WO2008129757A1 - Process for production of bisphenol a - Google Patents

Process for production of bisphenol a Download PDF

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Publication number
WO2008129757A1
WO2008129757A1 PCT/JP2008/000356 JP2008000356W WO2008129757A1 WO 2008129757 A1 WO2008129757 A1 WO 2008129757A1 JP 2008000356 W JP2008000356 W JP 2008000356W WO 2008129757 A1 WO2008129757 A1 WO 2008129757A1
Authority
WO
WIPO (PCT)
Prior art keywords
crystallization
bisphenol
batch
production
tank
Prior art date
Application number
PCT/JP2008/000356
Other languages
French (fr)
Japanese (ja)
Inventor
Yoshio Koga
Mitsuru Shoji
Shigeru Kanaeda
Hideto Hayashi
Original Assignee
Mitsubishi Chemical Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Chemical Corporation filed Critical Mitsubishi Chemical Corporation
Priority to CN200880007188.5A priority Critical patent/CN101626998B/en
Publication of WO2008129757A1 publication Critical patent/WO2008129757A1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A process for the production of bisphenol A which is improved in order that a low-viscosity slurry of crystals having large diameters can be formed in batch crystallization to enable smooth changeover from batch crystallization to continuous crystallization. In the crystallization step, the crystallization is initiated by conducting batch crystallization operation in a crystallization tank, and in the batch crystallization operation, the change of degree of supersaturation per unit time at the point of time when the bisphenol A concentration of the solution in the tank has reached saturation is adjusted to 0.1 to 8°C/h.
PCT/JP2008/000356 2007-03-30 2008-02-27 Process for production of bisphenol a WO2008129757A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN200880007188.5A CN101626998B (en) 2007-03-30 2008-02-27 Process for production of bisphenol a

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007094558 2007-03-30
JP2007-094558 2007-03-30

Publications (1)

Publication Number Publication Date
WO2008129757A1 true WO2008129757A1 (en) 2008-10-30

Family

ID=39875296

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/000356 WO2008129757A1 (en) 2007-03-30 2008-02-27 Process for production of bisphenol a

Country Status (3)

Country Link
JP (1) JP2008273933A (en)
CN (1) CN101626998B (en)
WO (1) WO2008129757A1 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010150249A (en) * 2008-11-26 2010-07-08 Mitsubishi Chemicals Corp Method for producing high-purity bisphenol a by using direct crystallization method of bisphenol a (bpa)
JP5690484B2 (en) * 2009-12-11 2015-03-25 日揮株式会社 Crystallization method and crystallizer
KR101812838B1 (en) 2013-07-11 2017-12-27 주식회사 엘지화학 Apparatus and metod for preparing bisphenol a
JP2014148540A (en) * 2014-05-13 2014-08-21 Mitsubishi Rayon Co Ltd Crystallization apparatus and method for removing crystallized product
KR102040365B1 (en) * 2017-05-26 2019-11-04 주식회사 엘지화학 An Apparatus for producing Bisphenole A and a Method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6038335A (en) * 1983-08-11 1985-02-27 Mitsui Toatsu Chem Inc Production of bisphenol a
JP2003528840A (en) * 2000-03-27 2003-09-30 バイエル アクチェンゲゼルシャフト Bisphenol production method
JP2004182642A (en) * 2002-12-03 2004-07-02 Mitsubishi Chemicals Corp Method for crystallizing bisphenol a-phenol adduct

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2683762B2 (en) * 1991-10-30 1997-12-03 千代田化工建設株式会社 Method for producing bisphenol A / phenol crystal adduct having good hue
JPH08333290A (en) * 1995-06-12 1996-12-17 Mitsubishi Chem Corp Production of bisphenol a
JP2002085960A (en) * 2000-09-14 2002-03-26 Sumitomo Chem Co Ltd Device and method for imparting temperature difference and application thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6038335A (en) * 1983-08-11 1985-02-27 Mitsui Toatsu Chem Inc Production of bisphenol a
JP2003528840A (en) * 2000-03-27 2003-09-30 バイエル アクチェンゲゼルシャフト Bisphenol production method
JP2004182642A (en) * 2002-12-03 2004-07-02 Mitsubishi Chemicals Corp Method for crystallizing bisphenol a-phenol adduct

Also Published As

Publication number Publication date
CN101626998A (en) 2010-01-13
CN101626998B (en) 2013-05-01
JP2008273933A (en) 2008-11-13

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