WO2002099534A9 - Beleuchtungssystem mit einer vielzahl von einzelgittern - Google Patents
Beleuchtungssystem mit einer vielzahl von einzelgitternInfo
- Publication number
- WO2002099534A9 WO2002099534A9 PCT/EP2002/005688 EP0205688W WO02099534A9 WO 2002099534 A9 WO2002099534 A9 WO 2002099534A9 EP 0205688 W EP0205688 W EP 0205688W WO 02099534 A9 WO02099534 A9 WO 02099534A9
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- lighting system
- grating
- individual
- plane
- grids
- Prior art date
Links
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
- G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
- G03F7/70—Microphotolithographic exposure; Apparatus therefor
- G03F7/70058—Mask illumination systems
- G03F7/7015—Details of optical elements
- G03F7/70158—Diffractive optical elements
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
- G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
- G03F7/70—Microphotolithographic exposure; Apparatus therefor
- G03F7/70058—Mask illumination systems
- G03F7/702—Reflective illumination, i.e. reflective optical elements other than folding mirrors, e.g. extreme ultraviolet [EUV] illumination systems
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21K—TECHNIQUES FOR HANDLING PARTICLES OR IONISING RADIATION NOT OTHERWISE PROVIDED FOR; IRRADIATION DEVICES; GAMMA RAY OR X-RAY MICROSCOPES
- G21K1/00—Arrangements for handling particles or ionising radiation, e.g. focusing or moderating
- G21K1/06—Arrangements for handling particles or ionising radiation, e.g. focusing or moderating using diffraction, refraction or reflection, e.g. monochromators
Definitions
- the invention relates to an illumination system for wavelengths ⁇ 100 nm, the illumination system having an object plane and a field plane.
- EUV lithography is one of the most promising future lithography techniques. Wavelengths in the range of 11-14 nm, in particular 13.5 nm, with a numerical aperture of 0.2-0.3 are currently being discussed as wavelengths for EUV lithography.
- the image quality in EUV lithography is determined on the one hand by the projection lens and on the other hand by the lighting system.
- the illumination system is intended to provide the most uniform possible illumination of the field plane in which the structure-bearing mask, the so-called reticle, is arranged.
- the projection lens depicts the field plane in an image plane, the so-called wafer plane, in which a light-sensitive object is arranged.
- Projection exposure systems for EUV lithography are designed with reflective optical elements.
- the shape of the field of an EUV projection exposure system is typically that of a ring field with a high aspect ratio of 2 mm (width) x 22-26 mm (arc length).
- the projection systems are usually operated in scanning mode.
- illumination systems for wavelengths ⁇ 100 nm The problem with illumination systems for wavelengths ⁇ 100 nm is that the light sources of such illumination systems emit radiation which can lead to undesired exposure of the light-sensitive object in the wafer plane of the projection exposure system and, in addition, optical components of the exposure system, such as the multilayer mirrors, are thereby heated ,
- Transmission filters for example made of zircon, are used in lighting systems for wavelengths ⁇ 100 nm to filter out the unwanted radiation.
- Such filters have the disadvantage of high light losses. Furthermore, they can be very easily destroyed by heat.
- the object of the invention is to provide an illumination system for wavelengths ⁇ 100 nm, in particular in the EUV range, in which the disadvantages mentioned above can be avoided. Furthermore, the components of such a lighting system should be simple in construction and manufacture.
- an illumination system which has at least one grating element which has a multiplicity of individual grids with a grating period assigned to the individual grating, and at least one physical diaphragm in a diaphragm plane which is arranged downstream of the grating element in the beam path from the object plane to the field plane.
- Grating elements for example reflection gratings, in particular echelette gratings with an overall efficiency of close to 60%, have been known for some time from monochromator construction for synchrotron radiation sources, and there is good experience in particular even at very high fluxes.
- the behavior on diffraction gratings is determined by the grating equation
- a grating element in the beam path from the object plane to the image plane for spectral filtering can be used in an illumination system for wavelengths ⁇ 100 nm if the individual diffraction orders and the wavelengths are clearly separated from one another. This is easiest in the focused beam. There is a focus or light source image with a limited diameter at the focal point. However, you have to choose a certain aperture for the focused beam in order not to get too long lengths. However, for higher-aperture beams, the grating design becomes more difficult or larger aberrations are obtained.
- the inventors have now recognized that a separation of the individual diffraction orders and sufficient imaging quality can also be achieved if a plurality of individual gratings are used instead of a grating element with, for example, a continuously changing grating constant.
- the individual gratings are preferably arranged one above the other or one behind the other in the direction of the impinging beam.
