US3266947A - Method of heat treating alloy steel rotor forgings - Google Patents

Method of heat treating alloy steel rotor forgings Download PDF

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US3266947A
US3266947A US306317A US30631763A US3266947A US 3266947 A US3266947 A US 3266947A US 306317 A US306317 A US 306317A US 30631763 A US30631763 A US 30631763A US 3266947 A US3266947 A US 3266947A
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forgings
forging
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John E Steiner
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United States Steel Corp
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United States Steel Corp
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/44Ferrous alloys, e.g. steel alloys containing chromium with nickel with molybdenum or tungsten

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  • Pretemper treatment (0ptional).Heating to a tempering temperature of fromllOO to 1275 F., holding at this temperature for about 30 hours and cooling usually in a furnace to room temperature.
  • Second austenitizing treatment Reheating to an austenitizing temperature of from 1475 to 1750 F. and holding at this temperature for about 30 hours.
  • Second normalizing trea tment.-Cooling in air, by fan, fog or spray) to about 300 to 600 F. and holding at this temperature for about 30 hours.
  • the steel composition for which the treatment is effective is as follows:
  • Cool at an accelerated rate in air by fan, fog, or spray, or in Water or oil to about 600 F. or lower, for example, room temperature is preferred, remove from the cooling environment, and allow to cool to ambient temperature in still air.
  • Specimens of these steels were heat treated in accordance with the method of this invention for heat treating heavy rotor forgings of the nickel-molybdenum-vanadium rotor steel as set forth in steps 1 to 4 above.
  • two 40-inch octagon by 60-inch long test pieces of steels 2 and 3 were produced and processed with a double normalizing and tempering treatment (utilizing austenitizing temperatures of 1700 and 1475 F.) to provide a basis for comparison of the effect of single versus double normalizing treatment on the properties of these steels when all other factors were held constant.
  • a method of producing large rotor forgings comprising forging a rotor from steel containing essentially iron and Carbon 15/.30% Manganese 15 .80 Silicon 40 max Nickel 1 50/425 Chromium 2.00 max. Molybdenum .20/ .70 Vanadium .30 max.
  • a method of producing large rotor forgings comprising forging a rotor from steel consisting of Carbon .15/.30% Manganese .15 .80 Silicon .40 max.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Heat Treatment Of Articles (AREA)

