US3408470A - Induction furnace employing high purity atmosphere - Google Patents
Induction furnace employing high purity atmosphere Download PDFInfo
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- US3408470A US3408470A US539847A US53984766A US3408470A US 3408470 A US3408470 A US 3408470A US 539847 A US539847 A US 539847A US 53984766 A US53984766 A US 53984766A US 3408470 A US3408470 A US 3408470A
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- retort
- wall
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- cooling
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D11/00—Arrangement of elements for electric heating in or on furnaces
- F27D11/06—Induction heating, i.e. in which the material being heated, or its container or elements embodied therein, form the secondary of a transformer
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- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/74—Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
- C21D1/773—Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material under reduced pressure or vacuum
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/25—Process efficiency
Definitions
- the furnace is a low frequency induction furnace having a covered, electrically conductive annular retort forming a short circuited secondary which is heated by currents induced therein.
- It has an electromagnetic core comprised of a plurality of O-shaped core pieces each arranged with one side passing through the central opening of the retort and the other sides extending along the outer walls of the retort and cover.
- the retort is enclosed in an evacuable sealing chamber and means are provided for evacuating the chamber and for admitting gaseous media into the retort.
- a labyrinth type seal is disposed between the retort and its cover.
- This invention relates to induction furnaces for brazing, sintering, and the like, and particularly to induction furnaces wherein a high purity atmosphere is to be maintained during the heating and cooling of articles therein.
- the general practice was to purge the air with an inert gas and then introduce a protective gas.
- a so-called sand sea was provided between the cover and body of the retort. Control gas was fed into the retort at pressures above that in the furnace chamber, and a continuous flow of the gas was maintained to reduce back diffusion from the chamber through the seal" into the retort.
- control gas In order to maintain control of the exfiltration of the gases so as to overcome the back diffusion, the flow of the control gas must be sufficiently high so that there is an assurance that gas is filtering out continuously throughout the entire periphery of the sand seal at a sufficient rate to prevent any re-entry of gas ihto the retort. This necessitates introduction of the atmosphere controlling gas in an amount greatly in excess of what would otherwise be required.
- the retort upon the cooling of the furnace and retort, due to the high thermal capacity of the sand seal, the retort is subjected to very large temperature gradients which cause resultant Warpage and rapid deterioration of the retort as well as slowing down the heating and cooling cycles. To reduce these gradients sufficiently to reduce warpage effectively, the time required for the heating and cooling cycle has to be greatly extended.
- Induction brazing generally involves heating the work piece by means of the current induced in it from an adjacent induction coil.
- This coil carries an alternating current that may range widely in frequency, for example, from 1 to 500 kilocycles, according to the conditions of the particular heating situation.
- the work is commonly heated in air with the joint area and the braze filler metal protected against oxidation by means of a suitable flux applied prior to heating.
- a protective gas may be used to provide a reducing or inert gas atmosphere surrounding the work piece during its heating and cooling. If the containing enclosure or envelope for this gas is an electrical conductor it is usually made large enough to encompass the entire primary coil together with the work assembly with suflicient clearance such that the envelope will not be heated by currents induced in it from the primary coil. This arrangement is quite satisfactory where the metals being heated do not form stable oxides and, therefore, the required gas purity is not extreme.
- the protective atmosphere in contact with the work piece must be extremely pure and free of oxidizing contaminants. This is necessary to maintain the work piece bright and clean for successful brazing. It is not feasible to achieve this high degree of gas purity in the presence of an induction coil structure with its thermal and electrical insulation and other parts that will give off adsorbed air and other contaminating gases during the heating cycle.
- molybdenum enclosure or envelope for the gas and located within the induction coil has been used in laboratory type work.
- the present invention offers in combination a large work space which is induction heated with 60 cyc-le current in a high purity protective gas atmosphere capable of operation at sub-atmospheric pressures at high temperatures with rapid heating and cooling; the use of hydrogen, helium, or argon with complete safety and economy of gas; ease and rapidity of opening and closing furnace; and low maintenance cost.
- a new and improved ring type induction furnace wherein an annular metal retort is employed and a high purity atmosphere is maintained continuously within the retort without back diffusion of gases into the interior of the retort; extremely rapid heating and cooling cycles relative to those heretofore required are obtained; the flow of atmosphere controlling gas for assuring the maintenance of high purity atmosphere within the retort free from back diffusion is effected with a low gas flow; low or sub-atmospheric pressures are maintained during heating, and pressures at substantially atmospheric pressure or above are maintained during cooling, so as to assure eflicient operation with a small flow of the control gas.
- Another advantage is that the heating and cooling are confined mostly to the retort and charge of articles so that a large mass of conventional furnace structure does not have to be subjected to the heating and cooling cycles, whereby the time required for the heating and cooling cycles is greatly reduced.
- a specific advantage is that the present structure permits the brazing of a large number of individual articles concurrently or in a batch while they are maintained out of contact with each other.
- Another specific object is to provide a balance between the wall thicknesses of the retort so that under the influence of the induced currents, the heating of each unit of wall area of the retort is the same as are the others throughout the heating cycle.
- FIG. 1 is a top plan view of the furnace embodying the principles of the present invention, parts thereof being cut away for clearness in illustration;
- FIG. 2 is a vertical section view of a furnace, taken on the line 22 in FIG. 1;
- FIG. 3 is a fragmentary plan view of the furnace, showing the central core thereof;
- FIG. 4 is a fragmentary vertical sectional view of a modified form of retort which may be used in connection with the present invention
- FIG. 5 is an enlarged fragmentary vertical sectional view of the retort and cover, showing spacing beads between the retort and its cover for assuring positive spacing therebetween for the labyrinth seal;
- FIG. 6 is an enlarged fragmentary sectional view on line 66 of FIG. 5.
- the furnace comprises a base or table 1 supported in horizontal position by a suitable frame.
- the upper surface of the table 1 carries at certain circu-mferentially spaced locations, radial strips 2 of heat resistant synthetic organic plastic material, such as Neoprene.
- a plurality of L-shaped core pieces 3 are disposed on the strips 2, each with the shorter leg of the L extending radially outwardly from the upright central axis of the base and with the longer leg of the L at the outer end of the shorter leg and extending upwardly.
- the core pieces 3 are spaced uniformly about the central axis.
- At the inner ends of the short legs 3a of the L-shaped core pieces are central core pieces 4 arranged in such relation about the central axis that they form, in effect, a single laminated central core.
