US2712072A - Calutron ion source - Google Patents

Calutron ion source Download PDF

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US2712072A
US2712072A US36233A US3623348A US2712072A US 2712072 A US2712072 A US 2712072A US 36233 A US36233 A US 36233A US 3623348 A US3623348 A US 3623348A US 2712072 A US2712072 A US 2712072A
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cathode
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Sayers James
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00Particle spectrometers or separator tubes
    • H01J49/26Mass spectrometers or separator tubes
    • H01J49/28Static spectrometers
    • H01J49/30Static spectrometers using magnetic analysers, e.g. Dempster spectrometer

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  • This invention relates to calutrons and more particularly to an electrode arrangement for automatically regulating the arc current of the ion generator for a calutron.
  • This application is a continuation-in-part of copending application, Serial No. 692,459, filed August 23, 1946, now abandoned.
  • Calutrons are described in general in Atomic Energy for Military Purposes, by H. D. Smyth, and in great detail in the co-pending application of Ernest 0. Lawrence, Serial No. 557,784, filed October 9, 1944.
  • Calutrons are principally employed in separating the isotopes of the elements. They are adaptable to the separation of macroscopic amounts of any mixture of iso topes which may be ionized.
  • an ion source projects ions of a polyisotopic material into a magnetic field. Thereafter, the ions travel in curved paths through the magnetic field, the ions of greater mass describing paths with flatter curves than the ions of lighter mass.
  • Collectors are disposed at suitable points along each path, preferably at the 180 point in the curved travel in order to discharge and collect the ions of the diiierent paths. In this manner the atoms of different mass that were originally in the polyisotopic mixture are distributed in different regions and thereby substantially separated from one another.
  • the degree of separation of the isotopes which is thus achieved will depend largely upon the stability of the forces acting to produce the aforementioned paths and the accuracy with which the beam is directed upon the collector elements. These forces are the result of the magnetic field and the accelerating potential employed. Various means are employed to regulate the magnetic field and accelerating potential and to keep them relatively constant. It is also highly desirable that a relatively intense, stable beam of positive ions be projected from the ion generator by the accelerating structure through the liner to the collector elements, which operating condition requires that the ion generator presents to the accelerating structure a high density plasma surface which is extremely stable in shape, position, and ion density. In order to obtain such a plasma surface, the rate of ion production by the arc discharge in the ion generator must be substantially constant. This has been accomplished by controlling the heating energy applied to the arc cathode plate inversely as the arc current.
  • Another object of this invention is to provide a regulator for stabilizing the operation of an ion generator of the arc discharge type.
  • Still another object of this invention is to provide a regulator for an ion generator of the hot cathode are discharge type which has a highly stable rate of ion production.
  • a further object of this invention is to provide a cathode heated by electron bombardment that is auto- "ice matically regulated so as to be electron emissive to a predetermined value.
  • Figure l is an isometric view of an ion generator comprising an arc block, a movable arc cathode and a filamentary cathode;
  • Fig. 2 is an isometric view of another embodiment of the invention in which the ion generator comprises an arc block, a fixed arc cathode plate, a movable grid and a filamentary cathode.
  • An ion generator of the arc discharge type is shown.
  • An arc block 1 con-' tains an arc discharge chamber 26 visible through an arc slit 2'7.
  • the are block 1 also contains a charge receptacle (not shown) and a communicating passage between the charge bottle and the arc discharge chamber 26.
  • Mounted on the arc block 1 and centered over the arc chamber 26 is a collimating electrode 2 containing a collimating slot 3.
  • Mounted adjacent to the collimating electrode 2 and in line with the collimating electrode 2 and the arc chamber 26 is a movable arc cathode 4.
  • This movable cathode 4 is supported by a lever arm 13 which is pivotally mounted by a pin 14 on a support bracket 16.
  • a wire 22 has one of its ends attached to a nonconducting support 23, and its other end attached to the outboard end of the lever arm 13.
  • One end of a spring 243 is attached to the same end of the lever arm 13 as is one end of the wire 22.
  • the other end of the spring 20 is attached to the nonconducting support bracket 16.
  • a filamentary cathode 8 is mounted adjacent to the arc cathode plate 4.
  • the are supply 5 has its positive terminal connected through a wire 6 to the arc block 1 and its negative terminal connected through wire 28 to the end of the control wire 22 which is attached to the nonconducting support 23.
  • the total are current of the arc discharge which takes place between the arc cathode plate 4 and a bottom plate 25 of the arc block 1, flows through the control wire 22.
  • An intermediate cathode supply 19 has its positive terminal connected to the arc cathode 4 through a wire 18 and the lever arm 13, and its negative terminal connected through a wire 29 to one terminal of a filament supply 9. This same terminal of the filament supply 9 is connected through a wire 30 to the filamentary cathode 8.
  • the other terminal of the filament supply 9 is connected through a variable resistor 10 to the other end of filamentary cathode 8.
  • the variable resistor 10 By means of the variable resistor 10 the amount of current flowing in the filamentary cathode 8 can be controlled and thus its temperature can be controlled.
  • the operation of the ion generator shown in Fig. l is conducted in a homogeneous magnetic field in which the lines of flux are parallel to the arc slit 27.
  • Conventional heaters (not shown) surround the charge receptacle for heating the arc block. After the arc block and the charge receptacle have been brought up to the correct operating temperature, the material contained in the charge bottle which has been vaporized by this heat is allowed to flow out into the arc chamber.
