US3928003A - Vacuum deaerator for viscous liquids - Google Patents

Vacuum deaerator for viscous liquids Download PDF

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US3928003A
US3928003A US372734A US37273473A US3928003A US 3928003 A US3928003 A US 3928003A US 372734 A US372734 A US 372734A US 37273473 A US37273473 A US 37273473A US 3928003 A US3928003 A US 3928003A
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flange
bowl
rotor
inch
deaerator
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US372734A
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Durward Fryar
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Procter and Gamble Co
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Procter and Gamble Co
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D19/00—Degasification of liquids
    • B01D19/0042—Degasification of liquids modifying the liquid flow
    • B01D19/0052—Degasification of liquids modifying the liquid flow in rotating vessels, vessels containing movable parts or in which centrifugal movement is caused
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S494/00—Imperforate bowl: centrifugal separators
    • Y10S494/90—Imperforate bowl: centrifugal separators involving mixture containing one or more gases

Definitions

  • a centrifugal vacuum deaerator including a rotor which comprises a flange adapted to receive the material which is being deaerated after it is accelerated by centrifugal force, said flange being unperforated in the area where the material impinges on said flange, and said flange being distinguished by the absence of any flow-impeding means which would substantially impede the spreading of'said material when it is deposited upon said flange.
  • VACUUM DEAERATOR FOR VISCOUS LIQUIDS BACKGROUND OF THE INVENTION 1.
  • This invention relates to centrifugal vacuum deaera tors to be used for deaerating viscous liquids'such as toothpastes and to a process of deaerating said viscous I liquids utilizing said deaerator.
  • FIG. 1 is a sectional plan view of the deaerator of this invention
  • FIG. 2 is a fragmentary sectional elevation of the deaerator taken along the line 2-2 in FIG. 1;
  • FIG. 3 is a sectional elevation view of a deaerator having a rotor with multiple perpendicular flanges.
  • the present invention relates to a centrifugal vacuum deaerator comprising a rotor which comprises a flange positioned to receive the material to be deaerated after it is accelerated by centrifugal force, said flange being distinguished by being unperforated in the area where the material impinges, and said flange being further distinguished by the absence of any flow-impeding 11 and maintain said vacuum.
  • the primary reason for the vacuum inside chamber 11 is to avoid retrapping air.
  • Inlet means 12 are provided whereby the product to be deaerated can be introduced into the vacuum chamber 11.
  • Inlet 12 is positioned so as toenable the product to be introduced into the rotor assembly 13 which comprises a shaft 14.- To the shaft 14 is attached either unitarily or removably a bowl 15 which receives the material to be deaerated.
  • the bowl l" has sides adapted to retain the material to be deaerated when the bowl is rotated by a power means coupled to the shaft 14.
  • the sidesof the bowl contain a series of small holes 16 which are from about l/64 inch to about /4 inch in diameter, preferably from about l/l6 inch to about Vainch in diameter. 1 l
  • the rotor also comprises a flange 17 which inFIG. 1
  • the deaerated material can be removed in any convenient manner, e.g., continuously removed through a means which would impede the spreading of said material into a thin film when it is deposited on said flange and the presence of an edge on said flange over which said thin film of said material can be sheared by centrifugal force.
  • the process of this invention is distinguished by making use of centrifugal force to create a thin film which is then sheared over an edge which is preferably sharp, but which can also be rounded.
  • the preferred embodiment of the process of this invention also includes a step in which the fluid to be deaerated is thrown through holes by centrifugal force. This step gets rid of the largest bubbles. The material then impinges against the flange where it is spread into a very thin film which permits the escape of small bubbles, and finally, when the thin film of the viscous liquid reaches the edge of the flange, it is sheared which elongates and ruptures the walls of even smaller bubbles.
  • the rotor speed can be varied widely depending upon the strength of the materials used in the fabrication of the deaerator. Rotor speeds of from about 500 to about 10,000 RPM can be used. Slower rotor speeds will normally be used with larger rotors, for example, rotors having an OD of about two feet, and faster rotor speeds will normally be used with smaller rotors, i.e., those with an OD of about one-half of a foot.
  • the advantages of the process of the present invention include simplicity, economy and ease of maintenance, especially cleaning.
  • the process also deaerates well at low vacuums (10-20 in. of Hg) which decreases the loss of volatile material from the viscous liquid.
  • the process can be used over a wide temperature range and can be either a batch or continuous process.
  • a centrifugal vacuum deaerator comprising an enclosed chamber connected to a source of vacuum for creating a vacuum within said chamber, and a rotor disposed within said chamber, said rotor comprising a flange positioned to receive the material to be deaerated after it is accelerated by centrifugal force, said flange being distinguished by being unperforated in the area where the material impinges, and said flange being further distinguished by the absence of any flow-impeding means which would substantially impede the spreading of said material into a thin film when it is deposited on said flange, and the presence of an edge on said flange over which said thin film of said material can be sheared by centrifugal force.
  • the rotor additionally comprises a centrally mounted bowl having a plurality of small apertures around its circumference, said bowl being adapted to receive the material to be deaerated and in spaced relationship to said flange, whereby when the rotor is rotated, centrifugal force accelerates said material through said apertures to impinge upon said flange.
  • a methodof deaerating a viscous liquid comprising the step of centrifuging said liquid in a bowl having a plurality of holes of a diameter of from about l/64 to 5 1 inch in its sides, thereby causing said liquid to be forced through said holes in the form of droplets and to impinge upon a flange which is rotating coaxially and outwardly of said bowl and which is characterized by the absence of any flow-impeding means, whereby the liquid is formed into a thin film which spreads over said flange and which is sheared as it passes over the edge of said flange, said method being conducted under a pressure of from about 10 to about 30 inches of mercury.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Centrifugal Separators (AREA)