- the core pieces 3 and 4 are radially extending upper core pieces 5, arranged one core piece 5 -to each core piece 3. At their outer ends, the upper core 4 pieces 5 rest on the upper ends of the core pieces 3, but are not connected thereto. The inner ends of the core pieces 5 are fixedly connected to the upper ends of the core pieces 4, so that all of the upper core pieces 5 for-m with all. of the core pieces 4 a single unit.
- the lower end of the core piece 4 rests on the upper surface of the shorter legs 3a of the L-shaped core pieces 3, but are not connected thereto. Thus, all of the core pieces 4 and 5 can be lifted as a unit by an overhead hoist to afford access to the retort.
- the coil 6 Disposed between the upright outer leg portions 312 and the core piece 4 is a combined heating and cooling coil 6, formed of copper or other electrical and heat conducting tube.
- the coil 6 comprises an upright inner coil portion 6a having a plurality of closely spaced convolutions surrounding the inner core piece 4, a planar base coil portion 6b having a plurality of convolutions of gradually increasing radius extending from the inner portion 6a outwardly and disposed adjacent the plane of the upper faces of the legs 3a, and an outer coil portion 60 with a plurality of convolutions which extend from the outer limit of the portion 6b upwardly to the top of the core pieces 3 adjacent the inner surface of the leg portions 3b.
- the tube forming the coil 6 has an inlet 7 which is adapted for connection to a suitable source of cooling water and has an outlet 8 for the discharge of Water.
- the trough 9 has an inner peripheral wall overlying the outer face of the coil portion 6a, a bottom wall overlying the coil portion 6b, and an outer peripheral wall overlying the inner face of the coil portion 60.
- the walls are preferably of the same thickness.
- the coil is mounted in suitable Ultracal plaster or other plaster 10.
- the trough 9 is composed of Fiberfax or other thermal insulating material. Both the plaster 10 and the trough 9 may be molded in situ.
- An annular metal retort 11 is supported on tier blocks 12 which are disposed in the bottom of the trough 9.
- the retort has an inner peripheral wall 11a, an outer peripheral wall 11b, and a bottom wall 110. Due to the flux patterns and resultant induced heating currents, and heat radiating patterns, the walls of the retort are made of different thicknesses so that all unit area of the walls can be heated to, and maintained at, the same temperature.
- the inner wall is thinner than the outer wall, the thickness being proportioned to the amount of current induced in each.
- the bottom wall preferably is of gradually increasing thickness outwardly, beginning with the thickness of the inner wall and ending with the thickness of the outer wall.
- a gas baffle wall 12a which preferably is horizontal and extends substantially from the inner wall 11a to the outer wall 11b of the retort.
- the bottom wall of the retort slopes downwardly from its inner to its outer periphery so that between the bafile wall 12 and bottom wall 11c, a gas distributing space is provided which is of gradually decreasing cross-sectional area, in the radial plane through the axis of retort, from its outer wall to its inner wall.
- a gas distribution ring 13, in the form of an annular length of perforated pipe, is disposed between the baffle wall 12 and the bottom wall 11c of the retort 11 near the outer periphery of the retort.
- the ring has flexible inlet tubes 13a for introduction of gas.
- This ring discharges into the gas distributing spa'ce between the bottom wall 110 and the baffie wall 12a.
- the baffie wall rests on suitable supporting lugs, as illustrated, but the gas discharged therebeneath can flow readily to the outer and inner peripheries and discharge freely upwardly along the walls 11a and 11b.
- Suitable supporting rails 14 of suitable material may be disposed on top of the baffle wall for supporting articles to be brazed in spaced relation thereto.
- annular detachable cover 15 For closing the open upper end of the retort 11, an annular detachable cover 15 is provided.
- the cover 15 has a usual top wall with inner and outer depending peripheral side walls 15a, each with upper and lower spacing beads 15b and 15c, respectively, which engage the adjacent walls 11a and 11b, respectively.
- the beads 15b and 150 are of slightly greater radial dimension than the seals 16, so as to assure a positive spacing of the seals 16 from the walls 11a and 11b.
- the beads 15a and 150 are notched at their peripheries as indicated at 15c, so as to assure positive clearance of the seal 16 and walls of the retort.
- Labyrinth seals are well known in the art and, though not true seals, they have special advantages in the present structure. Such seals function by necessitating repeated pronounced and sudden changes in velocity of flow of gases passing over their operating surfaces, being in effect not true seals but leakage controlling barriers. If desired, the labyrinth seals may be mounted on the outer surfaces of the walls 11a and 11b instead of on the cover.
- thermal insulation in the form of an annulus 17 of thermal insulating material, such as Fiberfax, is provided.
- This annulus is overlain with a plurality of cooling elements 18 through which cooling water from an extraneous source can be circulated which are separated from each other circumferentially.
- Each element 18 is in the form of an annular sector of copper sheet 18a with a copper tube 18b brazed to one of its faces and connectable in a water cooling circuit, by pipes 180, as illustrated in FIGS. 1 and 2.
- the annulus 17 preferably rests directly on the cover 15 and may be fixedly secured thereto if desired.
- the cover 15 is provided with a plurality of upright supporting bolts 19 which extend through suitable brackets 19a on the upper core pieces 5.
- the bolts are adjustable endwise by suitable nuts 20. Preferably they are adjusted so that they suspend the cover in a position wherein, when the core pieces rest upon the upper ends of the core pieces 3, the cover is fully seated and resting with its inner surface on the upper edges of the peripheral walls 11a and 11b. If desired, the
- an upright guide post 21 is secured in fixed coaxial relation with the base or table 1.
- An axial passage is provided at the inner ends of the short legs 3a of the L-shaped core pieces 3, through the central core in coaxial relation with the base 1 and at the inner ends of the core pieces 5.
- a guide tube 22 is disposed in the portion of this passage above the legs 3a, and is bonded to the core piece 4, and at its lower end is unconnected to the legs 3a.
- An internally threaded coupling 23 rests on an annulus 24, of electrical insulating material, which, in turn, rests on the upper surface of the upper core pieces 5 adjacent their inner ends.
- a suitable connecting nipple 25 is threaded into the coupling 23, is welded to the tube 22, and is arranged to receive axially the upper end of the post 21 with operating clearance.
- the guide pipe 22 receives the post 21 which thereby guides the core pieces 4 and 5 and the cover 15 into position.
- suitable complementary splines parallel to the axis of the post, may be provided in the nipple 25 and on the post to constrain the core pieces to proper position circumferentially of the post axis to mate with the upper ends of the leg portions 3b of the core pieces 3.
