO2012145802A3 WO 2012145802 A3 WO2012145802 A3 WO 2012145802A3 AU 2012000464 W AU2012000464 W AU 2012000464W WO 2012145802 A3 WO2012145802 A3 WO 2012145802A3
Authority
WO
WIPO (PCT)
Prior art keywords
mineral
chamber
reaction
reactor
feed
Prior art date
Application number
PCT/AU2012/000464
Other languages
French (fr)
Other versions
WO2012145802A2 (en
Inventor
Mark Geoffrey Sceats
Original Assignee
Calix Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from AU2011901545A external-priority patent/AU2011901545A0/en
Application filed by Calix Limited filed Critical Calix Limited
Publication of WO2012145802A2 publication Critical patent/WO2012145802A2/en
Publication of WO2012145802A3 publication Critical patent/WO2012145802A3/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J6/00Heat treatments such as Calcining; Fusing ; Pyrolysis
    • B01J6/001Calcining
    • B01J6/004Calcining using hot gas streams in which the material is moved
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00Compounds of aluminium
    • C01F7/02Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/04Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom
    • C01F7/06Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom by treating aluminous minerals or waste-like raw materials with alkali hydroxide, e.g. leaching of bauxite according to the Bayer process
    • C01F7/0613Pretreatment of the minerals, e.g. grinding
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B11/00Calcium sulfate cements
    • C04B11/02Methods and apparatus for dehydrating gypsum
    • C04B11/028Devices therefor characterised by the type of calcining devices used therefor or by the type of hemihydrate obtained
    • C04B11/0286Suspension heaters for flash calcining, e.g. cyclones
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2/00Lime, magnesia or dolomite
    • C04B2/10Preheating, burning calcining or cooling
    • C04B2/12Preheating, burning calcining or cooling in shaft or vertical furnaces
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B20/00Use of materials as fillers for mortars, concrete or artificial stone according to more than one of groups C04B14/00 - C04B18/00 and characterised by shape or grain distribution; Treatment of materials according to more than one of the groups C04B14/00 - C04B18/00 specially adapted to enhance their filling properties in mortars, concrete or artificial stone; Expanding or defibrillating materials
    • C04B20/02Treatment
    • C04B20/04Heat treatment
    • C04B20/06Expanding clay, perlite, vermiculite or like granular materials
    • C04B20/066Expanding clay, perlite, vermiculite or like granular materials in shaft or vertical furnaces
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B1/00Shaft or like vertical or substantially vertical furnaces
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • Y02P20/129Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/40Production or processing of lime, e.g. limestone regeneration of lime in pulp and sugar mills

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Structural Engineering (AREA)
  • Materials Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Geology (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Seasonings (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

A reactor arrangement and method for thermal activation of a mineral to increase porosity by flash volatilisation of gas from the mineral, comprising: a flash calciner reactor having a reaction chamber and a heating chamber separated by a reactor wall, the reaction chamber and the heating chamber being in heat transfer communication through the reactor wall; a reaction feed comprising the mineral in particulate form entrained in steam passing through the reaction chamber; a heating fluid flow passing through the heating chamber in counterflow to the reaction feed passing through the reaction chamber; whereby the thermal activation of the mineral proceeds by flash volatilisation of gases from the mineral in the reaction feed by means of heat transferred through reactor wall from the counterflow of heating fluid the chamber to the reaction feed, so that temperature of the mineral feed increases to reach a maximum temperature at exhaust of thermally activated mineral from the reactor.
PCT/AU2012/000464 2011-04-27 2012-04-27 Reactor system and method for thermally activating minerals WO2012145802A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AU2011901545A AU2011901545A0 (en) 2011-04-27 System And Method For Thermally Activating Minerals
AU2011901545 2011-04-27

Publications (2)

Publication Number Publication Date
WO2012145802A2 WO2012145802A2 (en) 2012-11-01
WO2012145802A3 true WO2012145802A3 (en) 2013-01-03

