WO2004037715A3 - Low temperature method for preparing trimetallic nitride endohedral metallofullerenes - Google Patents

Low temperature method for preparing trimetallic nitride endohedral metallofullerenes Download PDF

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Publication number
WO2004037715A3
WO2004037715A3 PCT/US2003/021692 US0321692W WO2004037715A3 WO 2004037715 A3 WO2004037715 A3 WO 2004037715A3 US 0321692 W US0321692 W US 0321692W WO 2004037715 A3 WO2004037715 A3 WO 2004037715A3
Authority
WO
WIPO (PCT)
Prior art keywords
endohedral metallofullerenes
metal
preparing
trimetallic nitride
low temperature
Prior art date
Application number
PCT/US2003/021692
Other languages
French (fr)
Other versions
WO2004037715A2 (en
Inventor
Harry C Dorn
Clayton Mckee
Jim Duchamp
Original Assignee
Virginia Tech Intell Prop
Harry C Dorn
Clayton Mckee
Jim Duchamp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Virginia Tech Intell Prop, Harry C Dorn, Clayton Mckee, Jim Duchamp filed Critical Virginia Tech Intell Prop
Priority to AU2003301557A priority Critical patent/AU2003301557A1/en
Publication of WO2004037715A2 publication Critical patent/WO2004037715A2/en
Publication of WO2004037715A3 publication Critical patent/WO2004037715A3/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00Manufacture or treatment of nanostructures
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/152Fullerenes
    • C01B32/154Preparation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00Compounds containing elements of Groups 3 or 13 of the Periodic System
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/10Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of rare earths
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24Nitrogen compounds

Abstract

A method for forming trimetallic nitride endohedral metallofullerenes having the general formula A3-nXnN@Cm, wherein A is a first metal, X is an optional second metal, n is an integer from 0-3, and m is an even integer from about 60 to about 200 is described. The method includes heating a mixture of carbon, a first metal, an option second metal, and a nitrogen containing compound in a reactor that has been sealed under vacuum at a temperature and for a time effective to form trimetallic nitride endohedral metallofullerenes.
PCT/US2003/021692 2002-07-12 2003-07-11 Low temperature method for preparing trimetallic nitride endohedral metallofullerenes WO2004037715A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2003301557A AU2003301557A1 (en) 2002-07-12 2003-07-11 Low temperature method for preparing trimetallic nitride endohedral metallofullerenes

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US39532702P 2002-07-12 2002-07-12
US60/395,327 2002-07-12

Publications (2)

Publication Number Publication Date
WO2004037715A2 WO2004037715A2 (en) 2004-05-06
WO2004037715A3 true WO2004037715A3 (en) 2004-11-18

Family

ID=32176410

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2003/021692 WO2004037715A2 (en) 2002-07-12 2003-07-11 Low temperature method for preparing trimetallic nitride endohedral metallofullerenes

Country Status (2)

Country Link
AU (1) AU2003301557A1 (en)
WO (1) WO2004037715A2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113023690B (en) * 2019-12-25 2023-01-24 中国科学院化学研究所 Metal nitride embedded fullerene and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6303760B1 (en) * 1999-08-12 2001-10-16 Virginia Tech Intellectual Properties, Inc. Endohedral metallofullerenes and method for making the same

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6303760B1 (en) * 1999-08-12 2001-10-16 Virginia Tech Intellectual Properties, Inc. Endohedral metallofullerenes and method for making the same

Also Published As

Publication number Publication date
WO2004037715A2 (en) 2004-05-06
AU2003301557A1 (en) 2004-05-13
AU2003301557A8 (en) 2004-05-13

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