US20030201053A1 - Method and apparatus for welding polymer fabrics - Google Patents
Method and apparatus for welding polymer fabrics Download PDFInfo
- Publication number
- US20030201053A1 US20030201053A1 US10/403,085 US40308503A US2003201053A1 US 20030201053 A1 US20030201053 A1 US 20030201053A1 US 40308503 A US40308503 A US 40308503A US 2003201053 A1 US2003201053 A1 US 2003201053A1
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- Prior art keywords
- horns
- vibratable
- welding
- horn
- vibrated
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/80—General aspects of machine operations or constructions and parts thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/08—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using ultrasonic vibrations
- B29C65/081—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using ultrasonic vibrations having a component of vibration not perpendicular to the welding surface
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/08—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using ultrasonic vibrations
- B29C65/081—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using ultrasonic vibrations having a component of vibration not perpendicular to the welding surface
- B29C65/082—Angular, i.e. torsional ultrasonic welding
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/08—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using ultrasonic vibrations
- B29C65/088—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using ultrasonic vibrations using several cooperating sonotrodes, i.e. interacting with each other, e.g. for realising the same joint
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/003—Protecting areas of the parts to be joined from overheating
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/01—General aspects dealing with the joint area or with the area to be joined
- B29C66/05—Particular design of joint configurations
- B29C66/10—Particular design of joint configurations particular design of the joint cross-sections
- B29C66/11—Joint cross-sections comprising a single joint-segment, i.e. one of the parts to be joined comprising a single joint-segment in the joint cross-section
- B29C66/112—Single lapped joints
- B29C66/1122—Single lap to lap joints, i.e. overlap joints
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/01—General aspects dealing with the joint area or with the area to be joined
- B29C66/349—Cooling the welding zone on the welding spot
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/40—General aspects of joining substantially flat articles, e.g. plates, sheets or web-like materials; Making flat seams in tubular or hollow articles; Joining single elements to substantially flat surfaces
- B29C66/41—Joining substantially flat articles ; Making flat seams in tubular or hollow articles
- B29C66/43—Joining a relatively small portion of the surface of said articles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/72—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the structure of the material of the parts to be joined
- B29C66/729—Textile or other fibrous material made from plastics
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/73—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset
- B29C66/739—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset
- B29C66/7392—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of at least one of the parts being a thermoplastic
- B29C66/73921—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of at least one of the parts being a thermoplastic characterised by the materials of both parts being thermoplastics
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/80—General aspects of machine operations or constructions and parts thereof
- B29C66/81—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps
- B29C66/814—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps
- B29C66/8141—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps characterised by the surface geometry of the part of the pressing elements, e.g. welding jaws or clamps, coming into contact with the parts to be joined
- B29C66/81411—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps characterised by the surface geometry of the part of the pressing elements, e.g. welding jaws or clamps, coming into contact with the parts to be joined characterised by its cross-section, e.g. transversal or longitudinal, being non-flat
- B29C66/81415—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps characterised by the surface geometry of the part of the pressing elements, e.g. welding jaws or clamps, coming into contact with the parts to be joined characterised by its cross-section, e.g. transversal or longitudinal, being non-flat being bevelled
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/80—General aspects of machine operations or constructions and parts thereof
- B29C66/81—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps
- B29C66/814—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps
- B29C66/8141—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps characterised by the surface geometry of the part of the pressing elements, e.g. welding jaws or clamps, coming into contact with the parts to be joined
- B29C66/81411—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps characterised by the surface geometry of the part of the pressing elements, e.g. welding jaws or clamps, coming into contact with the parts to be joined characterised by its cross-section, e.g. transversal or longitudinal, being non-flat
- B29C66/81421—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps characterised by the surface geometry of the part of the pressing elements, e.g. welding jaws or clamps, coming into contact with the parts to be joined characterised by its cross-section, e.g. transversal or longitudinal, being non-flat being convex or concave
- B29C66/81422—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the design of the pressing elements, e.g. of the welding jaws or clamps characterised by the surface geometry of the part of the pressing elements, e.g. welding jaws or clamps, coming into contact with the parts to be joined characterised by its cross-section, e.g. transversal or longitudinal, being non-flat being convex or concave being convex
