TW555584B - Vacuum extraction freeze drying machine - Google Patents
Vacuum extraction freeze drying machine Download PDFInfo
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- TW555584B TW555584B TW91132542A TW91132542A TW555584B TW 555584 B TW555584 B TW 555584B TW 91132542 A TW91132542 A TW 91132542A TW 91132542 A TW91132542 A TW 91132542A TW 555584 B TW555584 B TW 555584B
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555584 五、發明說明α) 【技術領域】 本發明係關於-種真空萃取乾燥 種:用固體物質、液體物質及固體液體混合化 取得較純之物質化:後,以除去雜質, 將分離出的物質冷;ρ燥^ 、乾秌、/辰縮等之方法,再 構保持不變或使物質=或=體;二=物料内部結 抑制細菌的繁殖,達到保藏的東:果r防止有機體的腐敗、 【先前技術】 在近代刀析化學中,蒸餾法除了用於 還是微量和痕量分析中的分離和的之外, ;的蒸德技術’-般只能做到部分分離,、匕用簡 離’就要進行多次的重複蒸餾,在=到完全分 可得到進一步的純化。萃取為一種用^复中各組分都 之不互溶的雙組分或多组分、容 〜'的卒取劑處理與 離過程,是-種廣泛應用的單元操y且分分離的傳質分 在現代工業生產中’常常需要 處理,如塑料的熱成型等。在農業生^進仃加熱和乾燥 一些產品作脫水乾燥處理,或二=’也常常需要對 熱乾燥工序都是耗能過程。冷^広l燥處理,然這些加 物料冷珠至水的冰點以下,;以::昇華乾燥,係將 供熱使物料中的水分,直接從固態:e的容器中,通過 燥方法。 “昇華為水汽的一種乾 域市垃圾經過壓縮處理可以減 體積,便於運輸和填 第5頁 555584 五、發明說明(2) f,在咼壓壓縮過程中,由於生活垃圾受到擠壓和升溫, 可使生活垃圾中的生化需氧量(B〇D)從6〇〇〇毫克/升降到 〇〇毫克/升,化學需氧量(C0D)從8 000毫克/升降到15〇毫 γ升,大大降低了腐化性’不再孽生昆蟲,從 對裱境的污染。 然上述之各個裝置各有各的功能,無法將之集中,由 :可見,Jl述習用裝置仍有諸多缺失,實非一良善之設計 者’而亟待加以改良。 本案發明人鑑於上述習用裝置所衍生的各項缺點,乃 二加以改良創新,並經多年苦心孤詣潛心研究後,終於 成功研發完成本件真空萃取冷凍乾燥機。 、 【發明目的】 笋由目的#在於提供一種真空萃取冷凍乾燥機, 二物暂::益將蒸餾萃取填充槽加熱,能使固體物質、液 同,Λ 2 ^固體液體混合化合物中,依各成分沸點的不 二質/飞化,然後冷凝收集,以除去雜質,取得較純之 機,藉由-真d:係在於提供一種真空萃取冷凍乾燥 冷束至水的冰;櫃内之冷來棒’能將除去水份之物質 離,m w Γ 因冷凍乾燥後之物質處於冰柬狀 &所以此維持内部結構保持不變。 本^ $务明rj 機,藉由轉動螺;::係在於提供一種真空萃取冷束乾燥 空冷束植内Γ4;Γ:ΐ螺桿轉軸前端之壓縮隔板在真 j移動’使真空冷凍櫃的内部空間縮小,以 555584 五、發明說明(3) 將物質再次壓縮處理 【發明内容】 、、、小物質之體積 可達成上述發明目 包括 有: 、〃空萃取冷凍乾燦機 一上旋蓋組,係由一 > 蓋固定座所組成,該上二5、一散熱風屬以及一上旋 之蒸餾萃取填充槽之上緣以提並設置於後述 内側设置有一散熱風扇 ^ 遮之功能,該上旋蓋 有一上旋蓋固定座,俾 Y政…,而該上旋蓋後側設置 之動作; #利於上旋蓋固定位置…升開啟 一上疑蓋,係為一中处凡 充槽之上緣; 二體叹置於後述之蒸餾萃取填 月丈熱風扇,係設置於上旌苔 氣,使空氣流通並帶動旋繞管之熱; 一上旋蓋固定座,係裝設於上旋蓋後側,其上方設置 上2穿之内螺紋圓孔,配合旋蓋轉轴之旋轉轉動,;^字 啟二上升至設定位置&,再旋轉上旋蓋,以達上旋蓋開 樹1之功能; —冷凝器組,係由一冷凝器、一收集孔、一旋繞管、 二旋繞管導出管以及一冷卻液導出孔所組成,該冷擬器係 、置於上凝蓋之中空體内’籍由S亥政熱風扇或冷束泵^送' t水儲存櫃中之冷卻水進行散熱,而冷擬器内設置有旋繞 β亥凝繞管的入口端為一收集孔’經由該收集孔導入高 第7頁 555584 發明說明(4) 二二Λ至,繞$内排除掉熱能,而後將低溫凝結的取液 經由旋繞導出管、冷卻液導出孔流至後述之儲存槽; 二冷凝器’係設置於上旋蓋之中空體内; 收集孔’係為旋繞管前端之入口; 咖 f、堯^,係為一設置於冷凝器内之多重迴轉環繞之 中空圓官’當高熱蒸氣進入收集孔後,高熱之蒸氣會在旋 繞ΐ内動,並經由散熱風扇或冷卻水除去熱量,使高散 蒸氣冷凝之; ” 一旋繞導出管,係樞接於冷凝器之旋繞管出口,提供 高熱蒸氣冷卻凝結成萃取液之流出用; 一冷卻液導出孔,係為旋繞管之旋繞導出管之一冷 液流出口; 一冷部液儲存裝置,係由一儲存槽、一通氣溢流孔以 及一電磁閥所組成; 一儲存槽’係提供旋繞管内冷卻凝結成萃取液之儲 容器; , 一通氣溢流孔,係設置於儲存槽上方,提空一平衡儲 存槽内外氣壓,以及儲存槽内之萃取液盛滿可向外流出之 一出口; 一電磁閥,係裝設於儲存槽與真空冷凍櫃之管路上,4 提供開閉該電磁閥來控制儲存槽内的冷卻液流至真空冷 櫃; 一蒸餾萃取裝置,係由一蒸餾萃取填充槽、一窺視 孔、一轉軸固定座、一旋蓋轉軸、一掀蓋馬達、一可調式555584 V. Description of the invention α) [Technical field] The present invention relates to a kind of vacuum extraction and drying seeds: a solid substance, a liquid substance and a solid liquid are mixed to obtain a more pure materialization: after that, the impurities are removed, and the separated The material is cold; ρ dry ^, dry, / Chen shrink and other methods, the reconstruction is kept unchanged or the material = or = body; two = the internal structure of the material inhibits the reproduction of bacteria, to achieve the preservation of the East: the fruit to prevent the organism Corruption, [previous technology] In modern knife chemistry, the distillation method is used for separation and summation in trace and trace analysis. The simple separation should be carried out several times of repeated distillation, further purification can be obtained at = to the complete fraction. Extraction is a two-component or multi-component immiscible agent extraction and treatment process that is incompatible with each other. It is a widely used unit operation and separate mass transfer. Divided in modern industrial production, it often requires processing, such as thermoforming of plastics. In the agricultural industry, heating and drying are carried out. Some products are dehydrated and dried, or two = ', often also require energy-consuming processes for the thermal drying process. Cold and dry treatment, then these added materials cold beads below the freezing point of water; :: Sublimation drying, the water in the material is supplied directly from the solid: e container by drying method. "A kind of dry land municipal waste that has been sublimated to water vapor can be reduced in volume after being compressed, which is convenient for transportation and filling. Page 5 555584 V. Description of the invention (2) f. During the squeezing compression process, due to the compression and heating of domestic waste, The biochemical oxygen demand (BOD) in domestic waste can be raised from 6,000 mg / liter to 0.00 mg / litre, and the chemical oxygen demand (C0D) can be raised from 8,000 mg / litre to 150 milliliter. Corrosiveness is greatly reduced. No longer infested insects and pollution to the environment. However, each of the above devices has its own functions and cannot be concentrated. From this, it can be seen that there are still many shortcomings in the Jl conventional device. A good designer is in urgent need of improvement. In view of the various shortcomings derived from the conventional device described above, the inventor of this case has improved and innovated it. After years of painstaking research, he finally successfully developed this vacuum extraction freeze dryer. [Objective of the invention] Bamboo shoots purpose # is to provide a vacuum extraction freeze dryer. The second thing is: heating the distillation extraction filling tank, which can make solid substances and liquids the same, Λ 2 ^ solid liquid In the bulk compound, according to the boiling point of each component, it is condensed and collected, and then collected by condensation to remove impurities and obtain a more pure machine. By-true d: is to provide a vacuum extraction freeze-dried cold beam to water. Ice; the cold rod in the cabinet can remove the moisture-removing material, mw Γ keeps the internal structure unchanged because the freeze-dried material is in the shape of ice & this ^ $ 务 明 rj machine, borrow Rotating screw :: is to provide a vacuum extraction cold beam drying air-cooled beam plant Γ4; Γ: ΐ The compression partition at the front end of the screw shaft is moved at true j to reduce the internal space of the vacuum freezer. 