WO2003075868A1 - Sourdough-based skin medication and skin care product, and production method - Google Patents

Sourdough-based skin medication and skin care product, and production method Download PDF

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Publication number
WO2003075868A1
WO2003075868A1 PCT/EP2003/002342 EP0302342W WO03075868A1 WO 2003075868 A1 WO2003075868 A1 WO 2003075868A1 EP 0302342 W EP0302342 W EP 0302342W WO 03075868 A1 WO03075868 A1 WO 03075868A1
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WIPO (PCT)
Prior art keywords
product
medicinal
cereal
care
sourdough
Prior art date
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PCT/EP2003/002342
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German (de)
French (fr)
Inventor
Gabriele Wolf
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Woresan Gmbh
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Priority to AU2003212315A priority Critical patent/AU2003212315A1/en
Publication of WO2003075868A1 publication Critical patent/WO2003075868A1/en

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
    • A61K35/66—Microorganisms or materials therefrom
    • A61K35/74—Bacteria
    • A61K35/741—Probiotics
    • A61K35/744—Lactic acid bacteria, e.g. enterococci, pediococci, lactococci, streptococci or leuconostocs
    • A61K35/747—Lactobacilli, e.g. L. acidophilus or L. brevis
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/02—Preparations for cleaning the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/12—Preparations containing hair conditioners

Definitions

  • the invention relates to a method for producing a medicinal and care agent for the skin based on an acidified leaven, a medicinal and care product obtainable by this process, a cosmetic containing a medicinal and care product and the use of the medicinal and care product according to the invention in one Cosmetic.
  • DE 38 02 840 02 has already disclosed a process for producing a fermentation product containing lactic acid and viable lactic acid bacteria by acidifying an aqueous slurry of baked bread mass based on sourdough in lactic acid medium, the baked product of an acidified bread dough being used as the bread mass.
  • This fermentation product is said to be u. a. can be used as an aid in the treatment of the holistic organism of humans, animals and plants.
  • EP 0 530 861 B1 discloses a topical, antimicrobial pharmaceutical composition which comprises a mixture of C 6 to C 8 fatty acids.
  • DE 299 23 627 Ul relates to a medicinal and care agent for promoting blood circulation, for relieving muscle tension, for skin cleansing and for skin regeneration, which is applied to parts of the body or used as an additive to a water bath.
  • the product is characterized in that it is formed from a fermentation product of an acidified leaven '.
  • CH-A5-623 207 relates to a process for the production of foods containing a product from cereal germs fermented by lactic acid bacteria. There are no indications of any other use of the product outside of the food sector.
  • DE-A-39 05 055 discloses a whole grain product and a method for its production. The production of baked products or dry products based on a starting product is described, which is inoculated with a Lactobacillus culture after briefly germinating a grain.
  • WO-A-96/13981 discloses dry baked products and processes for their manufacture.
  • GB-A-1 539 756 relates to a process for the production of food products using cereal germ products fermented with lactic acid bacteria.
  • the object of the present invention was to improve the positive influences, in particular the effects known from DE 299 23 627 Ul.
  • the range of valuable ingredients of the well-known fermentation products is to be expanded, e.g. B. the amount of vitamins and other biotic factors can be increased.
  • fermentation products from germinated cereal products with heterofermentative lactic acid bacteria are suitable for solving the task at hand.
  • Natural products formed by fermentation that are brought into contact with the skin have the potential to positively influence skin that requires care.
  • the present invention relates to a method for producing a healing and care agent for the skin from fermentation products based on an acidified leaven, wherein 1.1 a germinated cereal product water and a bacteriological inoculum from the group of heterofermentative lactic acid bacteria, preferably LactobaciUus DSM 6037 and LactobaciUus DSM 6129, are added 1.2 and the approach until the metabolic activity of the
  • Microorganisms is acidified.
  • the germinated grain product is obtained, for example, by washing germinable seeds, preferably from organic cultivation, swelling and bringing them to sowing. Germination preferably takes place in packaged cultures.
  • the germinated sprouts are harvested after 36 to 48 hours. After the harvest, washing is done with cold, preferably ice-cold water.
  • the germinated sprouts can then be processed immediately or stored at temperatures up to 7 ° C for a long time. The storage time should not exceed 1 week.
  • the fermentation product is subjected to a stabilizing heating process near the boiling point.
  • the invention relates to a healing and care agent for the skin based on an acidified leaven obtainable by the process according to the invention.
  • the medicinal and care agent according to the invention advantageously has a high proportion of lactic acid obtained by fermentation of> 60% by weight (as a proportion of the total amount of acid).
  • the medicinal and care products according to the invention can be mixed with auxiliaries and carriers customary in cosmetics in order to produce cosmetics.
  • the medicinal and care products according to the invention which can be used are used in particular in the form of powders, cereal fluids, cereal serums and cereal gels.
  • the cosmetic according to the invention which can be produced from the medicinal and care products according to the invention can be used in particular in the form of ointments, powders, creams, lotions, gels, shampoos, hair rinses, packs, lipsticks, face and body masks, or combinations thereof.