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/80—General aspects of machine operations or constructions and parts thereof
- B29C66/81—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps
- B29C66/818—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the cooling constructional aspects, or by the thermal or electrical insulating or conducting constructional aspects of the welding jaws or of the clamps ; comprising means for compensating for the thermal expansion of the welding jaws or of the clamps
- B29C66/8181—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the cooling constructional aspects, or by the thermal or electrical insulating or conducting constructional aspects of the welding jaws or of the clamps ; comprising means for compensating for the thermal expansion of the welding jaws or of the clamps characterised by the cooling constructional aspects
- B29C66/81811—General aspects of the pressing elements, i.e. the elements applying pressure on the parts to be joined in the area to be joined, e.g. the welding jaws or clamps characterised by the cooling constructional aspects, or by the thermal or electrical insulating or conducting constructional aspects of the welding jaws or of the clamps ; comprising means for compensating for the thermal expansion of the welding jaws or of the clamps characterised by the cooling constructional aspects of the welding jaws
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/80—General aspects of machine operations or constructions and parts thereof
- B29C66/83—General aspects of machine operations or constructions and parts thereof characterised by the movement of the joining or pressing tools
- B29C66/832—Reciprocating joining or pressing tools
- B29C66/8322—Joining or pressing tools reciprocating along one axis
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/80—General aspects of machine operations or constructions and parts thereof
- B29C66/83—General aspects of machine operations or constructions and parts thereof characterised by the movement of the joining or pressing tools
- B29C66/832—Reciprocating joining or pressing tools
- B29C66/8322—Joining or pressing tools reciprocating along one axis
- B29C66/83221—Joining or pressing tools reciprocating along one axis cooperating reciprocating tools, each tool reciprocating along one axis
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/93—Measuring or controlling the joining process by measuring or controlling the speed
- B29C66/934—Measuring or controlling the joining process by measuring or controlling the speed by controlling or regulating the speed
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/93—Measuring or controlling the joining process by measuring or controlling the speed
- B29C66/939—Measuring or controlling the joining process by measuring or controlling the speed characterised by specific speed values or ranges
- B29C66/9392—Measuring or controlling the joining process by measuring or controlling the speed characterised by specific speed values or ranges in explicit relation to another variable, e.g. speed diagrams
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/95—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94
- B29C66/951—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/95—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94
- B29C66/951—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools
- B29C66/9512—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools by controlling their vibration frequency
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/95—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94
- B29C66/951—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools
- B29C66/9516—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools by controlling their vibration amplitude
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/80—General aspects of machine operations or constructions and parts thereof
- B29C66/83—General aspects of machine operations or constructions and parts thereof characterised by the movement of the joining or pressing tools
- B29C66/836—Moving relative to and tangentially to the parts to be joined, e.g. transversely to the displacement of the parts to be joined, e.g. using a X-Y table
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/95—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94
- B29C66/951—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools
- B29C66/9513—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools characterised by specific vibration frequency values or ranges
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/95—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94
- B29C66/951—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools
- B29C66/9517—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 by measuring or controlling the vibration frequency and/or the vibration amplitude of vibrating joining tools, e.g. of ultrasonic welding tools characterised by specific vibration amplitude values or ranges
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/90—Measuring or controlling the joining process
- B29C66/95—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94
- B29C66/959—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 characterised by specific values or ranges of said specific variables
- B29C66/9592—Measuring or controlling the joining process by measuring or controlling specific variables not covered by groups B29C66/91 - B29C66/94 characterised by specific values or ranges of said specific variables in explicit relation to another variable, e.g. X-Y diagrams
Definitions
- the present invention relates to a method and apparatus for welding polymer fabrics using ultrasound. More particularly, but not exclusively, it relates to a method and apparatus for welding polymer fabrics or the like comprising a pair of ultrasonically vibrated horns acting on layers of fabrics to be welded.
- Preferred polymer fabrics to be welded by the method and apparatus of this invention are those containing nylon and polyethylene, although other materials may also be welded.
- an apparatus for welding ultrasonically two or more layers of fabric comprising two opposed ultrasonically vibratable horns so spaced one from another that the layers of fabric may be passed between them.
- At least one, optionally each, of the two horns is vibratable in axial mode.