  • the circuit to the filamentary cathode 8 is then closed, and the current flowing through the filamentary cathode 3 causes heating of the same.
  • the amount of current flowing through the filamentary cathode 8, and, therefore, its temperature, may be controlled by the variable resistor 10.
  • the temperature of the filamentary cathode 8 is adjusted by means of variable resistor so that thermionic emission takes place from said filamentary cathode.
  • the circuit to the intermediate cathode supply 19 is then closed, The electrons which have been emitted by filamentary cathode 8 are immediately attracted to the arc cathode plate 4.
  • the are cathode plate 4 is heated to a thermionically emissive temperature by electron bombardment from the filamentary cathode 8, and the electrons emitted from the arc cathode plate 4 are accelerated downward into the arc block 1 as soon as the connection to the arc supply 5 is completed.
  • An arc discharge thus takes place between the arc cathode plate 4 and the arc chamber bottom plate 25.
  • collimating slot 3 in collimating plate 2 is to give the arc discharge within the arc chamber 26 a desired configuration, which is accomplished by forming a slot of requisite cross section in the collimating plate 2 and allowing the arc discharge to pass therethrough.
  • the automatic control features of this ion generator operate in the following manner: Referring again to Fig. 1, it will be seen that the arc current (electron flow) flows from the negative terminal of the arc supply 5 through the connecting wire 28, then through the control wire 22 to the lever arm 13 and thus to the arc cathode 4. The are current then flows in the form of an arc discharge to the bottom plate of the arc chamber 1 and thence through the return wire 6 to the arc supply 5. Thus it is apparent that the total are current flows through the control wire 22.
  • This control wire 22 has been chosen of such diameter that the correct operating arc current will heat the wire 22 to a temperature approaching a dull red heat or a temperature much higher than that of the surrounding apparatus. Under these conditions the temperature of the wire 22, in accordance with the coefficient of expansion thereof, controls its length and is dependent only upon the arc current.
  • the are current is controlled by the number of thermionic electrons emitted from the arc cathode plate 4, which quantity is determined by the temperature of the arc cathode plate 4, and the temperature is in turn determined by the amount of electron bombardment received from the filamentary cathode 8.
  • the operating constants are preferably so selected that the current flowing between the filamentary cathode 8 and the arc cathode plate 4 is space-charge limited, and thus the current varies inversely as the distance between the cathodes 8 and 4.
  • the arc current is automatically decreased if, during operation, it exceeds the original predetermined value.
  • the control wire 22 cools and in cooling its length becomes less. This decrease in length, acting against spring 20, pivots the lever arm 13 about the pin 14. This action causes the arc cathode plate 4 to move closer to the filamentary cathode 8, which increases the amount of bombardment that the arc cathode plate receives, and in turn raises the temperature of the arc cathode plate 4.
  • This increase in temperature of the arc cathode plate 4 causes emission of a greater number of electrons which in turn increases the arc current. In this manner a mechanism is provided whereby the arc current may be maintained substantially constant.
  • FIG. 2 a second embodiment of the invention is shown.
  • an ion generator is shown which is similar in some respects to that of Fig. 1, but by the addition of a grid as hereinafter described, more precise control of the arc current may be effected.
  • This second embodiment of the invention as shown in Fig. 2 comprises an arc block 101 which contains an arc discharge chamber 126 visible through an arc slit 127.
  • the arc block 101 also contains a charge receptacle (not shown) and a communicating passageway between the charge bottle and the arc discharge chamber 126.
  • Mounted on the arc block 101 and centered over the arc chamber 121' is a collimating electrode 102 containing a collimating slot 103.
  • Mounted adjacent to the collimating electrode 102 and in line with the collimating electrode 192 and the arc chamber 126 is a fixed arc cathode 104.
  • a movable grid 107 is mounted adjacent to the arc cathode 104.
  • the movable grid 107 is supported by a lever arm 113 which is pivotally mounted by a pin 114 on one arm 116 of a support bracket 117.
  • a wire 122 has one of its ends attached to a nonconducting support 123 and its other end attached to a knife-edge block 121. Also attached to the knife-edge block 121 is one end of a spring the other end of tae spring 120 is attached to the support bracket 117. T he spring 120 is arranged so that it will keep the wire 122 taut at all times.
  • the knife-edge block 121 operates on the lever arm 113 and rotates this lever arm 113 about the pivot pin 114, thereby moving the grid 167 with respect to the fixed arc cathode plate 104.
  • the filamentary cathode 108 Situated in line with the collimating slot 103, the fixed arc cathode plate 104, and the grid 107, and also adjacent to the grid 107, is the filamentary cathode 108.
  • the first embodiment uses a filamentary cathode 3 and a movable are cathode plate 4; the spacing between the filamentary cathode 8 and the movable arc cathode plate 4 is controlled by the thermally responsive wire 22.
  • the arc cathode plate 104 is fixed in position relative to the filamentary cathode 108; and interposed between the filamentary cathode 108 and the fixed arc cathode plate 104 is a movable grid 167, whose position relative to the filamentary cathode 108 and the arc cathode plate 104 is determined by a thermally responsive wire 122.
  • the position of the arc cathode plate 4 is varied with respect to the filamentary cathode 8
  • the position of a movable grid 107 is varied with respect to a filamentary cathode 108 and a fixed arc cathode plate 104.