- the interior of the retort 11 be purged of all objectionable gases and that a high purity atmosphere of a selected gas, such as hydrogen, be maintained therein during the heating operation.
- a selected gas such as hydrogen
- the labyrinth seals 16 permit the escape of gas from the retort while eliminating back diffusion.
- the escape of hydrogen between the cover 15 and top end of the retort 11 results in the production of a hydrogen-oxygen mixture at the lower edge of the flanges of the cover 15. This is objectionable from the standpoint of the high temperature and thermal shock to which the retort and cover are subjected upon burning of the mixture, but also due to the heat to which the coil and core are subjected.
- a hood 30 is provided for enclosing the entire induction furnace.
- the hood 30 is preferably dome shaped with a depending peripheral side wall 31.
- a coupling element, or nipple 31a corresponding to the nipple is secured to its top wall.
- the nipples 25 and 31a are adapted for connection, successively, to the same internally threaded coupling, which latter may be carried by an overhead hoist.
- the table In order to provide a seal between the entire lower peripheral edge of the flange 31 of the hood and the upper surface of the table or base 1, the table is provided on its upper surface at its outer periphery with an upwardly open peripheral channel 32 in which is a rubber sealing cushion 33.
- Suitable circumferentially spaced brackets 34 are provided near the lower edge of the hood and are positioned to engage the outer wall of the channel 32 and support the weight of the hood while the lower edge of the flange 31 depresses the rubber seal 33. This assures an effective seal between the hood and the table 1.
- a rubber seal is effective at this location because it is not subjected to high temperatures such as would be present were an attempt made to use such a rubber seal between the cover 15 and the retort 11.
- the base or table 1 is provided with a screened filter port 35 which may be attached to any type of conventional vacuum pump so that the interior of the hood can be evacuated to the degree desired.
- the port is in the base. This is used for purging out the air before admitting hydrogen; for maintaining a discharge flow of gas at any desired partial pressure during the heating and cooling cycle; and finally to purge out the hydrogen before admitting air at the end of the cycle prior to lifting the cover.
- a filter may be arranged to rest on the base or table 1 between one pair of adjacent core pieces 3, as illustrated in FIG. 1.
- the filter may comprise a strip of copper sheet 36 bent into channel shape and disposed between the adjacent core pieces 3 with the width of the sheet upright.
- the open side of the resultant channel is closed by a cloth or other suitable filter strip 37 so that all gases passing to the port 35 from within the hood 30 are filtered. This eliminates the necessity for a separate extraneous container for the filter.
- the hood 30 may be provided at the lower margin of its side wall 31 with circumferentially spaced holddown yokes 38 which are engaged by bolts 39 pivotally secured to the base 1 for securing the hood in place.
- nuts 39a on the bolts may be tightened with the fingers, to assure retention of the 7 sealing relation of the hood with the seal 33 when the subatmospheric pressure is relieved and a superatmospheric pressure is built up in the hood due to heat or other causes.
- the outer wall of the retort is of greater thickness than the inner wall so that the heat input and output per square inch is equalized as between the walls.
- the ratio of the thickness of the outer to that of the inner wall is in proportion to the square of the respective radii. For instance, with an outer wall of two feet in diameter and the inner wall of one foot diameter, the ratio of thickness of the outer wall to the inner wall is four to one, assuming of course the same flux linkage with all walls of the retort and its cover.
- the bottom wall radially it preferably should be tapered gradually from the outer to the inner wall beginning with the same thickness as the outer wall at the outer periphery and tapering to the thickness of the inner wall at the inner periphery.
- a retort 40 may be used.
- This retort has a thin inner wall 40a, a thicker outer wall 40b, and a bottom wall 400 of uniform thickness on which a plurality of annular plates 41 are secured in firm face to face juxtaposition.
- the plates are of different internal diameters and arranged so that, when juxtaposed against the bottom wall of the retort, they form, in effect, a bottom wall which is of progressively less thickness from its outer periphery to its inner periphery.
- the walls of the retort should be as thin as possible consistent with adequate current flow for heating.
- the cover may have its top wall provided with plates so that it is of increasing thickness from the inner to the outer periphery, the same as the bottom wall illustrated in FIG. 4.
- the labyrinth seal 16 is especially desirable because it affords an accurate passage for exfiltration of control gas under light pressure of gas within the retort, yet can prevent back diffusion. This it can do in all stages of heating and cooling.
- the insulation trough 9 should be relatively thin, consistent with preventing overheating of the coils and cores and consistent with radiation of heat into the coils. It preferably has an outer peripheral wall which is the same thickness as its inner peripheral wall so as to assist in maintaining a balanced heating and radiating effect.
- the water cooled coils are desirable and very effective for heating the retort by the currents induced therein without themselves becoming overheated. At the same time, they operate effectively for cooling the retort and its contents rapidly. Meanwhile they prevent the transmission of a great amount of heat to the core pieces and hood so that the hood temperature does not endanger the seal between the lower edge of the hood and the sealing material 33 in the channel 32 on the base or table 1.
- the coil portion 6a, 6b and 60 generally are in the form of separate coils connected in series, but they may be connected individually, each to a desired source of power and cooling water.
- the difference in the thicknesses of the inner and outer walls of the retort is especially important in those instances wherein the inner radius is much less than the outer.
- the gas pressure may be raised to atmospheric pressure, thereby greatly increasing the heat dissipation.
- the loss of heat is negligible, but as the pressure of the gas increases above 1 millimeter, the heat dissipation increases rapidly, up to about atmospheric pressure.
- the gas flow must be high enough to prevent back diffusion through the seal.
- cooling coils on at least three sides of the thin walled retort provides for rapid or short cycle cooling. At the same time, the cores and other parts are protected from excessive heat.
- thermocouples For maintaining temperatures, conventional thermocouples may be employed in the retort and elsewhere if desired.
- An induction furnace comprising an annular retort of electrically conducting material in the form of an open top metal channel having thin circumferentially continuous inner and outer side walls, respectively, a bottom wall, and a detachable annular cover;
- electromagnetic means including core means and electric coil means for producing a magnetic flux field in inductive relation to the annular retort;
- said core means having a flux conducting portion extending through the central opening of the retort and cover;
- enclosing means providing an evacuable closed sealing chamber in which said electromagnetic means and retort are disposed;
- the electromagnetic means includes inner and outer coil means coaxial with the retort and disposed alongside the exterior of the inner and outer walls, respectively, of the insulating container; said coil means being in the form of tubular conductor means; inlet and outlet means connected to the coil means and extending to the outside of the chamber for admitting and discharging cooling media to and from the coil means, respectively, and adapted for connection to an extraneous source of circulatable cooling media.