Abstract

A centrifugal vacuum deaerator including a rotor which comprises a flange adapted to receive the material which is being deaerated after it is accelerated by centrifugal force, said flange being unperforated in the area where the material impinges on said flange, and said flange being distinguished by the absence of any flow-impeding means which would substantially impede the spreading of said material when it is deposited upon said flange.

Description

Umte States Patent 1 1 1111 3,9
Fryar 5] Dec. 23, 1975 [5 VACUUM DEAERATOR FOR VISCOUS 2,648,496 8/1953 Cresswell 55/203 x LIQUIDS 3,061,438 10/1962 Jacobs et al. 55/41 x 3,283,910 11/1966 Grieselhuber et al. 210/377 x Inventor: Durward Fryar, Burlington, Ky.
The Procter & Gamble Company, Cincinnati, Ohio Filed: June 22, 1973 Appl. No.: 372,734
Assignee:
References Cited UNITED STATES PATENTS ABSTRACT A centrifugal vacuum deaerator including a rotor which comprises a flange adapted to receive the material which is being deaerated after it is accelerated by centrifugal force, said flange being unperforated in the area where the material impinges on said flange, and said flange being distinguished by the absence of any flow-impeding means which would substantially impede the spreading of'said material when it is deposited upon said flange.
6 Claims, 3 Drawing Figures US. Patent Dec. 23, 1975 Sheet 1 of2 3,928,063
US. Patent Dec. 23, 1975 Sheet 2 f; 3,928,003
VACUUM DEAERATOR FOR VISCOUS LIQUIDS BACKGROUND OF THE INVENTION 1. Field of the Invention This invention relates to centrifugal vacuum deaera tors to be used for deaerating viscous liquids'such as toothpastes and to a process of deaerating said viscous I liquids utilizing said deaerator.
2. Prior Art The concept of deaerating a liquid using'centrifugal force to push the liquid through holes is disclosed in Pulleys US. Pat. No. 2,060,242,-'issued Nov. 10, 1936. Similarly, the use of centrifugalforce-'toprovide a shearing action at the edge of a platea'pp'ears-"to be disclosed in German Patent 935,534, issued Oct. 27, 1955 which appears to disclose a reservoir of-viscous material which discharges over the edge of the reservoir. The use of a plurality of baffle plates containing holes and arranged in concentric arrangement is disclosed in Martins U.S. Pat. No. 2,507,797, issued May 16, 1950. The concept of creating a thin film in order to degas a viscous composition is disclosed in Healds U.S. Pat. No. 2,306,265, issued Dec. 22, 1942, and Compas U.S. Pat. No. 2,420,356, issued May 13, 1947. Other patents using baffles to aid in the deaeration of liquids include Cornells U.S. Pat. No. 2,785,765, issued Mar. 19, 1957, and Edwards U.S. Pat. No. 2,922,375, issued Jan. 26, 1960.
BRIEF DESCRIPTION OF THE DRAWINGS While the specification concludes with claims particularly pointing out and distinctly claiming the subject matter regarded as forming the present invention, it is believed that the present invention will be better understood from the following description taken in connection with the accompanying drawings in which:
FIG. 1 is a sectional plan view of the deaerator of this invention;
FIG. 2 is a fragmentary sectional elevation of the deaerator taken along the line 2-2 in FIG. 1; and
FIG. 3 is a sectional elevation view of a deaerator having a rotor with multiple perpendicular flanges.
SUMMARY OF THE INVENTION The present invention relates to a centrifugal vacuum deaerator comprising a rotor which comprises a flange positioned to receive the material to be deaerated after it is accelerated by centrifugal force, said flange being distinguished by being unperforated in the area where the material impinges, and said flange being further distinguished by the absence of any flow-impeding 11 and maintain said vacuum. The primary reason for the vacuum inside chamber 11 is to avoid retrapping air. Inlet means 12 are provided whereby the product to be deaerated can be introduced into the vacuum chamber 11. v
Inlet 12 is positioned so as toenable the product to be introduced into the rotor assembly 13 which comprises a shaft 14.- To the shaft 14 is attached either unitarily or removably a bowl 15 which receives the material to be deaerated. The bowl l"has sides adapted to retain the material to be deaerated when the bowl is rotated by a power means coupled to the shaft 14. The sidesof the bowl contain a series of small holes 16 which are from about l/64 inch to about /4 inch in diameter, preferably from about l/l6 inch to about Vainch in diameter. 1 l
The rotor also comprises a flange 17 which inFIG. 1
