WO2006029792A3 - Elektrolysezelle zur herstellung von alkalimetall - Google Patents

Elektrolysezelle zur herstellung von alkalimetall Download PDF

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Publication number
WO2006029792A3
WO2006029792A3 PCT/EP2005/009786 EP2005009786W WO2006029792A3 WO 2006029792 A3 WO2006029792 A3 WO 2006029792A3 EP 2005009786 W EP2005009786 W EP 2005009786W WO 2006029792 A3 WO2006029792 A3 WO 2006029792A3
Authority
WO
WIPO (PCT)
Prior art keywords
alkali metal
tube
solid electrolyte
electrolyte tube
discharge
Prior art date
Application number
PCT/EP2005/009786
Other languages
English (en)
French (fr)
Other versions
WO2006029792A2 (de
Inventor
Guenther Huber
Reinhard Oettl
Manfred Munzinger
Heinz Neumann
Martina Schulz
Matthias Stahl
Gerhard Ruf
Ralph Hamleser
Hans-Juergen Bender
Volker Esswein
Original Assignee
Basf Ag
Guenther Huber
Reinhard Oettl
Manfred Munzinger
Heinz Neumann
Martina Schulz
Matthias Stahl
Gerhard Ruf
Ralph Hamleser
Hans-Juergen Bender
Volker Esswein
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag, Guenther Huber, Reinhard Oettl, Manfred Munzinger, Heinz Neumann, Martina Schulz, Matthias Stahl, Gerhard Ruf, Ralph Hamleser, Hans-Juergen Bender, Volker Esswein filed Critical Basf Ag
Priority to DE502005003027T priority Critical patent/DE502005003027D1/de
Priority to US11/575,219 priority patent/US7981260B2/en
Priority to EP05787394A priority patent/EP1794352B1/de
Priority to KR1020077008444A priority patent/KR101253787B1/ko
Priority to CN2005800308045A priority patent/CN101018893B/zh
Publication of WO2006029792A2 publication Critical patent/WO2006029792A2/de
Publication of WO2006029792A3 publication Critical patent/WO2006029792A3/de

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/02—Electrolytic production, recovery or refining of metals by electrolysis of melts of alkali or alkaline earth metals
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/06—Electrolytic production, recovery or refining of metals by electrolysis of melts of aluminium
    • C25C3/08—Cell construction, e.g. bottoms, walls, cathodes
    • C25C3/12—Anodes
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
    • C25C7/005—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells of cells for the electrolysis of melts
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
    • C25C7/04—Diaphragms; Spacing elements

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Electrolytic Production Of Metals (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)

Abstract

Die Erfindung bezieht sich auf eine Elektrolysezelle zur Herstellung von flüssigem Alkalimetall aus einer flüssigen Alkalimetall-Schwermetalllegierung, enthaltend - ein im Wesentlichen horizontal angeordnetes Rohr (1) mit je einer Verschlussvorrichtung (4) an jedem der zwei Enden des Rohres (1), - mindestens eine in dem Rohr (1) angeordnete, an einem Ende geschlossene, an dem anderen Ende eine Öffnung (11) aufweisende Festelektrolytröhre (12), die Alkalimetallionen leitet, wobei die Festelektrolytröhre (12) in dem Rohr (1) konzentrisch angeordnet und mit der Öffnung (11) einem Ende des Rohrs (1) zugewandt ist, so dass sich ein erster Ringspalt (13) zur Führung der eine Anode bildenden flüssigen Alkalimetall-Schwermetalllegierung zwischen der Innenseite des Rohrs (1) und der Außenseite der Festelektrolytröhre (12) befindet, - einen Innenraum (14) in der Festelektrolytröhre (12) zur Aufnahme des als Kathode nutzbaren flüssigen Alkalimetalls, wobei die Verschlussvorrichtung (4) eine in den ersten Ringspalt (13) mündende Alkalimetall-Schwermetalllegierungs-Zuführung (8) oder -Abführung (9), eine Halteeinrichtung für die Festelektrolytröhre (12), eine mit dem Innenraum (14) der Festelektrolytröhre (12) verbundene Alkalimetallabführung (15) und ein Dichtungssystem zur Abdichtung des Innenraums (14) der Festelektrolytröhre (12) und der Alkalimetallabführung (15) gegen den ersten Ringspalt (13), die Alkalimetall-Schwermetalllegierungs-Zuführung (8)- oder -Abführung (9) und gegen die Umgebung der Elektrolysezelle umfasst.
PCT/EP2005/009786 2004-09-14 2005-09-12 Elektrolysezelle zur herstellung von alkalimetall WO2006029792A2 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE502005003027T DE502005003027D1 (de) 2004-09-14 2005-09-12 Elektrolysezelle zur herstellung von alkalimetall
US11/575,219 US7981260B2 (en) 2004-09-14 2005-09-12 Electrolysis cell for producing alkali metal
EP05787394A EP1794352B1 (de) 2004-09-14 2005-09-12 Elektrolysezelle zur herstellung von alkalimetall
KR1020077008444A KR101253787B1 (ko) 2004-09-14 2005-09-12 알칼리 금속 제조용 전기분해 셀
CN2005800308045A CN101018893B (zh) 2004-09-14 2005-09-12 用于制备碱金属的电解电池

