USRE4477E - Improvement in silvering glass for mirrors and reflectors - Google Patents
Improvement in silvering glass for mirrors and reflectors Download PDFInfo
- Publication number
- USRE4477E USRE4477E US RE4477 E USRE4477 E US RE4477E
- Authority
- US
- United States
- Prior art keywords
- glass
- reflectors
- mirrors
- improvement
- silvering
- Prior art date
Links
- 239000011521 glass Substances 0.000 title description 24
- 150000001875 compounds Chemical class 0.000 description 22
- 239000011248 coating agent Substances 0.000 description 16
- 238000000576 coating method Methods 0.000 description 16
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 16
- BQCADISMDOOEFD-UHFFFAOYSA-N silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 12
- 229910052709 silver Inorganic materials 0.000 description 12
- 239000004332 silver Substances 0.000 description 12
- 229920001800 Shellac Polymers 0.000 description 10
- 239000012153 distilled water Substances 0.000 description 10
- 229940113147 shellac Drugs 0.000 description 10
- 235000013874 shellac Nutrition 0.000 description 10
- 239000004208 shellac Substances 0.000 description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
- 241000276489 Merlangius merlangus Species 0.000 description 6
- 241001272996 Polyphylla fullo Species 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 229910001018 Cast iron Inorganic materials 0.000 description 2
- 206010022114 Injury Diseases 0.000 description 2
- FEWJPZIEWOKRBE-XIXRPRMCSA-N Mesotartaric acid Chemical compound OC(=O)[C@@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-XIXRPRMCSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000036633 rest Effects 0.000 description 2
- 229960001367 tartaric acid Drugs 0.000 description 2
- 235000002906 tartaric acid Nutrition 0.000 description 2
- 239000011975 tartaric acid Substances 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N tin hydride Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
Definitions
- New York in the county of New York and State of New York, did invent a certain new and Improved Mode of Silver'ing Glass for Mirrors and Reflectors-and protecting the silvering on the ounces of concentratedliquid ammonia. These are mixed together in a vessel and left to stand for twelve hours. Then add one hundred and twenty ounces of distilled water; mix thoroughly, and filter through paper. 2d, I form another compound composed ofthe following ingredients in thespecifi'ed quantities, to wit: one ounce crystallizcd tartaric acid. Add to this eight ounces of distilled water. Let this stand for ,three or four months before using. Filter it through paper. 3d, take four and one-half ounces of the first solution or compound, to which add on'e ounce of the second solution or compound, and 'to which add twenty-two ounces of distilled water, when the compound is ready for use.
- the glass is then placed upon a cast-iron steam-table formed of a large iron box filled with water, through which several steam-pipes are passed, which, being filled with steam, generate a uniform heat upon the surface of the table upon which the glass rests, the heat being raised to about from 110 to 130
- the last chemical compound or solution is poured upon the surface of the glass plate sufficient to spread over the entire surface, which it will readily do when being poured on.
- the solution or compound has remained upon the glass half an hour, the silver having precipitated upon the glass, the surface is washed with distilled water and set to dry, when the silvering process is completed.
- the method of protecting the silver on the glass is applicable to those cases where the silver is deposited by other compounds or means as well as by that herein described; and p it is also obvious that the shellac coating may be used alone, without the coating of red lead, litharge, and oil, especially on reflectors, mirrors, and similar articles which are to have their silvered surface covered in such a manner as to protect them from injury by handlingror other-- wise; and I so contemplate using the shellac coating in such cases. In other cases I propose to use both the shellac and the lead, litha-rge and oil, applied as above described.
Description
UNITED Srrvrmzxs PATENT OFFICE.
WILLIAM AUGUSTUS WALKER, OF NEl/Y YORK, N. Y., ASSIGNEE OF HENRY BALEN WALKER, DECEASED.
IMPROVEMENT IN $ILVERING GLASS FOR MIRRORS AND REFLECTORS.
Specification forming part of Letters Patent No. 97,838, dated December 14, 1869 reissue No. 4,477, dated July 18, 18711.
' To all whom it may concern:
Be it known-that HENRY BALEN WALKER, of
New York, in the county of New York and State of New York, did invent a certain new and Improved Mode of Silver'ing Glass for Mirrors and Reflectors-and protecting the silvering on the ounces of concentratedliquid ammonia. These are mixed together in a vessel and left to stand for twelve hours. Then add one hundred and twenty ounces of distilled water; mix thoroughly, and filter through paper. 2d, I form another compound composed ofthe following ingredients in thespecifi'ed quantities, to wit: one ounce crystallizcd tartaric acid. Add to this eight ounces of distilled water. Let this stand for ,three or four months before using. Filter it through paper. 3d, take four and one-half ounces of the first solution or compound, to which add on'e ounce of the second solution or compound, and 'to which add twenty-two ounces of distilled water, when the compound is ready for use.
To prepare the glass for the silvering process, I cover the surface with a coat of whiting, rubbed on with a piece of flannel cloth, and afterward rubbed'ofl' with a piece of chamois-skin. Then apply a second coating of whiting, as before. Then polish it with a block covered with felt or fine French carpet, adding to the coat of whiting a small quantity of the oxide of iron or tin. After being polished the surface is washed with water and then rinsed with distilled Water, when the glass is ready for silverin'g. The glass is then placed upon a cast-iron steam-table formed of a large iron box filled with water, through which several steam-pipes are passed, which, being filled with steam, generate a uniform heat upon the surface of the table upon which the glass rests, the heat being raised to about from 110 to 130 After raising the temperature of the glass to the above degree of heat the last chemical compound or solution is poured upon the surface of the glass plate sufficient to spread over the entire surface, which it will readily do when being poured on. After the solution or compound has remained upon the glass half an hour, the silver having precipitated upon the glass, the surface is washed with distilled water and set to dry, when the silvering process is completed.
To protect the silvering thus put on, I proceed to cover it with a solution or compound of one ounce of shellac and ten ounces of ninety-fiveper-cent, alcohol, over which I spread a coating or compound of red lead and litharge ground in oil, thus forming a mirror superior in luster and reflective power to those produced by the usual methods, and at a much less expense to manufacture. a v
It is obvious that the method of protecting the silver on the glass is applicable to those cases where the silver is deposited by other compounds or means as well as by that herein described; and p it is also obvious that the shellac coating may be used alone, without the coating of red lead, litharge, and oil, especially on reflectors, mirrors, and similar articles which are to have their silvered surface covered in such a manner as to protect them from injury by handlingror other-- wise; and I so contemplate using the shellac coating in such cases. In other cases I propose to use both the shellac and the lead, litha-rge and oil, applied as above described.
What is claimed as the invention of said HENRY BALEN \NALKER is 1i A mirror or reflector, consisting of any desired form of glass, having a silver coating ap: plied thereto by the use of the silvering compounds, substantially as described.
2. A coating of shellac, dissolved in alcohol or its equivalent, applied to the silver coating for the purpose of protecting the same, as set forth. 3. The compound of litharge, red lead, and oil,
Family
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