  • a facial mask for cleaning can be produced from incidents known in cosmetic formulations, such as steareth-12 or steareth-21, glyceryl stearates, stearic acid, alkylbenzoates with chain lengths of in particular 12 to 15 carbon atoms, cetearylisononanoate, stearylheptanuate, octyl stearate, fragrance or aroma substances such as Persea Gratissima Avocadol (CosmoCare), the cereal gel or cereal fluid according to the invention, propylene glycol, fillers such as kaolin and water.
  • Another form of application can consist predominantly of serum according to the invention with a high lactic acid content as well as vitamins and other supplements.
  • a shampoo can typically contain increments, such as sodium laureth sulfate, disodium laureth sulfosuccinate, cocoamidopropyl betaine, PEG-7 glyceryl cocoate, the cereal serum according to the invention, fillers such as styrene-acrylate copolymers / Laureth-23, citric acid, polyquaternium-18 (Amer-Glychol) (Amereatol) -cocoate as well as water, preservatives and fragrances.
  • increments such as sodium laureth sulfate, disodium laureth sulfosuccinate, cocoamidopropyl betaine, PEG-7 glyceryl cocoate, the cereal serum according to the invention, fillers such as styrene-acrylate copolymers / Laureth-23, citric acid, polyquaternium-18 (Amer-Glychol) (Amereatol) -cocoate as well as water, preservatives
  • a typical spa pack can consist of cetearyl alcohol, ceteareth-12, ceteareth-20, PEG-75 lanolin, Triticum Vulgare (Dragoco), the cereal fluid or cereal serum according to the invention, hydroxycetyl or hedroxyethyl dimonium chlorite from Henkel, panthenol, citric acid as well as water, preservatives and fragrances.
  • a hair conditioner can in particular consist of the cereal fluid or cereal serum according to the invention with fragrances, preservatives and fillers, for example fruit vinegar, glycerol, cetearyl alcohol, ceteareth-12, cetrimonium chlorite, PEG-75 lanolin, preservatives, fragrances and water.
  • fragrances for example fruit vinegar, glycerol, cetearyl alcohol, ceteareth-12, cetrimonium chlorite, PEG-75 lanolin, preservatives, fragrances and water.
  • fragrances for example fruit vinegar, glycerol, cetearyl alcohol, ceteareth-12, cetrimonium chlorite, PEG-75 lanolin, preservatives, fragrances and water.
  • fragrances for example fruit vinegar, glycerol, cetearyl alcohol, ceteareth-12, cetrimonium chlorite, PEG-75 lanolin, preservatives, fragrances and water.
  • the medicinal and care agent according to the invention is used in the form of a cereal fluid. It is a creamy raw material obtained from cereal gel, which excels in creams, lotions, shampoos, hair conditioners and packs.
  • the cereal gel according to the invention is a rather viscous raw material that can also be used directly as a medicinal and care agent according to the invention. It is the product obtained more or less directly from the fermentation process, which can be used in an unchanged form as a natural face or body mask and as a bath additive.
  • An advantage of this embodiment is the absence of potentially incompatible constituents which are stressful to the organism. After application, improvements in the skin relief and slowing of the formation of skin imperfections become apparent.
  • the agent can serve as a biological peeling agent for dead skin flakes, with a moisturizing effect advantageously appearing.
  • a cereal serum can in turn be obtained from cereal fluid. It is suitable as a raw material for incorporation into face and body masks, lipsticks, shampoos and conditioners as well as hair packs.
  • grain powder for example, grain powder, grain fluid and grain serum can be produced.
  • the grain powder can be produced by separating the solids from the grain gel according to the invention, which is then dried and ground.
  • the solids of the cereal powder can be used as peeling bodies in the cosmetics according to the invention.
  • the cereal fluid is produced, for example, by separating it from the purified gel and enriching it with unfiltered grain serum until the viscosity suitable for the use has been set. This product is a raw material with a high proportion of active ingredients.
  • the cereal serum is produced, for example, by filtering the liquid supernatant of the cereal gel according to the invention obtained from the fermentation and then clarifying it. This creates a product with a very high proportion of active ingredients.
  • the invention also relates to the use of the medicinal and care agents according to the invention in a cosmetic according to the invention.
  • a preferred use of the medicinal and care agents according to the invention in liposomes should be mentioned.
  • the present invention also relates to liposomes with the medicinal and care products according to the invention.
  • Germination of the grain 10 kg of germinable grain, for example rye grain are washed with cold water and soaked in cold water for 4 hours to swell. The water is then removed. The grain treated in this way is filled into a container with a large base and spread out. The grain layer then has a layer thickness of about 2 to 3 cm. The container is then covered. The temperature during germination is approx. 20 ° C. Germination is improved if the container is well ventilated. After about 40 hours, the grain germs are removed and washed in ice-cold water. The grain germs can then be processed directly or the germs can be stored at a maximum of 7 ° C.
  • part of the grain germinated according to Example 1 is mixed with two parts of water. Fermentation media with LactobaciUus DSM 6037 and LactobaciUus DSM 6129 are added to this mixture. This mixture is fermented at temperatures of 30 to 34 C for 24 to 48 hours. The fermentation is finished when a constant pH value is reached. The from the initial fermentation The mixture obtained is made up with 87.5 parts, based on the total volume of the initial fermentation, with water. The fermentation time is 24 to 48 hours until a constant pH is reached at a typical temperature of 30 to 34 C. Thereafter there is a thermal treatment for 3 to 5 hours at a temperature of 92 to 100 C.
