UA73996C2 - A process for the production of urea (variants), a mechanism for the production of urea and method for modernization of the mechanism for the production of urea - Google Patents
A process for the production of urea (variants), a mechanism for the production of urea and method for modernization of the mechanism for the production of urea Download PDFInfo
- Publication number
- UA73996C2 UA73996C2 UA2003010386A UA2003010386A UA73996C2 UA 73996 C2 UA73996 C2 UA 73996C2 UA 2003010386 A UA2003010386 A UA 2003010386A UA 2003010386 A UA2003010386 A UA 2003010386A UA 73996 C2 UA73996 C2 UA 73996C2
- Authority
- UA
- Ukraine
- Prior art keywords
- urea
- carbon dioxide
- carbamate
- ammonia
- reactor
- Prior art date
Links
- 239000004202 carbamide Substances 0.000 title abstract description 92
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title abstract description 83
- 238000000034 method Methods 0.000 title abstract description 35
- 238000004519 manufacturing process Methods 0.000 title abstract description 22
- 230000008569 process Effects 0.000 title abstract description 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract description 210
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract description 191
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract description 105
- 239000001569 carbon dioxide Substances 0.000 abstract description 105
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 abstract description 101
- 229910021529 ammonia Inorganic materials 0.000 abstract description 86
- 238000006243 chemical reaction Methods 0.000 abstract description 34
- 239000011541 reaction mixture Substances 0.000 abstract description 20
- 238000011084 recovery Methods 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 abstract description 2
- 238000004064 recycling Methods 0.000 abstract description 2
- 238000005265 energy consumption Methods 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 description 113
- 230000008020 evaporation Effects 0.000 description 106
- 239000007864 aqueous solution Substances 0.000 description 50
- 238000009833 condensation Methods 0.000 description 35
- 230000005494 condensation Effects 0.000 description 35
- 230000015572 biosynthetic process Effects 0.000 description 33
- 238000003786 synthesis reaction Methods 0.000 description 33
- 239000012808 vapor phase Substances 0.000 description 32
- 238000009434 installation Methods 0.000 description 29
- 238000000926 separation method Methods 0.000 description 27
- 239000007789 gas Substances 0.000 description 26
- 239000007788 liquid Substances 0.000 description 18
- 238000000354 decomposition reaction Methods 0.000 description 15
- 239000000243 solution Substances 0.000 description 14
- 239000011261 inert gas Substances 0.000 description 8
- 238000002207 thermal evaporation Methods 0.000 description 8
- 150000003672 ureas Chemical class 0.000 description 8
- 239000012530 fluid Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000007792 gaseous phase Substances 0.000 description 4
- 230000008016 vaporization Effects 0.000 description 4
- 239000007791 liquid phase Substances 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 230000003134 recirculating effect Effects 0.000 description 3
- 239000003990 capacitor Substances 0.000 description 2
- 150000004657 carbamic acid derivatives Chemical class 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 229940125652 NAMI Drugs 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- IRIINYXGMWYHBL-UHFFFAOYSA-J [C+4].C(N)([O-])=O.C(N)([O-])=O.C(N)([O-])=O.C(N)([O-])=O Chemical compound [C+4].C(N)([O-])=O.C(N)([O-])=O.C(N)([O-])=O.C(N)([O-])=O IRIINYXGMWYHBL-UHFFFAOYSA-J 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 210000004268 dentin Anatomy 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- PEVNIEPIRVCPAW-UHFFFAOYSA-J sodium;1h-imidazole;methylsulfinylmethane;ruthenium(3+);tetrachloride Chemical compound [Na+].[Cl-].[Cl-].[Cl-].[Cl-].[Ru+3].CS(C)=O.C1=CNC=N1 PEVNIEPIRVCPAW-UHFFFAOYSA-J 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP00112688 | 2000-06-15 | ||
PCT/EP2001/001098 WO2001096287A1 (en) | 2000-06-15 | 2001-02-02 | Process and plant for the production of urea |
Publications (1)
Publication Number | Publication Date |
---|---|
UA73996C2 true UA73996C2 (en) | 2005-10-17 |
Family
ID=8168986
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
UA2003010386A UA73996C2 (en) | 2000-06-15 | 2001-02-02 | A process for the production of urea (variants), a mechanism for the production of urea and method for modernization of the mechanism for the production of urea |
UA2003010385A UA72819C2 (en) | 2000-06-15 | 2001-06-15 | A process for decomposing a carbamate aqueous solution coming from a urea recovery section of the urea production plant |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
UA2003010385A UA72819C2 (en) | 2000-06-15 | 2001-06-15 | A process for decomposing a carbamate aqueous solution coming from a urea recovery section of the urea production plant |
Country Status (10)
