WO2010130299A3 - Verfahren zur herstellung oxidbasierter metall-organischer gerüstmaterialien mittels inverser methode - Google Patents

Verfahren zur herstellung oxidbasierter metall-organischer gerüstmaterialien mittels inverser methode Download PDF

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Publication number
WO2010130299A3
WO2010130299A3 PCT/EP2009/066729 EP2009066729W WO2010130299A3 WO 2010130299 A3 WO2010130299 A3 WO 2010130299A3 EP 2009066729 W EP2009066729 W EP 2009066729W WO 2010130299 A3 WO2010130299 A3 WO 2010130299A3
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WO
WIPO (PCT)
Prior art keywords
compounds
organic framework
based metal
producing oxide
omof
Prior art date
Application number
PCT/EP2009/066729
Other languages
English (en)
French (fr)
Other versions
WO2010130299A2 (de
Inventor
Steffen Hausdorf
Florian Mertens
Felix Baitalow
Jürgen Seidel
Roland Fischer
Original Assignee
Technische Universität Bergakademie Freiberg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Technische Universität Bergakademie Freiberg filed Critical Technische Universität Bergakademie Freiberg
Priority to EP09807537A priority Critical patent/EP2429981A2/de
Publication of WO2010130299A2 publication Critical patent/WO2010130299A2/de
Publication of WO2010130299A3 publication Critical patent/WO2010130299A3/de

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G9/00—Compounds of zinc
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic System
    • C07F15/06—Cobalt compounds
    • C07F15/065—Cobalt compounds without a metal-carbon linkage
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic System
    • C07F3/003—Compounds containing elements of Groups 2 or 12 of the Periodic System without C-Metal linkages
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area

Abstract

Die Erfindung betrifft ein Verfahren zur Herstellung oxidbasierter metall-organischer Gerüstverbindungen, so genannter OMOF ' s, der allgemeinen Formel M4OBx (M = zweiwertiges Metall, x ≤ 3). OMOF-Verbindungen sind in einem regelmäßigen Gitter aufgebaut, welches eine definierte Porengrößeverteilung aufweist. Das hohe spezifische Porenvolumen und die damit verbundene große Äquivalentoberfläche machen diese Verbindungen zu ausgezeichneten Materialien unter anderem für Gasspeicher, zur chemischtechnischen Katalyse oder als Trennmaterial z.B. in der Gas- oder Flüssigchromatographie. Die erfindungsgemäßen Verbindungen werden so hergestellt, dass Verbindungen des Typs M4OA6, wobei M ein zweiwertiges Metallkation und A ein beliebiges Anion darstellt, mit Austauschverbindungen aus denen ein Anion B mit mindestens 2 funktionellen Gruppen und mindestens 4 Donoratomen entsteht, zu Verbindungen des Typs M4OBx mit x ≤ 3 in Anwesenheit eines Lösungsmittels umgesetzt werden.
PCT/EP2009/066729 2009-05-15 2009-12-09 Verfahren zur herstellung oxidbasierter metall-organischer gerüstmaterialien mittels inverser methode WO2010130299A2 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP09807537A EP2429981A2 (de) 2009-05-15 2009-12-09 Verfahren zur herstellung oxidbasierter metall-organischer gerüstmaterialien mittels inverser methode

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102009021479A DE102009021479A1 (de) 2008-06-04 2009-05-15 Verfahren zur Herstellung von oxidbasierten metall-organischen Gerüstmaterialien mittels inverser Synthese
DE102009021479.8 2009-05-15

Publications (2)

Publication Number Publication Date
WO2010130299A2 WO2010130299A2 (de) 2010-11-18
WO2010130299A3 true WO2010130299A3 (de) 2011-03-31

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2009/066729 WO2010130299A2 (de) 2009-05-15 2009-12-09 Verfahren zur herstellung oxidbasierter metall-organischer gerüstmaterialien mittels inverser methode

Country Status (3)

Country Link
EP (1) EP2429981A2 (de)
DE (1) DE102009021479A1 (de)
WO (1) WO2010130299A2 (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114632496B (zh) * 2020-12-15 2023-02-28 中国科学院大连化学物理研究所 一种沸石咪唑酯骨架材料的可逆晶格转变的方法
CN115819792B (zh) * 2022-12-16 2023-08-18 陕西煤业化工技术研究院有限责任公司 混金属基三羧酸配位聚合物及其制备方法和吸附方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004101575A2 (en) * 2003-05-09 2004-11-25 The Regents Of The University Of Michigan Implementation of a strategy for achieving extraordinary levels of surface and porosity in crystals
WO2007090864A1 (de) * 2006-02-10 2007-08-16 Basf Se Verfahren zur herstellung poröser organischer gerüstmaterialien
DE102006048043A1 (de) * 2006-10-11 2008-04-17 Bayer Materialscience Ag Verfahren zur Herstellung metallorganischer Gerüstverbindungen

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004101575A2 (en) * 2003-05-09 2004-11-25 The Regents Of The University Of Michigan Implementation of a strategy for achieving extraordinary levels of surface and porosity in crystals
WO2007090864A1 (de) * 2006-02-10 2007-08-16 Basf Se Verfahren zur herstellung poröser organischer gerüstmaterialien
DE102006048043A1 (de) * 2006-10-11 2008-04-17 Bayer Materialscience Ag Verfahren zur Herstellung metallorganischer Gerüstverbindungen

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
CHRISTIAN SERRE, FRANCK MILLANGE, SUZY SURBLÉ, GÉRARD FÉREY: "A Route to the Synthesis of Trivalent Transition-Metal Porous Carboxylates with Trimeric Secondary Building Units", ANGEWANDTE CHEMIE INTERNATIONAL EDITION, vol. 43, no. 46, 7 September 2004 (2004-09-07), pages 6285 - 6289, XP002604647 *
ROWSELL J L C ET AL: "Metal-organic frameworks: a new class of porous materials", MICROPOROUS AND MESOPOROUS MATERIALS, ELSEVIER SCIENCE PUBLISHING, NEW YORK, US LNKD- DOI:10.1016/J.MICROMESO.2004.03.034, vol. 73, no. 1-2, 6 August 2004 (2004-08-06), pages 3 - 14, XP004522126, ISSN: 1387-1811 *
TRANCHEMONTAGNE D J ET AL: "Room temperature synthesis of metal-organic frameworks: MOF-5, MOF-74, MOF-177, MOF-199, and IRMOF-0", TETRAHEDRON, ELSEVIER SCIENCE PUBLISHERS, AMSTERDAM, NL LNKD- DOI:10.1016/J.TET.2008.06.036, vol. 64, no. 36, 1 September 2008 (2008-09-01), pages 8553 - 8557, XP023315820, ISSN: 0040-4020, [retrieved on 20080614] *

Also Published As

Publication number Publication date
EP2429981A2 (de) 2012-03-21
DE102009021479A1 (de) 2010-09-16
WO2010130299A2 (de) 2010-11-18

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