  • a triode comprising a filament, a grid, and an anode, having suitable supplies of voltage and current connected thereto, will allow a definite current flow between the filament and anode; this current being determined by the geometry of the triode. If the voltages applied to the filament, the grid, and the anode of the triode are held constant, then the electron current which is flowing between the filament and the anode can be varied by allowing the grid to move back and forth between the filament and the anode.
  • the grid If the grid is allowed to move away from the anode and toward the filament, it has a greater influence on the electron stream than before and there will be fewer electrons reaching the anode and therefore less current will flow between the filament and anode. Conversely, if the grid moves toward the anode and away from the filament, the grid will have less influence on the electron stream than before and more electrons will reach the anode and therefore more current will flow between the filament and anode.
  • FIG. 2 there is disclosed an ion generator similar in many respects to that disclosed in Fig. l.
  • a movable grid is interposed between filamentary cathode 108 and fixed arc cathode plate 104.
  • This movable grid 107 controls the electron bombardment of arc cathode 104 according to the relative position of the grid with respect to the filamentary cathode 108 and the arc cathode plate 104.
  • the arc current (electron flow) flows from the negative terminal of the arc supply 105, through the wire 128 to one end of the control wire 122; through the control wire 122 and finally to the arc cathode plate 104 through a short jumper from the control wire 122.
  • the are current then flows as an arc discharge from the arc cathode plate 104 to the bottom plate 125 of arc block 101 and thence returns through the wire 106 to the positive terminal of the arc supply 105.
  • the total are current flows through the control wire 122.
  • the control wire 122 becomes hotter; and hence the control wire 122 increases in length thereby allowing the spring 120, acting through the knife-edge block 121, to rotate the lever arm 113 about pivot 114.
  • This allows the grid 107 to move closer to the filamentary cathode 108 and to move farther away from the arc cathode plate 104.
  • This action causes the arc cathode plate 104 to exert less attractive influence on the electrons which are emitted from the filamentary cathode 108.
  • the decrease in the electron bombardment of the arc cathode plate 104 allows its temperature to decrease accordingly and the arc cathode 104 to emit fewer electrons, thereby reducing the arc current. In this manner the arc current is automatically decreased if, during operation, it exceeds the original predetermined value.
  • An ion generator comprising an ionization chamber, a filamentary cathode in spaced relation to said ionization chamber, a grid pivotally disposed therebetween, an arc cathode located between said grid and said ionization chamber, electrical source means connected to said cathodes for establishing electron flow therebetween, a second electrical source means connected between said grid and said filamentary cathode for supplying grid bias voltage, and a third electrical source means for establishing electron flow between said are cathode and said ionization chamber, said are cathode being electrically connected to said third source by a thermally responsive conductor having insulated means connected to said grid for varying the position of said grid in response to changes in current flowing through said conductor.
  • an ion generator comprising an arc block having an arc chamber and an arc slit formed therein and a magnetic field parallel to said are slit passing therethrough, said are block containing conventional heaters and a charge receptacle of a material to be ionized, an arc anode plate covering one end of said are chamber, a collimating plate having a predetermined aperture formed therein covering the other end of said are chamber, an arc cathode disposed above said collimating plate and in line with said aperture, said are cathode having at least two electrodes of variable spacing, one of said electrodes being pivotally mounted, a thermally expansible conductor connected to said movable electrode at one end and having its other end attached to an insulating support bracket, tension means for positioning said movable electrode for initially positioning said movable electrode in a predetermined position, a first source of voltage connected to said are cathode electrodes for establishing electron flow therebetween, a second source of voltage connected to said
  • an arc discharge device comprising a plurality of electrodes having the paths therebetween in alignment, at least two of said electrodes serving as an arc cathode and one an arc anode, voltage supply means connected to said electrodes for impressing operating voltages thereon, one of said arc cathode electrodes having a lever arm extended therefrom which is pivotally mounted at a fulcrum disposed to one side of said paths, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said paths to a fixed point, and means for connecting said conductor between said arc anode and said voltage supply means whereby the position of said one of said are cathode electrodes relative to the other of said electrodes is changed in response to the heating produced by said current.
  • An ion source comprising a plurality of electrodes having the paths therebetween in alignment, at least two of said electrodes serving as an arc cathode and one an arc anode, structure defining an ionization chamber dis posed between said are cathode and anode, one of said arc cathode electrodes having a lever arm extending therefrom which is pivotally mounted at a fulcrum supported on said structure to one side of said paths, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said paths to a fixed point on said structure, voltage supply means connected to said electrodes for impressing operating voltages thereon, said conductor being included in said operating voltage connections so that current flow between said are cathode and anode flows therethrough whereby the position of said one of said are cathode electrodes relative to the other of said electrodes is changed in response to the heating produced by said current.