555584 V. Invention Explanation (3) Compressing the substance again [Content of the invention] The above objects can be achieved with the volume of small substances, including: 〃, air extraction freeze-drying machine, a capping group on the top, and a cap holder It consists of the upper two, a heat-dissipating wind, and an upper edge of the distilling extraction filling tank to be lifted and arranged on the inner side to be described later. A heat-dissipating fan is provided, and the upper cap has an upper cap fixing seat. , 俾 Y 政…, And the action set on the back side of the upper screw cap; # conducive to the upper screw cap fixed position ... lift and open an upper cap, which is the upper edge of the filling tank in the middle; The Yuezhang hot fan is installed on the upper moss gas to circulate the air and drive the heat of the winding tube; an upper screw cap fixing seat is installed on the rear side of the upper screw cap, and the upper part is provided with a two-threaded internal thread circle Hole, in conjunction with the rotation of the screw cap rotating shaft, the ^ character Kaiji rises to the set position & and then rotates the upper screw cap to achieve the function of the upper screw cap and open the tree 1-condenser unit, which consists of a condenser It consists of a collection hole, a spiral tube, two spiral tube lead-out tubes, and a coolant lead-out hole. The cold modeler is placed in the hollow body of the upper condensation cover. ^ Send the cooling water in the water storage cabinet to dissipate heat, and the inlet end of the coiled beta helium condensing tube provided in the cooler is a collection hole, which is introduced through the collection hole. Page 7 555584 Description of the invention (4) 222 to, remove the heat energy in the winding, and then take the low-temperature condensed liquid through the spiral outlet pipe, cool The liquid outlet hole flows to the storage tank described later; the two condensers are arranged in the hollow body of the upper screw cap; the collection holes are the inlets of the front end of the spiral tube; the f and Yao are arranged in the condenser. The multiple revolutions surround the hollow circle. When the high-heat steam enters the collection hole, the high-heat steam will move inside the spiral coil and remove the heat through the cooling fan or cooling water to condense the high-diffused vapor; It is pivotally connected to the outlet of the spiral tube of the condenser to provide high-temperature steam for cooling and condensing into the extraction liquid; a coolant outlet hole is a cold liquid outlet of the spiral outlet tube of the spiral tube; a cold liquid storage device , Is composed of a storage tank, a vent overflow hole and a solenoid valve; a storage tank 'is a storage container providing cooling condensed into an extraction liquid in a spiral tube;, a vent overflow hole is arranged above the storage tank, Elevate an air pressure inside and outside the storage tank, and an outlet filled with the extraction liquid in the storage tank, which can flow outwards; a solenoid valve is installed on the pipeline of the storage tank and the vacuum freezer. It is used to open and close the solenoid valve to control the cooling fluid in the storage tank to flow to the vacuum freezer. A distillation extraction device consists of a distillation extraction filling tank, a peep hole, a rotating shaft fixing seat, a screw cap rotating shaft, a cover motor, One adjustable
555584 五、發明說明(5) 安全洩壓閥、 器、一溫度感 一蒸氣加熱器 方設置有一卸 包覆有一隔熱 轉軸固定座, 蓋馬達帶動一 經旋轉提供上 一蒸餾萃 組置放於中空 接,提供欲蒸 乾知卒餘物之 一窺視孔 視窗’提供一 一轉軸固 侧,且該轉軸 内螺紋; 一旋蓋轉 固定座之内螺 輸出轉軸上, 一掀蓋馬 轉旋蓋轉軸之 一可調式 方,提供一可 隔熱保溫層 測裝置 所組成 料收集 保溫層 該轉軸 旋蓋轉 旋蓋組 取填充 槽體之 餾萃取 功能; ,係裝 檢視槽 定座, 固定座 、一無 ,該蒸 孔,並 ,而該 固定座 軸穿置 上升旋 槽,係 上緣, 之物質 、一卸 水感測 餾萃取 在該蒸 蒸餾萃 下方設 轉軸固 轉的功 為一圓 槽體之 篩取分 料收集 裝置、 填充槽 餾萃取 取填充 置有一 定座與 能; 桶狀之 下緣係 離後加 設於蒸顧萃取填充槽 内的工作情況; 係裝設於蒸餾萃取填 上方設置有一可至入 軸,係為一螺旋狀圓柱體, 紋内,該旋蓋轉軸之下端固 以提供上旋蓋組上升旋轉之 達’係設置於蒸餾萃取填充 功能; 安全洩壓閥,係設置於蒸館 依規格調整適當之工作壓力 孔、一溫度控制 一電加熱器以及 呈圓桶狀,其下 填充槽外部完整 槽後方設置有一 掀蓋馬達,該掀 上旋蓋固定座, 槽體’該上旋蓋 與卸料閥組相樞 熱〉t化以及再次 上之一透明玻璃 充槽之上方後 方疋盍轉轴外徑之 貫穿設置於轉軸 定於掀蓋馬達之 功能, 槽後方,提供旋 萃取填充槽後 ,以控制槽内氣 555584 五、發明說明(6) 壓; 一隔熱保溫層,係提供蒸餾萃取填充槽之外殼溫度保 持、熱源隔離之一保護層; 一卸料收集孔,係設置於蒸餾萃取填充槽内部下方一 具有錐度形狀之上寬下窄之圓孔,係當物質被加熱汽化 後’被分離的萃餘物會如欲轉移至真空冷凍櫃,則可利用 本身的重量經由卸料收集孔、卸料閥直至真空冷凍櫃; w 一溫度控制器,係裝設於電加熱器上一用以控制電加 熱f和蒸^加熱器之開關,透過溫度控制器上之顯示器, 可得知目前加熱蒸餾萃取物質之溫度; 一溫度感測裝置,係裝設於蒸餾萃取填充槽内,能將 槽内的溫度參數狀態,自動反饋溫度至溫度控制器上之顯 示器’以將確保溫度保持恆定或在給定的範圍之内; ,一無水感測裝置,係裝設於蒸餾萃取填充槽内具有錐 度形狀之位置,當槽内之液體物質在加熱分離時,可用來 偵測槽内的含水量以判斷工作進度,和自動停止加熱之一 一電加熱器,係裝設於蒸餾萃取填充槽外,利用 :::蒸:萃取填充槽加熱’讓固體物質與空氣作高速相、 _ 的高溫氣體將固體物質内具有揮發性的成 下方具有 物至沸 一蒸氣加熱器,係裝設於蒸餾萃取填充槽之 =度形狀,外殼上,係用電熱元件加熱液體混合 、,使之汽化和除去雜質之一裝置;555584 V. Description of the invention (5) A safety pressure relief valve, a device, a temperature-sensing and a steam heater are provided with a heat-insulating shaft fixing seat, and a cover motor drives the previous distillation group to be placed in the hollow upon rotation. Then, provide a peephole window for steaming the leftovers. Provide a fixed side of the rotating shaft, and the rotating shaft is internally threaded; on the output shaft of the internal screw of a screw cap rotation holder, a flip-crank horse One of the adjustable squares provides a material collection and insulation layer composed of a heat-insulating layer measuring device. The rotating shaft cap and rotating cap group take the distillation extraction function of the filled tank body; No, the steam hole, and the fixed seat shaft passes through the ascending spiral groove, the upper edge of the substance, a water-discharging sensing distillation extraction, and the work of rotating the shaft under the steam distillation is set as a circular groove body. Sieving, collecting and collecting device, filling tank distillation extraction and filling are equipped with a certain seat and capacity; the lower edge of the barrel