WO2005016824A3 - Synthesis of nanoparticles by an emulsion-gas contacting process - Google Patents

Synthesis of nanoparticles by an emulsion-gas contacting process Download PDF

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Publication number
WO2005016824A3
WO2005016824A3 PCT/US2004/014073 US2004014073W WO2005016824A3 WO 2005016824 A3 WO2005016824 A3 WO 2005016824A3 US 2004014073 W US2004014073 W US 2004014073W WO 2005016824 A3 WO2005016824 A3 WO 2005016824A3
Authority
WO
WIPO (PCT)
Prior art keywords
reactant
nanoparticles
emulsion
synthesis
stable emulsion
Prior art date
Application number
PCT/US2004/014073
Other languages
French (fr)
Other versions
WO2005016824A2 (en
Inventor
Triantafillos J Mountziaris
Paschalis Alexandridis
Original Assignee
York The Res Foundation Of Sta
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by York The Res Foundation Of Sta filed Critical York The Res Foundation Of Sta
Publication of WO2005016824A2 publication Critical patent/WO2005016824A2/en
Publication of WO2005016824A3 publication Critical patent/WO2005016824A3/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B19/00Selenium; Tellurium; Compounds thereof
    • C01B19/007Tellurides or selenides of metals
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G1/00Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
    • C01G1/02Oxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G1/00Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
    • C01G1/12Sulfides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G11/00Compounds of cadmium
    • C01G11/02Sulfides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G21/00Compounds of lead
    • C01G21/21Sulfides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G9/00Compounds of zinc
    • C01G9/08Sulfides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/04Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00Nanotechnology
    • Y10S977/70Nanostructure

Abstract

The present invention is directed to a process for synthesizing nanoparticles. This process involves providing a stable emulsion containing a plurality of droplets suspended in a continuous phase. The droplets, which are encapsulated by an interfacially-active material, contain a first reactant dissolved in a dispersed phase. The process also involves contacting a gas phase containing a second reactant diluted in a carrier gas with the stable emulsion under conditions effective to permit the first reactant and second reactant to react and form nanoparticles. The present invention further relates to nanoparticle-loaded emulsions and their uses in formulations for various purposes.
PCT/US2004/014073 2003-05-05 2004-05-05 Synthesis of nanoparticles by an emulsion-gas contacting process WO2005016824A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US46797503P 2003-05-05 2003-05-05
US60/467,975 2003-05-05

Publications (2)

Publication Number Publication Date
WO2005016824A2 WO2005016824A2 (en) 2005-02-24
WO2005016824A3 true WO2005016824A3 (en) 2006-02-16

Family

ID=34193003

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2004/014073 WO2005016824A2 (en) 2003-05-05 2004-05-05 Synthesis of nanoparticles by an emulsion-gas contacting process

Country Status (2)

Country Link
US (1) US8859000B2 (en)
WO (1) WO2005016824A2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8455088B2 (en) 2005-12-23 2013-06-04 Boston Scientific Scimed, Inc. Spun nanofiber, medical devices, and methods