  • Preservatives such as sorbic acid
  • benzoic acid Typically, 0.75 part of sorbic acid can be used based on the total volume.
  • the preservation step is followed by the separation processes for the production of the individual fractions, such as grain serum and grain
  • the table shows a comparison of selected ingredients from the product according to the invention and a product that was not produced on the basis of germinated rye.

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Abstract

Disclosed is a method for producing a medicament and care product for skin, which is based on fully leavened sourdough. According to the inventive method, water and a bacteriological inoculum from the group of heterofermentative lactic acid bacteria, preferably lactobacillus DSM 6037 and lactobacillus DSM 6129, are added to a germinated wheat product, and the batch is leavened until the microorganisms have ceased their metabolistic activity.

Description

HEIL- UND PFLEGEMITTEL AUF BASIS VON SAUERTEIG, SOWIE VERFAHREN ZUR HERSTELLUNG HEALTH AND CARE PRODUCTS BASED ON Sourdough, AND METHOD FOR THE PRODUCTION THEREOF
Die Erfindung betrifft ein Verfahren zur Herstellung eines Heil- und Pflegemittels für die Haut auf Basis eines ausgesäuerten Sauerteiges, ein Heil- und Pflegemittel erhältlich nach diesem Verfahren, ein Kosmetikum enthaltend ein Heil- und Pflegemittel sowie die Verwendung des erfindungsgemäßen Heil- und Pflegemittels in einem Kosmetikum.The invention relates to a method for producing a medicinal and care agent for the skin based on an acidified leaven, a medicinal and care product obtainable by this process, a cosmetic containing a medicinal and care product and the use of the medicinal and care product according to the invention in one Cosmetic.
Aus der DE 38 02 840 02 ist bereits ein Verfahren zur Herstellung eines Milchsäure und lebensfähige Milchsäurebakterien enthaltenden Gärproduktes durch Versauern einer wässrigen Aufschlämmung von gebackener Brotmasse auf Sauerteigbasis in milchsaurem Medium bekannt geworden, wobei als Brotmasse das Backprodukt eines ausgesäuerten Brotteiges eingesetzt wird. Dieses Gärprodukt soll als u. a. als Hilfsmittel bei der Behandlung des ganzheitlichen Organismus von Mensch, Tier und Pflanze einsetzbar sein.DE 38 02 840 02 has already disclosed a process for producing a fermentation product containing lactic acid and viable lactic acid bacteria by acidifying an aqueous slurry of baked bread mass based on sourdough in lactic acid medium, the baked product of an acidified bread dough being used as the bread mass. This fermentation product is said to be u. a. can be used as an aid in the treatment of the holistic organism of humans, animals and plants.
Aus der DE 38 46 186 AI ist es auch bereits bekannt geworden, aus dem Gär- schlämm der Spontanversäuerung von Sauerteigbroten gewonnene Präparate z. B. als Packungszuschlagstoff zur Behandlung von chronisch entzündlichen Krankheiten der Haut einzusetzen.From DE 38 46 186 AI it has also become known to prepare preparations obtained from the fermentation sludge from the spontaneous acidification of sourdough breads. B. as a pack additive for the treatment of chronic inflammatory diseases of the skin.
Durch die DT 26 11 972 Bl ist es bereits bekannt geworden, zum Herstellen eines Sauerteigs für die Bereitung von Broten und Backwaren aus Getreide- schroten und/oder Mehlen in der den Vorteig bildenden Getreidemaische die Sauerteigbakterien bis zur Einstellung jeglicher bakteriologischer Stoffwechselaktivität auszusäuern.From DT 26 11 972 Bl it has already become known to acidify the sourdough bacteria until the cessation of any bacteriological metabolic activity in order to produce a sourdough for the preparation of bread and baked goods from grain meal and / or flour in the cereal mash which forms the pre-dough.
In der EP 0 530 861 Bl ist eine topische, antimikrobielle pharmazeutische Zusammensetzung offenbart, die ein Gemisch aus C6- bis Cι8-Fettsäuren um- fasst.EP 0 530 861 B1 discloses a topical, antimicrobial pharmaceutical composition which comprises a mixture of C 6 to C 8 fatty acids.
DE 299 23 627 Ul betrifft ein Heil- und Pflegemittel zur Förderung der Durchblutung, zur Lösung von Muskelverspannungen, zur Hautreinigung und zur Hautregenerierung, das auf Körperteile aufgetragen oder als Zusatz zu einem Wasserbad verwendet wird. Das Produkt ist dadurch gekennzeichnet, dass es von einem Fermentationsprodukt eines ausgesäuerten Sauerteiges gebildet' ist. Die CH-A5-623 207 betrifft ein Verfahren zur Herstellung von Nahrungsmitteln, enthaltend ein durch Milchsäurebakterien fermentiertes Produkt aus Getreidekeimen. Hinweise auf anderweitige Verwendung des Produkts außerhalb des Nahrungsmittelbereichs sind nicht erkennbar. DE-A-39 05 055 offenbart ein Getreidevollkornprodukt sowie ein Verfahren zu seiner Herstellung. Es wird die Herstellung von Backprodukten oder Trockenprodukten auf Basis von einem Ausgangsprodukt beschrieben, das nach Kurzkeimung eines Getreides mit einer Lactobacillus-Kultur beimpft wird.DE 299 23 627 Ul relates to a medicinal and care agent for promoting blood circulation, for relieving muscle tension, for skin cleansing and for skin regeneration, which is applied to parts of the body or used as an additive to a water bath. The product is characterized in that it is formed from a fermentation product of an acidified leaven '. CH-A5-623 207 relates to a process for the production of foods containing a product from cereal germs fermented by lactic acid bacteria. There are no indications of any other use of the product outside of the food sector. DE-A-39 05 055 discloses a whole grain product and a method for its production. The production of baked products or dry products based on a starting product is described, which is inoculated with a Lactobacillus culture after briefly germinating a grain.