is separated and installed in the distillation and filling tank; it is installed in the distillation An accessible shaft is arranged above the filling, which is a helical cylinder. Inside the rib, the lower end of the screw cap shaft is fixed to provide the upper screw cap group to rise and rotate. It is set in the distillation extraction filling function; safety relief valve It is set in the steaming hall to adjust the appropriate working pressure hole according to the specifications, a temperature control, an electric heater, and a barrel shape. There is a cover motor behind the complete groove outside the lower filling tank. Slot body: The upper cap is connected to the discharge valve group, and the upper and rear sides of the upper transparent glass tank are filled again. The outer diameter of the rotating shaft is set on the rotating shaft to determine the function of the cover motor. At the rear, a rotary extraction filling tank is provided to control the gas in the tank. 555584 V. Description of the invention (6) Pressure; A heat insulation layer is a protective layer that provides the temperature maintenance and heat source isolation of the shell of the distillation extraction filling tank; The material collecting hole is a round hole with a tapered shape above and below the inside of the distillation extraction filling tank. It is a 'separated raffinate' that will be transferred as desired after the substance is heated and vaporized. To the vacuum freezer, it can use its own weight to reach the vacuum freezer through the discharge collection hole and the discharge valve; w A temperature controller is installed on the electric heater to control the electric heating f and steam heating The switch of the device can know the current temperature of the heating and distillation extraction substance through the display on the temperature controller. A temperature sensing device is installed in the distillation extraction filling tank, which can automatically feedback the temperature parameter status in the tank. The display on the temperature-to-temperature controller 'will ensure that the temperature is kept constant or within a given range; a waterless sensing device is installed in the taper-shaped position in the distillation extraction filling tank. When the liquid substance is heated and separated, it can be used to detect the water content in the tank to determine the progress of the work, and to automatically stop heating. An electric heater is installed outside the distillation extraction filling tank. The tank is heated to allow the solid material to form a high-speed phase with air. The high-temperature gas of _ will volatile the solid material into a boiling-steam heater, which is installed in the distillation. The shape of the extraction filling tank is a device on the shell, which is heated by an electric heating element to mix the liquid and vaporize it and remove impurities.
555584 五、發明說明(7) 一萃取混合卸料 為一底 内’該 之錐度 質蒸餾 一萃取混合桶, 蒸顧萃取填充槽内, 形角卸料孔; 一篩取桶,係為 桶,重疊設置於萃取 一齒條,可與卸料馬 使篩取 度扇形 裝置 部具 萃取 底部 後之 係為 於該 一桶 混合 達組 桶底 角卸 桶所組成,係 餾萃取填充槽 置,並於該桶 以提供固體物 轉動篩取桶, 取混合桶之90 能; ’係由一萃取混合桶以及一篩取 有錐度之萃取混合桶,固定於蒸 混合桶内提供筛取桶相疊之設 ^ 對稱之9 〇度扇形角卸料孔, 萃餘物卸料用; 一底部具有錐度之圓桶,固定於 桶之錐度底部有一對稱之9 0度扇 身鑽有篩孔且底部具有錐度之圓 桶内,於篩取桶内側上方環繞著 之齒輪組之3號齒輪嚙合運行以 邛之9 0度扇形角卸料孔,可與萃 料孔準確對準,以達到卸料之功 一卸料馬達組,係由一焉一 齒輪、一2號齒輪以及二達 減速齒輪組、一1號 乙說茴輪以及一3旒齒輪所組成, 輪組設置於蒸顧萃取冑充槽外 7達和減速齒 減逆:輪組,使輸出轴連接設置於萃取混 輪二轉帶動固定於萃取混合桶上之2號齒輪,使相互= 之2唬齒輪和3號齒輪轉動,以提供筛取桶旋轉 „,係由一授拌器和一 5號齒輪所組:,該 =拌;,Ή利用攪拌馬達組上4號齒輪帶 動攪拌益組之5號齒輪,使樞接於5號齒輪 ζ 轉攪拌篩取桶内之物質; < 攪捽益此方疋 555584 五、發明說明(8) 一攪拌 说齒輪所組 槽外,藉由 組轉動輸出 说齒輪旋轉 一卸料 係裝設於蒸 所控制,提 冷凍櫃之流 蒸餾萃取填 一卸料 卒餘物以及 一卸料 或手動旋轉 啟、關閉卸 馬達組,係由一馬達、一減速齒輪 成,該馬達和減速齒輪組設置於蒸 馬達動力之輸出帶動減速齒輪組了 軸上的4號齒輪,使該4號齒輪將攪 之; 閥組, 餾萃取 供可控 量,以 充槽施 閥,係 萃取液 轉運泵 卸料轉 料閥之 一真空冷凍組 包括一卸料閥及一卸料轉運 填充槽 制萃餘 及控制 以精餾 裝設於 流量之 ,係裝 下方,該卸料閥以一 物從蒸顧萃取填充槽 萃取液從後述真空冷 操作之一裝置; 蒸餾举取填充槽下方 閥門; 設於卸料閥外,利用 運泵上方之圓盤,以帶動減 一裝置; 組以及一 4 餾萃取填充 使減速齒輪 拌器組之5 粟所組成, 卸料轉運泵 移動至真空 凍櫃移動至 ,為一控制 一電動馬達 速齒輪來開 空洩壓閥、一壓縮 冷凍機、一調節過 真空泵所組 於左側設置 軸穿置壓縮轉運系 動和移動螺桿轉軸 部空間,提 ,係由 轉運泵 渡器、 成,該真空冷 有一壓縮轉運 與真空 前端之 供一萃餘物之 一真空冷凍櫃、一冷凍棒、一真 、一螺桿轉軸、一壓 一冰水儲水櫃、_ $ 凍櫃’係裝設於卸料 泵,該壓縮轉運泵帶 冷凍櫃,經旋轉提供 壓縮隔板以縮小真空 壓縮處理功能; 縮隔板、一 水系以及^ 闊組下方, 動一螺桿轉 螺桿轉轴轉 冷凍櫃之内 一真空冷凍櫃,該櫃上方係與卸料閱組相樞接,下方555584 V. Description of the invention (7) An extraction mixing discharge is a bottom of the taper distillation, an extraction mixing barrel, steaming the extraction filling tank, angled discharge holes; a sieve extraction barrel, which is a barrel, It is superimposed on the extraction rack and can be connected with the discharge horse to make the sieve extraction fan-shaped device part with the extraction bottom. The system is composed of unloading the barrel at the bottom corner of the barrel, and the distillation extraction fills the tank. Rotate the sieve extraction barrel to provide solids in the barrel, and take the 90 energy of the mixing barrel; 'It consists of an extraction mixing barrel and a taper extraction mixing barrel, fixed in the steam mixing barrel to provide the sieve barrels stacked on top of each other. Symmetrical 90-degree fan-shaped angle discharge hole is used for extracting residual material; a barrel with a taper at the bottom, fixed to the taper of the barrel; a 90-degree fan with a sieve hole drilled at the bottom and a taper at the bottom In the drum, the No. 3 gear of the gear set surrounding the inside of the sieve extraction bucket meshes with a 90-degree fan-shaped discharge hole, which can be accurately aligned with the extraction hole to achieve the function of discharging. The unloading motor unit consists of a gear, a gear, It consists of No. 2 gear and Er Da reduction gear set, No. 1 B gear wheel, and No. 3 gear. The wheel set is located outside the steam extraction tank and the 7 gear and reduction gear reduction: the wheel set makes the output shaft It is connected to the second rotation of the extraction mixing wheel to drive the No. 2 gear fixed on the extraction mixing barrel, so that the two gears and No. 3 gear are rotated to