US2338446A - Bubble cap shield - Google Patents

Bubble cap shield Download PDF

Info

Publication number
US2338446A
US2338446A US447949A US44794942A US2338446A US 2338446 A US2338446 A US 2338446A US 447949 A US447949 A US 447949A US 44794942 A US44794942 A US 44794942A US 2338446 A US2338446 A US 2338446A
Authority
US
United States
Prior art keywords
deck
cap
bubble
weir
shield
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US447949A
Inventor
Lambert Pierre
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CB&I Technology Inc
Original Assignee
Lummus Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lummus Co filed Critical Lummus Co
Priority to US447949A priority Critical patent/US2338446A/en
Application granted granted Critical
Publication of US2338446A publication Critical patent/US2338446A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/16Fractionating columns in which vapour bubbles through liquid
    • B01D3/18Fractionating columns in which vapour bubbles through liquid with horizontal bubble plates
    • B01D3/20Bubble caps; Risers for vapour; Discharge pipes for liquid
    • B01D3/205Bubble caps

Definitions

  • This invention relates-to liquid-vapor contact devices and particularly to an improved bubble cap assembly.
  • the liquid contained on each tray is brought into contact with the rising vapors.
  • the effect of such contact is to create a more or less turbulent condition in the liquid and, in many cases, to create a foam which may seriously interfere with satisfactory operation.
  • the foam begins to break as soon as it is formed; but in customary operation the continuous passage of the rising vapors'through" the liquid causes interference with the settling of the foamy liquid which continues until it enters the downpipe. Even if the downpipe is designed fer a low velocity to assist the "freeing of the vapors, it is sometimes found that foam carries over. I have now found that the settling of this foam can be substantially accelerated by eliminating such interference as the foamy liquid approaches the downpipe on each deck, and I have also determined that the velocity of liquid through the downpipe can be increased without adversely affecting the breaking of the foam.
  • the primary object of my invention is to provide means in conjunction with a bubble cap, particularly those caps located near the downpipe on a bubble deck, whereby settling of foamy liquid formed on the deck can be accelerated.
  • a particular object of my invention is to provide a shield for those bubble caps adjacent the downpipe on a bubble deck for the purpose of restricting the discharge of vapors on the side thereof next to the down-pipe whereby interference with the breaking of the foam on the side of such caps facing the downpipe is substantially eliminated.
  • Fig. 1 is a plan view of a bubble deck provided with my improved bubble cap assembly
  • Fig. 2 is a detailed vertical cross-sectional view' of one of my improved bubble caps taken substantially along the line 22 of Fig. 1;
  • Fig. 3 is a perspective view of one of my improved bubble caps; and v Fig. 4 is a detailed elevation view partlyin sectio'n'of a modified form 'of my improved bubble cat
  • reference numeral l0 designates a distillation column or the like provided with a plurality of spaced bubble decks I! to effect a contact between the downflowing liquid and the rising vapors within the column.
  • Each deck is provided with a plurality of bubble caps ll, each of which surmounts a riser It in communication with a suitable aperture in the deck.
  • Each bubble cap is supported on its corresponding riser by means of a supporting member II, which rests on the upper edge of the riser and which may be madeintegral with the cap.
  • Clamping member 20 is provided so that the, bubble cap can be fastened in position as means of stud 2
  • Each deck is also deck.
  • this downpipe comprises an apron down-pipe formed by a portion of the column wall and the apron 26. This apron extends a short distance above the deck as shown to form a weir 26a that maintains the desired depth or liquid on the deck.
  • the bubble caps Ila adjacent the weir 26a are modified so as to allow the foam to begin to break before it passes over the weir into downpipe 24.
  • I provide a baffle or shield 28 that surrounds each cap Mo on the side thereof facing weir 26a.
  • This shield 28 is desirably provided with a flange 29 whereby it can be fastened to deck I! as by means of the stud 30 and the nuts 3!.
  • the construction of this flanged shield is such that the flange is vapor-tight with the deck.
  • bave 28 extends above the slots in the bubble can so that the slots on one side are completely covered, without blocking of! the passage 01 vapors through the remaining slots.
  • FIG. 4 A modified form of construction is shown in Fig. 4, in which the bubble cap 40 is provided with an integral shield member 400 engaging the bubble deck 12 in vapor-tight relation.