Country | Link |
---|---|
US (2) | US6552224B2 (ru) |
EP (2) | EP1289942B1 (ru) |
CN (2) | CN1216041C (ru) |
AT (2) | ATE394367T1 (ru) |
AU (2) | AU2001230231A1 (ru) |
DE (2) | DE60133894D1 (ru) |
MX (2) | MXPA02012329A (ru) |
RU (2) | RU2258063C2 (ru) |
UA (2) | UA73996C2 (ru) |
WO (2) | WO2001096287A1 (ru) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1918273A1 (en) * | 2006-11-04 | 2008-05-07 | Urea Casale S.A. | Process for urea production and related plant |
CN101823984B (zh) * | 2010-04-29 | 2012-11-28 | 聊城市鲁西化工工程设计有限责任公司 | 水解解吸热能的回收工艺及设备 |
EP2502881A1 (en) | 2011-03-24 | 2012-09-26 | Urea Casale S.A. | Process and plant for ammonia-urea production |
WO2014104893A1 (en) * | 2012-12-28 | 2014-07-03 | Stamicarbon B.V. | Urea plant revamping method |
GB2557081B (en) * | 2015-09-08 | 2020-05-13 | Toyo Engineering Corp | Urea manufacturing method and urea manufacturing apparatus |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3929878A (en) * | 1971-05-10 | 1975-12-30 | Ivo Mavrovic | Decomposition of ammonium carbamate |
US4110374A (en) * | 1976-03-02 | 1978-08-29 | Mitsui Toatsu Chemicals Inc. | Process for separating and recovering unreacted materials in urea synthesis |
US4088684A (en) * | 1976-07-30 | 1978-05-09 | Ivo Mavrovic | Urea reactor effluent solution recycle in urea synthesis |
NL8104040A (nl) * | 1981-09-01 | 1983-04-05 | Unie Van Kunstmestfab Bv | Werkwijze voor de bereiding van ureum. |
NL8303888A (nl) * | 1983-11-13 | 1985-06-03 | Unie Van Kunstmestfab Bv | Werkwijze voor de bereiding van ureum. |
IN169678B (ru) * | 1987-08-13 | 1991-11-30 | Austral Pacific Fertilizers | |
IT1232669B (it) * | 1989-09-15 | 1992-03-02 | Snam Progetti | Procedimento per la produzione di urea con elevato rendimento energetico. |
EP0495418B1 (en) * | 1991-01-15 | 1997-10-15 | Urea Casale S.A. | Process and device for increasing the yield and the production potential of urea reactors |
IT1245396B (it) * | 1991-03-22 | 1994-09-20 | Snam Progetti | Procedimento per la produzione di urea ad elevata efficienza energetica |
US5523482A (en) * | 1993-05-14 | 1996-06-04 | Urea Casale S.A. | Process and plant for the production of urea in reaction spaces with different yields |
ZA96686B (en) * | 1995-02-01 | 1996-08-16 | Urea Casale Sa | Process and plant for the production of urea with high conversion yield and low energy consumption |
NL1004977C2 (nl) * | 1997-01-13 | 1998-07-15 | Dsm Nv | Methode om de capaciteit van een bestaand ureum proces te verhogen. |
NL1009516C2 (nl) * | 1998-06-29 | 2000-01-04 | Dsm Nv | Werkwijze voor de bereiding van ureum. |
-
2001
- 2001-02-02 WO PCT/EP2001/001098 patent/WO2001096287A1/en active IP Right Grant
- 2001-02-02 CN CN018112943A patent/CN1216041C/zh not_active Expired - Lifetime
- 2001-02-02 US US10/049,687 patent/US6552224B2/en not_active Expired - Lifetime
- 2001-02-02 AT AT01902384T patent/ATE394367T1/de not_active IP Right Cessation
- 2001-02-02 MX MXPA02012329A patent/MXPA02012329A/es active IP Right Grant
- 2001-02-02 RU RU2002133441/04A patent/RU2258063C2/ru active
- 2001-02-02 UA UA2003010386A patent/UA73996C2/uk unknown
- 2001-02-02 DE DE60133894T patent/DE60133894D1/de not_active Expired - Lifetime
- 2001-02-02 AU AU2001230231A patent/AU2001230231A1/en not_active Abandoned
- 2001-02-02 EP EP01902384A patent/EP1289942B1/en not_active Revoked
- 2001-06-15 AT AT01951596T patent/ATE275128T1/de not_active IP Right Cessation
- 2001-06-15 WO PCT/EP2001/006775 patent/WO2001096288A1/en active IP Right Grant
- 2001-06-15 RU RU2002135632/04A patent/RU2247108C2/ru active
- 2001-06-15 EP EP01951596A patent/EP1289943B1/en not_active Expired - Lifetime
- 2001-06-15 AU AU2001272480A patent/AU2001272480A1/en not_active Abandoned
- 2001-06-15 UA UA2003010385A patent/UA72819C2/uk unknown
- 2001-06-15 US US10/049,686 patent/US6649795B2/en not_active Expired - Lifetime
- 2001-06-15 CN CNB018107648A patent/CN1219755C/zh not_active Expired - Lifetime
- 2001-06-15 DE DE60105292T patent/DE60105292T2/de not_active Expired - Lifetime
- 2001-06-15 MX MXPA02011818A patent/MXPA02011818A/es active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
CN1216041C (zh) | 2005-08-24 |
US6649795B2 (en) | 2003-11-18 |
MXPA02012329A (es) | 2003-04-25 |
MXPA02011818A (es) | 2003-04-10 |
UA72819C2 (en) | 2005-04-15 |
EP1289942B1 (en) | 2008-05-07 |
EP1289943A1 (en) | 2003-03-12 |
US20020151749A1 (en) | 2002-10-17 |
RU2247108C2 (ru) | 2005-02-27 |
WO2001096287A1 (en) | 2001-12-20 |
CN1433400A (zh) | 2003-07-30 |
ATE275128T1 (de) | 2004-09-15 |
EP1289943B1 (en) | 2004-09-01 |
DE60105292D1 (de) | 2004-10-07 |
EP1289942A1 (en) | 2003-03-12 |
US6552224B2 (en) | 2003-04-22 |
CN1219755C (zh) | 2005-09-21 |
AU2001272480A1 (en) | 2001-12-24 |
ATE394367T1 (de) | 2008-05-15 |
DE60133894D1 (de) | 2008-06-19 |
CN1436169A (zh) | 2003-08-13 |
DE60105292T2 (de) | 2005-02-17 |
US20030013914A1 (en) | 2003-01-16 |
WO2001096288A1 (en) | 2001-12-20 |
AU2001230231A1 (en) | 2001-12-24 |
RU2258063C2 (ru) | 2005-08-10 |
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