- both horns are vibratable in axial mode
- the frequencies at which the horns are adapted to vibrate may be so varied that one is vibratable at a frequency plus or minus between 1 and 20%, preferably in the region of 10%, of the frequency of the other.
- an axially vibratable horn may have an angled end face, and a second axially vibratable horn may vibrate in a direction substantially perpendicular to said end face.
- the welding apparatus described above may further include a source of air directable generally toward a zone in which welding takes place.
- the source of air may be a passageway extending substantially longitudinally of at least one of the welding horns to exit substantially centrally of the welding zone.
- the source of air or other cooling fluid may be a passageway longitudinal of one or both welding horns, the or each said passageway difurcating to permit exit of air through a plurality of annularly spaced outlets.
- an opposed co-operating horn is vibratable in a torsional mode.
- a method of welding ultrasonically two or more layers of fabric comprising the steps of providing two opposed ultrasonically vibratable horns spaced one from another, and passing the layers of fabric between them whilst vibrating ultrasonically the horns.
- At least one, optionally each, of the two horns is vibrated in axial mode.
- the horns may be so vibrated that one vibrates at a frequency plus or minus between 1 and 20%, preferably in the region of 10%, of the frequency of the other.
- one horn is vibrated in an axial mode whilst an opposed co-operating horn is vibrated in a torsional mode.
- the method described above further includes the step of directing air or other cooling fluid toward a zone in which welding takes place.
- FIG. 1 shows a pair of axial mode vibratable horns in longitudinally opposed relationship and, graphically, the effect of phase control thereon;
- FIG. 2 shows welding by one axial mode horn opposed by a torsional mode horn
- FIG. 3 shows welding by an axial mode vibratable horn having an angled face and a second horn vibratable in a direction perpendicular to said angled face;
- FIG. 3A is an end view of the horn of FIG. 3;
- FIG. 4 shows an opposed pair of longitudinally vibratable horns, each having a central passage for introduction of cooling air
- FIG. 5 shows an opposed pair of vibratable horns, each having a central passage for introduction of cooling air which passage splits into a plurality of annularly spaced outlets;
- FIG. 6 is a graph of breaking strength against weld speed, under various welding conditions.
- FIG. 1 this illustrates the effect on energy absorption of phase shift between two longitudinally opposed horns 1 and 1 a, each in axial vibrational mode.
- This principle utilises two systems each operating in the longitudinal mode. However, if the horn is excited longitudinally and the anvil is excited in a transverse or orbital mode the resultant weld characteristic will be quite different. Relative oscillatory movement between adjacent fibres will produce very local heating and by defining carefully the contact pressure and energy input, local fusion can be produced in a controlled way.
- FIG. 2 shows an axial mode horn 1 with counterposed torsional mode horn 2 .
- the fabric layers 3 are transported through a gap between the horns 1 and 2 in the direction indicated by arrow 4 .
- FIG. 3 illustrates two opposed horns with the fabric layers passing through them at an angle.
- one of the horns 7 is vibratable in an axial mode and has an angled end face 8 whilst the other horn 6 is vibratable in an axial mode perpendicular to the plane of the end face 8 of the first horn 7 .
- the offset angle between them causes localised heating and some rearrangement of the fibres of the fabrics passing between them, thereby welding the fabrics together.
- FIGS. 4 and 5 There is shown in FIGS. 4 and 5 an air cooled welding system in which air is introduced through vibratable horns 9 .
- the air passes along tube 10 arranged axially to the horn or horns 9 to be discharged centrally of the welding zone ⁇ .
- the passages 10 each split into a plurality of passages, which exit through a corresponding plurality of holes 15 arranged annularly to surround the centre of the welding zone ⁇ .
- FIG. 6 is a graph of breaking strength versus weld speed for different horn characteristics. High gain horns with air cooling produce good weld strength with low speed sensitivity. The results without air suggest that careful balance of the energy input per unit volume of material (a function of speed) with the cooling effect of injected air, could lead to optimised weld quality. The objective of high speed welding with consistent high strength could be achieved with a relatively simple mechanical system.