- the individual grids can be grids with different grating periods.
- individual grids are arranged tilted relative to one another.
- cooling devices can be provided on the side facing away from the incident rays. In this way, excessive heating of the grid can be prevented.
- the individual gratings are preferably designed as blaze gratings, which are optimized for maximum efficiency in a diffraction order.
- Blaze grids are known, for example, from Lexikon der Optik, edited by Heinz Hagerborn, pages 48-49. They are characterized by an almost triangular furrow profile. As previously stated, the different diffraction orders and wavelengths can be clearly separated from one another with the grating element ...
- the at least one physical diaphragm according to the invention serves to prevent false light with wavelengths far above 100 nm from entering the lighting system via the O diffraction order.
- the at least one physical aperture essentially blocks the light of the 0th diffraction order.
- the rays after the physical diaphragm have wavelengths in the range from 7 to 25 nm.
- the lighting system advantageously comprises a collector unit for generating a convergent light bundle and the convergent light bundle strikes the grating element.
- the focus of the light beam of the nth diffraction order of the grating element particularly preferably comes to lie at the location of the physical aperture or in the vicinity of the physical aperture, whereby
- part of the undesired radiation can be filtered out by further diaphragms in the lighting system.
- the invention also provides a projection exposure system with such a lighting system and a method for producing microelectronic components.
- a projection exposure system with such a lighting system and a method for producing microelectronic components.
- FIG. 4A spot diagram in the diaphragm plane of the lighting system with 21 linear grids of different grating periods arranged one behind the other
- Figure 4B spot diagram in the diaphragm plane of the lighting system with 31 linear grids of different grating periods arranged one behind the other
- FIGS. 6A and 6B Laue construction for calculating the angle of inclination of a grating according to FIG. 5
- Figure 7 spot diagram in the diaphragm plane of the lighting system with a grating element with differently inclined linear grids
- Figure 9 grating element with linear grids arranged one above the other FIG. 10 maximum possible diffraction efficiency for grating elements designed as blaze gratings and consisting of different materials
- FIG. 11 EUV projection exposure system with an illumination system according to the invention.
- FIG. 1 shows a grating element with a multiplicity of individual grids 9 in the beam path of an illumination system.
- the individual grids 9 are arranged one behind the other in the beam direction.
- the light from the light source 3 is collected by a collecting component, the collector 5.
- the collector 5 is an ellipsoidal mirror, which generates an image of the light source 3.
- Unwanted radiation can already be filtered out by several partial diaphragms 7.1, 7.2 arranged in front of the physical diaphragm 7.3 in order to reduce the thermal load on the physical diaphragm 7.3 with the circular opening, which is located in the focal plane of the desired diffraction order, here the -1. Order 16, located, to decrease.
- the screens 7.1, 7.2 can also be cooled, which is not shown.
- the grid element 1 can also be cooled, for example by cooling on the back.
- the rear cooling device 8 of the grid element 1 with a plurality of individual grids 9 arranged one behind the other is preferably a liquid cooling device with inlet and outlet 10.1, 10.2.
- the grating element 1 and the physical diaphragm 7.3 make it possible to completely block the 0th order, which comprises all wavelengths of the light source, in the lighting system according to the invention. In addition, all higher orders except the -1. Order blocked.
- the discrete grid periods for an arrangement according to the invention of individual grids 9 arranged one behind the other are to be specified below.
- the optics should image the light from a virtual intermediate image, which corresponds to the 0th order, into a real image, which is the +1. or -1. Order corresponds.
- the solution is then given through a hyperboloid.
- a lattice element laid out in one plane must have lattice furrows, which are given by the intersection points of a hyperbolic family with this plane, the hyperbolic family being defined by hyperbolas, which for the point-to-point mapping between focal point without mirror and n.- Order have a light path difference of n * ⁇ .
- this grating element with optical effect can be solved sufficiently well by an array of individual grids arranged one behind the other or one above the other without the imaging quality of the lighting system being impaired inadmissibly.
- ⁇ Angle at which the light beam strikes the grating element
- ⁇ t angle at which the beam is deflected by the grating element
- h, h ' the height of the image locations
- a certain beam that hits the grating element 1 at the angle ctj is reflected in the 0th diffraction order at the angle ⁇ t .
- the first order of diffraction for this beam should be so far away that a separation of the orders of diffraction is possible taking into account the diameter of the image of the source at the focal point. Then, by arranging an aperture 7.3 in the plane in which the focal point lies, complete blocking of the 0th diffraction order, which encompasses all wavelengths, can be achieved.