Family

ID=47072821

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/AU2012/000464 WO2012145802A2 (en) 2011-04-27 2012-04-27 Reactor system and method for thermally activating minerals

Country Status (1)

Country Link
WO (1) WO2012145802A2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109320107A (en) * 2018-10-26 2019-02-12 辽宁科技大学 Suspension-boiling multithread state combination preparation high activity light calcined magnesia method

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105658580B (en) 2013-10-24 2017-05-31 卡利有限公司 The preparation method and device of hydroxide slurry
EP3074360B1 (en) * 2013-11-29 2020-01-01 Calix Ltd Process for manufacture of portland cement
AU2014374829B2 (en) * 2014-01-02 2018-01-04 Calix Ltd Oxide products formed from calcined carbonate powder for use as biocide, chemical detoxifier and catalyst support products.
CA2966539C (en) 2014-11-18 2023-04-11 Calix Ltd Process and apparatus for manufacture of calcined compounds for the production of calcined products
RU2587115C1 (en) * 2014-12-25 2016-06-10 Открытое акционерное общество "Научно-исследовательский институт металлургической теплотехники" (ОАО "ВНИИМТ") Counterflow shaft furnace for burning carbonaceous materials, heated with gaseous fuel
AU2017282719B2 (en) * 2016-06-20 2021-04-08 Calix Ltd A bioactive material
CN109982775B (en) * 2016-11-22 2022-03-29 奥图泰(芬兰)公司 Method and apparatus for heat treatment in a fluidized bed reactor
CN111099844B (en) * 2020-01-03 2023-06-23 中冶长天国际工程有限责任公司 Multi-row inserting plate type lime shaft kiln material distribution system and material distribution method
CN111620572A (en) * 2020-06-09 2020-09-04 唐山市丰南区金泉冶金能源新技术开发有限公司 Device and process for producing high-activity lime
CN113772971A (en) * 2021-08-20 2021-12-10 中钢集团鞍山热能研究院有限公司 Process and system for preparing high-purity magnesium oxide in low-carbon circulation mode
WO2023064981A1 (en) * 2021-10-18 2023-04-27 Calix Ltd Processes and methods for the production of iron and steel
CA3236967A1 (en) * 2021-11-30 2023-06-08 Cemal Unlu Improvement in a vertical kiln

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007045048A1 (en) * 2005-10-21 2007-04-26 Calix Pty Ltd System and method for calcination/carbonation cycle processing
WO2007112496A1 (en) * 2006-03-31 2007-10-11 Calix Ltd System and method for the calcination of minerals
WO2008061305A1 (en) * 2006-11-22 2008-05-29 Orica Explosives Technology Pty Ltd Integrated chemical process
WO2009010542A1 (en) * 2007-07-16 2009-01-22 Eberhard Karls Universität Tübingen Cyclic amide compounds, method for the production thereof and the use thereof
WO2009105239A1 (en) * 2008-02-20 2009-08-27 Rossi Robert A Process and system for calcining fine particle limestone

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007045048A1 (en) * 2005-10-21 2007-04-26 Calix Pty Ltd System and method for calcination/carbonation cycle processing
WO2007112496A1 (en) * 2006-03-31 2007-10-11 Calix Ltd System and method for the calcination of minerals
WO2008061305A1 (en) * 2006-11-22 2008-05-29 Orica Explosives Technology Pty Ltd Integrated chemical process
WO2009010542A1 (en) * 2007-07-16 2009-01-22 Eberhard Karls Universität Tübingen Cyclic amide compounds, method for the production thereof and the use thereof
WO2009105239A1 (en) * 2008-02-20 2009-08-27 Rossi Robert A Process and system for calcining fine particle limestone

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109320107A (en) * 2018-10-26 2019-02-12 辽宁科技大学 Suspension-boiling multithread state combination preparation high activity light calcined magnesia method

Also Published As

Publication number Publication date
WO2012145802A2 (en) 2012-11-01

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