provide the rotation of the sifting barrel. It consists of a blender and a 5 No. gear group :, this = mix;, Ή use the No. 4 gear on the stirring motor group to drive the No. 5 gear of the mixing benefit group, so that the pivot is connected to the No. 5 gear ζ to stir and sieve the material in the barrel; < Benefit this side 疋 555584 V. Description of the invention (8) A stirring gear is outside the groove of the gear group, and the gear is rotated by the output of the gear. The discharge is installed in the steaming station, and the flow of the freezer is distilled, extracted and filled. The leftover material and a discharging or manual rotating opening and closing motor unit are composed of a motor and a reduction gear. The motor and the reduction gear set are arranged on the output of the steam motor to drive the reduction gear set on the shaft. No. gear, so that the No. 4 gear will stir; Distillation extraction is for controllable volume, and the valve is filled in the tank, which is one of the extraction liquid transfer pump discharge transfer valve. The vacuum freezing group includes a discharge valve and a discharge transfer filling tank to make raffinate and control the installation by rectification. At the bottom of the flow, the discharge valve is a device that extracts the filling liquid from the distillation tank and extracts the liquid from one of the vacuum cold operations described below; the distillation lifts the valve below the filling tank; it is located outside the discharge valve and uses a pump The upper disc is used to drive a minus one device; the group and a 4-distillation extraction filling make up the 5 millet of the reduction gear mixer group. The unloading transfer pump is moved to the vacuum freezer to move to control an electric motor speed gear. To open the air pressure relief valve, a compression freezer, and an adjusted vacuum pump, set the shaft on the left side to put the compression transfer system and move the screw shaft space. The lift is made of a transfer pump. The vacuum cooling system has a The compression transfer and vacuum front-end vacuum extraction cabinet, a freezing rod, a true, a screw shaft, a pressurized ice water storage cabinet, a _ $ freezer 'are installed on the discharge pump, The Retractable transfer pump with freezer, rotating to provide compression partition to reduce the vacuum compression processing function; shrink the partition, a water system and the bottom of the ^ wide group, move a screw to the screw shaft to a vacuum freezer inside the freezer, the The upper part of the cabinet is pivotally connected to the unloading group, and the lower part
第12頁 555584 五、發明說明(9) 與出料閥組相樞接,係提供一將加熱過後的萃餘物冷凍至 水的冰點以下,也提供將壓力抽成低於大氣壓力之隔埶 體; …、 一冷凍棒,係設置於真空冷凍櫃内,提供真空冷凍櫃 内之物質冷凍乾燥之一裝置; 一真空洩壓閥,係設置於真空冷凍櫃上方,用以恢復 真空冷凍櫃内之大氣壓力值; 一壓縮轉運泵,係設置固定於真空冷凍櫃外,利用一 電動馬達或手動旋轉壓縮轉運泵上方之圓盤,以帶動減速 齒輪轉動貫穿於壓縮轉運泵之螺桿轉軸,使螺桿轉軸前端 之壓縮隔板能前後移動; 一螺桿轉軸,係貫穿設置於壓縮轉運泵和真空冷凍櫃 之一側箱體,提供壓縮隔板於真空冷凍櫃内移動之功能; 一壓縮隔板,係設置於真空冷凍櫃内,藉由壓縮隔板 將真空冷凍櫃内之物質壓縮後,再次冷凍乾燥該物質,以 減小該物質之體積,另可再配合卸料閥之開啟,可將萃餘 物或萃取液擠推至蒸餾萃取填充槽施做再次蒸餾萃取之動 作; 一冷凍機,係設置於蒸餾萃取填充槽外之一裝置,提 供冷凍棒和冰水儲存櫃之動力來源; 一調節過濾器,係設置於真空冷凍櫃至冷凍機和真空 泵之管路上,提供控制經過之空氣,以保持設定之溫度、 濕度,以控制灰塵及有害氣體含量之一裝置; 一冰水儲水櫃,係利用一管路與冷凍機連接, 冷 555584 五、發明說明(ίο) 凍機將冰水儲水櫃内之冷卻水溫度降低,以 卻冷凝器内之旋繞管之裝置; 一冰水泵,係與冷凍機之輸出端相連接, 儲水櫃内之冰水輪送至冷凝器之功能; 一真空泵,係裝設於蒸餾萃取填充槽外, ^空冷凍櫃内之大氣壓力降低,以獲得和維持 一裝置; ' 一出料閥組,係由一出料閥、一 餘物出料孔所組成,係裝設於真空冷凍櫃下方 △;東::=f所控制’提供控制萃餘物和萃 冷凍櫃移動至卒餘物出料孔之流量之一裝置; 一出料閥,係裝設於真空冷凍M ^;,盔 取物流量之裝置; 為 一出料轉運泵,係裝設於出料閥上,利 ΐ手料轉運系上方之圓盤,以帶動減 啟關閉出料閥之一裝置;以及 一萃餘物出料孔,係為出料閥之出口, 料用。 ^ 【實施方式】 請參閱圖一,本發明所提供之真空萃取冷 5括有:一上旋蓋組(Α)、一冷凝器組(β; 儲存裝置(C)、一蒸餾萃取裝置(D)、一萃取混 (^)、一卸料閥組(F)、一真空冷;東組(G)以及 (H)所組成。 久 供冰水以冷 提供將冰水 能提供一將 真空狀態之 栗以及一萃 ’該出料閥 取液從真空 一可控制萃 一電動馬達 速齒輪來開 供萃餘物出 〉東乾無機, 、一冷卻液 合卸料裝置 •出料閥組Page 12 555584 V. Description of the invention (9) It is pivotally connected to the discharge valve group. It provides a method to freeze the heated raffinate below the freezing point of water, and also provides a pressure to draw the pressure below the atmospheric pressure. …, A freezing rod is a device installed in a vacuum freezer to provide freeze drying of the contents of the vacuum freezer; a vacuum pressure relief valve is installed above the vacuum freezer to restore the inside of the vacuum freezer Atmospheric pressure value; A compression transfer pump is set outside the vacuum freezer. An electric motor or manual rotation of the disk above the compression transfer pump is used to drive the reduction gear to rotate through the screw shaft of the compression transfer pump to make the screw The compression partition at the front end of the shaft can move back and forth; a screw shaft is penetrated through the side box of the compression transfer pump and the vacuum freezer, providing the function of the compression partition to move in the vacuum freezer; a compression partition, It is set in a vacuum freezer. After compressing the material in the vacuum freezer by a compression partition, the material is freeze-dried again to reduce the volume of the material. It can be matched with the opening of the discharge valve to squeeze the raffinate or extraction liquid to the distillation extraction filling tank to perform the operation of re-distillation extraction. A refrigerator is a device installed outside the distillation extraction filling tank to provide refrigeration. Power source for sticks and ice water storage cabinets; an adjustment filter is installed on the pipeline from the vacuum freezer to the freezer and vacuum pump to provide control of the passing air to maintain the set temperature and humidity to control dust and harmful gases One device of content; an ice water storage tank, which is connected to the freezer by a pipeline, cold 555584 V. Description of the invention (ίο) The freezer reduces the temperature of the cooling water in the ice water storage tank to the condenser Inside the coiled pipe device; an ice water pump, which is connected to the output of the refrigerator, the ice water wheel in the water