Description

United States Patent 3,266,947 METHOD OF HEAT TREATING ALLOY STEEL ROTOR FORGINGS John E. Steiner, Churchill Borough, Allegheny County,
Pa., assignor to United States Steel Corporation, a corporation of Delaware No Drawing. Filed Sept. 3, 1963, Ser. No. 306,317
2 Claims. (Cl. 14812) 7 This invention relates to improvements in heat treating heavy alloy steel forgings and more particularly to forgings which are used in the production of large generator and turbine rotors.
Heretofore in the production of alloy steel forgings for generator and turbine rotors the heavy forgings, i.e. forgings over 30 inches in diameter have been subjected to very long and expensive heat treatment to develop required physical and mechanical properties. The steps in the heat treatment have been as follows:
(1) Slowly cooling after forging, usually from a temperature of about 1500 F., at a rate of about 10 F. per hour to about 600 F. and holding at this temperature for about 30 hours.
(2) First austenitizing treatment.Reheating to an austenitizing temperature of from 1750 to 1850' F. and
holding at this temperature for about 30 hours.
(3) First normalizing treatment.Cooling (usually in air) to about 600 F. and holding at this temperature for about 30 hours.
(4) Pretemper treatment (0ptional).Heating to a tempering temperature of fromllOO to 1275 F., holding at this temperature for about 30 hours and cooling usually in a furnace to room temperature.
(5) Second austenitizing treatment.Reheating to an austenitizing temperature of from 1475 to 1750 F. and holding at this temperature for about 30 hours.
(6) Second normalizing trea tment.-Cooling (in air, by fan, fog or spray) to about 300 to 600 F. and holding at this temperature for about 30 hours.
(7) Reheating to a tempering temperature of from about 1050 to 1275 F., holding at this temperature for about 30 hours and cooling at a rate of about 10 F. per hour to room temperature. Machining and testing is usually performed after steps 4 and 7 above.
We have discovered that the foregoing heat treatment time can be reduced from between 400 to 600 hours to between 150 to 300 hours for nickel-molybdenum-vanadium steels of the following composition, not only Without impairment of the properties obtained but with actual improvements therein. The steel composition for which the treatment is effective is as follows:
Carbon /.'30% Manganese 15/.80 Silicon 40 max Nickel 1 50/ 4.25 Chromium 2.00 max. Molybdenum .20/ .70 Vanadium .30 max.
balance iron and residual impurities and other elements such as copper, aluminum, nitrogen, etc. in small amounts which do not adversely affect the properties.
I have discovered that with such steel a heat treatment consisting of air cooling after forging, austenitizing and tempering will produce results as good or better than the prior art treatment. My treatment is as follows:
ice
(1) Air cool the forging directly to room temperature after the forging operation.
(2) Heat to an austenitizing temperature of 1475 to 1525 F., i.e. about 1500 F. and hold at this temperature for at least about 3-0 hours (the only austenitizing treatment).
(3) Cool at an accelerated rate in air by fan, fog, or spray, or in Water or oil to about 600 F. or lower, for example, room temperature is preferred, remove from the cooling environment, and allow to cool to ambient temperature in still air.
(4) Heat to a tempering temperature of 1025 to 1175" F., hold at this temperature for at least 30 hours, and furnace cool (i.e. slow cool at a rate less than 30 per hour) to room temperature. Machining and testing may be performed after steps 1 and 4.
Studies have been conducted on nickel-molybdenumvanadium steels of the following chemical composition, percent.
Specimens of these steels were heat treated in accordance with the method of this invention for heat treating heavy rotor forgings of the nickel-molybdenum-vanadium rotor steel as set forth in steps 1 to 4 above. In addition, two 40-inch octagon by 60-inch long test pieces of steels 2 and 3, were produced and processed with a double normalizing and tempering treatment (utilizing austenitizing temperatures of 1700 and 1475 F.) to provide a basis for comparison of the effect of single versus double normalizing treatment on the properties of these steels when all other factors were held constant.
Mechanical test results in the transverse test direction of the above-mentioned forgings are given in the following Table I.
These data. show that none of the mechanical properties of these three nickel-molybdenum-vanadium rotor steels are significantly aifected 'by single normalizing instead of double normalizing, by the elimination of the initial slow cooling from the forging operation, and by cooling to and holding at room temperature after the austenitizing treatment (steel 1 was not treated in this manner, it was held at about 600 F. for about 30 hours and then reheated to the tempering temperature). In fact, some of the mechanical properties are improved by this new method of heat treatment, for example, see the improved (lower) transition temperature of steels 2 and 3, which were cooled to room temperature after austenizing as compared to steel 1 which was held at 600 F. after austenitizing. In every respect, the properties of the single normalized and tempered steels are equivalent to the properties of the same steels doublenormalized and tempered.
While I have shown and described several specific embodiments of my invention, it will be understood that these embodiments are merely for the purpose of illustration and description and that various other forms may be devised within the scope of my invention, as defined in the appended claims.
Table 1 Charpy V-Notch, 50 Yield Strength, Percent Shear Fracp.s.i. ture Appearance Tensile Elong. Reduction Transition Tem- Steel Strength, in 2", of Area, peratures' p.s.i. percent percent 0.02% 0.2% F Ft.-lbs. at Ofiset Odset 50% Shear 99, 540 24. 0 58. 0 40 99, 21. 5 49. 3 102, 600 21. 5 59. 0 85 38 102, 600 20. 5 56. 8 3 79, 590 83, 370 101, 050 18.0 52. 5 70 41 DN & T 77, 81, 730 100, 300 19. 5 51. 0
ND-Not determined.
1 N & T-Normalize and temper as specified in procedure outlined above except that the forging was held at 600 F. for about 40 hours after cooling from austenitizing and then reheated to temper-temperatures used: l,500 F. austenitize, 1,120 F. temper.
2 N & T-Normalize and temper as specified in procedure outlined above-temperatures used: 1,475 F. austenitize, 1,140 F. temper.
3 DN & T-Double normalize and temper, as specified in procedure outlined for normalize and temper except that an additional normalize (equivalent to Step 2) was addedtemperatures used: 1,700 F. first austenitize, 1,475 F. second austenitize, 1,140 F. temper.
I claim:
1. A method of producing large rotor forgings comprising forging a rotor from steel containing essentially iron and Carbon 15/.30% Manganese 15 .80 Silicon 40 max Nickel 1 50/425 Chromium 2.00 max. Molybdenum .20/ .70 Vanadium .30 max.
air cooling said forging after the forging operation, auste nitizing it at a temperature of 1475 to 1525 F. and hold at such temperature for at least about 30 hours, cool to room temperature, temper at a temperature be tween 1025 and 1175 F. for at least about 30 hours and thereafter slow cool to room temperature.
2. A method of producing large rotor forgings comprising forging a rotor from steel consisting of Carbon .15/.30% Manganese .15 .80 Silicon .40 max.
Nickel 1.50/4.25
Chromium 2.00 max. Molybdenum .20/ .70 Vanadium .30 max.
References Cited by the Examiner UNITED STATES PATENTS 2,992,148 7/1961 Yeo et a1. 14836 DAVID L. RECK, Primary Examiner.
H. F. SAITO, Assistant Examiner.