  • This form of construction likewise prevents thedisoharge of vapors from the bubble cap on the weir side thereof and, thus, substantially eliminates interference with the settling of the foam in this area of the bubble deck.
  • My invention is also applicable to that type of bubble cap having the slots in its side wall, the bottom edge of which rests on the deck.
  • a separate shield it need only be in vapor-tight relation with the cap wall.
  • the shield is made integral with the cap, the cap wall facing the downpipe weir is imperforate like that in Fig. 4.
  • each cap is determined by the proximity thereof to the downpipe weir. Or-, dinarily. however, approximately one-quarter to one-third of the periphery of each cap adjacent the weir is shielded, The extent of this shielded portion may also be expressed in terms of the subtended chord of the angle thereof on the weir,
  • a device or the type described including a deck supporting a bubble cap and weir, a shield for shielding one side only 01 said bubble cap, and means mounting said shield adjacent said bubble cap on the side thereof towards said weir. said shield extending from the lower edge of the cap to the deck and around the major portion of the side of the cap toward the weir, for the purpose set forth.
  • a partially cylindrical shield adjacent the side of said bubble cap towards said weir and constructed and arranged to prevent direct passage of fluid from beneath the cap to the'weir, for the purpose set forth.
  • a, bubble cap having outlet openings around the side wall thereof, a shield substantially complementary with a portion of said side wall and surrounding a portion only of said bubble cap, and means for mounting said shield adjacent said bubble cap side wall to prevent fluid from escapingbfrom certain portions of said cap while leaving certain of said openings unbaffled.
  • a device of thetype described including a deck, a bubble cap having an annular side wall and outlet means around the lower portion thereof. an arcuate shield closely adjacent said side wall extending upwardly-from said deck for baffling fluid escaping from said outlet means on cne side of said bubble cap.
  • a device for surrounding one side of a bubble cap comprising a base portion adapted for securement to a deck and a semi-cylindrical shield portion extendingeupwardly from said base portion, said shield portion being adapted to lie adjacent the side wall of a bubble cap.
  • a shield extending upwardly from said deck' adjacent the side of said bubble cap towards said weir and extending around the major portion of said side of the cap, the top edge of said shield lying below the top of said weir, the side of said bubble cap away from said weir being unshielded.
  • a device of the type described including a deck, a plurality of bubble caps distributed over said deck, and a weir, individual shield means for the bubble caps relatively near said weir, said shield means being mounted on the sides of their respective bubble caps towards said weir and beingsemi-cylindrical in internal form whereby to surround only aportion of their respective 8.
  • a bubble cap supported over said deck, a downpipe for said deck and a weir extending upwardly from said deck and located between said bubble cap and said downpipe, an imperforate shield for the bubble cap extending laterally around the major portion of the side of the bubble cap directed toward the weir and extending vertically the entire distance between the lower edge of the cap and the deck to prevent direct passage of fluid from beneath the cap to the weir, for the purpose set forth.
  • a device of the Et-YDB described including a deck, a plurality of bubble caps distributed and supported over said deck, a downpipe for the deck and a weir extending upwardly from the deck and located between saidbubble caps and said downpipe, imperforate shields individual to type described, including the bubble caps nearest said weir, each of said shields extending laterally around the major portion of the side oi its respective bubble cap directed toward the weir and extending vertically the entire distance between the lower edge of the cap and the deck to prevent direct passage of fluid irom beneath the cap to the weir, tor the purpose set forth.
  • a device of the type described including a deck, a bubble cap thereon, a downpipe for said deck and a weir extending upwardly from the deck and located between said bubble cap and said downpipe, a shield having a base flange secured to the deck adjacent to said bubble cap and an imperforate shield body extending upwardly from said flange and laterally around the major portion of the side of the cap directed toward said weir and fitting against the lower edge margin of the cap to prevent direct passage of fluid from beneath the cap to the weir. tor the purpose set forth.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