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7190264B2 (en) * 2004-03-05 2007-03-13 Simon Fraser University Wireless computer monitoring device with automatic arming and disarming
CN1232608C (en) * 2004-04-06 2005-12-21 中国科学院长春应用化学研究所 Method for synthesizing nano semiconductor luminescence material on interface bewteen liquid-liquid
CA2520670A1 (en) * 2004-09-23 2006-03-23 National Research Council Of Canada Nanocrystal coated surfaces
US20060240590A1 (en) * 2004-11-09 2006-10-26 The Research Foundation Of State University Of New York Controlled synthesis of nanowires, nanodiscs, and nanostructured materials using liquid crystalline templates
US20060216508A1 (en) * 2005-03-24 2006-09-28 3M Innovative Properties Company Polymer nanocomposite having surface modified nanoparticles and methods of preparing same
US7405001B2 (en) * 2005-03-24 2008-07-29 3M Innovative Properties Company Surface modified nanoparticle and method of preparing same
US7172811B2 (en) * 2005-03-24 2007-02-06 3M Innovative Properties Company Methods of preparing polymer nanocomposite having surface modified nanoparticles
WO2006105102A2 (en) * 2005-03-28 2006-10-05 The Research Foundation Of State University Of New York Synthesis of nanostructured materials using liquid crystalline templates
CA2608226C (en) 2005-06-07 2015-02-24 University Of South Australia Dried formulations of nanoparticle-coated capsules
US7470466B2 (en) 2005-12-23 2008-12-30 Boston Scientific Scimed, Inc. Nanoparticle structures and composite materials comprising a silicon-containing compound having a chemical linker that forms a non-covalent bond with a polymer
AU2007247770B2 (en) * 2006-05-04 2013-07-18 Reformpharm Pty Ltd Drug release from nanoparticle-coated capsules
EP2087525A4 (en) * 2006-10-19 2010-10-13 Univ California Hybrid solar cells with 3-dimensional hyperbranched nanocrystals
EP2150235A4 (en) * 2007-04-20 2013-07-03 Univ South Australia Nanoparticle-coated capsule formulation for dermal drug delivery
ITSA20070024A1 (en) 2007-07-27 2009-01-28 Univ Degli Studi Salerno CONTINUOUS PROCESS FOR THE PRODUCTION OF MICROSPHERES WITH EXPANDED LIQUIDS.
US8092719B2 (en) * 2007-09-04 2012-01-10 Samsung Electronics Co., Ltd. Nanocrystal-metal oxide composites and preparation method thereof
US8778400B2 (en) * 2008-04-21 2014-07-15 University Of South Australia Nanoparticle-stabilized capsule formulation for treatment of inflammation
CN101503624B (en) * 2009-03-19 2012-05-30 吉林大学 Aqueous phase synthesizing method for transient metal Mn doped ZnSe quantum dot
TWI397239B (en) * 2010-02-02 2013-05-21 Sanyang Industry Co Ltd Rental electric car charging system
CN101905862A (en) * 2010-03-31 2010-12-08 济南大学 Method for preparing ZnSe:Mn quantum dot
CN107792839B (en) * 2017-10-18 2021-01-29 苏州大学 Lead selenide nanorod, preparation method and application in field effect transistor
CN109007943A (en) * 2018-07-12 2018-12-18 王兰玺 A kind of quick-fried pearl squeezes tear drop device automatically
CN111729623B (en) * 2020-05-24 2021-12-07 同济大学 Preparation method and application of three-dimensional copper ferricyanide composite polypyrrole/polyvinyl alcohol conductive hydrogel material
CN112517014B (en) * 2020-11-11 2022-02-22 中国科学院长春应用化学研究所 Ferroelectric semiconductor nano-particles with narrow band gap, preparation method and application thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5019400A (en) * 1989-05-01 1991-05-28 Enzytech, Inc. Very low temperature casting of controlled release microspheres
US6235224B1 (en) * 1995-07-21 2001-05-22 Brown University Research Foundation Process for preparing microparticles through phase inversion phenomena