storage tank sends the function to the condenser; a vacuum pump, which is installed outside the distillation extraction filling tank, ^ The atmospheric pressure in the empty freezer is reduced to obtain and maintain a device; 'A discharge valve group is composed of a discharge valve and a residue discharge hole, which is installed below the vacuum freezer △; East :: = f controlled 'provides a device that controls the flow rate of extractive residue and extractive freezer to move to the discharge hole of the residual residue; a discharge valve is installed in the vacuum freezing M ^; Device: It is a discharge transfer pump, which is installed on the discharge valve, which is a device above the hand transfer system to drive the opening and closing of the discharge valve; and a extraction residue discharge hole, It is the outlet of the discharge valve. ^ [Embodiment] Please refer to FIG. 1. The vacuum extraction cold 5 provided by the present invention includes: an upper capping group (A), a condenser group (β; storage device (C), a distillation extraction device (D ), An extraction mixing (^), a discharge valve group (F), a vacuum cold; East group (G) and (H). Long supply of ice water to provide cold water will provide ice water to a vacuum state Li and Yicui'The discharge valve takes liquid from a vacuum-controllable pumping-electric motor speed gear to open the extraction residue> Donggan Inorganic, a cooling liquid unloading device • Discharging valve group
555584555584
本發明之真空萃取冷束乾燥機所提供之功能,包八 餾、萃取、乾燥、精餾、濃縮、冷凍乾燥、體積壓縮二^ 能’其中適合使用之物質包括為環保、廢油水、化工一 泥、污水、食品…等固體物質、液體物質以及 體= 合化合物。 菔欣體此 下就本發明之真空萃取冷凍乾燥機蒸餾萃取 進行一詳細之解說步驟 物The functions provided by the vacuum extraction cold beam dryer of the present invention include eight distillation, extraction, drying, rectification, concentration, freeze drying, and volume compression dual energy. Among them, suitable materials include environmental protection, waste oil and water, chemical industry Mud, sewage, food, and other solid, liquid, and bulk compounds. Xin Xin will now perform a detailed explanation of the vacuum extraction freeze-dryer distillation extraction of the present invention.
步驟一:先啟動掀蓋馬達(42b),以旋轉旋蓋轉轴 (42)帶動上旋蓋組(A)上升至設定位置後,再旋轉上旋蓋 (1 ),以將上旋蓋(1)開啟之,將欲蒸餾萃取之物質由高處 置入蒸餾萃取填充槽(4)中之篩取桶(51),因篩取桶(^) 本身鑽有篩孔,因此,較細小之固體物質會穿過篩孔,掉 落於蒸餾萃取填充槽(4)下方之卸料收集孔(4a)上,而體 積較大之固體物質則會留在篩取桶(5丨)内,在固體物質置 入篩取桶(51)後,則可將上旋蓋組(A)關閉之。Step 1: Start the capping motor (42b), rotate the capping shaft (42) to drive the capping group (A) to the set position, and then rotate the capping (1) to turn the capping ( 1) When it is turned on, the material to be distilled and extracted is processed into the sieve barrel (51) in the distillation extraction filling tank (4) from a high level, because the sieve barrel (^) is drilled with sieve holes, so the finer solid The material will pass through the sieve hole and fall on the discharge collection hole (4a) under the distillation extraction filling tank (4), while the solid material with a larger volume will remain in the sieve barrel (5 丨), and After the material is placed in the screening barrel (51), the upper screw cap group (A) can be closed.
步驟二:啟動溫度控制器(4 5 ),將電加熱器内之電熱 元件加熱,使蒸餾萃取填充槽(4)内產生的高溫氣體後, 讓固體物質内具有揮發性的成份(如水份),慢慢的因固體 物質内各成份的彿點不同,使彿點較低的成份因此而汽 化’而被分離出來。在加熱汽化的過程中,可透過窺視孔 (41)之玻璃視窗,來檢查、觀察固體物質乾燥、萃取之狀 態’為了使固體物質内具有揮發性的成份(如水份)能均勻 的被加熱,另可藉由攪拌馬達組(5 4)之動力輸出帶動減速 齒輪組,使減速齒輪組轉動輸出軸上的4號齒輪(54a) ’使Step 2: Start the temperature controller (45), heat the electric heating element in the electric heater, and extract and extract the high-temperature gas generated in the filling tank (4) by distillation, so that the solid substance has volatile components (such as water) ), Slowly due to the different Buddha points of the various components in the solid matter, the lower Buddha points are therefore vaporized 'and separated. In the process of heating and vaporization, the glass window of the peephole (41) can be used to check and observe the dry and extracted state of the solid matter. 'In order to make the volatile components (such as water) in the solid matter can be uniformly heated In addition, the reduction gear group can be driven by the power output of the stirring motor group (5 4), so that the reduction gear group can rotate the No. 4 gear (54a) on the output shaft.
第15頁 555584 五、發明說明(12) 該4號齒輪(54a)將攪拌器組(53)之5號齒輪(53a)旋轉之, 以轉動揽拌器之旋轉槳,如此,可充分攪拌篩取桶(5丨)内 之固體物質,使固體物質内沸點較低之成份因加熱而汽 化0Page 15 555584 V. Description of the invention (12) The No. 4 gear (54a) rotates the No. 5 gear (53a) of the agitator group (53) to rotate the rotating paddle of the agitator, so that the sieve can be fully stirred Take the solid material in the barrel (5 丨) to make the lower boiling point of the solid material vaporize by heating.
然蒸餾和精餾之不同是在於,A •通過加熱汽化揮發和 後繼的冷凝過程分離不同物質的操作稱為蒸餾。β•在本發 明之真空萃取冷凍乾燥機中,將冷凝後放置於儲存槽(3 ) 的萃取液多次交替進行加熱汽化與冷凝,使不同物質儘可 能地完全分離之精餾操作,該操作是開啟真空泵(7 9 )和電 磁閥(32) ’將儲存槽(3)中的萃取液吸引至該真空冷凍櫃 (7)後’開啟卸料閥(61)並啟動壓縮轉運泵(73)將壓縮隔 板(7 5 )移動,以縮小真空冷凍櫃(7 )内部空間,以將萃取 液擠壓至蒸餾萃取填充槽(4 )實施多次交替進行加熱汽化 與冷凝之一操作。However, the difference between distillation and rectification is that A • The operation of separating different substances by heating vaporization and subsequent condensation process is called distillation. β • In the vacuum extraction freeze dryer of the present invention, a distillation operation in which the condensed extraction liquid placed in the storage tank (3) is alternately heated and vaporized and condensed to separate different substances as completely as possible. This operation Is to open the vacuum pump (7 9) and the solenoid valve (32) 'After attracting the extraction liquid in the storage tank (3) to the vacuum freezer (7)', open the discharge valve (61) and start the compression transfer pump (73) The compression partition (7 5) is moved to reduce the internal space of the vacuum freezer (7), and the extraction liquid is squeezed into the distillation extraction filling tank (4) to perform multiple operations of heating, vaporization and condensation.