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102004044405A DE102004044405A1 (de) 2004-09-14 2004-09-14 Elektrolysezelle zur Herstellung von Alkalimetall
DE102004044405.6 2004-09-14

Publications (2)

Publication Number Publication Date
WO2006029792A2 WO2006029792A2 (de) 2006-03-23
WO2006029792A3 true WO2006029792A3 (de) 2006-08-03

Family

ID=35911108

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2005/009786 WO2006029792A2 (de) 2004-09-14 2005-09-12 Elektrolysezelle zur herstellung von alkalimetall

Country Status (10)

Country Link
US (1) US7981260B2 (de)
EP (1) EP1794352B1 (de)
KR (1) KR101253787B1 (de)
CN (1) CN101018893B (de)
AR (1) AR054312A1 (de)
AT (1) ATE387521T1 (de)
DE (2) DE102004044405A1 (de)
ES (1) ES2300052T3 (de)
TW (1) TWI404831B (de)
WO (1) WO2006029792A2 (de)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9758881B2 (en) 2009-02-12 2017-09-12 The George Washington University Process for electrosynthesis of energetic molecules
JP2013531738A (ja) * 2010-06-30 2013-08-08 シー アメンドラ スティーヴン リチウム金属の電解生成
CN104313645B (zh) * 2014-10-28 2017-08-08 苏州萨伯工业设计有限公司 含钪铝合金材料的制备装置及制备工艺
CN105742727B (zh) * 2014-12-09 2018-05-22 中国科学院物理研究所 一种二次电池、用途及其负极的制备方法
CN104805469B (zh) * 2015-05-11 2017-04-05 中国东方电气集团有限公司 一种电解制备金属钠装置的阴极电解槽
CN106972192A (zh) * 2017-03-16 2017-07-21 江苏大学 为锂离子储能器件负极预制锂的方法及电解池装置、锂离子储能器件
WO2022155752A1 (en) * 2021-01-21 2022-07-28 Li-Metal Corp. Electrorefining apparatus and process for refining lithium metal
AU2022211401A1 (en) * 2021-01-21 2023-08-10 Li-Metal Corp. Process for production refined lithium metal
US11976375B1 (en) 2022-11-11 2024-05-07 Li-Metal Corp. Fracture resistant mounting for ceramic piping
CN116695185B (zh) * 2023-08-04 2023-10-17 四川澳晟新材料科技有限责任公司 一种金属锂熔盐电解工艺参数模拟仿真测试装置

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1114330B (de) * 1959-05-06 1961-09-28 Dr Dr E H Karl Ziegler Verfahren zur kathodischen Abscheidung von Natrium durch Elektrolyse von natriumhaltigen organischen Aluminiumverbindungen
EP1114883A1 (de) * 1998-12-22 2001-07-11 Basf Aktiengesellschaft Verfahren zur elektrochemischen Herstellung von Alkalimetall aus Alkalimetallamalgam

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1155927A (en) 1967-02-20 1969-06-25 Ici Ltd Electrolytic manufacture of alkali metals.
US4089770A (en) * 1977-07-11 1978-05-16 E. I. Du Pont De Nemours And Company Electrolytic cell
CN1204700A (zh) * 1997-07-08 1999-01-13 国营建中化工总公司 一种金属锂电解槽
DE19926724A1 (de) * 1999-06-11 2000-12-14 Basf Ag Elektrolysezelle zur Herstellung eines Alkalimetalls

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1114330B (de) * 1959-05-06 1961-09-28 Dr Dr E H Karl Ziegler Verfahren zur kathodischen Abscheidung von Natrium durch Elektrolyse von natriumhaltigen organischen Aluminiumverbindungen
EP1114883A1 (de) * 1998-12-22 2001-07-11 Basf Aktiengesellschaft Verfahren zur elektrochemischen Herstellung von Alkalimetall aus Alkalimetallamalgam

Also Published As

Publication number Publication date
DE502005003027D1 (de) 2008-04-10
ATE387521T1 (de) 2008-03-15
CN101018893A (zh) 2007-08-15
ES2300052T3 (es) 2008-06-01
KR101253787B1 (ko) 2013-04-15
TWI404831B (zh) 2013-08-11
US7981260B2 (en) 2011-07-19
CN101018893B (zh) 2010-08-11
EP1794352A2 (de) 2007-06-13
WO2006029792A2 (de) 2006-03-23
US20070246368A1 (en) 2007-10-25
TW200624606A (en) 2006-07-16
EP1794352B1 (de) 2008-02-27
KR20070055592A (ko) 2007-05-30
AR054312A1 (es) 2007-06-20
DE102004044405A1 (de) 2006-03-30

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