is a tapered straight flange which receives the material to be deaerated as it is accelerated through the: holes 16. When the material to be deaerated impinges on the flange 17, it is moved by centrifugal force down the flange, around the braces 18 which hold the flange 17 in proper position with respect to the shaft 14, to the bottom edge of the flange 17 where centrifugal force again accelerates the material to be deaerated, thereby throwing it against the side of the chamber 11 from whence it falls by gravity to the bottom of chamber 11. The deaerated material can be removed in any convenient manner, e.g., continuously removed through a means which would impede the spreading of said material into a thin film when it is deposited on said flange and the presence of an edge on said flange over which said thin film of said material can be sheared by centrifugal force.
DETAILED DESCRIPTION OF THE INVENTION hole (not shown) at the bottom of the chamber 11. It will be evident from FIG. 3 that a similar mode of operation is envisioned for this embodiment which simply provides multiple flanges. In FIG. 3, like reference numerals denote similar structural aspects to those of the apparatus of FIG. 1.
The process of this invention is distinguished by making use of centrifugal force to create a thin film which is then sheared over an edge which is preferably sharp, but which can also be rounded. The preferred embodiment of the process of this invention also includes a step in which the fluid to be deaerated is thrown through holes by centrifugal force. This step gets rid of the largest bubbles. The material then impinges against the flange where it is spread into a very thin film which permits the escape of small bubbles, and finally, when the thin film of the viscous liquid reaches the edge of the flange, it is sheared which elongates and ruptures the walls of even smaller bubbles.
The rotor speed can be varied widely depending upon the strength of the materials used in the fabrication of the deaerator. Rotor speeds of from about 500 to about 10,000 RPM can be used. Slower rotor speeds will normally be used with larger rotors, for example, rotors having an OD of about two feet, and faster rotor speeds will normally be used with smaller rotors, i.e., those with an OD of about one-half of a foot.
As previously indicated and as shown in FIG. 3, a series of flanges provides even greater deaeration.
The advantages of the process of the present invention include simplicity, economy and ease of maintenance, especially cleaning. The process also deaerates well at low vacuums (10-20 in. of Hg) which decreases the loss of volatile material from the viscous liquid. The process can be used over a wide temperature range and can be either a batch or continuous process.
What is claimed is:
1. A centrifugal vacuum deaerator comprising an enclosed chamber connected to a source of vacuum for creating a vacuum within said chamber, and a rotor disposed within said chamber, said rotor comprising a flange positioned to receive the material to be deaerated after it is accelerated by centrifugal force, said flange being distinguished by being unperforated in the area where the material impinges, and said flange being further distinguished by the absence of any flow-impeding means which would substantially impede the spreading of said material into a thin film when it is deposited on said flange, and the presence of an edge on said flange over which said thin film of said material can be sheared by centrifugal force.
2. The deaerator of claim 1 wherein the rotor additionally comprises a centrally mounted bowl having a plurality of small apertures around its circumference, said bowl being adapted to receive the material to be deaerated and in spaced relationship to said flange, whereby when the rotor is rotated, centrifugal force accelerates said material through said apertures to impinge upon said flange.
3. The deaerator of claim 2 wherein said aperature has a diameter of from about 1/64 inch to about A inch.
4. A methodof deaerating a viscous liquid comprising the step of centrifuging said liquid in a bowl having a plurality of holes of a diameter of from about l/64 to 5 1 inch in its sides, thereby causing said liquid to be forced through said holes in the form of droplets and to impinge upon a flange which is rotating coaxially and outwardly of said bowl and which is characterized by the absence of any flow-impeding means, whereby the liquid is formed into a thin film which spreads over said flange and which is sheared as it passes over the edge of said flange, said method being conducted under a pressure of from about 10 to about 30 inches of mercury.
5. The process of claim 4 wherein the holes in the bowl are from about l/l6 to about A inch in diameter.
6. The process of claim 5 wherein the pressure is from about 10 to about 20 inches of mercury.