步驟三’當汽化後不斷產生之高溫蒸氣會聚集進入收 集孔(21) ’並由收集孔(21)進入設置於冷凝器(2)内之多 重迴轉環繞之旋繞管(22)内,當高熱之蒸氣在旋繞管(22) 内流動時’旋繞管(22)内之高熱蒸氣可經由散熱風扇(11) $循環冷卻水散熱之方式除去熱量,使高熱蒸氣冷卻凝 結’進而轉變成低溫之萃取液,然不斷產生之萃取液會經 由旋繞導出管(23)、冷卻液導出孔(24)流至儲存槽(3)。 步驟四:當固體物質内具有揮發性的成份(如水份)完 全被分離後的固體物質會變成粉狀物質,然該放置於篩取 桶(51)内之粉狀物質要從篩取桶(5 1)内卸下時,可經由卸Step 3 'When the high-temperature steam continuously generated after vaporization will collect into the collection hole (21)' and enter the collection tube (21) into the multi-revolving spiral tube (22) provided in the condenser (2), when the high heat When the steam flows in the coiled pipe (22), the high-heated steam in the coiled pipe (22) can be removed through the cooling fan (11) $ circulating cooling water to remove heat, so that the high-heated steam is cooled and condensed, and then converted into low-temperature extraction. Liquid, but the continuously produced extraction liquid will flow to the storage tank (3) through the spiral outlet pipe (23) and the cooling liquid outlet hole (24). Step 4: When the volatile components (such as water) in the solid substance are completely separated, the solid substance will become a powdery substance, but the powdery substance that should be placed in the sieve barrel (51) must be removed from the sieve barrel (5 1) When unloading inside,
第16頁 555584 五、發明說明(13) " -------- 料馬達組(52)之馬達輸出動力帶動減速齒輪組,藉由 於輸出軸之1號齒輪(52&)轉動固定於萃取混合桶(5)上 互連接之2號齒輪(52b)和3號齒輪(52c),使卸料馬達纟 號齒輪(52c)嚙合於篩取桶(51)内側上方的齒條,以帶 師取桶(51)旋轉90度,使篩取桶(51)底部之9〇度扇形 料孔,與萃取混合桶(5)之9〇度扇形角卸料孔(5a)準確 準後,再將攪拌器轉動,即可將粉狀物質掉落於蒸餾 填充槽(4 )下方之卸料收集孔(4a )上。 办步驟五:當粉狀物質要從蒸餾萃取填充槽(4 )轉移至 真空冷凍櫃(7)時,則可開啟卸料閥(61)讓粉狀物質利用 ^身的重量經由卸料收集孔(4a)、卸料閥(61)直接 真空冷康櫃⑺,粉狀物質掉落完後即可關閉卸料間 (61j,開啟真空泵(79)使該真空冷凍櫃(?)壓力降低,以 得和維持真空後,透過冷凍棒(7 1 )將粉狀物質冷凍至水 ϋ i ϋ以下,因冷凍乾燥後的粉狀物質處於冰凍狀態,粉 、内部結構可以保持不變,如此也可以抑制細菌的繁 殖防止有機體的腐敗,達到保藏的效果。 =驟六:放置於真空冷凍櫃(7)中的粉狀物質,可 縮轉運泵(73)帶動貫穿於壓縮轉運泵(73)之螺桿轉 、胳亩二使螺桿轉軸(74)前端之壓縮隔板(75)往前移動, =字真空冷涞櫃⑺的内部空間縮小 質再次壓縮處理以縮小粉狀物質之體積。 观物 驟七:開啟設置於真空冷凍櫃(7)上方之真空洩壓 以將真空冷凍櫃(7 )内之壓力自動排放後,再啟Page 16 555584 V. Description of the invention (13) " -------- The motor output power of the material motor group (52) drives the reduction gear group, which is fixed by the No. 1 gear (52 &) of the output shaft. The No. 2 gear (52b) and No. 3 gear (52c) connected to the extraction mixing bucket (5), the unloading motor No. gear (52c) is meshed with the rack above the inside of the sieve barrel (51), The master take bucket (51) is rotated 90 degrees, so that the 90-degree fan-shaped material hole at the bottom of the sieve pick-up bucket (51) is accurately aligned with the 90-degree fan-shaped angle discharge hole (5a) of the extraction mixing bucket (5). Then turn the stirrer to drop the powdery substance on the discharge collecting hole (4a) under the distillation filling tank (4). Step 5: When the powdery substance is to be transferred from the distillation extraction filling tank (4) to the vacuum freezer (7), the discharge valve (61) can be opened to allow the powdery substance to use the weight of the body through the discharge collection hole (4a) The discharge valve (61) directly vacuum-cools the cold storage cabinet ⑺. After the powdery substance is dropped, the discharge room (61j) can be closed. The vacuum pump (79) is turned on to reduce the pressure of the vacuum freezer (?). After obtaining and maintaining the vacuum, the powdery substance is frozen to below ϋ i 透过 through a freezing stick (7 1). Since the powdery substance after freeze-drying is in a frozen state, the powder and internal structure can remain unchanged, which can also be suppressed. The proliferation of bacteria prevents the organism from spoiling and achieves the effect of preservation. = Step 6: The powdery substance placed in the vacuum freezer (7), the shrinkable transfer pump (73) drives the screw rotation of the compression transfer pump (73). 1. Move the compression baffle (75) at the front end of the screw shaft (74) forward, and reduce the quality of the internal space of the vacuum cold heading cabinet again to reduce the volume of the powdery substance. Open the truth set above the vacuum freezer (7) Air pressure relief to automatically discharge the pressure in the vacuum freezer (7), then start
第17頁 555584 發明說明(14) 動出料轉運泵(82)控制出料閥(81)開啟,將冷凍乾燥後之 粉狀物質輸送出真空冷凍櫃(7 )後,粉狀物質會由萃餘物 出1孔(83 )卸下至儲存袋,如此,經過壓縮處理後的粉狀 物質可以減小體積,便於運輸和後續處理(如填埋)。 步驟八:於步驟六時,當真空冷凍櫃(7)的壓縮隔板 (75)往前移動將粉狀物質體積壓縮後,可再開啟卸料閥 (61),讓粉狀物質再次進入蒸餾萃取填充槽(4),再次加 熱’使粉狀物質之揮發性的成份(如水份)更加完全的被分 離0 .步驟九:在冷凝後放置於儲存槽(3)的萃取液,可再鲁 配合開啟真空泵(79)和電磁閥(32),將儲存槽(3)中的萃 取液吸引至該真空冷凍櫃(7)後,關閉電磁閥(32)開啟卸 料閥(61)並啟動壓縮轉運泵(73)將壓縮隔板(75)移動,以 縮小真空冷凍櫃(7 )内部空間,以將真空冷凍櫃(7 )内之萃 取液擠壓至蒸餾萃取填充槽(4)進行精餾操作,該萃取液 可依使用者之需要,可擠壓二分之一(三分之一、四分之 一…專)之萃取液至蒸餾萃取填充槽(4),在實施多次交替 進行加熱汽化與冷凝後,可使不同物質儘可能地完全分 離’在擠壓二分之一之萃取液至蒸餾萃取填充槽後, 可將卸料閥(61)關閉並啟動冷凍機(76),將留至於真空冷_ 凍櫃(7 )之萃取液進行冷凍乾燥處理。 如欲使用本發明所提供之真空萃取冷凍乾燥機來萃取 液體物質(如:碘的水溶液)時,可將萃取劑(四氣化碳)、 液體物質(如:碘的水溶液)置入蒸餾萃取填充槽(4 )中的555584 Description of the invention (14) The discharge discharge pump (82) is controlled to open the discharge valve (81), and the freeze-dried powdered material is sent out of the vacuum freezer (7). The remaining material is discharged from a hole (83) to a storage bag. In this way, the powdered material after the compression treatment can be reduced in volume, which is convenient for transportation and subsequent processing (such as landfill). Step 8: At step 6, when the compression partition (75) of the vacuum freezer (7) moves forward to compress the volume of the powdery substance, the discharge valve (61) can be opened again to allow the powdery substance to enter the distillation again. Extract the filling tank (4) and reheat it to make the volatile components (such as water) of the powdery substance more completely separated. Step 9: After condensing, the extraction solution placed in the storage tank (3) can be re- Lu cooperated to open the vacuum pump (79) and the solenoid valve (32), and after