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Textile Engineering (AREA)
- Lining Or Joining Of Plastics Or The Like (AREA)
- Treatment Of Fiber Materials (AREA)
Abstract
The apparatus is adapted to weld ultrasonically two or more layers of fabric 14. The fabrics 14 may be a woven or non-woven fabric of nylon, polyethylene or other polymeric material. It comprises two opposed ultrasonically vibratable horns (1, 1 a) so spaced one from another that the layers of fabric (3) may be passed between them. At least one, optionally both, of the two horns (1, 1 a) is vibratable in axial mode.
Description
- The present invention relates to a method and apparatus for welding polymer fabrics using ultrasound. More particularly, but not exclusively, it relates to a method and apparatus for welding polymer fabrics or the like comprising a pair of ultrasonically vibrated horns acting on layers of fabrics to be welded.
- It is well known that certain polymers absorb ultrasound readily and by virtue of that property, offer scope for fusion bonding and other joining techniques. These phenomena have established a general application in the welding of engineering plastics, covering a wide range of techniques and encompassing products in many different markets. Of equal interest but less widely practised is the application of ultrasound to welding of woven or non-woven polymer fabrics. Considerable effort has been expended in developing ultrasound processing equipment for the manufacture of high strength non-woven or reinforced fabrics and specialised elasticated products.
- One method of undertaking ultrasonic welding is disclosed by the present applicant in an earlier patent number GB 2299538 B, but other similar procedures are also known from U.S. Pat. No. 835,068, WO 94/11189, U.S. Pat. No. 249,416, U.S. Pat. No. 4,400,227, GB 8805949, U.S. Pat. No. 4,305,988, FR 2255023 and WO 95/09593.
- However, not all the methods disclosed are entirely satisfactory and it is therefore an object of the present invention to provide a method and apparatus for welding polymer fabrics using ultrasound, which method is both effective, quick and is able to deal with different materials and different thicknesses of material.
- Preferred polymer fabrics to be welded by the method and apparatus of this invention are those containing nylon and polyethylene, although other materials may also be welded.
- According to a first aspect of the present invention, there is provided an apparatus for welding ultrasonically two or more layers of fabric comprising two opposed ultrasonically vibratable horns so spaced one from another that the layers of fabric may be passed between them.
- Preferably at least one, optionally each, of the two horns is vibratable in axial mode.
- Where both horns are vibratable in axial mode, the relative phase between the vibrations of the horns may be varied, whereby for constant amplitude vibrations the energy imparted may vary between a minimum at phase difference Ø=0° and a maximum at phase difference Ø=180°.
- Alternatively the frequencies at which the horns are adapted to vibrate may be so varied that one is vibratable at a frequency plus or minus between 1 and 20%, preferably in the region of 10%, of the frequency of the other.
- In another embodiment, an axially vibratable horn may have an angled end face, and a second axially vibratable horn may vibrate in a direction substantially perpendicular to said end face.
- The welding apparatus described above may further include a source of air directable generally toward a zone in which welding takes place.
- The source of air may be a passageway extending substantially longitudinally of at least one of the welding horns to exit substantially centrally of the welding zone.
- Alternatively the source of air or other cooling fluid may be a passageway longitudinal of one or both welding horns, the or each said passageway difurcating to permit exit of air through a plurality of annularly spaced outlets.
- In another embodiment where one horn is vibratable in an axial mode, an opposed co-operating horn is vibratable in a torsional mode.
- According to a second aspect of the present invention, there is provided a method of welding ultrasonically two or more layers of fabric comprising the steps of providing two opposed ultrasonically vibratable horns spaced one from another, and passing the layers of fabric between them whilst vibrating ultrasonically the horns.
- Preferably at least one, optionally each, of the two horns is vibrated in axial mode.
- Where both horns are vibrated in axial mode, the horns may be vibrated with a relative phase difference between them, said phase shift being variable between Ø=0° for minimum energy and Ø=180° for maximum energy.
- Alternatively the horns may be so vibrated that one vibrates at a frequency plus or minus between 1 and 20%, preferably in the region of 10%, of the frequency of the other.
- In another embodiment, one horn is vibrated in an axial mode whilst an opposed co-operating horn is vibrated in a torsional mode.
- The method described above further includes the step of directing air or other cooling fluid toward a zone in which welding takes place.
