WO2010013937A3 - Flame retardant water-soluble polyurethane resin and preparation method thereof - Google Patents

Flame retardant water-soluble polyurethane resin and preparation method thereof Download PDF

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Publication number
WO2010013937A3
WO2010013937A3 PCT/KR2009/004216 KR2009004216W WO2010013937A3 WO 2010013937 A3 WO2010013937 A3 WO 2010013937A3 KR 2009004216 W KR2009004216 W KR 2009004216W WO 2010013937 A3 WO2010013937 A3 WO 2010013937A3
Authority
WO
WIPO (PCT)
Prior art keywords
flame retardant
polyurethane resin
soluble polyurethane
retardant water
preparation
Prior art date
Application number
PCT/KR2009/004216
Other languages
French (fr)
Korean (ko)
Other versions
WO2010013937A2 (en
Inventor
권오승
김재명
김철완
문시완
김우영
Original Assignee
합동고분자주식회사
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 합동고분자주식회사 filed Critical 합동고분자주식회사
Priority to CN2009801384400A priority Critical patent/CN102164980B/en
Publication of WO2010013937A2 publication Critical patent/WO2010013937A2/en
Publication of WO2010013937A3 publication Critical patent/WO2010013937A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/46—Polycondensates having carboxylic or carbonic ester groups in the main chain having heteroatoms other than oxygen
    • C08G18/4684—Polycondensates having carboxylic or carbonic ester groups in the main chain having heteroatoms other than oxygen containing phosphorus
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/82—Post-polymerisation treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/34—Carboxylic acids; Esters thereof with monohydroxyl compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
    • C08L75/04—Polyurethanes

Abstract

The present invention relates to a flame retardant water-soluble polyurethane resin. More specifically, the present invention relates to a flame retardant water-soluble polyurethane resin containing phosphorus which is prepared by the steps of: preparing a halogen-free prepolymer by the reaction of a halogen-free diol or triol compound containing phosphorus, optionally a polyester diol compound, and a diisocyanate compound; and introducing a hydrophilic group to the prepolymer to neutralize the prepolymer introduced with the hydrophilic group and disperse it in water, followed by chain-extending it with a chain extender.
PCT/KR2009/004216 2008-07-30 2009-07-29 Flame retardant water-soluble polyurethane resin and preparation method thereof WO2010013937A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009801384400A CN102164980B (en) 2008-07-30 2009-07-29 Flame retardant water-soluble polyurethane resin and preparation method thereof

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020080074555A KR100877709B1 (en) 2008-07-30 2008-07-30 Flame retardant, aqueous polyurethane resin and process for preparation thereof
KR10-2008-0074555 2008-07-30

Publications (2)

Publication Number Publication Date
WO2010013937A2 WO2010013937A2 (en) 2010-02-04
WO2010013937A3 true WO2010013937A3 (en) 2010-05-14

Family

ID=40482363

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2009/004216 WO2010013937A2 (en) 2008-07-30 2009-07-29 Flame retardant water-soluble polyurethane resin and preparation method thereof

Country Status (3)

Country Link
KR (1) KR100877709B1 (en)
CN (1) CN102164980B (en)
WO (1) WO2010013937A2 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20140272237A1 (en) * 2013-03-15 2014-09-18 Prc-Desoto International, Inc. Strippable film assembly and coating for drag reduction
CN104479531B (en) * 2014-12-09 2016-11-23 张和庆 A kind of solid wood granule plate isophorone diisocyanate fireproof coating and preparation method
CN105542120A (en) * 2015-12-28 2016-05-04 安徽安大华泰新材料有限公司 Flame-retardant polyurethane resin and preparation method thereof
CN105504225A (en) * 2015-12-28 2016-04-20 安徽安大华泰新材料有限公司 Method for preparing flame-retardant water-based polyurethane resin
CN110079888B (en) * 2019-04-22 2020-11-13 烟台泰和新材料股份有限公司 Polyurethane elastic fiber with flame retardant function and preparation method thereof
KR102343933B1 (en) * 2021-08-25 2021-12-27 아이씨이아이우방(주) Phosphorus urethane flame retardant for cellulose fiber, Manufacturing method thereof and Flame retarding cellulose fiber using the same

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3142650A (en) * 1961-05-15 1964-07-28 Union Carbide Corp Polyurethanes from tris-polypropylene glycol phosphites
US4102828A (en) * 1976-04-28 1978-07-25 Texaco Development Corporation Polyurethanes derived from novel novolak polyols
US4110271A (en) * 1975-06-30 1978-08-29 Union Carbide Corporation Formation of polyurethane foam in the presence of sulfolanyl-bearing polysiloxane-polyoxyalkylene polymers
EP1238997A1 (en) * 2001-03-07 2002-09-11 Ucb S.A. Phosphorus containing materials, their preparation and use

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2937330A1 (en) 1979-09-14 1981-04-02 Bayer Ag, 5090 Leverkusen METHOD FOR THE PRODUCTION OF ELASTIC, FLAME-LAYABLE AND HIGH-FREQUENCY-WELDABLE POLYURETHANE FOAMS
CN100482741C (en) * 2007-05-29 2009-04-29 吴波 Polyurethane flame-proof additive and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3142650A (en) * 1961-05-15 1964-07-28 Union Carbide Corp Polyurethanes from tris-polypropylene glycol phosphites
US4110271A (en) * 1975-06-30 1978-08-29 Union Carbide Corporation Formation of polyurethane foam in the presence of sulfolanyl-bearing polysiloxane-polyoxyalkylene polymers
US4102828A (en) * 1976-04-28 1978-07-25 Texaco Development Corporation Polyurethanes derived from novel novolak polyols
EP1238997A1 (en) * 2001-03-07 2002-09-11 Ucb S.A. Phosphorus containing materials, their preparation and use

Also Published As

Publication number Publication date
CN102164980B (en) 2013-05-01
CN102164980A (en) 2011-08-24
WO2010013937A2 (en) 2010-02-04
KR100877709B1 (en) 2009-01-07

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