the extraction liquid in the storage tank (3) was attracted to the vacuum freezer (7), the solenoid valve (32) was closed to open the discharge valve (61) and start The compression transfer pump (73) moves the compression partition (75) to reduce the internal space of the vacuum freezer (7), so as to squeeze the extraction liquid in the vacuum freezer (7) to the distillation extraction filling tank (4) for fine Distillation operation, according to the needs of the user, the extraction liquid can be squeezed to one-half (one-third, one-quarter ...) to the distillation extraction filling tank (4). After heating, vaporization and condensation, the different materials can be separated as completely as possible. A distillation of the extract to the extraction tank is filled, the discharge valve can (61) to close and start the refrigerating machine (76), as to leave the vacuum cold refrigerated _ (7) of the extract was freeze-dried. To use the vacuum extraction freeze dryer provided by the present invention to extract liquid substances (such as an aqueous solution of iodine), the extractant (four-gasified carbon) and liquid substances (such as an aqueous solution of iodine) can be placed in a distillation extraction Fill the tank (4)
第18頁 555584 五、發明說明(15)Page 18 555584 V. Description of the Invention (15)
4取桶(5 1 )’待液態萃取劑(四氯化碳)將液體物質中之可 溶性溶質溶入,然後靜置沉降後分離成為兩層液體,因幾 乎f有的礙都移到四氣化碳中,碘得以與大量的水分開, 即是由萃取劑轉變成的萃取液(碘)和液體物質轉變成的萃 餘液(水)後,啟動溫度控制器(45),將蒸氣加熱器(49)内 之電熱元件加熱,使蒸餾萃取填充槽(4 )内的沸點較低的 成份’慢慢的被加熱成高溫氣體而被分離出來,其實施之 步驟和上述之步驟二相同,待加熱後之高溫氣體可實施上 述步騍三進行冷卻收集之動作;重複步驟九之操作可將放 置於儲存槽(3 )的萃取液,經由真空冷凍組(G )、卸料閥組 (F )以及萃取混合卸料裝置(E),實施多次交替進行加熱汽 化與冷凝器組(B )之冷凝後,使不同物質儘可能地完全分 離之一精餾操作。 然如欲使用本發明之真空萃取冷凍乾燥機來蒸餾萃取 固體液體混合化合物(如含油廢水一 〇ily Wastewater)時,4Take the bucket (5 1) 'until the liquid extractant (carbon tetrachloride) dissolves the soluble solute in the liquid material, and then it is allowed to stand and settle down to separate into two layers of liquid. Due to almost any obstacles, it is moved to the four gases. In the carbonization, iodine can be separated from a large amount of water, that is, the extraction liquid (iodine) converted by the extractant and the raffinate liquid (water) converted by the liquid substance, and the temperature controller (45) is started to heat the steam. The electric heating element in the device (49) is heated, so that the components with a lower boiling point in the distillation extraction filling tank (4) are slowly heated to a high temperature gas and separated out. The implementation steps are the same as the above step two. After heating, the high-temperature gas can be cooled and collected as described in step 3; Repeat the operation in step 9 to pass the extraction liquid placed in the storage tank (3) through the vacuum freezing group (G) and the discharge valve group (F ) And extraction mixing discharge device (E), a rectification operation in which the heating and vaporization and the condensation of the condenser group (B) are alternately performed multiple times to separate the different substances as completely as possible. However, if the vacuum extraction freeze dryer of the present invention is to be used for distillation and extraction of solid-liquid mixed compounds (such as oily wastewater),
可實施上述之步驟一至步驟八之動作,將固體液體混合化 合物(如含油廢水)中的水份加熱汽化後再使用冷凝器組 (B)將之冷卻收集,而固體液體混合化合物(如含油廢水) 分離後的油化合物會變成細粉狀,可送至真空冷束組(G) 冷凍乾燥後,體積壓縮再包裝處理之。 本發明之真空萃取冷凍乾燥機之冷凝器(?)之散熱方 式除了採用散熱風扇(11)轉動螺旋槳葉帶動空氣,使空氣 流通來帶動旋繞管(22)之熱量來排放至周圍,另可使用循 環冷卻水方式來散熱,為使本發明之真空萃取冷凍乾燥機The above steps 1 to 8 can be implemented, and the water in the solid-liquid mixed compound (such as oily wastewater) is heated and vaporized, and then cooled and collected by using the condenser group (B), while the solid-liquid mixed compound (such as oil-containing wastewater) is collected. ) The separated oil compound will turn into a fine powder, which can be sent to the vacuum cold beam group (G) for freeze-drying, and then compressed and repacked. In addition to the heat dissipation method of the condenser (?) Of the vacuum extraction freeze dryer of the present invention, in addition to using a cooling fan (11) to rotate the propeller blades to drive the air, air is circulated to drive the heat of the spiral tube (22) to be discharged to the surroundings, and it can also be used. Cooling water is circulated to dissipate heat. In order to make the vacuum extraction freeze dryer of the present invention
第19頁 555584 五、發明說明(16) 如何利用循環冷卻水散熱,請參閱圖二,該冷凍機(76 ), 除了提供冷滚棒(71)之動力外,也提供了冰水储存櫃(77) 内之動力’當冰水儲水櫃(77)内的冷卻水藉由冰水泵(78) 將冰水儲水櫃(77)内之冷卻水輸送至冷凝器(2)時,能吸 ,冷凝器(2)内之旋繞管(22)之熱量,當旋繞管(22)内之 高熱蒸氣除去熱量後,高熱蒸氣會冷凝成為 =流至儲存槽⑻,然吸收完熱能之水會再移動至 堵存槽(3)内,藉由如此之一冷卻水循環方式,將可大量 吸收冷卻冷凝器組(B )的熱量。 【特點及功效】 本 及其他 餾、萃 質、液 蒸餾萃 態,且 固體物 或其他 明,惟 離本發 發 習 取 體 I ) 取 也 質 液 列 該 明 月所&供之真空萃取冷束乾燥機,與前 用技術相互比較時,更具有下列之優點·· 、配Λ本發Λ之真空萃取冷来乾燥機,能提供蒸 物ίϊ及ίΐ、冷;東乾燥等功能應用於固體物 物為以及固體液體混合化合物身上。 後,°放本置發直明*之真空萃取冷凍乾燥機,可將食品 可维持ΐί:冷來櫃中冷來’使食品處於冰束相 ΛΛ内部結構可以保持不變。 體,以延長固體物質之儲力=其除去適量的水长 詳細說明係針對本發:‘間二 例並非用以限制本;明之具體激 技藝精神所為之等 t利範圍,凡未艰 双貫施或變更,例如:真空專 555584 五、發明說明(17) 取冷床乾燥機所提供之蒸餾、萃取、乾燥、濃縮、冷滚乾 燥、體積壓縮之等效性實施例,均應包含於本案之^利範 圍中。 、 綜上所述,本案不但在空間型態上確屬創新,並能較 進上述多項功效’應已充分符 專;要件,爱依法提出申請,㈣貴局核 隹本件明專利申請案’以勵發明,至感德便。