EP-A-0 806 144 betrifft die Herstellung eines flüssigen oder pastösen biologi- sehen Backmittels mit Hilfe von Milchsäurebakterien, dem, je nach Anwendung und Brotrezeptur noch Enzyme, Malzmehl und Ascorbinsäure oder ascorbin- säurehaltige Fruchtpulver zugegeben werden können, sowie ein danach hergestelltes biologisches Backmittel.EP-A-0 806 144 relates to the production of a liquid or pasty biological baking agent with the help of lactic acid bacteria, to which, depending on the application and bread recipe, enzymes, malt flour and ascorbic acid or fruit powder containing ascorbic acid can be added, as well as a biological product produced thereafter caking agent.
WO-A-96/13981 offenbart Trocken-Backprodukte und Verfahren zu ihrer Her- Stellung. Die GB-A-1 539 756 betrifft ein Verfahren zur Herstellung von Nahrungsprodukten untr Verwendung von mit Milchsäure Bakterien fermentierten Getreidekeimprodukten.WO-A-96/13981 discloses dry baked products and processes for their manufacture. GB-A-1 539 756 relates to a process for the production of food products using cereal germ products fermented with lactic acid bacteria.
Aufgabe der vorliegenden Erfindung war es, die positiven Einflüsse, insbesondere die aus der DE 299 23 627 Ul bekannten Wirkungen, zu verbessern. Ins- besondere soll die Palette wertvoller Inhaltsstoffe der bekannten Fermentationsprodukte erweitert werden, z. B. die Menge an Vitaminen und anderen biotischen Faktoren erhöht werden.The object of the present invention was to improve the positive influences, in particular the effects known from DE 299 23 627 Ul. In particular, the range of valuable ingredients of the well-known fermentation products is to be expanded, e.g. B. the amount of vitamins and other biotic factors can be increased.
Überraschenderweise sind Fermentationsprodukte von gekeimten Getreideprodukten mit heterofermentativen Milchsäurebakterien geeignet, die gestellte Aufgabe zu lösen. Natürliche durch Fermentation gebildete Produkte, die mit der Haut in Kontakt gebracht werden besitzen ein Potential, pflegebedürftige Haut positiv zu beeinflussen.Surprisingly, fermentation products from germinated cereal products with heterofermentative lactic acid bacteria are suitable for solving the task at hand. Natural products formed by fermentation that are brought into contact with the skin have the potential to positively influence skin that requires care.
Gegenstand der vorliegenden Erfindung ist ein Verfahren zur Herstellung eines Heil- und Pflegemittels für die Haut aus Fermentationsprodukten auf Basis ei- nes ausgesäuerten Sauerteiges, wobei 1.1 einem gekeimten Getreideprodukt Wasser sowie ein bakteriologisches Impfgut aus der Gruppe der heterofermentativen Milchsäurebakterien, vorzugsweise LactobaciUus DSM 6037 und LactobaciUus DSM 6129, zugegeben wird 1.2 und der Ansatz bis zur Einstellung der Stoffwechseltätigkeit derThe present invention relates to a method for producing a healing and care agent for the skin from fermentation products based on an acidified leaven, wherein 1.1 a germinated cereal product water and a bacteriological inoculum from the group of heterofermentative lactic acid bacteria, preferably LactobaciUus DSM 6037 and LactobaciUus DSM 6129, are added 1.2 and the approach until the metabolic activity of the
Mikroorganismen ausgesäuert wird.Microorganisms is acidified.
Erfindungsgemäß wird insbesondere das gekeimte Getreideprodukt nach der Keimung vermählen und mit dem bakteriologischen Impfgut vermischt.According to the invention, the germinated cereal product in particular is ground after germination and mixed with the bacteriological inoculum.
Das gekeimte Getreideprodukt wird beispielsweise erhalten, indem keimfähi- ges Saatgut vorzugsweise aus biologischem Anbau gewaschen, gequollen und zur Aussaat gebracht wird. Die Keimung erfolgt vorzugsweise in abgepackten Kulturen. Die Ernte der gekeimten Sprossen erfolgt nach 36 bis 48 Stunden. Nach der Ernte erfolgen Waschvorgänge mit kaltem, vorzugsweise eiskaltem Wasser. Die gekeimten Sprossen können danach sofort weiterverarbeitet wer- den oder bei Temperaturen bis maximal 7° C auch längere Zeit gelagert werden. Die Lagerzeit sollte 1 Woche nicht überschreiten..The germinated grain product is obtained, for example, by washing germinable seeds, preferably from organic cultivation, swelling and bringing them to sowing. Germination preferably takes place in packaged cultures. The germinated sprouts are harvested after 36 to 48 hours. After the harvest, washing is done with cold, preferably ice-cold water. The germinated sprouts can then be processed immediately or stored at temperatures up to 7 ° C for a long time. The storage time should not exceed 1 week.