  • An ion source comprising an arc cathode of the bombardment heated type having a plurality of electrodes, an arc anode disposed in spaced-apart relation to said arc cathode, an arc block having an ionization chamber therein disposed between said are cathode and anode, one of said are cathode electrodes having a laterally extending lever arm pivoted at a fulcrum supported on said are block to one side of the path between said are cathode and anode, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said path to a fixed point on said are block, a first source of voltage connected to said are cathode electrodes for impressing operating voltages thereon and for rendering said are cathode electron emissive, a second source of voltage connected between said are cathode and anode for establishing an arc therebetween, said last named connections including said conductor so that
  • An ion generator comprising an ionization chamber, an arc cathode having a plurality of electrodes for supplying a stream of electrons into said ionization chamber, one of said electrodes having an elongated portion extending to a fulcrum disposed to one side of the path between said electrodes and being movable about said fulcrum, a first electrical source connected to said are cathode electrodes for establishing electron flow therebetween, a second electrical source connected by electrical conductors to said are cathode and ionization chamber for establishing an arc discharge therebetween, one of said conductors, being thermally expansible and varying in length with variations of current flowing therethrough, connected to said elongated electrode portion and extending parallel to said path to a fixed point whereby variations in length of said conductor upon heating by said ally extending lever arm pivoted at a fulcrum supported on said structure to one side of the path between said cathodes, a thermally responsive conductor, variable in length upon heating by
  • an ion source comprising an arc block having an arc chamber and an arc slit formed therein, said block also having a magnetic field therethrough, a collimating plate having a predetermined aperture formed therein disposed at one end of said are chamber, an arc cathode of the bombardment heated type having a plurality of electrodes disposed in spaced relation with said are block and overlying said aperture, the paths between said electrodes being parallel to said magnetic field, one of said electrodes having a laterally extending lever arm pivoted at a fulcrum supported on said are block to one side of said paths, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said magnetic field to a fixed point on said are block, a first source of voltage connected to said electrodes for impressing operating voltages thereon and for rendering said are cathode electron emissive, a second source of voltage connected between said are cathode and
  • An ion generator comprising an ionization chamber
  • a filamentary cathode in spaced relation to said ionization chamber, an arc cathode pivotally disposed between said filamentary cathode and said ionization chamber, electrical source means connected to said cathodes for establishing electron flow therebetween, a second electrical source means connected between said are cathode and said ionization chamber for establishing electron flow therebetween, said are cathode being electrically connected to said second source by a thermally responsive conductor for varying the position of said are cathode in response to changes in current flowing through said conductor.

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Description

June 28, 1955 J. SAYERS 2,712,072
CALUTRON ION SOURCE Filed June 30, 1948 2 Sheets-Sheet 1 F/LAMENT SUPPL Y 9 CA THODE SUFFL V INTERMEDIATE 5 ARC 22 UPPLY INVENTOR. JAMES 5A YERS A TTORNEY June 28, SAYERS CALUTRON ION SOURCE 2 Sheets-Sheet 2 Filed June 30, 1948 F/LAMENT SUPPLY GR/D SUPPL Y INTERMEDMTE 04 77/006 SUPPLY APc SUPPLY INVENTOR. JA MES 5A yePs WM/Q 4246,,
A TTORNE v United tates Patent (IALUTRGN ION SOURCE James Sayers, Birmingham, England Application June 30, 1948, Serim No. 36,233
9 Claims. (Cl. 250-413) This invention relates to calutrons and more particularly to an electrode arrangement for automatically regulating the arc current of the ion generator for a calutron. This application is a continuation-in-part of copending application, Serial No. 692,459, filed August 23, 1946, now abandoned.
Calutrons are described in general in Atomic Energy for Military Purposes, by H. D. Smyth, and in great detail in the co-pending application of Ernest 0. Lawrence, Serial No. 557,784, filed October 9, 1944.
Calutrons are principally employed in separating the isotopes of the elements. They are adaptable to the separation of macroscopic amounts of any mixture of iso topes which may be ionized.
in general, an ion source projects ions of a polyisotopic material into a magnetic field. Thereafter, the ions travel in curved paths through the magnetic field, the ions of greater mass describing paths with flatter curves than the ions of lighter mass. Collectors are disposed at suitable points along each path, preferably at the 180 point in the curved travel in order to discharge and collect the ions of the diiierent paths. In this manner the atoms of different mass that were originally in the polyisotopic mixture are distributed in different regions and thereby substantially separated from one another.
The degree of separation of the isotopes which is thus achieved will depend largely upon the stability of the forces acting to produce the aforementioned paths and the accuracy with which the beam is directed upon the collector elements. These forces are the result of the magnetic field and the accelerating potential employed. Various means are employed to regulate the magnetic field and accelerating potential and to keep them relatively constant. It is also highly desirable that a relatively intense, stable beam of positive ions be projected from the ion generator by the accelerating structure through the liner to the collector elements, which operating condition requires that the ion generator presents to the accelerating structure a high density plasma surface which is extremely stable in shape, position, and ion density. In order to obtain such a plasma surface, the rate of ion production by the arc discharge in the ion generator must be substantially constant. This has been accomplished by controlling the heating energy applied to the arc cathode plate inversely as the arc current.
It is therefore an object of this invention to provide a regulator for stabilizing the operation of an ion generator.
Another object of this invention is to provide a regulator for stabilizing the operation of an ion generator of the arc discharge type.
Still another object of this invention is to provide a regulator for an ion generator of the hot cathode are discharge type which has a highly stable rate of ion production.
A further object of this invention is to provide a cathode heated by electron bombardment that is auto- "ice matically regulated so as to be electron emissive to a predetermined value.
The invention, both as to its organization and method of operation together with other objects and advantages thereof, will best be understood by reference to the following specification taken in conjunction with the accompanying drawings, in which:
Figure l is an isometric view of an ion generator comprising an arc block, a movable arc cathode and a filamentary cathode;
Fig. 2 is an isometric view of another embodiment of the invention in which the ion generator comprises an arc block, a fixed arc cathode plate, a movable grid and a filamentary cathode.