Page 19 555584 V. Description of the invention (16) How to use circulating cooling water to dissipate heat, please refer to Figure 2. In addition to the power of the cold roller (71), the freezer (76) also provides an ice water storage cabinet ( 77) Internal Power 'When the cooling water in the ice water storage tank (77) sends the cooling water in the ice water storage tank (77) to the condenser (2) by the ice water pump (78), it can absorb The heat of the coiled tube (22) in the condenser (2). When the high-heated vapor in the coiled tube (22) removes the heat, the high-heated vapor will condense to = flow to the storage tank, but the water that has absorbed the heat energy will again Moving into the holding tank (3), by such a cooling water circulation method, a large amount of heat of the cooling condenser group (B) can be absorbed. [Features and effects] This and other distillates, extracts, liquid distillation extracts, and solids or other materials, but away from the hair removal body I) take the liquid and extract the vacuum extraction cold for the Mingyue Institute & When compared with the previous technology, the beam dryer has the following advantages. It is equipped with a vacuum extraction cold-drying dryer with Λ 本 发 Λ, which can provide steamed products ίϊ and ίΐ, cold; East drying and other functions applied to solid objects The substance is a mixture of solid and liquid compounds. After that, the vacuum extraction freeze-dryer with a straight and straight-out vacuum can be used to keep the food:: Cold in the cabinet ’to keep the food in an ice bundle phase. The internal structure of ΛΛ can be maintained. System to extend the storage capacity of solid substances = its removal of an appropriate amount of water length. The detailed description is directed to the issue: 'The two cases are not intended to limit the scope; the specific scope of the specific spirit of the technical skills is equal to the scope of profit. Apply or change, for example: Vacuum 555584 V. Description of the invention (17) Equivalent embodiments of distillation, extraction, drying, concentration, cold-roll drying, and volume compression provided by the cold-bed dryer should be included in this case In the range of profits. In summary, this case is not only innovative in terms of space type, but also better than the above-mentioned multiple effects 'should have been fully qualified; requirements, love to file an application in accordance with the law, ㈣ your bureau to verify this patent application case' to Encourage invention, to the utmost.
第21頁 555584 圖式簡單說明 【圖式簡單說明】 請參閱以下有關本發明一較佳實施例之詳細說明及其 附圖,將可進一步瞭解本發明之技術内容及其目的功效; 有關該實施例之附圖為: 圖一為本發明真空萃取冷凍乾燥機之利用散熱風扇方 式之剖視前視圖; 圖二為該真空萃取冷凍乾燥機之利用循環冷卻水散熱 方式之剖視前視圖;以及 圖三為本發明真空萃取冷凍乾燥機之上旋蓋組之開啟 狀態前視圖。 【主要部分代表符號】 A 上旋蓋組 1上旋蓋 11散熱風扇 1 2上旋蓋固定座 B 冷凝器組 2 冷凝器 21收集孔 22旋繞管 23旋繞導出管 24冷卻液導出孔 C冷卻液儲存裝置 3儲存槽 31 通氣溢流孔Page 555584 Brief description of the drawings [Simplified description of the drawings] Please refer to the following detailed description of a preferred embodiment of the present invention and the accompanying drawings for further understanding of the technical content of the present invention and its purpose and effects; The drawings of the example are: FIG. 1 is a sectional front view of a vacuum extraction freeze dryer using a cooling fan method of the present invention; FIG. 2 is a sectional front view of the vacuum extraction freeze dryer using a circulating cooling water method of heat dissipation; and FIG. 3 is a front view of an open state of the capping group on the vacuum extraction freeze dryer of the present invention. [Representative symbols of main parts] A Upper screw cap group 1 Upper screw cap 11 Cooling fan 1 2 Upper screw cap holder B Condenser group 2 Condenser 21 Collection hole 22 Swivel tube 23 Swivel outlet tube 24 Coolant outlet hole C Coolant Storage device 3 Storage tank 31 Vent overflow hole
第22頁 555584 圖式簡單說明 32 D 4 4a 41 42 42a 42b 43 44 45 46 47 48 49 E 5 5a 51 52 52a 52b 52c 53 電磁閥 蒸餾萃取裝置 蒸餾萃取填充槽 卸料收集孔 窺視孔 轉軸固定座 旋蓋轉軸 掀蓋馬達 可調式安全洩壓閥 隔熱保溫層 溫度控制器 溫度感測裝置 無水感測裝置 電加熱器 蒸氣加熱器 萃取混合卸料裝置 萃取混合桶 9 0度扇形角卸料孔 篩取桶 卸料馬達組 1號齒輪 2號齒輪 3號齒輪 攪拌器組Page 22 555584 Brief description of drawings 32 D 4 4a 41 42 42a 42b 43 44 45 46 47 48 49 E 5 5a 51 52 52a 52b 52c 53 Solenoid valve distillation extraction device Distillation extraction filling tank Discharging collection hole Peephole Rotary shaft fixing seat Rotary shaft, flip-clip motor, adjustable safety pressure relief valve, thermal insulation layer, temperature controller, temperature sensing device, water-free sensing device, electric heater, steam heater extraction, mixing discharge device, extraction mixing bucket, 90 degree fan angle discharge hole screen No. 1 gear, 2 gear, 3 gear agitator
第23頁 555584 圖式簡單說明 5 3 a 5號齒輪 54攪拌馬達組 54a 4號齒輪 F卸料閥組 61 卸料閥 62卸料轉運泵 G 真空冷束組 7真空冷凍櫃 71 冷凍棒 72真空洩壓閥 73壓縮轉運泵 74 螺桿轉軸 75壓縮隔板 7 6 冷凍機 76a調節過濾器 7 7冰水儲水櫃 7 8 冰水泵 79真空泵 Η出料閥組 81出料閥 82出料轉運泵 83萃餘物出料孔Page 23 555584 Simple illustration of the diagram 5 3 a Gear 5 No. 54 Stirring Motor Group 54a Gear No. 4 F Discharge valve group 61 Discharge valve 62 Discharge transfer pump G Vacuum cold beam group 7 Vacuum freezer 71 Freezer rod 72 Vacuum Pressure relief valve 73 Compression transfer pump 74 Screw rotating shaft 75 Compression diaphragm 7 6 Freezer 76a Adjusting filter 7 7 Ice water storage tank 7 8 Ice water pump 79 Vacuum pump Η Discharge valve group 81 Discharge valve 82 Discharge transfer pump 83 Residue discharge hole
第24頁Page 24
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TW91132542A TW555584B (en) | 2002-11-01 | 2002-11-01 | Vacuum extraction freeze drying machine |
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TW91132542A TW555584B (en) | 2002-11-01 | 2002-11-01 | Vacuum extraction freeze drying machine |
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Cited By (1)
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TWI652210B (en) | 2017-11-20 | 2019-03-01 | 國璽幹細胞應用技術股份有限公司 | Smart automation storage device for bio-material |
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TWI623270B (en) * | 2016-08-30 | 2018-05-11 | 東鉅能源科技實業有限公司 | Vacuum drying-extraction system and method of manipulating the same |
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Publication number | Priority date | Publication date | Assignee | Title |
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TWI652210B (en) | 2017-11-20 | 2019-03-01 | 國璽幹細胞應用技術股份有限公司 | Smart automation storage device for bio-material |
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