- Embodiments of the present invention will now be more particularly described by way of example and with reference to the accompanying drawings, in which:
- FIG. 1 shows a pair of axial mode vibratable horns in longitudinally opposed relationship and, graphically, the effect of phase control thereon;
- FIG. 2 shows welding by one axial mode horn opposed by a torsional mode horn;
- FIG. 3 shows welding by an axial mode vibratable horn having an angled face and a second horn vibratable in a direction perpendicular to said angled face;
- FIG. 3A is an end view of the horn of FIG. 3;
- FIG. 4 shows an opposed pair of longitudinally vibratable horns, each having a central passage for introduction of cooling air;
- FIG. 5 shows an opposed pair of vibratable horns, each having a central passage for introduction of cooling air which passage splits into a plurality of annularly spaced outlets; and
- FIG. 6 is a graph of breaking strength against weld speed, under various welding conditions.
- Since the mechanism of fabric welding is dependent on generating heat in the workpiece, the oscillatory process should be designed to optimise this effect. The ideal process would result in adjacent fibres being fused locally rather than in bulk. This would form a union which was flexible and retained the “feel” of fabric, rather than giving a solid fused mass of amorphous material. Control of the welding process is conventionally effected by varying the ultrasonic power cycle and the force applied between the welding tool and supporting anvil placed beneath the workpiece. With fabrics having relatively fine fibres it would be a great advantage to have additional parameters allowing more delicate control of the fusion process.
- One technique which would encourage this objective requires both a horn and an anvil horn to be vibrated but at different frequencies. One, say the anvil frequency, is deliberately moved to be approximately 300 Hz higher or lower than the frequency of the other. As a result, phase shifted opposed vibrations of ultrasonic energy would be applied at a frequency represented by the difference between the two systems, (namely one at 28 kHz, and the other at say 28.3 kHz or 27.7 kHz). This beating effect would greatly reduce the energy for a given amplitude of, say c. 80 μm, to about 100 Watts for each transducer, and permit hand controlled welding of small delicate materials which necessarily involves slower relative translational movement of fabric and tools.
- Referring now to FIG. 1, this illustrates the effect on energy absorption of phase shift between two longitudinally opposed
horns - The application of vibrations simultaneously via both an anvil horn and a welding horn with phase shift between the two energised systems has the effect of varying the energy absorption from a minimum, probably zero, at 0° phase angle to a maximum at 180°.
- This principle utilises two systems each operating in the longitudinal mode. However, if the horn is excited longitudinally and the anvil is excited in a transverse or orbital mode the resultant weld characteristic will be quite different. Relative oscillatory movement between adjacent fibres will produce very local heating and by defining carefully the contact pressure and energy input, local fusion can be produced in a controlled way.
- This effect can be seen in FIG. 2 which shows an
axial mode horn 1 with counterposedtorsional mode horn 2. Thefabric layers 3 are transported through a gap between thehorns arrow 4. - The effect of the torsional mode excitation at
annular surface 5 rotates the fibres of the fabric whilst they are simultaneously being compressed by the axial displacement ofhorn 1 under direct pressure P. This oscillatory motion, if sufficiently energetic, creates friction heating between fibres, sufficient to induce fusing without the need to compress fully the fabric layers. - FIG. 3 illustrates two opposed horns with the fabric layers passing through them at an angle. In this case, one of the
horns 7 is vibratable in an axial mode and has anangled end face 8 whilst the other horn 6 is vibratable in an axial mode perpendicular to the plane of theend face 8 of thefirst horn 7. Given the directions of vibrations of the horns, the offset angle between them causes localised heating and some rearrangement of the fibres of the fabrics passing between them, thereby welding the fabrics together. - There is shown in FIGS. 4 and 5 an air cooled welding system in which air is introduced through
vibratable horns 9. In FIG. 4, the air passes alongtube 10 arranged axially to the horn orhorns 9 to be discharged centrally of the welding zone α. In FIG. 5, thepassages 10 each split into a plurality of passages, which exit through a corresponding plurality ofholes 15 arranged annularly to surround the centre of the welding zone α. - In both FIGS. 4 and 5, the passage of the materials to be welded is shown as16. In both cases, alternative forms of introduction of cooling fluid are possible.