Jan. 4, 1944. P. LAMBERT BUBBLE CAP SHIELD Filed June 22, 1942 Patented Jan. 4, 1944 BUBBLE CAP SHIELD Pierre Lambert, New Rochelle, N. Y., assignor to The Lummus Company, New York, N. I a
corporation of Delaware Application June 22, 1942, Serial No. 447,949
11 Claims. (01. 261-114) This invention relates-to liquid-vapor contact devices and particularly to an improved bubble cap assembly.
In the operation of a distillation column or the like provided with a plurality of bubble decks,'
the liquid contained on each tray is brought into contact with the rising vapors. The effect of such contact is to create a more or less turbulent condition in the liquid and, in many cases, to create a foam which may seriously interfere with satisfactory operation. In order to obtain the desired operating efllciency, it is necessary to effect a settling or breaking of the foam whereby the entrapped vapor bubbles can disengage themselves from the liquid. Since the foam tends to be carried across each deck and down" the corresponding downpipe with the liquid, it is apparent that this foam-breaking must take place substantially completely before the liquid is dis-' charged onto the next lower deck foroptimum performance.
The foam, of course, begins to break as soon as it is formed; but in customary operation the continuous passage of the rising vapors'through" the liquid causes interference with the settling of the foamy liquid which continues until it enters the downpipe. Even if the downpipe is designed fer a low velocity to assist the "freeing of the vapors, it is sometimes found that foam carries over. I have now found that the settling of this foam can be substantially accelerated by eliminating such interference as the foamy liquid approaches the downpipe on each deck, and I have also determined that the velocity of liquid through the downpipe can be increased without adversely affecting the breaking of the foam.
The primary object of my invention is to provide means in conjunction with a bubble cap, particularly those caps located near the downpipe on a bubble deck, whereby settling of foamy liquid formed on the deck can be accelerated.
A particular object of my invention is to provide a shield for those bubble caps adjacent the downpipe on a bubble deck for the purpose of restricting the discharge of vapors on the side thereof next to the down-pipe whereby interference with the breaking of the foam on the side of such caps facing the downpipe is substantially eliminated.
I foaming effect is normally most critical.
Further objects and advantages of my invention will be apparent from the following description of a preferred form of embodiment thereof taken in connection with the. attached drawing provided with a'suitable downpipe 24 for the passage of the downflowing liquid to the next lower illustrative thereof, inwhich: 7
Fig. 1 is a plan view of a bubble deck provided with my improved bubble cap assembly;
Fig. 2 is a detailed vertical cross-sectional view' of one of my improved bubble caps taken substantially along the line 22 of Fig. 1;
Fig. 3 is a perspective view of one of my improved bubble caps; and v Fig. 4 is a detailed elevation view partlyin sectio'n'of a modified form 'of my improved bubble cat In the drawing, reference numeral l0 designates a distillation column or the like provided with a plurality of spaced bubble decks I! to effect a contact between the downflowing liquid and the rising vapors within the column. Each deck is provided with a plurality of bubble caps ll, each of which surmounts a riser It in communication with a suitable aperture in the deck. Each bubble cap is supported on its corresponding riser by means of a supporting member II, which rests on the upper edge of the riser and which may be madeintegral with the cap.
Clamping member 20 is provided so that the, bubble cap can be fastened in position as means of stud 2| and nuts 22. Each deck is also deck. In the form of embodiment shown, this downpipe comprises an apron down-pipe formed by a portion of the column wall and the apron 26. This apron extends a short distance above the deck as shown to form a weir 26a that maintains the desired depth or liquid on the deck.
In accordance with my invention, the bubble caps Ila adjacent the weir 26a are modified so as to allow the foam to begin to break before it passes over the weir into downpipe 24. To accomplish this purpose, I provide a baffle or shield 28 that surrounds each cap Mo on the side thereof facing weir 26a. This shield 28 is desirably provided with a flange 29 whereby it can be fastened to deck I! as by means of the stud 30 and the nuts 3!. The construction of this flanged shield is such that the flange is vapor-tight with the deck.
upper edge of baiile 28 extends above the slots in the bubble can so that the slots on one side are completely covered, without blocking of! the passage 01 vapors through the remaining slots.
With this construction substantially no vapors can issue from the bubble cap on the side thereof facing weir 26a. At the same time, however, the eifectiveness of bubble caps Ila is not greatly diminished since more than one-half of the slot area of each cap is still available to distribute the rising vapors in the liquid on deck i2. Interi'el'ence with the settling or breaking of the foam in the space between bubble caps Ma and weir 26a is thus substantially prevented inasmuch as the rising vapor can not pass through the bubble cap on the weir side thereof. Accordingly, the wall of rising vapors normally adjacent weir 26a, through which the liquid flowing across deck I! to downpipe 24 ordinarily must pass, is there-,
by eliminated.
In this manner,- for a given velocity for the downfiowing liquid, an increased time for set-' tling or breaking got the foam is provided; or, for a column of fixed size, the'velocity of the down-flowing liquid'fparticularly through downpipes 24, can be increased since a preliminary settling or breaking of the foam is accomplished before the foamy liquid enters downpipes 2|.
It will be apparent that my invention is equally applicable to a deck provided with individual circular, rectangular, or the. like downpipes as distinguished from an "apron downpipe. Furthermore, although the use of the shield 28 has been disclosed in connectionwith a circular bubble cap, it will be appreciated that a rectangular, hexagonal, or otherwise shaped bubble cap may also be provided with a shield for the above purpose. It is necessary. however, that the shield be substantially tight against the bubble cap and the bubbl deck on the side of the cap facing the downpipe weir so that passage of vapors through the bubble cap on such side thereof is substantially prevented.