Als Getreide kommen insbesondere Roggen, Weizen und Gerste in Betracht. In einer Weiterbildung des erfindungsgemäßen Verfahrens wird dem Fermentationsprodukt ein zweites kohlehydrathaltiges Substrat und Wasser zugegeben. Die Mischung wird ausgesäuert,Rye, wheat and barley are particularly suitable cereals. In a further development of the method according to the invention, a second carbohydrate-containing substrate and water are added to the fermentation product. The mixture is acidified
- der letzte Verfahrensschritt ggf. ein oder mehrmals wiederholt, wobei die Mischung abschließend bis zur Einstellung jeglicher bakteriologischer Stoffwechselaktivität ausgesäuert wird und- Repeat the last process step, if necessary, one or more times, the mixture finally being acidified until all bacteriological metabolic activity ceases, and
- das Fermentationsprodukt wird einem stabilisierenden Erhitzungsprozess nahe der Siedetemperatur unterzogen.- The fermentation product is subjected to a stabilizing heating process near the boiling point.
Gegenstand der Erfindung ist ein Heil- und Pflegemittel für die Haut auf Basis eines ausgesäuerten Sauerteiges erhältlich nach dem erfindungsgemäßen Verfahren. Das erfindungsgemäße Heil- und Pflegemittel weist vorteilhafterweise einen hohen Anteil auf fermentativem Wege gewonnener Milchsäure von > 60 Gew.- % (als Anteil der Gesamtsäuremenge) auf.The invention relates to a healing and care agent for the skin based on an acidified leaven obtainable by the process according to the invention. The medicinal and care agent according to the invention advantageously has a high proportion of lactic acid obtained by fermentation of> 60% by weight (as a proportion of the total amount of acid).
Die erfindungsgemäßen Heil- und Pflegemittel sind mit in der Kosmetik übli- chen Hilfs- und Trägerstoffen versetzbar, um Kosmetika herzustellen.The medicinal and care products according to the invention can be mixed with auxiliaries and carriers customary in cosmetics in order to produce cosmetics.
Die einsetzbaren erfindungsgemäßen Heil- und Pflegemittel werden insbesondere in Form von Pulvern, Getreidefluiden, Getreideseren, Getreidegelen verwendet.The medicinal and care products according to the invention which can be used are used in particular in the form of powders, cereal fluids, cereal serums and cereal gels.
Das aus den erfindungsgemäßen Heil- und Pflegemittel herstellbare erfin- dungsgemäße Kosmetikum kann insbesondere in Form von Salben, Pulvern, Cremes, Lotionen, Gelen, Shampoos, Haarspülungen, Packungen, Lippenstiften, Gesichts- und Körpermasken, oder Kombinationen davon eingesetzt werden.The cosmetic according to the invention which can be produced from the medicinal and care products according to the invention can be used in particular in the form of ointments, powders, creams, lotions, gels, shampoos, hair rinses, packs, lipsticks, face and body masks, or combinations thereof.
So kann beispielsweise eine Gesichtsmaske zur Reinigung hergestellt werden aus in kosmetischen Rezepturen geläufigen Inkredenzien, wie Steareth-12 oder Steareth-21, Glycerylstearaten, Stearinsäure, Alkylbenzoaten mit Kettenlängen von insbesondere 12 bis 15 Kohlenstoffatomen, Cetearylisononanoat, Stearylheptanuat, Octylstearat, Duft- oder Aromastoffen, wie beispielsweise Persea Gratissima Avocadol (Firma CosmoCare), dem erfindungsgemäßen Getreidegel oder Getreidefluid, Propyleneglycol, Füllstoffen wie Kaolin und Wasser. Eine andere Anwendungsform kann bestehen aus überwiegend erfindungsgemäßem Serum mit hohem Milchsäuregehalt sowie Vitaminen und anderen Ergänzungsstoffen. Ein Shampoo kann typischerweise Inkredenzien enthalten, wie Sodiumlaurethsulfat, Dinatriumlaurethsulfosuccinat, Cocoami- dopropylbetain, PEG-7 Glycerylcocoate, dem erfindungsgemäßen Getreideserum, Füllstoffen wie Styrolacrylatcopolymeren/Laureth-23, Zitronensäure, Po- lyquaternium-10 (Firma Amerchol), PEG-18 Glyceryloleat oder -cocoate sowie Wasser, Konservierungsstoffen und Duftstoffen. Eine typische Kurpackung kann bestehen aus Cetearylalkohol, Ceteareth-12, Ceteareth-20, PEG-75 La- nolin, Triticum Vulgäre (Firma Dragoco), dem erfindungsgemäßen Getreidefluid oder Getreideserum, Hydroxycetyl oder Hedroxyethyl Dimonium Chlorith der Firma Henkel, Panthenol, Zitronensäure sowie Wasser, Konservierungsstoffe und Duftstoffe.For example, a facial mask for cleaning can be produced from incidents known in cosmetic formulations, such as steareth-12 or steareth-21, glyceryl stearates, stearic acid, alkylbenzoates with chain lengths of in particular 12 to 15 carbon atoms, cetearylisononanoate, stearylheptanuate, octyl stearate, fragrance or aroma substances such as Persea Gratissima Avocadol (CosmoCare), the cereal gel or cereal fluid according to the invention, propylene glycol, fillers such as kaolin and water. Another form of application can consist predominantly of serum according to the invention with a high lactic acid content as well as vitamins and other supplements. A shampoo can typically contain increments, such as sodium laureth sulfate, disodium laureth sulfosuccinate, cocoamidopropyl betaine, PEG-7 glyceryl cocoate, the cereal serum according to the invention, fillers such as styrene-acrylate copolymers / Laureth-23, citric acid, polyquaternium-18 (Amer-Glychol) (Amereatol) -cocoate as well as water, preservatives and fragrances. A typical spa pack can consist of cetearyl alcohol, ceteareth-12, ceteareth-20, PEG-75 lanolin, Triticum Vulgare (Dragoco), the cereal fluid or cereal serum according to the invention, hydroxycetyl or hedroxyethyl dimonium chlorite from Henkel, panthenol, citric acid as well as water, preservatives and fragrances.