- FIG. 6 is a graph of breaking strength versus weld speed for different horn characteristics. High gain horns with air cooling produce good weld strength with low speed sensitivity. The results without air suggest that careful balance of the energy input per unit volume of material (a function of speed) with the cooling effect of injected air, could lead to optimised weld quality. The objective of high speed welding with consistent high strength could be achieved with a relatively simple mechanical system.
Claims (19)
1. An apparatus for welding ultrasonically two or more layers of fabric comprising two opposed ultrasonically vibratable horns so spaced one from another that the layers of fabric may be passed between them.
2. An apparatus as claimed in claim 1 , wherein at least one of the two horns is vibratable in axial mode.
3. An apparatus as claimed in claim 2 , wherein both horns are vibratable in axial mode.
4. An apparatus as claimed in claim 3 , wherein the relative phase between the vibrations of the horns is so variable that, for constant amplitude vibrations, the energy to be imparted varies between a minimum at phase difference Ø=0° and a maximum at phase difference Ø=180°.
5. An apparatus as claimed in claim 3 , wherein the frequencies at which the horns are adapted to vibrate are so variable that one is vibratable at a frequency plus or minus between 1 and 20% of the frequency of the other.
6. An apparatus as claimed in claim 5 , wherein one horn is adapted to vibrate at a frequency plus or minus 10% of the frequency of the other.
7. An apparatus as claimed in any one of claims 2 to 6 , wherein one axially vibratable horn has an end face angled with respect to the vibrational axis, and the second axially vibratable horn is vibratable in a direction substantially perpendicular to said end face.
8. An apparatus as claimed in claim 2 , wherein one horn is vibratable in an axial mode and an opposed co-operating horn is vibratable in a torsional mode.
9. An apparatus as claimed in any one of the preceding claims, further comprising a source of air or other cooling fluid directed generally toward a zone in which welding takes place.
10. An apparatus as claimed in claim 9 , wherein the source of air or other cooling fluid comprises a passageway extending substantially longitudinally of at least one of the welding horns to exit centrally of the welding zone.
11. An apparatus as claimed in claim 9 , wherein the source of air or other cooling fluid comprises a passageway extending longitudinally of at least one of the welding horns, at least one of the or each said passageway difurcating to permit exit of air or cooling fluid through a plurality of annularly spaced outlets.
12. A method of welding ultrasonically two or more layers of fabric comprising the steps of providing two opposed ultrasonically vibratable horns spaced one from another, and passing the layers of fabric between them whilst vibrating ultrasonically the horns.
13. A method as claimed in claim 12 , wherein at least one of the two horns is vibrated in axial mode.
14. A method as claimed in claim 13 , wherein both of the horns are vibrated in axial mode.
15. A method as claimed in claim 14 , wherein the horns are vibrated with a relative phase difference between them, said phase shift being variable between Ø=0° for minimum energy and Ø=180° for maximum energy.
16. A method as claimed in claim 14 wherein the horns are so vibrated that one vibrates at a frequency plus or minus between 1 and 20% of the frequency of the other.
17. A method as claimed in claim 16 , wherein the horns are so vibrated that one vibrates at a frequency plus or minus 10% of the frequency of the other.
18. A method as claimed in claim 13 , wherein one horn is vibrated in an axial mode whilst an opposed co-operating horn is vibrated in a torsional mode.