Claims (1)

1. A METHOD OF PRODUCING LARGE ROTOR FORGINGS CAMPRISING FORGING A ROTOR FROM STEEL CONTAINING ESSENTIALLY IRON AND CARBON .15/.30% MANGANESE .15/.80 SILICON .40 MAX. NICKEL 1.50/4.25 CHROMIUM 2.00 MAX. MOLYBDENUM .20/.70 VANADIUM .30 MAX. AIR COOLING SAID FORGING AFTER THE FORGING OPERATION, AUSTENITIZING IT AT A TEMPERATURE OF 1475 TO 1525*C. AND HOLD AT SUCH TEMPRATURE FOR AT LEAST ABOUT 30 HOURS, COOL TO ROOM TEMPERATURE, TEMPER AT A TEMPERATURE BETWEEN 1025 AND 1175*F. FOR AT LEAST ABOUT 30 HOURS AND THEREAFTER SLOW COOL TO ROOM TEMPERATURE.
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3379582A (en) * 1967-02-15 1968-04-23 Harry J. Dickinson Low-alloy high-strength steel
US3438822A (en) * 1966-10-31 1969-04-15 United States Steel Corp Method of making fine-grained steel
US3619302A (en) * 1968-11-18 1971-11-09 Yawata Iron & Steel Co Method of heat-treating low temperature tough steel
USRE28645E (en) * 1968-11-18 1975-12-09 Method of heat-treating low temperature tough steel
US4820486A (en) * 1985-04-05 1989-04-11 Kabushiki Kaisha Kobe Seiko Sho Low alloy steel having good stress corrosion cracking resistance
US6087013A (en) * 1993-07-14 2000-07-11 Harsco Technologies Corporation Glass coated high strength steel

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2992148A (en) * 1959-04-23 1961-07-11 Int Nickel Co Alloy steels

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2992148A (en) * 1959-04-23 1961-07-11 Int Nickel Co Alloy steels

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3438822A (en) * 1966-10-31 1969-04-15 United States Steel Corp Method of making fine-grained steel
US3379582A (en) * 1967-02-15 1968-04-23 Harry J. Dickinson Low-alloy high-strength steel
US3619302A (en) * 1968-11-18 1971-11-09 Yawata Iron & Steel Co Method of heat-treating low temperature tough steel
USRE28645E (en) * 1968-11-18 1975-12-09 Method of heat-treating low temperature tough steel
US4820486A (en) * 1985-04-05 1989-04-11 Kabushiki Kaisha Kobe Seiko Sho Low alloy steel having good stress corrosion cracking resistance
US6087013A (en) * 1993-07-14 2000-07-11 Harsco Technologies Corporation Glass coated high strength steel

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