- the electromagnetic means includes core pieces of O-shape extending generally radially of the retort and surrounding the retort exteriorly of the coil means and spaced apart from each other circumferentially of the retort.
- said enclosing means comprises an upwardly facing base and a hood having a dependent peripheral wall; a peripherally continuous resilient annular seal disposed between the lower edge of the wall and the upper face of the base and in sealing engagement with both the wall and the base for sealing the joint therebetween; and
- stop means independent of the seal for limiting the deformation of the seal by the hood.
- the electromagnetic means includes a lower core portion and an upper core portion separable from the lower core portion by upward movement, said upper core portion having portions spaced above the retort and extending thereacross;
- means are connected to the upper core portions and are adapted for connection to a hoist for lifting the upper core portions and thereby the cover.
- retort cover and extends radially of the retort substantially from the inner to the outer peripheral wall of the insulating container.
- the electromagnetic means include a coil means coaxial with the retort and extending circumferentially of the insulating container along the inner wall, bottom wall, and outer wall of the insulating container, said coil means being in the form of tubes;
- cooling tube means embedded in said thermal insulator means and adapted for connection to an extraneous cooling circuit for circulating cooling media therethrough.
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Description
J. R. GIER, JR
Oct. 29, 1968 INDUCTION FURNACE EMPLOYING HIGH PURITY ATMOSPHERE 2 Sheets-Sheet 1 Filed April 4, 1966 INVLFNTOR. BY 21/. I
Oct. 29, 1968 J. R. GIER, JR 3,408,470
INDUCTION FURNACE EMPLOYING HIGH PURITY ATMOSPHERE Filed April 4. 1966 2 Sheets-Sheet 2 a Q a \a & 1 w "*5 (\I W a; INVENTOR.
MM, L21 BY g i 2 ?3 I I254 ATTOF/VEK United States Patent 3,408,470 INDUCTION FURNACE EMPLOYING HIGH PURITY ATMOSPHERE John R. Gier, Jr., Hines Hill Road, Hudson, Ohio 44236 Filed Apr. 4, 1966, Ser. No. 539,847 Claims. (Cl. 21910.49)
ABSTRACT OF THE DISCLOSURE The furnace is a low frequency induction furnace having a covered, electrically conductive annular retort forming a short circuited secondary which is heated by currents induced therein. I
It has an electromagnetic core comprised of a plurality of O-shaped core pieces each arranged with one side passing through the central opening of the retort and the other sides extending along the outer walls of the retort and cover.
The retort is enclosed in an evacuable sealing chamber and means are provided for evacuating the chamber and for admitting gaseous media into the retort. A labyrinth type seal is disposed between the retort and its cover.
This invention relates to induction furnaces for brazing, sintering, and the like, and particularly to induction furnaces wherein a high purity atmosphere is to be maintained during the heating and cooling of articles therein.
For purposes of illustration the invention will be described as applied to a ring type brazing furnace, its use for purposes other than brazing being apparent from the illustrative example.
Heretofore in brazing, one practice has been to place the article within a heating chamber of a furnace. If controlled atmosphere was desired, the article was placed in a retort closed by a removal cover and disposed in the chamber. The retort was provided with suitable conduits by which the gas for the atmosphere desired could be introduced into or removed.
With such a structure, the general practice was to purge the air with an inert gas and then introduce a protective gas. Generally, a so-called sand sea was provided between the cover and body of the retort. Control gas was fed into the retort at pressures above that in the furnace chamber, and a continuous flow of the gas was maintained to reduce back diffusion from the chamber through the seal" into the retort.
The infiltration and exfiltration of gasses through sand seals cannot be precisely controlled. They provide a myriad of passages for the exfiltration of gas from the interior of the retort into the furnace chamber. These passages vary much in size and are heterogeneously arranged. Consequently, the seal may be much more porous at one portion than at another. As a result, there is a pronounced tendency toward back diffusion of gasses from the chamber into the retort. In order to maintain control of the exfiltration of the gases so as to overcome the back diffusion, the flow of the control gas must be sufficiently high so that there is an assurance that gas is filtering out continuously throughout the entire periphery of the sand seal at a sufficient rate to prevent any re-entry of gas ihto the retort. This necessitates introduction of the atmosphere controlling gas in an amount greatly in excess of what would otherwise be required.
Further, upon the cooling of the furnace and retort, due to the high thermal capacity of the sand seal, the retort is subjected to very large temperature gradients which cause resultant Warpage and rapid deterioration of the retort as well as slowing down the heating and cooling cycles. To reduce these gradients sufficiently to reduce warpage effectively, the time required for the heating and cooling cycle has to be greatly extended.
In cases where the maintenance of a high purity atmosphere is critical, the practice is to seal the juncture of the cover and retort by welding the cover and retort together about the entire periphery of the cover. In such cases, the cover or the retort is provided with'pipes for evacuating and introducing the controlled atmosphere gas. Obviously the cost and expense in time and money of Welding and breaking such a seal is very great.
Induction brazing generally involves heating the work piece by means of the current induced in it from an adjacent induction coil. This coil carries an alternating current that may range widely in frequency, for example, from 1 to 500 kilocycles, according to the conditions of the particular heating situation.
For induction brazing the work is commonly heated in air with the joint area and the braze filler metal protected against oxidation by means of a suitable flux applied prior to heating. When flux is undesirable, a protective gas may be used to provide a reducing or inert gas atmosphere surrounding the work piece during its heating and cooling. If the containing enclosure or envelope for this gas is an electrical conductor it is usually made large enough to encompass the entire primary coil together with the work assembly with suflicient clearance such that the envelope will not be heated by currents induced in it from the primary coil. This arrangement is quite satisfactory where the metals being heated do not form stable oxides and, therefore, the required gas purity is not extreme.
However, when the metals of the work piece contain substantial amounts of chromium or lesser amounts of aluminum or titanium, all of which do form relatively stable oxides, then the protective atmosphere in contact with the work piece must be extremely pure and free of oxidizing contaminants. This is necessary to maintain the work piece bright and clean for successful brazing. It is not feasible to achieve this high degree of gas purity in the presence of an induction coil structure with its thermal and electrical insulation and other parts that will give off adsorbed air and other contaminating gases during the heating cycle.