Ein Haarkonditionierer kann insbesondere bestehen aus dem erfindungsgemä- ßen Getreidefluid oder Getreideserum mit Duft-, Konservierungs- und Füllstof- fen, beispielsweise Obstessig, Glycerin, Cetearylalkohol, Ceteareth-12, Cetri- moniumchlorith, PEG-75 Lanolin, Konservierungsstoffe, Duftstoffe sowie Wasser. Die genannten Inkredenzien sind in der Kosmetik üblicherweise eingesetzte Chemikalien und sämtlich kommerziell erhältlich.A hair conditioner can in particular consist of the cereal fluid or cereal serum according to the invention with fragrances, preservatives and fillers, for example fruit vinegar, glycerol, cetearyl alcohol, ceteareth-12, cetrimonium chlorite, PEG-75 lanolin, preservatives, fragrances and water. The above-mentioned increments are chemicals commonly used in cosmetics and all are commercially available.
In einer Ausführungsform der vorliegenden Erfindung wird das erfindungsge- maß Heil- und Pflegemittel in Form eines Getreidefluid eingesetzt. Dabei handelt es sich um einen cremigen aus Getreidegel gewonnenen Rohstoff, der sich auszeichnet in Cremes, Lotionen, Shampoos, Haarspülungen und Packungen. Das erfindungsgemäße Getreidegel ist ein eher dickflüssiger Rohstoff, der auch direkt als erfindungsgemäßes Heil- und Pflegemittel eingesetzt werden kann. Es handelt sich dabei um das mehr oder weniger unmittelbar aus dem Fer- mentationsprozess gewonnenen Produkt, was sich in unveränderter Form als natürliche Gesichts- oder Körpermaske sowie als Badezusatz einsetzen lässt. Vorteil an dieser Ausführungsform ist das Fehlen von den Organismus belastender möglicherweise unverträglicher Bestandteile. Nach Anwendung zeigen sich Verbesserungen des Hautreliefs und Verlangsamung der Bildung von Hautunreinheiten. Das Mittel kann als biologisches Peelingmittel abgestorbener Hautschuppen dienen, wobei Vorteilhafterweise ein Moisturizing-Effekt in Erscheinung tritt.In one embodiment of the present invention, the medicinal and care agent according to the invention is used in the form of a cereal fluid. It is a creamy raw material obtained from cereal gel, which excels in creams, lotions, shampoos, hair conditioners and packs. The cereal gel according to the invention is a rather viscous raw material that can also be used directly as a medicinal and care agent according to the invention. It is the product obtained more or less directly from the fermentation process, which can be used in an unchanged form as a natural face or body mask and as a bath additive. An advantage of this embodiment is the absence of potentially incompatible constituents which are stressful to the organism. After application, improvements in the skin relief and slowing of the formation of skin imperfections become apparent. The agent can serve as a biological peeling agent for dead skin flakes, with a moisturizing effect advantageously appearing.
Aus Getreidefluid kann seinerseits ein Getreideserum gewonnen werden. Es eignet sich als Rohstoff zum Einarbeiten in Gesichts- und Körpermasken, Lippenstiften, Shampoos und Spülungen sowie Haarpackungen.A cereal serum can in turn be obtained from cereal fluid. It is suitable as a raw material for incorporation into face and body masks, lipsticks, shampoos and conditioners as well as hair packs.
Ausgehend vom Getreidegel können beispielsweise Getreidepulver, Getreidefluid sowie das Getreideserum hergestellt werden. Ausgehend von Getreidegel kann das Getreidepulver hergestellt werden durch Separieren der Feststof- fe aus dem erfindungsgemäßen Getreidegel, das anschließend getrocknet und vermählen wird. Die Feststoffe des Getreidepulvers können als Peelingkörper in den erfindungsgemäßen Kosmetika eingesetzt werden. Das Getreidefluid wird beispielsweise hergestellt durch Abtrennung vom gereinigten Gel und Anreicherung mit unfiltriertem Getreideserum bis die für die Verwendung geeignete Viskosität eingestellt ist. Es handelt sich bei diesem Produkt um einen Rohstoff mit hohem Wirkstoffanteil. Das Getreideserum wird beispielsweise hergestellt durch Filtrieren des flüssigen Überstandes des aus der Fermentation gewonnenen erfindungsgemäßen Getreidegels und anschließende Klärung. Dabei entsteht ein Produkt mit sehr hohem Wirkstoffanteil.Starting from the grain gel, for example, grain powder, grain fluid and grain serum can be produced. Starting from grain gel, the grain powder can be produced by separating the solids from the grain gel according to the invention, which is then dried and ground. The solids of the cereal powder can be used as peeling bodies in the cosmetics according to the invention. The cereal fluid is produced, for example, by separating it from the purified gel and enriching it with unfiltered grain serum until the viscosity suitable for the use has been set. This product is a raw material with a high proportion of active ingredients. The cereal serum is produced, for example, by filtering the liquid supernatant of the cereal gel according to the invention obtained from the fermentation and then clarifying it. This creates a product with a very high proportion of active ingredients.