A modified form of construction is shown in Fig. 4, in which the bubble cap 40 is provided with an integral shield member 400 engaging the bubble deck 12 in vapor-tight relation. This form of construction likewise prevents thedisoharge of vapors from the bubble cap on the weir side thereof and, thus, substantially eliminates interference with the settling of the foam in this area of the bubble deck.
My invention is also applicable to that type of bubble cap having the slots in its side wall, the bottom edge of which rests on the deck. In such case, when a separate shield is used, it need only be in vapor-tight relation with the cap wall. Where the shield is made integral with the cap, the cap wall facing the downpipe weir is imperforate like that in Fig. 4.
It will be appreciated that the extent of the shielded portion of each cap is determined by the proximity thereof to the downpipe weir. Or-, dinarily. however, approximately one-quarter to one-third of the periphery of each cap adjacent the weir is shielded, The extent of this shielded portion may also be expressed in terms of the subtended chord of the angle thereof on the weir,
which angle is suificient to prevent vapors from modifications may be made thereto; therefore,
only such limitations as appear in, the claims appended hereinafter should be applied.
' bubble caps.
I claim:
1. In a device or the type described, including a deck supporting a bubble cap and weir, a shield for shielding one side only 01 said bubble cap, and means mounting said shield adjacent said bubble cap on the side thereof towards said weir. said shield extending from the lower edge of the cap to the deck and around the major portion of the side of the cap toward the weir, for the purpose set forth.
2. In a device of the type described, including a deck supporting abubble cap, and a weir, a partially cylindrical shield adjacent the side of said bubble cap towards said weir and constructed and arranged to prevent direct passage of fluid from beneath the cap to the'weir, for the purpose set forth. j I
3. In combination, a, bubble cap having outlet openings around the side wall thereof, a shield substantially complementary with a portion of said side wall and surrounding a portion only of said bubble cap, and means for mounting said shield adjacent said bubble cap side wall to prevent fluid from escapingbfrom certain portions of said cap while leaving certain of said openings unbaffled.
4. In a device of thetype described, including a deck, a bubble cap having an annular side wall and outlet means around the lower portion thereof. an arcuate shield closely adjacent said side wall extending upwardly-from said deck for baffling fluid escaping from said outlet means on cne side of said bubble cap.
5. A device for surrounding one side of a bubble cap, comprising a base portion adapted for securement to a deck and a semi-cylindrical shield portion extendingeupwardly from said base portion, said shield portion being adapted to lie adjacent the side wall of a bubble cap.
6. In a device of the type described, including a deck, a bubble cap, and'a weir extending upwardly from said deck, a shield extending upwardly from said deck' adjacent the side of said bubble cap towards said weir and extending around the major portion of said side of the cap, the top edge of said shield lying below the top of said weir, the side of said bubble cap away from said weir being unshielded.
7. In a device of the type described, including a deck, a plurality of bubble caps distributed over said deck, and a weir, individual shield means for the bubble caps relatively near said weir, said shield means being mounted on the sides of their respective bubble caps towards said weir and beingsemi-cylindrical in internal form whereby to surround only aportion of their respective 8. In a device of the a deck, a bubble cap supported over said deck, a downpipe for said deck and a weir extending upwardly from said deck and located between said bubble cap and said downpipe, an imperforate shield for the bubble cap extending laterally around the major portion of the side of the bubble cap directed toward the weir and extending vertically the entire distance between the lower edge of the cap and the deck to prevent direct passage of fluid from beneath the cap to the weir, for the purpose set forth.
9. In a device of the Et-YDB described, including a deck, a plurality of bubble caps distributed and supported over said deck, a downpipe for the deck and a weir extending upwardly from the deck and located between saidbubble caps and said downpipe, imperforate shields individual to type described, including the bubble caps nearest said weir, each of said shields extending laterally around the major portion of the side oi its respective bubble cap directed toward the weir and extending vertically the entire distance between the lower edge of the cap and the deck to prevent direct passage of fluid irom beneath the cap to the weir, tor the purpose set forth.
10. In a device of the type described, including a deck, a bubble cap thereon, a downpipe for said deck and a weir extending upwardly from the deck and located between said bubble cap and said downpipe, a shield having a base flange secured to the deck adjacent to said bubble cap and an imperforate shield body extending upwardly from said flange and laterally around the major portion of the side of the cap directed toward said weir and fitting against the lower edge margin of the cap to prevent direct passage of fluid from beneath the cap to the weir. tor the purpose set forth.
11. In a device of, the type described and including a deck, a bubble cap thereon, a downpipe for said deck and a weir extending upwardly from the deck and located between said bubble cap and said downpipe, an imperiorate shield integral with said, cap and extending laterally around the major portion or the side of the cap directed toward said weir and extending downwardly from the lower edge of the cap to the deck, to prevent direct passage of fluid from beneath the cap to the weir, -ior the purpose set forth.
/ PIERRE LAMBERT.
US447949A 1942-06-22 1942-06-22 Bubble cap shield Expired - Lifetime US2338446A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US447949A US2338446A (en) 1942-06-22 1942-06-22 Bubble cap shield