Family Cites Families (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5133955A (en) * 1988-12-22 1992-07-28 Arizona Technology Development Corporation Low temperature preparation of ultrafine oxide particles using organized reaction media
US5147841A (en) * 1990-11-23 1992-09-15 The United States Of America As Represented By The United States Department Of Energy Method for the preparation of metal colloids in inverse micelles and product preferred by the method
WO1993010564A1 (en) * 1991-11-22 1993-05-27 The Regents Of The University Of California Semiconductor nanocrystals covalently bound to solid inorganic surfaces using self-assembled monolayers
US5505928A (en) * 1991-11-22 1996-04-09 The Regents Of University Of California Preparation of III-V semiconductor nanocrystals
US5262357A (en) * 1991-11-22 1993-11-16 The Regents Of The University Of California Low temperature thin films formed from nanocrystal precursors
US5260957A (en) * 1992-10-29 1993-11-09 The Charles Stark Draper Laboratory, Inc. Quantum dot Laser
US5537000A (en) * 1994-04-29 1996-07-16 The Regents, University Of California Electroluminescent devices formed using semiconductor nanocrystals as an electron transport media and method of making such electroluminescent devices
AU733930B2 (en) * 1997-06-27 2001-05-31 University Of Southampton Porous film and method of preparation thereof
US6692660B2 (en) * 2001-04-26 2004-02-17 Nanogram Corporation High luminescence phosphor particles and related particle compositions
US20040072937A1 (en) * 2001-02-10 2004-04-15 Tomalia Donald A. Nanocomposites of dendritic polymers
US6607829B1 (en) * 1997-11-13 2003-08-19 Massachusetts Institute Of Technology Tellurium-containing nanocrystalline materials
US6322901B1 (en) * 1997-11-13 2001-11-27 Massachusetts Institute Of Technology Highly luminescent color-selective nano-crystalline materials
US6207392B1 (en) * 1997-11-25 2001-03-27 The Regents Of The University Of California Semiconductor nanocrystal probes for biological applications and process for making and using such probes
US6699723B1 (en) * 1997-11-25 2004-03-02 The Regents Of The University Of California Organo luminescent semiconductor nanocrystal probes for biological applications and process for making and using such probes
US5990479A (en) * 1997-11-25 1999-11-23 Regents Of The University Of California Organo Luminescent semiconductor nanocrystal probes for biological applications and process for making and using such probes
US6501091B1 (en) * 1998-04-01 2002-12-31 Massachusetts Institute Of Technology Quantum dot white and colored light emitting diodes
US6426513B1 (en) * 1998-09-18 2002-07-30 Massachusetts Institute Of Technology Water-soluble thiol-capped nanocrystals
US6306610B1 (en) * 1998-09-18 2001-10-23 Massachusetts Institute Of Technology Biological applications of quantum dots
US6617583B1 (en) * 1998-09-18 2003-09-09 Massachusetts Institute Of Technology Inventory control
US6251303B1 (en) * 1998-09-18 2001-06-26 Massachusetts Institute Of Technology Water-soluble fluorescent nanocrystals
US6326144B1 (en) * 1998-09-18 2001-12-04 Massachusetts Institute Of Technology Biological applications of quantum dots
EP1179185B1 (en) * 1999-05-07 2009-08-12 Life Technologies Corporation A method of detecting an analyte using semiconductor nanocrystals
US6696299B1 (en) * 1999-05-11 2004-02-24 Massachusetts Institute Of Technology Polarization label for measuring 3-dimensional orientation
US6440213B1 (en) * 1999-10-28 2002-08-27 The Regents Of The University Of California Process for making surfactant capped nanocrystals
US6306736B1 (en) * 2000-02-04 2001-10-23 The Regents Of The University Of California Process for forming shaped group III-V semiconductor nanocrystals, and product formed using process
US6225198B1 (en) * 2000-02-04 2001-05-01 The Regents Of The University Of California Process for forming shaped group II-VI semiconductor nanocrystals, and product formed using process
WO2001071043A1 (en) * 2000-03-22 2001-09-27 Quantum Dot Corporation Loop probe hybridization assay for polynucleotide analysis
US6548264B1 (en) * 2000-05-17 2003-04-15 University Of Florida Coated nanoparticles
US6649138B2 (en) * 2000-10-13 2003-11-18 Quantum Dot Corporation Surface-modified semiconductive and metallic nanoparticles having enhanced dispersibility in aqueous media
US6576291B2 (en) * 2000-12-08 2003-06-10 Massachusetts Institute Of Technology Preparation of nanocrystallites
US20020083888A1 (en) * 2000-12-28 2002-07-04 Zehnder Donald A. Flow synthesis of quantum dot nanocrystals
US6846565B2 (en) * 2001-07-02 2005-01-25 Board Of Regents, The University Of Texas System Light-emitting nanoparticles and method of making same
US20040007169A1 (en) * 2002-01-28 2004-01-15 Mitsubishi Chemical Corporation Semiconductor nanoparticles and thin film containing the same
US6805904B2 (en) * 2002-02-20 2004-10-19 International Business Machines Corporation Process of forming a multilayer nanoparticle-containing thin film self-assembly
US7001669B2 (en) * 2002-12-23 2006-02-21 The Administration Of The Tulane Educational Fund Process for the preparation of metal-containing nanostructured films
JP4769448B2 (en) * 2004-10-08 2011-09-07 キヤノン株式会社 Exposure apparatus having interferometer and device manufacturing method
US20060240590A1 (en) * 2004-11-09 2006-10-26 The Research Foundation Of State University Of New York Controlled synthesis of nanowires, nanodiscs, and nanostructured materials using liquid crystalline templates
WO2006105102A2 (en) * 2005-03-28 2006-10-05 The Research Foundation Of State University Of New York Synthesis of nanostructured materials using liquid crystalline templates

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5019400A (en) * 1989-05-01 1991-05-28 Enzytech, Inc. Very low temperature casting of controlled release microspheres
US6235224B1 (en) * 1995-07-21 2001-05-22 Brown University Research Foundation Process for preparing microparticles through phase inversion phenomena

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
ZHU J, KOLTYPIN Y, GEDANKEN A.: "General sonochemical method for the preparation of nanophasic selenides: synthesis of ZnSe nanoparticles.", CHEM MATER., vol. 12, no. 1, 28 February 1991 (1991-02-28), pages 73 - 78, XP000919562 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8455088B2 (en) 2005-12-23 2013-06-04 Boston Scientific Scimed, Inc. Spun nanofiber, medical devices, and methods

Also Published As

Publication number Publication date
WO2005016824A2 (en) 2005-02-24
US8859000B2 (en) 2014-10-14
US20050006800A1 (en) 2005-01-13

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