Gegenstand der Erfindung ist auch die Verwendung der erfindungsgemäßen Heil- und Pflegemittel in einem Kosmetikum gemäß der Erfindung. Dabei ist eine bevorzugte Verwendung der erfindungsgemäßen Heil- und Pflegemittel in Liposomen zu erwähnen. Gegenstand der vorliegenden Erfindung sind auch Liposomen mit den erfindungsgemäßen Heil- und Pflegemitteln.The invention also relates to the use of the medicinal and care agents according to the invention in a cosmetic according to the invention. A preferred use of the medicinal and care agents according to the invention in liposomes should be mentioned. The present invention also relates to liposomes with the medicinal and care products according to the invention.
Beispiel 1example 1
Keimung des Getreides 10 Kilogramm keimfähiges Getreide, zum Beispiel Roggengetreide, werden mit kaltem Wasser gewaschen und zur Quellung in kaltem Wasser für 4 Stunden eingeweicht. Danach wird das Wasser entfernt. Das so behandelte Getreide wird in einen Behälter mit großer Bodenfläche gefüllt und ausgebreitet. Die Getreideschicht weist danach etwa eine Schichtdicke von 2 bis 3 cm auf. Da- nach wird der Behälter abgedeckt. Die Temperatur während der Keimung beträgt ca. 20° C. Die Keimung wird verbessert, wenn der Behälter gut belüftet ist. Nach etwa 40 Stunden werden die Getreidekeime entnommen und in eiskaltem Wasser gewaschen. Die Getreidekeime können danach direkt weiterverarbeitet werden oder die Keime sind bei maximal 7° C lagerfähig. Beispiel 2Germination of the grain 10 kg of germinable grain, for example rye grain, are washed with cold water and soaked in cold water for 4 hours to swell. The water is then removed. The grain treated in this way is filled into a container with a large base and spread out. The grain layer then has a layer thickness of about 2 to 3 cm. The container is then covered. The temperature during germination is approx. 20 ° C. Germination is improved if the container is well ventilated. After about 40 hours, the grain germs are removed and washed in ice-cold water. The grain germs can then be processed directly or the germs can be stored at a maximum of 7 ° C. Example 2
Zur Herstellung des erfindungsgemäßen Getreidegels wird ein Teil des nach Beispiel 1 gekeimten Getreides mit zwei Teilen Wasser vermischt. Dieser Mischung werden Fermentationsmedien mit LactobaciUus DSM 6037 sowie LactobaciUus DSM 6129 zugegeben. Diese Mischung wird für 24 bis 48 Stunden bei Temperaturen von 30 bis 34 C fermentiert. Die Fermentation ist beendet, wenn sich ein konstanter pH-Wert einstellt. Die aus der Startfermentation ge- wonnene Mischung wird mit 87,5 Teilen, bezogen auf das Gesamtvolumen der Startfermentation, mit Wasser aufgefüllt. Die Fermentationszeit beträgt 24 bis 48 Stunden bis ein konstanter pH-Wert erreicht wird bei einer typischen Temperatur von 30 bis 34 C. Danach erfolgt eine thermische Behandlung für 3 bis 5 Stunden bei einer Temperatur von 92 bis 100 C. Gegebenenfalls werden Konservierungsmittel, wie Sorbinsäure und Benzoesäure, hinzugegeben. Typischerweise können 0,75 Teile Sorbinsäure bezogen auf das Gesamtvolumen eingesetzt werden. An den Konservierungsschritt schließen sich die Trennverfahren zur Herstellung der einzelnen Fraktionen, wie Getreideserum, Getrei¬To produce the cereal gel according to the invention, part of the grain germinated according to Example 1 is mixed with two parts of water. Fermentation media with LactobaciUus DSM 6037 and LactobaciUus DSM 6129 are added to this mixture. This mixture is fermented at temperatures of 30 to 34 C for 24 to 48 hours. The fermentation is finished when a constant pH value is reached. The from the initial fermentation The mixture obtained is made up with 87.5 parts, based on the total volume of the initial fermentation, with water. The fermentation time is 24 to 48 hours until a constant pH is reached at a typical temperature of 30 to 34 C. Thereafter there is a thermal treatment for 3 to 5 hours at a temperature of 92 to 100 C. Preservatives, such as sorbic acid, may be used and benzoic acid added. Typically, 0.75 part of sorbic acid can be used based on the total volume. The preservation step is followed by the separation processes for the production of the individual fractions, such as grain serum and grain
10 defluid oder Getreidepulver an.10 defluid or cereal powder.