Claims (6)

1. A CENTRIFUGAL VACUUM DEAERATOR COMPRISING AN ENCLOSED CHAMBER CONNECTED TO A SOURCE OF VACUUM FOR CREATING A VACUUM WITHIN SAID CHAMBER, AND A ROTOR DISPOSED WITHIN SAID CHAMBER, SAID ROTOR COMPRISING A FLANGE POSITIONED TO RECEIVE THE MATERIAL TO BE DEAERATED AFTER IT IS ACCELERATED BY CENTRIFUGAL FORE, SAID FLANGE BEING DISTINGUISHED BY BEING UNPERFORATED IN THE AREA WHERE THE MATERIAL IMPINGES, AND SAID FLANGE BEING FURTHER DISTINGUISHED BY THE ABSENCE OF ANY FLOW-IMPEDING MEANS WHICH WOULD SUBSTANTIALLY IMPEDE THE SPREADING OF SAID MATERIAL INTO A THIN FILM WHEN IT IS DEPOSITED ON SAID FLANGE, AND THE PRESENCE OF AN EDGE ON SAID FLANGE OVER WHICH SAID THIN FILM OF SAID MATERIAL CAN BE SHEARED BY CENTRIFUGAL FORCE.
2. The deaerator of claim 1 wherein the rotor additionally comprises a centrally mounted bowl having a plurality of small apertures around its circumference, said bowl being adapted to receive the material to be deaerated and in spaced relationship to said flange, whereby when the rotor is rotated, centrifugal force accelerates said material through said apertures to impinge upon said flange.
3. The deaerator of claim 2 wherein said aperature has a diameter of from about 1/64 inch to about 1/4 inch.
4. A method of deaerating a viscous liquid comprising the step of centrifuging said liquid in a bowl having a plurality of holes of a diameter of from about 1/64 to 1/4 inch in its sides, thereby causing said liquid to be forced through said holes in the form of droplets and to impinge upon a flange which is rotating coaxially and outwardly of said bowl and which is characterized by the absence of any flow-impeding means, whereby the liquid is formed into a thin film which spreads over said flange and which is sheared as it passes over the edge of said flange, said method being conducted under a pressure of from about 10 to about 30 inches of mercury.
5. The process of claim 4 wherein the holes in the bowl are from about 1/16 to about 1/8 inch in diameter.
6. The process of claim 5 wherein the pressure is from about 10 to about 20 inches of mercury.
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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4030897A (en) * 1974-11-28 1977-06-21 Saint-Gobain Industries Degassing of liquids
US4360428A (en) * 1980-05-01 1982-11-23 Comparetto John E Inverted vortex, particle separation chamber
US4908048A (en) * 1981-02-18 1990-03-13 Agfa-Gevaert Aktiengesellschaft Apparatus for degassing liquids by centrifugal force in a frustum shaped body
US5500039A (en) * 1993-07-23 1996-03-19 Mitsubishi Jukogyo Kabushiki Kaisha Gas-liquid separating apparatus
US20030232711A1 (en) * 2002-06-17 2003-12-18 Berit Bradley I. Centrifuge for extracting interstitial fluid
US6726743B2 (en) 2002-06-18 2004-04-27 3M Innovative Properties Company Electrostatic deaeration method and apparatus
WO2017192916A1 (en) * 2016-05-05 2017-11-09 Cook and Cook Incorporated d/b/a Royal Welding & Fabricating De-aeration system and method
RU2636732C1 (en) * 2016-06-08 2017-11-27 Федеральное государственное бюджетное учреждение науки Институт теоретической и прикладной механики им. С.А. Христиановича Сибирского отделения Российской академии наук (ИТПМ СО РАН) Method for separating dissolved gases from pumped fluid and device for its implementation (versions)
US10357787B2 (en) * 2009-03-06 2019-07-23 Alfa Laval Corporate Ab Centrifugal separator having energy consumption reducing devices