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US447949A US2338446A (en) 1942-06-22 1942-06-22 Bubble cap shield

Publications (1)

Publication Number Publication Date
US2338446A true US2338446A (en) 1944-01-04

Family

ID=23778405

Family Applications (1)

Application Number Title Priority Date Filing Date
US447949A Expired - Lifetime US2338446A (en) 1942-06-22 1942-06-22 Bubble cap shield

Country Status (1)

Country Link
US (1) US2338446A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2568749A (en) * 1941-12-16 1951-09-25 Kittel Walter Contact plate construction
US2693949A (en) * 1950-10-19 1954-11-09 Koch Eng Co Inc Apparatus for contacting gases and liquids
US2786082A (en) * 1951-03-20 1957-03-19 Koppers Co Inc Dephenolization process and apparatus
US3040439A (en) * 1959-07-21 1962-06-26 Gen Am Transport Solids fluidizing vessel and gas diffuser plate and nozzle elements therefor
US4207276A (en) * 1977-10-14 1980-06-10 Oy Alko Ab Easily maintained bubble-cap column for the distillation of clogging and high-sediment liquids
US5006283A (en) * 1988-10-06 1991-04-09 General Signal Corporation Mixing system for dispersing a compressible fluid such as gas into liquid in a vessel

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2568749A (en) * 1941-12-16 1951-09-25 Kittel Walter Contact plate construction
US2693949A (en) * 1950-10-19 1954-11-09 Koch Eng Co Inc Apparatus for contacting gases and liquids
US2786082A (en) * 1951-03-20 1957-03-19 Koppers Co Inc Dephenolization process and apparatus
US3040439A (en) * 1959-07-21 1962-06-26 Gen Am Transport Solids fluidizing vessel and gas diffuser plate and nozzle elements therefor
US4207276A (en) * 1977-10-14 1980-06-10 Oy Alko Ab Easily maintained bubble-cap column for the distillation of clogging and high-sediment liquids
US5006283A (en) * 1988-10-06 1991-04-09 General Signal Corporation Mixing system for dispersing a compressible fluid such as gas into liquid in a vessel

Similar Documents

Publication Publication Date Title
US1741519A (en) Dephlegmator or fractionating column
US5454989A (en) Vapor-liquid contact apparatus
US4472325A (en) Liquid distributor apparatus for a vapor-liquid contact column
US4133645A (en) Vapor/liquid distributor for fixed-bed catalytic reaction chambers
US2523126A (en) Apparatus for countercurrent contact of fluid materials
CN107820443B (en) Contact valve tray for mass transfer column
US3997633A (en) Contact towers with leak-proof support of improved plate subassembly
US5895608A (en) Downcomer for chemical process tower and method of forming the same
US3259380A (en) Total redistributor
US2338446A (en) Bubble cap shield
US4235847A (en) Vapor/liquid distributor for fixed-bed catalytic reaction chambers
US2055048A (en) Entrainment separator for fractionating towers
US2428922A (en) Liquid distributing apparatus
US2222565A (en) Contact device
US2982527A (en) Gas-liquid contact apparatus
US3864439A (en) Gas-liquid contacting apparatus
US2510590A (en) Liquid-contact device
US2819049A (en) Bubble cap towers
US2772081A (en) Vapor-liquid contacting apparatus
US3025041A (en) Vapor liquid contacting devices
US1862758A (en) Art of rectification
US1858158A (en) Gas and liquid contact apparatus
US2582688A (en) Contacting tower construction
US2507325A (en) Bubble tower construction and method of fractionating vapors
US2385355A (en) Downspout for bubble trays