Die Tabelle zeigt eine Gegenüberstellung ausgewählter Inhaltsstoffe aus dem erfindungsgemäßen Produkt und einem Produkt, das nicht auf Basis von gekeimten Roggen hergestellt worden ist.The table shows a comparison of selected ingredients from the product according to the invention and a product that was not produced on the basis of germinated rye.
Tabelletable
1515
Figure imgf000008_0001
Figure imgf000008_0001

Claims

PatentansprücheVerfahren zur Herstellung eines Heil- und Pflegemittels für die Haut auf Basis eines ausgesäuerten Sauerteiges, wobei 1.1 einem gekeimten Getreideprodukt Wasser sowie ein bakteriologisches Impfgut aus der Gruppe der heterofermentativen Milchsäurebakterien, vorzugsweise LactobaciUus DSM 6037 und LactobaciUus DSM 6129, zugegeben wird Process for the production of a healing and care agent for the skin based on an acidified leaven, whereby 1.1 water and a bacteriological inoculum from the group of heterofermentative lactic acid bacteria, preferably LactobaciUus DSM 6037 and LactobaciUus DSM 6129, are added to a germinated cereal product
1.2 und der Ansatz bis zur Einstellung der Stoffwechseltätigkeit der Mikroorganismen ausgesäuert wird. Verfahren nach Anspruch 1, wobei das gekeimte Getreideprodukt unmittelbar nach der Keimung vermählen wird. Verfahren nach Anspruch 1 und/oder 2, wobei das gekeimte Getreideprodukt erhältlich ist aus keimfähigem Saatgut, das gewaschen, gequollen und ausgesät wurde. Verfahren nach Anspruch mindestens einem der Ansprüche 1 bis 3, wobei dem Fermentationsprodukt ein zweites kohlehydrathaltiges Substrat und Wasser zugegeben wird,1.2 and the approach is acidified until the metabolic activity of the microorganisms ceases. The method of claim 1, wherein the germinated grain product is milled immediately after germination. A method according to claim 1 and / or 2, wherein the germinated cereal product is obtainable from germinable seeds which have been washed, swelled and sown. A method according to claim at least one of claims 1 to 3, wherein a second carbohydrate-containing substrate and water are added to the fermentation product,
- der letzte Verfahrensschritt ggf. ein oder mehrmals wiederholt wird, wo- bei die Mischung abschließend bis zur Einstellung jeglicher bakteriologischer Stoffwechselaktivität ausgesäuert wird und- The last process step is possibly repeated one or more times, the mixture finally being acidified until all bacteriological metabolic activity ceases, and
- das Fermentationsprodukt einem stabilisierenden Erhitzungsprozess nahe der Siedetemperatur unterzogen wird. Heil- und Pflegemittel für die Haut auf Basis eines ausgesäuerten Sauertei- ges erhältlich nach dem Verfahren nach mindestens einem der Ansprüche- The fermentation product is subjected to a stabilizing heating process near the boiling point. Medicinal and care products for the skin based on an acidified sourdough obtainable by the process according to at least one of the claims
1 bis 5. Heil- und Pflegemittel nach Anspruch 5, dadurch gekennzeichnet, dass das Heil- und Pflegemittel einen hohen Anteil auf fermentativem Wege gewonnenen Milchsäure von > 60 % (als Anteil der Gesamtsäuremenge) auf- weist, wobei vor der Aussäuerung des Sauerteigs eine Behandlung mit - Amylase erfolgt. eil- und Pflegemittel nach Anspruch 5 und/oder 6 mit in der Kosmetik üblichen Hilfs- und Trägerstoffen. eil- und Pflegemittel nach mindestens einem der Ansprüche 5 bis 7 in Form Pulvern, Getreidefluiden, Getreideseren, Getreidegelen. osmetikum enthaltend ein Heil- und Pflegemittel nach mindestens einem der Ansprüche 3 bis 6, in Form von Salben, Cremes, Lotionen, Gelen, Shampoos, Haarspülungen, Packungen, Lippenstiften, Gesichts- und Kör- permasken, oder Kombinationen davon. Verwendung von Heil- und Pflegemittel nach mindestens einem der Ansprüche 5 bis 8 in einem Kosmetikum nach Anspruch 9. Liposomen enthaltend ein Heil- und Pflegemittel nach mindestens einem der Ansprüche 5 bis 8. 1 to 5. Medicinal and care agent according to claim 5, characterized in that the medicinal and care agent has a high proportion of lactic acid obtained by fermentation of> 60% (as a proportion of the total amount of acid). points, treatment with - amylase taking place before the acidification of the sourdough. Express and care products according to claim 5 and / or 6 with auxiliaries and carriers customary in cosmetics. Urgent and maintenance products according to at least one of claims 5 to 7 in the form of powders, cereal fluids, cereal serums, cereal gels. Osmetikum containing a medicinal and care product according to at least one of claims 3 to 6, in the form of ointments, creams, lotions, gels, shampoos, hair rinses, packs, lipsticks, face and body masks, or combinations thereof. Use of medicinal and care products according to at least one of claims 5 to 8 in a cosmetic according to claim 9. Liposomes containing a medicinal and care product according to at least one of claims 5 to 8.
PCT/EP2003/002342 2002-03-13 2003-03-07 Sourdough-based skin medication and skin care product, and production method WO2003075868A1 (en)

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