- the beam angle of the first diffraction order relative to the grating surface ⁇ t must be larger or smaller than ⁇ by ⁇ , whereby
- Diffraction order in filter plane I distance between the reflection location on the mirror with grating and the image point
- the main beam - For the central beam - hereinafter referred to as the main beam - let the angle of incidence c_i (0).
- the heights h and h 1 of the image locations can be determined from this.
- the z coordinates of the image locations relative to the beam penetration point of the main beam with the mirror also follow:
- grating spectral filters with individual gratings arranged one behind the other Two exemplary embodiments of grating spectral filters with individual gratings arranged one behind the other are to be given below, the grating period of the individual gratings being different. Arranging the individual grids in one plane is particularly advantageous for cooling the grille, since the grille can be provided with a cold trap, for example cooling channels, on the rear.
- the values for ⁇ i ⁇ ⁇ t , the grating period, the start value and the end value along the z-axis and the blaze depth of the grating element resulting from individual grids arranged one behind the other are given in Tables 1 and 2. With regard to the definition of the blaze depth, reference is made to the following description of FIG. 8.
- Table 1 shows an embodiment for 21 linear grids.
- Table 2 shows an embodiment for 31 linear grids.
- the individual grids are designed as so-called blaze grids, i.e. they are optimized for maximum efficiency in the desired diffraction order. This is achieved almost by a triangular furrow profile.
- the ideal blaze depth B in a scalar approximation is calculated
- grating segments made up of individual grids which, arranged in a plane one behind the other, together form the spectral filter; the start and end positions of the grids with respect to the main beam intersection with the area in which the grids lie are given.
- FIG. 3 shows the grating period of the individual grids as a function of the angle of incidence Oj.
- the points represent the discrete values of the exemplary embodiment with 31 individual grids according to Table 2.
- FIGS. 4A and 4B show spot diagrams of a point image in FIGS. Diffraction order for the design wavelength of 13.5 nm in the aperture plane, Figure 4A with 21, Figure 4B with 31 individual gratings.
- the discretization of the lattice element is noticeable in a slight blurring in the y-direction, which is negligibly small with ⁇ 0.5 mm, in particular with N> 30 lattices; the light source image is washed out in the y direction by this amount.
- the scale given in FIGS. 4A and 4B relates both to the scaling in the x and the y direction.
- the grating element 1 comprises a plurality of individual grids 9 inclined against the plane of incidence E.
- Table 3 shows an embodiment with 40 individual grids, the following parameters being specified:
- FIG. 6C shows the angle of inclination ⁇ of the individual grids as a function of the angle of incidence ctj.
- the points represent the discrete points of the exemplary embodiment with 40 individual grids according to Table 3.
- Figure 7 shows the spot diagram of a point image of -1. Diffraction order in the aperture plane. The discretization of the lattice element is noticeable in a slight blurring in the y direction, which, however, is negligibly small at £ ⁇ 0.5 mm; the light source image is washed out in the y direction by this amount.
- the scale given in FIG. 7 relates both to the scaling in the x and y directions.
- the individual grids 9 can also be arranged one above the other.
- An arrangement one above the other results in a grating spectral filter 1 as shown in FIG. 9.
- the individual grids of the individual levels are labeled 9.1 and 9.2.
- the same components as in the embodiment according to FIG. 1 are given the same reference numbers.
- the grids arranged one above the other can have a different grating period or can be arranged tilted relative to one another.
- each individual grating of the grating element is preferably designed as a blaze grating.
- FIG. 8 shows a blaze grating with an approximately triangular furrow profile.
- the reference number 11 designates the beam impinging on the linear grating 9 designed as a blaze grating with the grating period P; 12 the on the grid in the 0th order reflected and 16 the beam diffracted into the -1st order. Since the blaze depth according to equation (8) is angle-dependent, ideally each individual grid of the grid element has a different blaze depth B.
- the highest efficiency of 0.7 can be achieved with ruthenium.
- all individual gratings can be produced with the same blaze depth of, for example, 25 nm, which overall still achieves a diffraction efficiency ⁇ (-1) of> 55% or 0.55.
- FIG. 11 shows an EUV projection exposure system with a grating element 1 according to the invention.
- Projection exposure system comprises a light source 3, a collecting optical component, a so-called collector Registration is included, is trained.
- the collector 5 forms that in the object area of the lighting system lying light source 3 into a secondary light source 4 in or in the vicinity of a diaphragm plane 7.3.
- the light source 3 which can be, for example, a laser plasma source or a plasma discharge source, is arranged in the object plane of the lighting system; the image of the primary light source, which is also referred to as the secondary light source, comes to rest in the image plane of the lighting system.