This difficulty can be avoided by making the enclosure or gas containing envelope of an electrical non-conductor capable of standing high temperature and thermal shock, such as fused quartz, and placing this envelope around the work piece, while maintaining the envelope or enclosure itself within the coil so that the coil and its related sources of gas contamination are all external to the enclosure. This procedure is clearly impractical for any use where the quartz tube must be more than a few inches in diameter.
In very special cases involving small work space and temperature over 2100 F., molybdenum enclosure or envelope for the gas and located within the induction coil has been used in laboratory type work.
The present invention offers in combination a large work space which is induction heated with 60 cyc-le current in a high purity protective gas atmosphere capable of operation at sub-atmospheric pressures at high temperatures with rapid heating and cooling; the use of hydrogen, helium, or argon with complete safety and economy of gas; ease and rapidity of opening and closing furnace; and low maintenance cost.
In accordance with the present invention, a new and improved ring type induction furnace is provided wherein an annular metal retort is employed and a high purity atmosphere is maintained continuously within the retort without back diffusion of gases into the interior of the retort; extremely rapid heating and cooling cycles relative to those heretofore required are obtained; the flow of atmosphere controlling gas for assuring the maintenance of high purity atmosphere within the retort free from back diffusion is effected with a low gas flow; low or sub-atmospheric pressures are maintained during heating, and pressures at substantially atmospheric pressure or above are maintained during cooling, so as to assure eflicient operation with a small flow of the control gas.
Specific advantages of the present invention reside in the provision of a socalled labyrinth seal between the retort and its cover whereby great precision and uniformity in the passages for exfiltration of gases through the seal from the retort are obtained about the entire juncture of the retort and its cover; in the manner in which the parts are related so that ready access is afforded to the interior of the furnace and interior of the retort for charging the articles in the retort and for removing them therefrom; and in the use of a thin walled retort in which heat can be generated rapidly and from which the generated heat can be radiated quickly to the contents of the retort.
Another advantage is that the heating and cooling are confined mostly to the retort and charge of articles so that a large mass of conventional furnace structure does not have to be subjected to the heating and cooling cycles, whereby the time required for the heating and cooling cycles is greatly reduced.
A specific advantage is that the present structure permits the brazing of a large number of individual articles concurrently or in a batch while they are maintained out of contact with each other.
Another specific object is to provide a balance between the wall thicknesses of the retort so that under the influence of the induced currents, the heating of each unit of wall area of the retort is the same as are the others throughout the heating cycle.
Various other specific objects and advantages will become apparent from the following description wherein reference is made to the drawings, in which:
FIG. 1 is a top plan view of the furnace embodying the principles of the present invention, parts thereof being cut away for clearness in illustration;
FIG. 2 is a vertical section view of a furnace, taken on the line 22 in FIG. 1;
FIG. 3 is a fragmentary plan view of the furnace, showing the central core thereof;
FIG. 4 is a fragmentary vertical sectional view of a modified form of retort which may be used in connection with the present invention;
FIG. 5 is an enlarged fragmentary vertical sectional view of the retort and cover, showing spacing beads between the retort and its cover for assuring positive spacing therebetween for the labyrinth seal; and
FIG. 6 is an enlarged fragmentary sectional view on line 66 of FIG. 5.
Referring to the drawings, the furnace comprises a base or table 1 supported in horizontal position by a suitable frame. The upper surface of the table 1 carries at certain circu-mferentially spaced locations, radial strips 2 of heat resistant synthetic organic plastic material, such as Neoprene. A plurality of L-shaped core pieces 3 are disposed on the strips 2, each with the shorter leg of the L extending radially outwardly from the upright central axis of the base and with the longer leg of the L at the outer end of the shorter leg and extending upwardly. The core pieces 3 are spaced uniformly about the central axis. At the inner ends of the short legs 3a of the L-shaped core pieces are central core pieces 4 arranged in such relation about the central axis that they form, in effect, a single laminated central core.
At the top of the core pieces 3 and 4 are radially extending upper core pieces 5, arranged one core piece 5 -to each core piece 3. At their outer ends, the upper core 4 pieces 5 rest on the upper ends of the core pieces 3, but are not connected thereto. The inner ends of the core pieces 5 are fixedly connected to the upper ends of the core pieces 4, so that all of the upper core pieces 5 for-m with all. of the core pieces 4 a single unit.
The lower end of the core piece 4 rests on the upper surface of the shorter legs 3a of the L-shaped core pieces 3, but are not connected thereto. Thus, all of the core pieces 4 and 5 can be lifted as a unit by an overhead hoist to afford access to the retort.
Disposed between the upright outer leg portions 312 and the core piece 4 is a combined heating and cooling coil 6, formed of copper or other electrical and heat conducting tube. The coil 6 comprises an upright inner coil portion 6a having a plurality of closely spaced convolutions surrounding the inner core piece 4, a planar base coil portion 6b having a plurality of convolutions of gradually increasing radius extending from the inner portion 6a outwardly and disposed adjacent the plane of the upper faces of the legs 3a, and an outer coil portion 60 with a plurality of convolutions which extend from the outer limit of the portion 6b upwardly to the top of the core pieces 3 adjacent the inner surface of the leg portions 3b. The tube forming the coil 6 has an inlet 7 which is adapted for connection to a suitable source of cooling water and has an outlet 8 for the discharge of Water.
Disposed within the coil 6 is an open top annular trough 9 of thermal insulating material. The trough 9 has an inner peripheral wall overlying the outer face of the coil portion 6a, a bottom wall overlying the coil portion 6b, and an outer peripheral wall overlying the inner face of the coil portion 60. The walls are preferably of the same thickness.
The coil is mounted in suitable Ultracal plaster or other plaster 10. The trough 9 is composed of Fiberfax or other thermal insulating material. Both the plaster 10 and the trough 9 may be molded in situ.
An annular metal retort 11 is supported on tier blocks 12 which are disposed in the bottom of the trough 9. The retort has an inner peripheral wall 11a, an outer peripheral wall 11b, and a bottom wall 110. Due to the flux patterns and resultant induced heating currents, and heat radiating patterns, the walls of the retort are made of different thicknesses so that all unit area of the walls can be heated to, and maintained at, the same temperature. In the form illustrated, the inner wall is thinner than the outer wall, the thickness being proportioned to the amount of current induced in each. The bottom wall preferably is of gradually increasing thickness outwardly, beginning with the thickness of the inner wall and ending with the thickness of the outer wall.