Referring particularly to Fig. 1, an ion generator of the arc discharge type is shown. An arc block 1 con-' tains an arc discharge chamber 26 visible through an arc slit 2'7. The are block 1 also contains a charge receptacle (not shown) and a communicating passage between the charge bottle and the arc discharge chamber 26. Mounted on the arc block 1 and centered over the arc chamber 26 is a collimating electrode 2 containing a collimating slot 3. Mounted adjacent to the collimating electrode 2 and in line with the collimating electrode 2 and the arc chamber 26 is a movable arc cathode 4. This movable cathode 4 is supported by a lever arm 13 which is pivotally mounted by a pin 14 on a support bracket 16. A wire 22 has one of its ends attached to a nonconducting support 23, and its other end attached to the outboard end of the lever arm 13. One end of a spring 243 is attached to the same end of the lever arm 13 as is one end of the wire 22. The other end of the spring 20 is attached to the nonconducting support bracket 16. Thus the spring 29 tends to keep the wire 22 taut at all times. A filamentary cathode 8 is mounted adjacent to the arc cathode plate 4.
Suitable supplies of voltage and current are connected to the various units. The are supply 5 has its positive terminal connected through a wire 6 to the arc block 1 and its negative terminal connected through wire 28 to the end of the control wire 22 which is attached to the nonconducting support 23. Thus the total are current of the arc discharge which takes place between the arc cathode plate 4 and a bottom plate 25 of the arc block 1, flows through the control wire 22. An intermediate cathode supply 19 has its positive terminal connected to the arc cathode 4 through a wire 18 and the lever arm 13, and its negative terminal connected through a wire 29 to one terminal of a filament supply 9. This same terminal of the filament supply 9 is connected through a wire 30 to the filamentary cathode 8. The other terminal of the filament supply 9 is connected through a variable resistor 10 to the other end of filamentary cathode 8. By means of the variable resistor 10 the amount of current flowing in the filamentary cathode 8 can be controlled and thus its temperature can be controlled. The operation of the ion generator shown in Fig. l is conducted in a homogeneous magnetic field in which the lines of flux are parallel to the arc slit 27. Conventional heaters (not shown) surround the charge receptacle for heating the arc block. After the arc block and the charge receptacle have been brought up to the correct operating temperature, the material contained in the charge bottle which has been vaporized by this heat is allowed to flow out into the arc chamber. The circuit to the filamentary cathode 8 is then closed, and the current flowing through the filamentary cathode 3 causes heating of the same. The amount of current flowing through the filamentary cathode 8, and, therefore, its temperature, may be controlled by the variable resistor 10. The temperature of the filamentary cathode 8 is adjusted by means of variable resistor so that thermionic emission takes place from said filamentary cathode.
The circuit to the intermediate cathode supply 19 is then closed, The electrons which have been emitted by filamentary cathode 8 are immediately attracted to the arc cathode plate 4. The are cathode plate 4 is heated to a thermionically emissive temperature by electron bombardment from the filamentary cathode 8, and the electrons emitted from the arc cathode plate 4 are accelerated downward into the arc block 1 as soon as the connection to the arc supply 5 is completed. An arc discharge thus takes place between the arc cathode plate 4 and the arc chamber bottom plate 25.
The purpose of the collimating slot 3 in collimating plate 2 is to give the arc discharge within the arc chamber 26 a desired configuration, which is accomplished by forming a slot of requisite cross section in the collimating plate 2 and allowing the arc discharge to pass therethrough.
The are discharge as it passes through the arc chamber 26 ionizes the vapor within said are chamber, producing ions of the material contained within the charge receptacle.
The automatic control features of this ion generator operate in the following manner: Referring again to Fig. 1, it will be seen that the arc current (electron flow) flows from the negative terminal of the arc supply 5 through the connecting wire 28, then through the control wire 22 to the lever arm 13 and thus to the arc cathode 4. The are current then flows in the form of an arc discharge to the bottom plate of the arc chamber 1 and thence through the return wire 6 to the arc supply 5. Thus it is apparent that the total are current flows through the control wire 22. This control wire 22 has been chosen of such diameter that the correct operating arc current will heat the wire 22 to a temperature approaching a dull red heat or a temperature much higher than that of the surrounding apparatus. Under these conditions the temperature of the wire 22, in accordance with the coefficient of expansion thereof, controls its length and is dependent only upon the arc current.
The are current is controlled by the number of thermionic electrons emitted from the arc cathode plate 4, which quantity is determined by the temperature of the arc cathode plate 4, and the temperature is in turn determined by the amount of electron bombardment received from the filamentary cathode 8.
The operating constants are preferably so selected that the current flowing between the filamentary cathode 8 and the arc cathode plate 4 is space-charge limited, and thus the current varies inversely as the distance between the cathodes 8 and 4.
Assuming that the ion generator has been placed in operation as described above, that the operating are current has been set at the desired predetermined value, and that the control wire 22 has been heated to an elevated temperature by the passage of arc current therethrough, then, when the arc current increases, the control wire 22, due to an increase in temperature, elongates and allows the spring 20 to pivot the lever arm 13 about the pin 14. This moves the arc cathode plate 4 farther away from the filamentary cathode 8 and decreases the bombardment intensity of the arc cathode 4 and therefore its temperature decreases accordingly. The decrease in temperature causes the arc cathode 4 to emit fewer electrons, thereby reducing the arc current. In this manner the arc current is automatically decreased if, during operation, it exceeds the original predetermined value. Conversely, if the are current decreases, the control wire 22 cools and in cooling its length becomes less. This decrease in length, acting against spring 20, pivots the lever arm 13 about the pin 14. This action causes the arc cathode plate 4 to move closer to the filamentary cathode 8, which increases the amount of bombardment that the arc cathode plate receives, and in turn raises the temperature of the arc cathode plate 4. This increase in temperature of the arc cathode plate 4 causes emission of a greater number of electrons which in turn increases the arc current. In this manner a mechanism is provided whereby the arc current may be maintained substantially constant.
