WO2008151759A3 - Process and apparatus for mixing gases - Google Patents

Process and apparatus for mixing gases Download PDF

Info

Publication number
WO2008151759A3
WO2008151759A3 PCT/EP2008/004511 EP2008004511W WO2008151759A3 WO 2008151759 A3 WO2008151759 A3 WO 2008151759A3 EP 2008004511 W EP2008004511 W EP 2008004511W WO 2008151759 A3 WO2008151759 A3 WO 2008151759A3
Authority
WO
WIPO (PCT)
Prior art keywords
mixing chamber
mixing
converter
gas flow
mixing gases
Prior art date
Application number
PCT/EP2008/004511
Other languages
French (fr)
Other versions
WO2008151759A2 (en
Inventor
Karl-Heinz Daum
Wolfram Schalk
Ventosa David Cachero
Original Assignee
Outotec Oyj
Karl-Heinz Daum
Wolfram Schalk
Ventosa David Cachero
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outotec Oyj, Karl-Heinz Daum, Wolfram Schalk, Ventosa David Cachero filed Critical Outotec Oyj
Priority to AU2008261291A priority Critical patent/AU2008261291B2/en
Priority to CN2008800197686A priority patent/CN101687641B/en
Priority to MX2009013477A priority patent/MX2009013477A/en
Publication of WO2008151759A2 publication Critical patent/WO2008151759A2/en
Publication of WO2008151759A3 publication Critical patent/WO2008151759A3/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496Heating or cooling the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/10Mixing gases with gases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20Jet mixers, i.e. mixers using high-speed fluid streams
    • B01F25/23Mixing by intersecting jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0461Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds
    • B01J8/0469Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds the beds being superimposed one above the other
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0492Feeding reactive fluids
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/76Preparation by contact processes
    • C01B17/765Multi-stage SO3-conversion
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/76Preparation by contact processes
    • C01B17/80Apparatus
    • C01B17/803Converters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F2025/91Direction of flow or arrangement of feed and discharge openings
    • B01F2025/915Reverse flow, i.e. flow changing substantially 180° in direction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F2025/91Direction of flow or arrangement of feed and discharge openings
    • B01F2025/918Counter current flow, i.e. flows moving in opposite direction and colliding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00168Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796Details of the reactor or of the particulate material
    • B01J2208/00823Mixing elements
    • B01J2208/00831Stationary elements
    • B01J2208/00849Stationary elements outside the bed, e.g. baffles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Accessories For Mixers (AREA)

Abstract

When mixing two gases of different temperature and/or composition in a converter for producing SO3 from an SO2-containing gas, a first gas flow is introduced into a mixing chamber from below, whereas a second gas flow is countercurrently introduced into the mixing chamber from above. The gas mixture obtained in the mixing chamber is discharged from the mixing chamber via an upwardly directed connecting tube and supplied to a heat exchanger integrated in the converter.
PCT/EP2008/004511 2007-06-13 2008-06-06 Process and apparatus for mixing gases WO2008151759A2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
AU2008261291A AU2008261291B2 (en) 2007-06-13 2008-06-06 Process and apparatus for mixing gases
CN2008800197686A CN101687641B (en) 2007-06-13 2008-06-06 Process and apparatus for mixing gases
MX2009013477A MX2009013477A (en) 2007-06-13 2008-06-06 Process and apparatus for mixing gases.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102007027841A DE102007027841B4 (en) 2007-06-13 2007-06-13 Method and apparatus for mixing gases
DE102007027841.3 2007-06-13

Publications (2)

Publication Number Publication Date
WO2008151759A2 WO2008151759A2 (en) 2008-12-18
WO2008151759A3 true WO2008151759A3 (en) 2009-02-12

Family

ID=39938100

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2008/004511 WO2008151759A2 (en) 2007-06-13 2008-06-06 Process and apparatus for mixing gases

Country Status (7)

Country Link
CN (1) CN101687641B (en)
AU (1) AU2008261291B2 (en)
CL (1) CL2008001717A1 (en)
DE (1) DE102007027841B4 (en)
MX (1) MX2009013477A (en)
PE (1) PE20090340A1 (en)
WO (1) WO2008151759A2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103072956B (en) * 2012-12-31 2015-04-15 中国瑞林工程技术有限公司 Flue gas processing method and system

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2846291A (en) * 1951-10-10 1958-08-05 Basf Ag Process and apparatus for the production of gases containing sulfur trioxide
GB2139914A (en) * 1980-09-19 1984-11-21 Chemetics Int Catalytic converter
RU2174945C2 (en) * 1999-12-15 2001-10-20 Кобяков Анатолий Иванович Method of processing concentrated sulfur dioxide
DE10249782A1 (en) * 2002-10-24 2004-05-06 Outokumpu Oyj Process and plant for the production of sulfuric acid from sulfur dioxide-rich gases
DE202006016783U1 (en) * 2006-11-03 2007-01-18 Heilig, Hubert Contamination-insensitive gas mixer, with mechanically fixed mixing geometry and temperature adaptation, has pipes of longer, thin-walled construction, and formed out in funnel form in flow direction

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2104858A (en) * 1935-01-23 1938-01-11 Gen Chemical Corp Manufacture of sulphuric acid
AT195406B (en) * 1955-10-01 1958-02-10 Chemie Linz Ag Method and device for mixing two or more gases or liquids with one another
DE1926239U (en) * 1964-01-31 1965-11-04 Uhde Gmbh Friedrich DEVICE FOR MIXING GASES OF DIFFERENT DENSITY.
US5480620A (en) * 1994-08-17 1996-01-02 Cameron; Gordon M. Catalytic converter
DE19800800C2 (en) 1998-01-13 2001-05-23 Metallgesellschaft Ag Process for the production of sulfuric acid
CN1384805A (en) * 1999-11-01 2002-12-11 孟山都公司 Method for making sulfur trioxide, sulfuric acid, and oleum from sulfur dioxide
DE10023178A1 (en) 2000-05-11 2001-11-15 Mg Technologies Ag Two-stage catalytic production of sulfur trioxide gas with low sulfur dioxide content from high sulfur dioxide-content gas comprises use of two catalyst layers with temperature at each layer controlled

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2846291A (en) * 1951-10-10 1958-08-05 Basf Ag Process and apparatus for the production of gases containing sulfur trioxide
GB2139914A (en) * 1980-09-19 1984-11-21 Chemetics Int Catalytic converter
RU2174945C2 (en) * 1999-12-15 2001-10-20 Кобяков Анатолий Иванович Method of processing concentrated sulfur dioxide
DE10249782A1 (en) * 2002-10-24 2004-05-06 Outokumpu Oyj Process and plant for the production of sulfuric acid from sulfur dioxide-rich gases
DE202006016783U1 (en) * 2006-11-03 2007-01-18 Heilig, Hubert Contamination-insensitive gas mixer, with mechanically fixed mixing geometry and temperature adaptation, has pipes of longer, thin-walled construction, and formed out in funnel form in flow direction

Also Published As

Publication number Publication date
AU2008261291A1 (en) 2008-12-18
MX2009013477A (en) 2010-01-18
CN101687641A (en) 2010-03-31
CL2008001717A1 (en) 2008-08-01
WO2008151759A2 (en) 2008-12-18
DE102007027841B4 (en) 2012-02-16
AU2008261291B2 (en) 2013-08-01
CN101687641B (en) 2013-11-13
PE20090340A1 (en) 2009-04-23
DE102007027841A1 (en) 2008-12-18

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