Within the retort 11 is a gas baffle wall 12a which preferably is horizontal and extends substantially from the inner wall 11a to the outer wall 11b of the retort. The bottom wall of the retort slopes downwardly from its inner to its outer periphery so that between the bafile wall 12 and bottom wall 11c, a gas distributing space is provided which is of gradually decreasing cross-sectional area, in the radial plane through the axis of retort, from its outer wall to its inner wall. A gas distribution ring 13, in the form of an annular length of perforated pipe, is disposed between the baffle wall 12 and the bottom wall 11c of the retort 11 near the outer periphery of the retort. The ring has flexible inlet tubes 13a for introduction of gas. This ring discharges into the gas distributing spa'ce between the bottom wall 110 and the baffie wall 12a. The baffie wall rests on suitable supporting lugs, as illustrated, but the gas discharged therebeneath can flow readily to the outer and inner peripheries and discharge freely upwardly along the walls 11a and 11b.
Suitable supporting rails 14 of suitable material, for example, Mulite, may be disposed on top of the baffle wall for supporting articles to be brazed in spaced relation thereto.
For closing the open upper end of the retort 11, an annular detachable cover 15 is provided. The cover 15 has a usual top wall with inner and outer depending peripheral side walls 15a, each with upper and lower spacing beads 15b and 15c, respectively, which engage the adjacent walls 11a and 11b, respectively. Mounted on the inner surfaces of both the inner and outer peripheral walls 11a and 11b, respectively, are annular labyrinth seals 16. These seals are in very close, but positive, spaced relation to the adjacent wall surfaces of the upper margins of the walls 11a and 11b, respectively, so as to cause the outflowing gas to undergo a succession of abrupt increases and decreases in velocity, thus obtaining the full benefit of a labyrinth type seal. The beads 15b and 150 are of slightly greater radial dimension than the seals 16, so as to assure a positive spacing of the seals 16 from the walls 11a and 11b. The beads 15a and 150 are notched at their peripheries as indicated at 15c, so as to assure positive clearance of the seal 16 and walls of the retort.
Labyrinth seals are well known in the art and, though not true seals, they have special advantages in the present structure. Such seals function by necessitating repeated pronounced and sudden changes in velocity of flow of gases passing over their operating surfaces, being in effect not true seals but leakage controlling barriers. If desired, the labyrinth seals may be mounted on the outer surfaces of the walls 11a and 11b instead of on the cover.
It is desirable that heat losses from the cover be balanced with the losses from the remainder of the retort. For this purpose thermal insulation, in the form of an annulus 17 of thermal insulating material, such as Fiberfax, is provided. This annulus is overlain with a plurality of cooling elements 18 through which cooling water from an extraneous source can be circulated which are separated from each other circumferentially. Each element 18 is in the form of an annular sector of copper sheet 18a with a copper tube 18b brazed to one of its faces and connectable in a water cooling circuit, by pipes 180, as illustrated in FIGS. 1 and 2. The annulus 17 preferably rests directly on the cover 15 and may be fixedly secured thereto if desired.
In order to gain access to the retort, it is necessary, of course, to remove the upper core pieces 5, and also the cover 15. Accordingly, the cover 15 is provided with a plurality of upright supporting bolts 19 which extend through suitable brackets 19a on the upper core pieces 5. The bolts are adjustable endwise by suitable nuts 20. Preferably they are adjusted so that they suspend the cover in a position wherein, when the core pieces rest upon the upper ends of the core pieces 3, the cover is fully seated and resting with its inner surface on the upper edges of the peripheral walls 11a and 11b. If desired, the
bolts can be such that they can slide through the brackets 19a slightly, so that axial lost motion is provided between the cover and core pieces 5 for facilitating guiding the cover into position. Since the cover must be held precisely in axial alignment with the upper end of the retort 11 to effect initial engagement without damaging the labyrinth seals, it is desirable that the core pieces 5 be guided effectively as they are lifted and lowered. For this purpose, an upright guide post 21 is secured in fixed coaxial relation with the base or table 1. An axial passage is provided at the inner ends of the short legs 3a of the L-shaped core pieces 3, through the central core in coaxial relation with the base 1 and at the inner ends of the core pieces 5. A guide tube 22 is disposed in the portion of this passage above the legs 3a, and is bonded to the core piece 4, and at its lower end is unconnected to the legs 3a. An internally threaded coupling 23 rests on an annulus 24, of electrical insulating material, which, in turn, rests on the upper surface of the upper core pieces 5 adjacent their inner ends. A suitable connecting nipple 25 is threaded into the coupling 23, is welded to the tube 22, and is arranged to receive axially the upper end of the post 21 with operating clearance. The guide pipe 22 receives the post 21 which thereby guides the core pieces 4 and 5 and the cover 15 into position. If desired, suitable complementary splines, parallel to the axis of the post, may be provided in the nipple 25 and on the post to constrain the core pieces to proper position circumferentially of the post axis to mate with the upper ends of the leg portions 3b of the core pieces 3.
It is desirable that the interior of the retort 11 be purged of all objectionable gases and that a high purity atmosphere of a selected gas, such as hydrogen, be maintained therein during the heating operation. This may be done by the admission of hydrogen or selected control gas through the ring 13, heretofore described after the cover 15 is installed. The labyrinth seals 16 permit the escape of gas from the retort while eliminating back diffusion. However, if the structure is exposed to the air, the escape of hydrogen between the cover 15 and top end of the retort 11 results in the production of a hydrogen-oxygen mixture at the lower edge of the flanges of the cover 15. This is objectionable from the standpoint of the high temperature and thermal shock to which the retort and cover are subjected upon burning of the mixture, but also due to the heat to which the coil and core are subjected.
For rapid heating and cooling, a hood 30 is provided for enclosing the entire induction furnace. The hood 30 is preferably dome shaped with a depending peripheral side wall 31. For its removal, a coupling element, or nipple 31a corresponding to the nipple is secured to its top wall. The nipples 25 and 31a are adapted for connection, successively, to the same internally threaded coupling, which latter may be carried by an overhead hoist. Thus the hood 30, the core pieces 4 and 5, the cover 15, and the insulating annulus 17 can be installed and removed readily.
In order to provide a seal between the entire lower peripheral edge of the flange 31 of the hood and the upper surface of the table or base 1, the table is provided on its upper surface at its outer periphery with an upwardly open peripheral channel 32 in which is a rubber sealing cushion 33. Suitable circumferentially spaced brackets 34 are provided near the lower edge of the hood and are positioned to engage the outer wall of the channel 32 and support the weight of the hood while the lower edge of the flange 31 depresses the rubber seal 33. This assures an effective seal between the hood and the table 1. A rubber seal is effective at this location because it is not subjected to high temperatures such as would be present were an attempt made to use such a rubber seal between the cover 15 and the retort 11. The base or table 1 is provided with a screened filter port 35 which may be attached to any type of conventional vacuum pump so that the interior of the hood can be evacuated to the degree desired. The port is in the base. This is used for purging out the air before admitting hydrogen; for maintaining a discharge flow of gas at any desired partial pressure during the heating and cooling cycle; and finally to purge out the hydrogen before admitting air at the end of the cycle prior to lifting the cover.