Referring to Fig. 2, a second embodiment of the invention is shown. In this figure an ion generator is shown which is similar in some respects to that of Fig. 1, but by the addition of a grid as hereinafter described, more precise control of the arc current may be effected.
This second embodiment of the invention as shown in Fig. 2 comprises an arc block 101 which contains an arc discharge chamber 126 visible through an arc slit 127. The arc block 101 also contains a charge receptacle (not shown) and a communicating passageway between the charge bottle and the arc discharge chamber 126. Mounted on the arc block 101 and centered over the arc chamber 121' is a collimating electrode 102 containing a collimating slot 103. Mounted adjacent to the collimating electrode 102 and in line with the collimating electrode 192 and the arc chamber 126 is a fixed arc cathode 104. A movable grid 107 is mounted adjacent to the arc cathode 104. The movable grid 107 is supported by a lever arm 113 which is pivotally mounted by a pin 114 on one arm 116 of a support bracket 117. A wire 122 has one of its ends attached to a nonconducting support 123 and its other end attached to a knife-edge block 121. Also attached to the knife-edge block 121 is one end of a spring the other end of tae spring 120 is attached to the support bracket 117. T he spring 120 is arranged so that it will keep the wire 122 taut at all times.
The knife-edge block 121 operates on the lever arm 113 and rotates this lever arm 113 about the pivot pin 114, thereby moving the grid 167 with respect to the fixed arc cathode plate 104. Situated in line with the collimating slot 103, the fixed arc cathode plate 104, and the grid 107, and also adjacent to the grid 107, is the filamentary cathode 108.
Referring again to Figs. 1 and 2, which show the first and second embodiments of this invention respectively, it is seen that the first embodiment uses a filamentary cathode 3 and a movable are cathode plate 4; the spacing between the filamentary cathode 8 and the movable arc cathode plate 4 is controlled by the thermally responsive wire 22.
In the second embodiment of this invention, as shown in Fig. 2, it is seen that the arc cathode plate 104 is fixed in position relative to the filamentary cathode 108; and interposed between the filamentary cathode 108 and the fixed arc cathode plate 104 is a movable grid 167, whose position relative to the filamentary cathode 108 and the arc cathode plate 104 is determined by a thermally responsive wire 122.
Thus it is seen that in the first embodiment the position of the arc cathode plate 4 is varied with respect to the filamentary cathode 8, and in the second embodiment the position of a movable grid 107 is varied with respect to a filamentary cathode 108 and a fixed arc cathode plate 104.
Consideration will now be given to the theory of operation of the form of the invention shown in Fig. 2. It is well known in the art that a triode comprising a filament, a grid, and an anode, having suitable supplies of voltage and current connected thereto, will allow a definite current flow between the filament and anode; this current being determined by the geometry of the triode. If the voltages applied to the filament, the grid, and the anode of the triode are held constant, then the electron current which is flowing between the filament and the anode can be varied by allowing the grid to move back and forth between the filament and the anode. If the grid is allowed to move away from the anode and toward the filament, it has a greater influence on the electron stream than before and there will be fewer electrons reaching the anode and therefore less current will flow between the filament and anode. Conversely, if the grid moves toward the anode and away from the filament, the grid will have less influence on the electron stream than before and more electrons will reach the anode and therefore more current will flow between the filament and anode.
Returning again to Fig. 2, there is disclosed an ion generator similar in many respects to that disclosed in Fig. l. A movable grid is interposed between filamentary cathode 108 and fixed arc cathode plate 104. This movable grid 107 controls the electron bombardment of arc cathode 104 according to the relative position of the grid with respect to the filamentary cathode 108 and the arc cathode plate 104.
The actual regulating action of the ion generator disclosed in Fig. 2 will now be described. This ion generator is placed in operation in much the same way that the generator shown in Fig. 1 is placed in operation. The connections to the various supplies are completed and the arc block 101 brought up to the correct tenperature; then the arc discharge is started between the arc cathode plate 104 and the bottom plate 125 of the arc block 101. The are current is adjusted until the conditions are optimum for ionization of the vapor released from the charge receptacle.
Referring to Fig. 2, we see that the arc current (electron flow) flows from the negative terminal of the arc supply 105, through the wire 128 to one end of the control wire 122; through the control wire 122 and finally to the arc cathode plate 104 through a short jumper from the control wire 122. The are current then flows as an arc discharge from the arc cathode plate 104 to the bottom plate 125 of arc block 101 and thence returns through the wire 106 to the positive terminal of the arc supply 105. Thus it is apparent from this description that the total are current flows through the control wire 122.
When the arc current increases, the control wire 122 becomes hotter; and hence the control wire 122 increases in length thereby allowing the spring 120, acting through the knife-edge block 121, to rotate the lever arm 113 about pivot 114. This allows the grid 107 to move closer to the filamentary cathode 108 and to move farther away from the arc cathode plate 104. This action causes the arc cathode plate 104 to exert less attractive influence on the electrons which are emitted from the filamentary cathode 108. The decrease in the electron bombardment of the arc cathode plate 104 allows its temperature to decrease accordingly and the arc cathode 104 to emit fewer electrons, thereby reducing the arc current. In this manner the arc current is automatically decreased if, during operation, it exceeds the original predetermined value.