19. A method as claimed in any one of claims 12 to 18 , further comprising the step of directing air or other cooling fluid toward a zone in which welding takes place.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/403,085 US20030201053A1 (en) | 1998-01-30 | 2003-04-01 | Method and apparatus for welding polymer fabrics |
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GB9801983.9 | 1998-01-30 | ||
GB9801983A GB9801983D0 (en) | 1998-01-30 | 1998-01-30 | Welding polymer fabrics using ultrasound |
US09/600,154 US6547904B1 (en) | 1998-01-30 | 1999-01-29 | Method and apparatus for welding polymer fabrics |
US10/403,085 US20030201053A1 (en) | 1998-01-30 | 2003-04-01 | Method and apparatus for welding polymer fabrics |
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PCT/GB1999/000122 Continuation WO1999038667A2 (en) | 1998-01-30 | 1999-01-29 | Method and apparatus for welding polymer fabrics |
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CN (1) | CN1291936A (en) |
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US20100024956A1 (en) * | 2006-04-26 | 2010-02-04 | Ulrich Vogler | Device for processing workpieces using ultrasound and method for operating that device |
US20100320257A1 (en) * | 2009-06-18 | 2010-12-23 | Telsonic Holding Ag | Ultrasonic welding device and method for welding two components together |
US20100326586A1 (en) * | 2009-06-30 | 2010-12-30 | Telsonic Holding Ag | Device, Use of the Device and Method for Torsional Ultrasonic Welding |
US20130299558A1 (en) * | 2010-11-25 | 2013-11-14 | Telsonic Holding Ag | Device for Torsionally Welding Metal Parts By Means Of Ultrasound |
US8974478B2 (en) | 2011-09-20 | 2015-03-10 | Covidien Lp | Ultrasonic surgical system having a fluid cooled blade and related cooling methods therefor |
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GB9801983D0 (en) * | 1998-01-30 | 1998-03-25 | Young Michael J R | Welding polymer fabrics using ultrasound |
GB0030733D0 (en) * | 2000-12-16 | 2001-01-31 | Don & Low Nonwovens Ltd | Sheeting |
US7220331B2 (en) * | 2001-11-20 | 2007-05-22 | Josef Gmeiner | Device for connecting a multilayered web by ultrasound |
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US20050223615A1 (en) * | 2004-04-09 | 2005-10-13 | Fencel Jeffery J | Wind activated decoy |
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EP2133191A4 (en) * | 2007-03-02 | 2013-05-15 | Compania Espanola De Ultrasonidos Sa | Ultrasonic head and transducer for ultrasonic soldering of plastics |
US7897018B2 (en) * | 2007-09-05 | 2011-03-01 | Albany International Corp. | Process for producing papermaker's and industrial fabrics |
US8088256B2 (en) * | 2007-09-05 | 2012-01-03 | Albany International Corp. | Process for producing papermaker's and industrial fabric seam and seam produced by that method |
US7794555B2 (en) * | 2007-09-05 | 2010-09-14 | Albany International Corp. | Formation of a fabric seam by ultrasonic gap welding of a flat woven fabric |
MX2010002549A (en) | 2007-09-05 | 2010-05-20 | Albany Int Corp | Process for producing papermaker's and industrial fabric seam and seam produced by that method. |
JP5899938B2 (en) * | 2012-01-12 | 2016-04-06 | 日産自動車株式会社 | Secondary battery manufacturing method, secondary battery |
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US20100024956A1 (en) * | 2006-04-26 | 2010-02-04 | Ulrich Vogler | Device for processing workpieces using ultrasound and method for operating that device |
US20130213198A1 (en) * | 2006-04-26 | 2013-08-22 | Herrmann Ultraschalltechnik Gmbh & Co. Kg | Device for processing workpieces using ultrasound and method for operating that device |
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US8974478B2 (en) | 2011-09-20 | 2015-03-10 | Covidien Lp | Ultrasonic surgical system having a fluid cooled blade and related cooling methods therefor |
US9987034B2 (en) | 2011-09-20 | 2018-06-05 | Covidien Lp | Ultrasonic surgical system having a fluid cooled blade and related cooling methods therefor |
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JP2020114593A (en) * | 2019-01-17 | 2020-07-30 | 株式会社ダイヘン | Joint device |
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WO2020239341A1 (en) * | 2019-05-29 | 2020-12-03 | Airbus Operations Gmbh | System and method for welding two thermoplastic workpieces |
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DE69904700T2 (en) | 2003-10-16 |
EP1058615A2 (en) | 2000-12-13 |
DE69904700D1 (en) | 2003-02-06 |
ATE230341T1 (en) | 2003-01-15 |
WO1999038667A2 (en) | 1999-08-05 |
US6547904B1 (en) | 2003-04-15 |
GB2351697A (en) | 2001-01-10 |
EP1058615B1 (en) | 2003-01-02 |
WO1999038667A3 (en) | 1999-11-25 |
GB0018195D0 (en) | 2000-09-13 |
CN1291936A (en) | 2001-04-18 |
AU2067099A (en) | 1999-08-16 |
GB9801983D0 (en) | 1998-03-25 |
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