For screening the port 35, a filter may be arranged to rest on the base or table 1 between one pair of adjacent core pieces 3, as illustrated in FIG. 1. The filter may comprise a strip of copper sheet 36 bent into channel shape and disposed between the adjacent core pieces 3 with the width of the sheet upright. The open side of the resultant channel is closed by a cloth or other suitable filter strip 37 so that all gases passing to the port 35 from within the hood 30 are filtered. This eliminates the necessity for a separate extraneous container for the filter.
The hood 30 may be provided at the lower margin of its side wall 31 with circumferentially spaced holddown yokes 38 which are engaged by bolts 39 pivotally secured to the base 1 for securing the hood in place. Generally, when the hood is seated while under subatmospheric internal pressure, nuts 39a on the bolts may be tightened with the fingers, to assure retention of the 7 sealing relation of the hood with the seal 33 when the subatmospheric pressure is relieved and a superatmospheric pressure is built up in the hood due to heat or other causes.
As hereinbefore mentioned briefly, the outer wall of the retort is of greater thickness than the inner wall so that the heat input and output per square inch is equalized as between the walls. The ratio of the thickness of the outer to that of the inner wall is in proportion to the square of the respective radii. For instance, with an outer wall of two feet in diameter and the inner wall of one foot diameter, the ratio of thickness of the outer wall to the inner wall is four to one, assuming of course the same flux linkage with all walls of the retort and its cover. As to the bottom wall, radially it preferably should be tapered gradually from the outer to the inner wall beginning with the same thickness as the outer wall at the outer periphery and tapering to the thickness of the inner wall at the inner periphery. However, such a wall as this is somewhat expensive to manufacture. Consequently, as illustrated in FIG. 4, a retort 40 may be used. This retort has a thin inner wall 40a, a thicker outer wall 40b, and a bottom wall 400 of uniform thickness on which a plurality of annular plates 41 are secured in firm face to face juxtaposition. The plates are of different internal diameters and arranged so that, when juxtaposed against the bottom wall of the retort, they form, in effect, a bottom wall which is of progressively less thickness from its outer periphery to its inner periphery. In any event, the walls of the retort should be as thin as possible consistent with adequate current flow for heating. This is necessary not only for rapid heating and cooling, but also to eliminate thermal shocks and warpage which would otherwise occur. In like manner, the cover may have its top wall provided with plates so that it is of increasing thickness from the inner to the outer periphery, the same as the bottom wall illustrated in FIG. 4.
The labyrinth seal 16 is especially desirable because it affords an accurate passage for exfiltration of control gas under light pressure of gas within the retort, yet can prevent back diffusion. This it can do in all stages of heating and cooling.
The insulation trough 9 should be relatively thin, consistent with preventing overheating of the coils and cores and consistent with radiation of heat into the coils. It preferably has an outer peripheral wall which is the same thickness as its inner peripheral wall so as to assist in maintaining a balanced heating and radiating effect.
The water cooled coils are desirable and very effective for heating the retort by the currents induced therein without themselves becoming overheated. At the same time, they operate effectively for cooling the retort and its contents rapidly. Meanwhile they prevent the transmission of a great amount of heat to the core pieces and hood so that the hood temperature does not endanger the seal between the lower edge of the hood and the sealing material 33 in the channel 32 on the base or table 1.
Here it is to be noted that the coil portion 6a, 6b and 60 generally are in the form of separate coils connected in series, but they may be connected individually, each to a desired source of power and cooling water.
The difference in the thicknesses of the inner and outer walls of the retort is especially important in those instances wherein the inner radius is much less than the outer.
In operation, after the retort 11 is charged and the cover 15 thereof installed in place, along with the hood 30, vacuum is applied to the interior of the hood 30. Purging of the retort with hydrogen or selected gas is effected and the heating cycle is then started. The hydrogen is continuously delivered through the inlet pipes 13a to the ring 13, the hydrogen being diffused throughout the interior of the retort. While vacuum is maintained in the hood, a very low flow of hydrogen under low pressure may be maintained to minimize heat loss and gas consumption. The conduction of heat by the gas is in an inverse relation to the pressure of the gas. Gas flow outward through the labyrinth seals is maintained at a space velocity greater than the back diffusion rate of the impure gas surrounding the exterior of the retort. The mass flow rate to accomplish this is in approximate relation to the absolute pressure in the furnace.
For rapid heat-up, low gas pressure is employed, combined with a low ga flow; for example, one mm. of mercury greatly reduces the heat loss.
On the other hand, in cooling, the gas pressure may be raised to atmospheric pressure, thereby greatly increasing the heat dissipation. Thus, with the vacuum or very low pressure, the loss of heat is negligible, but as the pressure of the gas increases above 1 millimeter, the heat dissipation increases rapidly, up to about atmospheric pressure. For operation at atmospheric pressure, as for rapid cooling, the gas flow must be high enough to prevent back diffusion through the seal.
The use of the cooling coils on at least three sides of the thin walled retort provides for rapid or short cycle cooling. At the same time, the cores and other parts are protected from excessive heat. Employing cooling coils above the insulation annulus 17 overlying the cover 15, provides symmetry of cooling and core protection.
For maintaining temperatures, conventional thermocouples may be employed in the retort and elsewhere if desired.
As a result, very rapid cycles of both in heating and cooling are obtained. The heat generation is uniform throughout the retort, severe thermal shocks and strains are eliminated so that the life of the retort is greatly increased, a high purity atmosphere without back diffusion is maintained economically, and ready access is provided for cleaning the retort and removing the articles therefrom.
Having thus described my invention, I claim:
1. An induction furnace comprising an annular retort of electrically conducting material in the form of an open top metal channel having thin circumferentially continuous inner and outer side walls, respectively, a bottom wall, and a detachable annular cover;
electromagnetic means including core means and electric coil means for producing a magnetic flux field in inductive relation to the annular retort;
said core means having a flux conducting portion extending through the central opening of the retort and cover;
enclosing means providing an evacuable closed sealing chamber in which said electromagnetic means and retort are disposed;
means connected to the interior of the chamber and adapted for connection to an extraneous evacuating means for providing sub-atmospheric pressure within said chamber; and
means for admitting preselected gaseous media into the interior of the retort.