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US624596A (en) * 1899-05-09 Centrifugal cream-separator
US2060242A (en) * 1936-07-11 1936-11-10 George N Pulley Apparatus for deaerating liquids
US2507797A (en) * 1949-02-14 1950-05-16 Schwarz Engineering Company In Apparatus and method for deaeration of liquids
US2648496A (en) * 1946-12-03 1953-08-11 American Cyanamid Co Centrifugal apparatus for separating gases from liquids
US3061438A (en) * 1962-10-30 Treatment of grain alcohol
US3283910A (en) * 1964-04-02 1966-11-08 Western States Machine Co Centrifugal basket

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US624596A (en) * 1899-05-09 Centrifugal cream-separator
US3061438A (en) * 1962-10-30 Treatment of grain alcohol
US2060242A (en) * 1936-07-11 1936-11-10 George N Pulley Apparatus for deaerating liquids
US2648496A (en) * 1946-12-03 1953-08-11 American Cyanamid Co Centrifugal apparatus for separating gases from liquids
US2507797A (en) * 1949-02-14 1950-05-16 Schwarz Engineering Company In Apparatus and method for deaeration of liquids
US3283910A (en) * 1964-04-02 1966-11-08 Western States Machine Co Centrifugal basket

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4030897A (en) * 1974-11-28 1977-06-21 Saint-Gobain Industries Degassing of liquids
US4360428A (en) * 1980-05-01 1982-11-23 Comparetto John E Inverted vortex, particle separation chamber
US4908048A (en) * 1981-02-18 1990-03-13 Agfa-Gevaert Aktiengesellschaft Apparatus for degassing liquids by centrifugal force in a frustum shaped body
US5500039A (en) * 1993-07-23 1996-03-19 Mitsubishi Jukogyo Kabushiki Kaisha Gas-liquid separating apparatus
US6817970B2 (en) 2002-06-17 2004-11-16 Large Scale Biology Corporation Centrifuge for extracting interstitial fluid
US20030232711A1 (en) * 2002-06-17 2003-12-18 Berit Bradley I. Centrifuge for extracting interstitial fluid
WO2003106039A1 (en) * 2002-06-17 2003-12-24 Large Scale Biology Corporation Centrifuge for extracting interstitial fluid
US6726743B2 (en) 2002-06-18 2004-04-27 3M Innovative Properties Company Electrostatic deaeration method and apparatus
US10357787B2 (en) * 2009-03-06 2019-07-23 Alfa Laval Corporate Ab Centrifugal separator having energy consumption reducing devices
US10427171B2 (en) * 2009-03-06 2019-10-01 Alfa Laval Corporate Ab Centrifugal separator having energy consumption reducing devices
US11396026B2 (en) * 2009-03-06 2022-07-26 Alfa Laval Corporate Ab Centrifugal separator having energy consumption reducing devices
WO2017192916A1 (en) * 2016-05-05 2017-11-09 Cook and Cook Incorporated d/b/a Royal Welding & Fabricating De-aeration system and method
US10035084B2 (en) 2016-05-05 2018-07-31 Cook and Cook Incorporated De-aeration system and method
RU2636732C1 (en) * 2016-06-08 2017-11-27 Федеральное государственное бюджетное учреждение науки Институт теоретической и прикладной механики им. С.А. Христиановича Сибирского отделения Российской академии наук (ИТПМ СО РАН) Method for separating dissolved gases from pumped fluid and device for its implementation (versions)

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