- Additional apertures 7.1, 7.2 are arranged between grating element 1 and the physical aperture 7.3 in order to block the light of undesired wavelengths, in particular wavelengths greater than 30 nm.
- the focus of the -1st order comes to lie in the plane of the aperture 7.3, i.e. the light source 3 is through the collector and grating spectral filter in the -1.
- Diffraction order mapped almost stigmatically in the plane of the aperture 7.3. The representation in all other diffraction orders is not stigmatic.
- the illumination system of the projection system comprises an optical system 20 for shaping and illuminating the field plane 22 with an annular field.
- the optical system comprises, as a mixing unit for homogeneous illumination of the field, two facet mirrors 29.1, 29.2 and two imaging mirrors 30.1, 30.2 and a field-forming grazing-incidence mirror 32.
- In the optical system 20 there are additional apertures 7.4, 7.5, 7.6, 7.7 for suppressing false light arranged.
- the first facet mirror 29.1 the so-called field facet mirror, generates a multiplicity of secondary light sources in or in the vicinity of the plane of the second facet mirror 29.2, the so-called pupil facet mirror.
- the following imaging optics images the pupil facet mirror 29.2 in the exit pupil 34 of the illumination system, which comes to rest in the entry pupil of the projection objective 26.
- the angles of inclination of the individual facets of the first and second facet mirrors 29.1, 29.2 are designed such that the images of the individual field facets of the first facet mirror 29.1 overlap in the field plane 22 of the lighting system and thus a largely homogenized illumination of the structure-bearing mask, which comes to rest in this field level 22, is made possible.
- the segment of the ring field is formed via the grazing incidence mirror 32, which operates under grazing incidence.
- a double faceted lighting system is disclosed, for example, in US Pat. No. 6,198,793, imaging and field-shaping components in PCT / EP / 00/07258. The content of the disclosure of these documents is fully incorporated into the present application.
- the projection lens 26 is a 6-mirror projection lens as disclosed, for example, in US application 60/255214, filed on December 13, 2000 at the US Patent Office for the applicant or DE-A-10037870, the disclosure content of which is fully incorporated in the present application becomes.
- the object to be exposed for example a wafer, is arranged in the image plane 28.
- the invention provides for the first time an illumination system with which it is possible to select undesired wavelengths directly after the primary light source.
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Exposure And Positioning Against Photoresist Photosensitive Materials (AREA)
- Non-Portable Lighting Devices Or Systems Thereof (AREA)
- Microscoopes, Condenser (AREA)
- Exposure Of Semiconductors, Excluding Electron Or Ion Beam Exposure (AREA)
Abstract
Description
Claims
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP02743087A EP1393134A2 (de) | 2001-06-07 | 2002-05-24 | Beleuchtungssystem mit einer vielzahl von einzelgittern |
JP2003502587A JP2004528726A (ja) | 2001-06-07 | 2002-05-24 | 複数の単一回折格子を有する照明光学系 |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10127449A DE10127449A1 (de) | 2001-06-07 | 2001-06-07 | Beleuchtungssystem mit einer Vielzahl von Einzelgittern |
DE10127449.1 | 2001-06-07 |
Publications (3)
Publication Number | Publication Date |
---|---|
WO2002099534A2 WO2002099534A2 (de) | 2002-12-12 |
WO2002099534A9 true WO2002099534A9 (de) | 2003-03-20 |
WO2002099534A3 WO2002099534A3 (de) | 2003-10-02 |
Family
ID=7687371
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2002/005688 WO2002099534A2 (de) | 2001-06-07 | 2002-05-24 | Beleuchtungssystem mit einer vielzahl von einzelgittern |
Country Status (5)
Country | Link |
---|---|
US (1) | US6836530B2 (de) |
EP (1) | EP1393134A2 (de) |
JP (1) | JP2004528726A (de) |
DE (1) | DE10127449A1 (de) |
WO (1) | WO2002099534A2 (de) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7248667B2 (en) * | 1999-05-04 | 2007-07-24 | Carl Zeiss Smt Ag | Illumination system with a grating element |