Conversely, if the arc current decreases, the control wire cools and in cooling its length becomes less. This decrease in length, acting in opposition to spring 120, operates on lever arm 113 through knife-edge block 121, and rotates lever arm 113 on pivot 114. As lever arm 113 rotates about pivot 114, it causes grid 107 to move away from filamentary cathode 108 and toward arc cathode plate 104. This action allows the arc cathode plate to exert a greater attractive influence on the electrons which are emitted from the filamentary cathode 108, which in turn increases the amount of bombardment that the arc cathode plate 104 receives, and, therefore, its temperature increases accordingly. This increase in temperature of the arc cathode plate 104 causes emission of a greater number of electrons which in turn increases the arc current.
In this manner a mechanism is provided whereby the are current may be maintained substantially constant.
Although I have described my invention with respect to a particular embodiment thereof, it is not limited to this embodiment nor otherwise except by the terms of the following claims.
What is claimed is:
1. An ion generator comprising an ionization chamber, a filamentary cathode in spaced relation to said ionization chamber, a grid pivotally disposed therebetween, an arc cathode located between said grid and said ionization chamber, electrical source means connected to said cathodes for establishing electron flow therebetween, a second electrical source means connected between said grid and said filamentary cathode for supplying grid bias voltage, and a third electrical source means for establishing electron flow between said are cathode and said ionization chamber, said are cathode being electrically connected to said third source by a thermally responsive conductor having insulated means connected to said grid for varying the position of said grid in response to changes in current flowing through said conductor.
2. In a calutron, an ion generator comprising an arc block having an arc chamber and an arc slit formed therein and a magnetic field parallel to said are slit passing therethrough, said are block containing conventional heaters and a charge receptacle of a material to be ionized, an arc anode plate covering one end of said are chamber, a collimating plate having a predetermined aperture formed therein covering the other end of said are chamber, an arc cathode disposed above said collimating plate and in line with said aperture, said are cathode having at least two electrodes of variable spacing, one of said electrodes being pivotally mounted, a thermally expansible conductor connected to said movable electrode at one end and having its other end attached to an insulating support bracket, tension means for positioning said movable electrode for initially positioning said movable electrode in a predetermined position, a first source of voltage connected to said are cathode electrodes for establishing electron flow therebetween, a second source of voltage connected to said thermally expansible conductor and to said are anode plate for establishing an arc discharge in said arc chamber, said thermally expansible conductor varying in length with the current flowing therethrough, said variations in length serving to vary the spacing of the arc cathode electrodes thereby altering the quantity of electrons emitted by said are cathode so as to maintain the current flowing in said are discharge substantially constant.
3. In an arc discharge device, the combination comprising a plurality of electrodes having the paths therebetween in alignment, at least two of said electrodes serving as an arc cathode and one an arc anode, voltage supply means connected to said electrodes for impressing operating voltages thereon, one of said arc cathode electrodes having a lever arm extended therefrom which is pivotally mounted at a fulcrum disposed to one side of said paths, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said paths to a fixed point, and means for connecting said conductor between said arc anode and said voltage supply means whereby the position of said one of said are cathode electrodes relative to the other of said electrodes is changed in response to the heating produced by said current.
4. An ion source comprising a plurality of electrodes having the paths therebetween in alignment, at least two of said electrodes serving as an arc cathode and one an arc anode, structure defining an ionization chamber dis posed between said are cathode and anode, one of said arc cathode electrodes having a lever arm extending therefrom which is pivotally mounted at a fulcrum supported on said structure to one side of said paths, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said paths to a fixed point on said structure, voltage supply means connected to said electrodes for impressing operating voltages thereon, said conductor being included in said operating voltage connections so that current flow between said are cathode and anode flows therethrough whereby the position of said one of said are cathode electrodes relative to the other of said electrodes is changed in response to the heating produced by said current.
5. An ion source comprising an arc cathode of the bombardment heated type having a plurality of electrodes, an arc anode disposed in spaced-apart relation to said arc cathode, an arc block having an ionization chamber therein disposed between said are cathode and anode, one of said are cathode electrodes having a laterally extending lever arm pivoted at a fulcrum supported on said are block to one side of the path between said are cathode and anode, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said path to a fixed point on said are block, a first source of voltage connected to said are cathode electrodes for impressing operating voltages thereon and for rendering said are cathode electron emissive, a second source of voltage connected between said are cathode and anode for establishing an arc therebetween, said last named connections including said conductor so that the arc current is carried thereby whereby the position of said one of said are cathode electrodes is changed in response to the heating produced in said conductor by said are current.
6. An ion generator comprising an ionization chamber, an arc cathode having a plurality of electrodes for supplying a stream of electrons into said ionization chamber, one of said electrodes having an elongated portion extending to a fulcrum disposed to one side of the path between said electrodes and being movable about said fulcrum, a first electrical source connected to said are cathode electrodes for establishing electron flow therebetween, a second electrical source connected by electrical conductors to said are cathode and ionization chamber for establishing an arc discharge therebetween, one of said conductors, being thermally expansible and varying in length with variations of current flowing therethrough, connected to said elongated electrode portion and extending parallel to said path to a fixed point whereby variations in length of said conductor upon heating by said ally extending lever arm pivoted at a fulcrum supported on said structure to one side of the path between said cathodes, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said path to a fixed point on said structure, and a second voltage source connected between said bombardment cathode and said structure for establishing an arc therebetween through said chamber, said last named connections including said conductor so that the arc current is carried thereby whereby the position of said bombardment cathode is changed in response to the heating .roduced in said conductor by said are current.