2. A structure according to claim 1 wherein an annular open top container of thermal insulating material is disposed within said chamber; the retort is contained within said insulating container; and the walls of said insulating container are between and thermally insulate the electromagnetic means and the retort.
3. A structure according to claim 2 wherein the electromagnetic means includes inner and outer coil means coaxial with the retort and disposed alongside the exterior of the inner and outer walls, respectively, of the insulating container; said coil means being in the form of tubular conductor means; inlet and outlet means connected to the coil means and extending to the outside of the chamber for admitting and discharging cooling media to and from the coil means, respectively, and adapted for connection to an extraneous source of circulatable cooling media.
4. A structure according to claim 3 wherein the electromagnetic means includes core pieces of O-shape extending generally radially of the retort and surrounding the retort exteriorly of the coil means and spaced apart from each other circumferentially of the retort.
5. A structure according to claim 1 wherein the inner Wall of the retort is of less thickness than the outer Wall of the retort so that, under the influence of the magnetic flux, the heating per unit surface of the inner Wall and outer wall more nearly equalize.
6. A structure according to claim 1 wherein said enclosing means comprises an upwardly facing base and a hood having a dependent peripheral wall; a peripherally continuous resilient annular seal disposed between the lower edge of the wall and the upper face of the base and in sealing engagement with both the wall and the base for sealing the joint therebetween; and
stop means independent of the seal for limiting the deformation of the seal by the hood.
7. A structure according to claim 1 wherein the electromagnetic means includes a lower core portion and an upper core portion separable from the lower core portion by upward movement, said upper core portion having portions spaced above the retort and extending thereacross;
means connecting said last mentioned portions together for lifting upwardly as a unit for affording access to the retort, and means connecting the retort cover to said last mentioned portions for lifting by said last mentioned portions when the upper core portions are lifted; and
means are connected to the upper core portions and are adapted for connection to a hoist for lifting the upper core portions and thereby the cover.
8. A structure according to claim 7 wherein an insulating container is provided and has inner and outer walls 3.
retort cover and extends radially of the retort substantially from the inner to the outer peripheral wall of the insulating container.
9. A structure according to claim 8 wherein the insulating container is annular and coaxial with the retort, the electromagnetic means include a coil means coaxial with the retort and extending circumferentially of the insulating container along the inner wall, bottom wall, and outer wall of the insulating container, said coil means being in the form of tubes;
means on the tubes adapted for connection to a circuit for circulating cooling media through the tubes; and
cooling tube means embedded in said thermal insulator means and adapted for connection to an extraneous cooling circuit for circulating cooling media therethrough.
10. An induction furnace according to claim 1 wherein said cover has inner and outer circumferentially extending flanges disposed alongside the upper margins of the inner and outer side walls, respectively, when the cover is in place; and
a labyrinth seal between each cover flange and the upper margin of its associated side wall operative to prevent back diffusion of gaseous media into the retort between the cover and channel.
References Cited UNITED STATES PATENTS 2,851,582. 9/1958 Meyers et a1 219-1049 X 3,036,888 5/1962 Lowe 219-1049 X 3,056,847 10/1962 Junker l3-27 3,350,494 10/1967 Kunitsky et al. 219-10.49 X
RICHARD M. WOOD, Primary Examiner.
L. H. BENDER, Assistant Examiner.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US539847A US3408470A (en) | 1966-04-04 | 1966-04-04 | Induction furnace employing high purity atmosphere |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US539847A US3408470A (en) | 1966-04-04 | 1966-04-04 | Induction furnace employing high purity atmosphere |
Publications (1)
Publication Number | Publication Date |
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US3408470A true US3408470A (en) | 1968-10-29 |
Family
ID=24152900
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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US539847A Expired - Lifetime US3408470A (en) | 1966-04-04 | 1966-04-04 | Induction furnace employing high purity atmosphere |
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US4539645A (en) * | 1982-08-23 | 1985-09-03 | Conoco Inc. | Automated sample analyzer for induction furnace analysis |
US20030189965A1 (en) * | 2002-04-04 | 2003-10-09 | Miller Douglas J. | Induction furnace for high temperature operation |
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US2851582A (en) * | 1954-07-21 | 1958-09-09 | Western Electric Co | Apparatus for brazing parts together |
US3036888A (en) * | 1959-12-29 | 1962-05-29 | Norton Co | Process for producing titanium nitride |
US3056847A (en) * | 1958-04-12 | 1962-10-02 | Junker Otto | Vacuum melting induction furnace |
US3350494A (en) * | 1965-01-12 | 1967-10-31 | Tsnii Chernoj Metallurg | Induction furnace |
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US2851582A (en) * | 1954-07-21 | 1958-09-09 | Western Electric Co | Apparatus for brazing parts together |
US3056847A (en) * | 1958-04-12 | 1962-10-02 | Junker Otto | Vacuum melting induction furnace |
US3036888A (en) * | 1959-12-29 | 1962-05-29 | Norton Co | Process for producing titanium nitride |
US3350494A (en) * | 1965-01-12 | 1967-10-31 | Tsnii Chernoj Metallurg | Induction furnace |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
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US4539645A (en) * | 1982-08-23 | 1985-09-03 | Conoco Inc. | Automated sample analyzer for induction furnace analysis |
US20030189965A1 (en) * | 2002-04-04 | 2003-10-09 | Miller Douglas J. | Induction furnace for high temperature operation |
WO2003087689A1 (en) | 2002-04-04 | 2003-10-23 | Ucar Carbon Company, Inc. | Induction furnace for high temperature operation |
US6724803B2 (en) * | 2002-04-04 | 2004-04-20 | Ucar Carbon Company Inc. | Induction furnace for high temperature operation |
US20050013339A1 (en) * | 2002-04-04 | 2005-01-20 | Miller Douglas J. | Induction furnace for high temperature operation |
US6898232B2 (en) | 2002-04-04 | 2005-05-24 | Ucar Carbon Company Inc. | Induction furnace for high temperature operation |
JP2005521855A (en) * | 2002-04-04 | 2005-07-21 | ユーカー、カーボン、カンパニー、インコーポレーテッド | Induction furnace for high temperature operation |
CN1659415B (en) * | 2002-04-04 | 2010-05-26 | 格拉弗技术国际控股有限公司 | Induction furnace for high temperature operation |
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