US7080257B1 (en) * | 2000-03-27 | 2006-07-18 | Microsoft Corporation | Protecting digital goods using oblivious checking |
US20050180013A1 (en) * | 2002-03-21 | 2005-08-18 | Carl Zeiss Smt Ag | Grating element for filtering wavelengths < 100 nm |
DE10214259A1 (de) * | 2002-03-28 | 2003-10-23 | Zeiss Carl Semiconductor Mfg | Kollektoreinheit für Beleuchtungssysteme mit einer Wellenlänge <193 nm |
US7084412B2 (en) | 2002-03-28 | 2006-08-01 | Carl Zeiss Smt Ag | Collector unit with a reflective element for illumination systems with a wavelength of smaller than 193 nm |
EP1517183A1 (de) * | 2003-08-29 | 2005-03-23 | ASML Netherlands B.V. | Lithographischer Apparat, Verfahren zur Herstellung eines Artikels und damit erzeugter Artikel |
EP1510869A3 (de) * | 2003-08-29 | 2009-07-29 | ASML Netherlands B.V. | Lithographischer Apparat, Verfahren zur Herstellung einer Vorrichtung und damit erzeugte Vorrichtung |
JP4500996B2 (ja) * | 2004-04-30 | 2010-07-14 | 国立大学法人 千葉大学 | 基盤に固着した貴金属膜からなるホログラフィック光学素子 |
EP1782128A2 (de) * | 2004-08-23 | 2007-05-09 | Carl Zeiss SMT AG | Beleuchtungssystem einer mikrolithographischen belichtungsvorrichtung |
JP4710406B2 (ja) * | 2005-04-28 | 2011-06-29 | ウシオ電機株式会社 | 極端紫外光露光装置および極端紫外光光源装置 |
AU2007208311A1 (en) * | 2006-01-24 | 2007-08-02 | Brookhaven Science Associates | Systems and methods for detecting an image of an object by use of an X-ray beam having a polychromatic distribution |
ES2311409A1 (es) | 2007-07-13 | 2009-02-01 | Samcla-Esic, S.L. | Sistema de riego automatizado, remoto y centralizado. |
EP2370807A4 (de) | 2008-12-01 | 2015-11-11 | Univ North Carolina | Systeme und verfahren zur bilderfassung eines objekts mittels mehrstrahlbildgebung aus einem röntgenstrahl mit polychromatischer verteilung |
US8204174B2 (en) | 2009-06-04 | 2012-06-19 | Nextray, Inc. | Systems and methods for detecting an image of an object by use of X-ray beams generated by multiple small area sources and by use of facing sides of adjacent monochromator crystals |
CA2763367C (en) * | 2009-06-04 | 2016-09-13 | Nextray, Inc. | Strain matching of crystals and horizontally-spaced monochromator and analyzer crystal arrays in diffraction enhanced imaging systems and related methods |
DE102017204312A1 (de) | 2016-05-30 | 2017-11-30 | Carl Zeiss Smt Gmbh | Optische Wellenlängen-Filterkomponente für ein Lichtbündel |
DE102016212361A1 (de) * | 2016-07-06 | 2018-01-11 | Carl Zeiss Smt Gmbh | Optisches Gitter und optische Anordnung damit |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4798446A (en) * | 1987-09-14 | 1989-01-17 | The United States Of America As Represented By The United States Department Of Energy | Aplanatic and quasi-aplanatic diffraction gratings |
US4915463A (en) * | 1988-10-18 | 1990-04-10 | The United States Of America As Represented By The Department Of Energy | Multilayer diffraction grating |
US5905571A (en) * | 1995-08-30 | 1999-05-18 | Sandia Corporation | Optical apparatus for forming correlation spectrometers and optical processors |
US5920380A (en) * | 1997-12-19 | 1999-07-06 | Sandia Corporation | Apparatus and method for generating partially coherent illumination for photolithography |
US6118577A (en) * | 1998-08-06 | 2000-09-12 | Euv, L.L.C | Diffractive element in extreme-UV lithography condenser |
TWI282909B (en) * | 1999-12-23 | 2007-06-21 | Asml Netherlands Bv | Lithographic apparatus and a method for manufacturing a device |
US20020105725A1 (en) * | 2000-12-18 | 2002-08-08 | Sweatt William C. | Electrically-programmable optical processor with enhanced resolution |
-
2001
- 2001-06-07 DE DE10127449A patent/DE10127449A1/de not_active Withdrawn
-
2002
- 2002-05-24 EP EP02743087A patent/EP1393134A2/de not_active Withdrawn
- 2002-05-24 JP JP2003502587A patent/JP2004528726A/ja active Pending
- 2002-05-24 WO PCT/EP2002/005688 patent/WO2002099534A2/de active Application Filing
- 2002-06-05 US US10/163,262 patent/US6836530B2/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
US20030099040A1 (en) | 2003-05-29 |
JP2004528726A (ja) | 2004-09-16 |
US6836530B2 (en) | 2004-12-28 |
DE10127449A1 (de) | 2002-12-12 |
WO2002099534A2 (de) | 2002-12-12 |
EP1393134A2 (de) | 2004-03-03 |
WO2002099534A3 (de) | 2003-10-02 |
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