8. In a calutron, an ion source comprising an arc block having an arc chamber and an arc slit formed therein, said block also having a magnetic field therethrough, a collimating plate having a predetermined aperture formed therein disposed at one end of said are chamber, an arc cathode of the bombardment heated type having a plurality of electrodes disposed in spaced relation with said are block and overlying said aperture, the paths between said electrodes being parallel to said magnetic field, one of said electrodes having a laterally extending lever arm pivoted at a fulcrum supported on said are block to one side of said paths, a thermally responsive conductor, variable in length upon heating by a current flowing therethrough, connected to said lever arm at one end and extending substantially parallel to said magnetic field to a fixed point on said are block, a first source of voltage connected to said electrodes for impressing operating voltages thereon and for rendering said are cathode electron emissive, a second source of voltage connected between said are cathode and are block for establishing an are through said chamber, said last named connections including said conductor so that the arc current is carried thereby whereby the position of said one of said electrodes is changed in response to the heating produced by said are current.
9. An ion generator comprising an ionization chamber,
' a filamentary cathode in spaced relation to said ionization chamber, an arc cathode pivotally disposed between said filamentary cathode and said ionization chamber, electrical source means connected to said cathodes for establishing electron flow therebetween, a second electrical source means connected between said are cathode and said ionization chamber for establishing electron flow therebetween, said are cathode being electrically connected to said second source by a thermally responsive conductor for varying the position of said are cathode in response to changes in current flowing through said conductor.
References Cited in the file of this patent UNlTED STATES PATENTS 1,610,552 James n Dec. 14, 1926 1,617,065 Lorenz Feb. 8, 1927 1,969,955 Thomas Aug. 14, 1934 2,042,865 Ruttenberg June 2, 1936 2,075,614 Horton Mar. 30, 1937 2,095,579 Werner Oct. 12, 1937 FOREIGN PATENTS 645,466 France June 27, 1928

Claims (1)

1. AN ION GENERATOR COMPRISING AN IONIZATION CHAMBER, A FILAMENTARY CATHODE IN SPACED RELATION TO SAID IONIZATION CHAMBER, A GRID PIVOTALLY DISPOSED THEREBETWEEN, AN ARC CATHODE LOCATED BETWEEN SAID GRID AND SAID IONIZATION CHAMBER, ELECTRICAL SOURCE MEANS CONNECTED TO SAID CATHODES FOR ESTABLISHING ELECTRON FLOW THEREBETWEEN, A SECOND ELECTRICAL SOURCE MEANS CONNECTED BETWEEN SAID GRID AND SAID FILAMENTARY CATHODE FOR SUPPLYING GRID BIAS VOLTAGE, AND THIRD ELECTRICAL SOURCE MEANS FOR ESTABLISHING ELECTRON FLOW BETWEEN SAID ARC CATHODE AND
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Cited By (2)

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US2975277A (en) * 1955-05-10 1961-03-14 Vakutronik Veb Ion source
US20150287582A1 (en) * 2012-11-16 2015-10-08 Thermo Fisher Scientific (Bremen) GmbH a Limited Liability Company (GmbH) Ion Source Assembly for Static Mass Spectrometer

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US1610552A (en) * 1919-12-22 1926-12-14 Westinghouse Electric & Mfg Co Relay
US1617065A (en) * 1923-03-17 1927-02-08 Westinghouse Lamp Co Intermittent glow lamp
FR645466A (en) * 1927-12-09 1928-10-26 Etablissements Ind De E C Gram Self-adjusting rectifier valve
US1969955A (en) * 1929-05-08 1934-08-14 Adolph A Thomas Current controlling apparatus
US2042865A (en) * 1933-05-12 1936-06-02 Ruttenberg Samuel Electrical switch
US2075614A (en) * 1933-05-10 1937-03-30 Trico Products Corp Electric switch
US2095579A (en) * 1934-09-06 1937-10-12 Gen Motors Corp Control system

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Publication number Priority date Publication date Assignee Title
US1610552A (en) * 1919-12-22 1926-12-14 Westinghouse Electric & Mfg Co Relay
US1617065A (en) * 1923-03-17 1927-02-08 Westinghouse Lamp Co Intermittent glow lamp
FR645466A (en) * 1927-12-09 1928-10-26 Etablissements Ind De E C Gram Self-adjusting rectifier valve
US1969955A (en) * 1929-05-08 1934-08-14 Adolph A Thomas Current controlling apparatus
US2075614A (en) * 1933-05-10 1937-03-30 Trico Products Corp Electric switch
US2042865A (en) * 1933-05-12 1936-06-02 Ruttenberg Samuel Electrical switch
US2095579A (en) * 1934-09-06 1937-10-12 Gen Motors Corp Control system

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2975277A (en) * 1955-05-10 1961-03-14 Vakutronik Veb Ion source
US20150287582A1 (en) * 2012-11-16 2015-10-08 Thermo Fisher Scientific (Bremen) GmbH a Limited Liability Company (GmbH) Ion Source Assembly for Static Mass Spectrometer
US9472389B2 (en) * 2012-11-16 2016-10-18 Thermo Fisher Scientific (Bremen) Gmbh Ion source assembly for static mass spectrometer

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