SU1429922A3 - Способ борьбы с вредными насекомыми - Google Patents

Способ борьбы с вредными насекомыми Download PDF

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SU1429922A3
SU1429922A3 SU843791614A SU3791614A SU1429922A3 SU 1429922 A3 SU1429922 A3 SU 1429922A3 SU 843791614 A SU843791614 A SU 843791614A SU 3791614 A SU3791614 A SU 3791614A SU 1429922 A3 SU1429922 A3 SU 1429922A3
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halogenated
alkyl
chlorine
fluorine
hydrogen
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SU843791614A
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Кох Фолькер
Бургхардт Герхард
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Хехст Аг (Фирма)
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
    • C07D295/135—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms separated by carbocyclic rings or by carbon chains interrupted by carbocyclic rings
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C275/28—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C275/40—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton being further substituted by nitrogen atoms not being part of nitro or nitroso groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C275/28—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C275/42—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton being further substituted by carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C275/44—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups doubly-bound to carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C317/00—Sulfones; Sulfoxides
    • C07C317/26—Sulfones; Sulfoxides having sulfone or sulfoxide groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
    • C07C317/32—Sulfones; Sulfoxides having sulfone or sulfoxide groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton with sulfone or sulfoxide groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C317/34—Sulfones; Sulfoxides having sulfone or sulfoxide groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton with sulfone or sulfoxide groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having sulfone or sulfoxide groups and amino groups bound to carbon atoms of six-membered aromatic rings being part of the same non-condensed ring or of a condensed ring system containing that ring
    • C07C317/38—Sulfones; Sulfoxides having sulfone or sulfoxide groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton with sulfone or sulfoxide groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having sulfone or sulfoxide groups and amino groups bound to carbon atoms of six-membered aromatic rings being part of the same non-condensed ring or of a condensed ring system containing that ring with the nitrogen atom of at least one amino group being part of any of the groups, X being a hetero atom, Y being any atom, e.g. N-acylaminosulfones
    • C07C317/42—Y being a hetero atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/23—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
    • C07C323/39—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton at least one of the nitrogen atoms being part of any of the groups, X being a hetero atom, Y being any atom
    • C07C323/43—Y being a hetero atom
    • C07C323/44—X or Y being nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C335/00—Thioureas, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C335/04—Derivatives of thiourea
    • C07C335/16—Derivatives of thiourea having nitrogen atoms of thiourea groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C335/18—Derivatives of thiourea having nitrogen atoms of thiourea groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton being further substituted by singly-bound oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Indole Compounds (AREA)
  • Hydrogenated Pyridines (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)

Abstract

Изобретение относитс  к химичес КИМ способам защиты растений,конкретно к способу борьбы с вредными насекомыми . Изобретение позвол ет повысить на 30-40% инсектицидное действие за счет использовани  в дозе 0,01-1 кг/га соединени  формулы R.R,2.C6H4CXNCONHC HR,, где R, - хлор, фтор; R,j, - водород, хлор, фтор; R, - водород, фтор; R - водород, хлор, OCF,j,CHClF; Rj хлор, фтор, трифторметил, окситрифторметнп, OCClFj , .2, OCFaCHClF, OCF CHFCF,-, Rg - водород, хлор; X -.метокси, эток- си, 0(CHi)2CH,, 0(СН21зСНз. 2 табл.

Description

Изобретение относитс  к химическим способам защиты растений, конкретно к способу борьбы с вредными насекомыми .
Цель изобретени  - усиление инсектицидного действи .
Пример 1о Смесь 11,95 г (30 ммоль) 6-(2,6-дифторфенил)-3-(А- трифторметоксифенил)19253,47тетра- Ю ГНДРО-2Н, 4Н-1j3,5 оксадиазин-2,4- диона и 100 мг этилата натри  кип т т в течение 4 ч в 50 мл абсолютного эта- нола, затем охлаждают ее до комнатной температуры, разбавл ют водой и отса-15 сывают выпавший осадок, который высушивают и подвергают кристаллизации из н-гексана.
Выход искомого соединени  3 (табло1у 5 г (43%), 90-93°С„20
Другие соединени  1-19 получают аналогичным образом, данные о соединени х 1-19, используемых в предлагаемом способе, представлены в табл.1.
25
Пример 2, (проведение биологи ческих испытаний). В колбы Эрленмейера заливают водные препараты активного вещества нужной концентрации и затем помещают в них 24-дневные личинки маров - переносчиков желтой лихорадки (Aedes agupti),
Через определенное врем  (вплоть до момента по влени  из личинок комаров ) определ ют процентное количест-. во погибших личинок и соответственно количество по вившихс  комаров.
При этом 100% означает 100%-ную гибель.личинок или отсутствие вылупив35
шихс  комаров. Результаты испытаний приведены в табл.2, где дл  сравнени  представлены данные испытаний известных соединений, близких по структуре, и указаны дозы соединений (кг/га), в пересчете на разбрызгиваемый бульон. При дозе активного вещества 1 кг/га предлагаемый способ на 30-40% эффективнее известных.

Claims (1)

  1. Формула изобретени 
    Способ борьбы с вредными насекомыми путем обработки их эфиром боксиимидной кислоты, отличающийс  тем, что, с целью усил€--и  инсектицидного действи , в качестве эфира карбоксиимидной кислоты используют соединение общей формулы
    (OL С N-СО - TSIH нбьв 5
    tBS Кц
    где R, - хлор, фтор;
    Rj - водород, хлор, фтор;
    R, - водород, фтор;
    R4 - водород, хлор, OCF CHCIF ;
    Rj --хлор, фтор, трифторметил, окситрифторметил, OCCIF , ,, . OCFjCHClF, OCFj,CHFCF,;
    Rg - водород, хлор;
    X - меток си, этокси, 0(СН,2)СН, 0(СН)СН5, в дозе 0,01-1 кг/га.
    Т а б л и ц а 1
    А - дифлюбензурон формулы (по за вке ФРГ № 2123236)
    ОУ-С О-ТШ-СО -
    Ь - соединение формулы
    (по патенту ША W 4200653)
    I
    O-CgHs -C N-CO№l- §)-С1
    Р
    ВНИИПИ Заказ 5149/58
    Произв.-полигр. пр-тие, г. Ужгород, ул. Проектна , 4
    Тираж 455
    Подписное
SU843791614A 1983-09-22 1984-09-20 Способ борьбы с вредными насекомыми SU1429922A3 (ru)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19833334207 DE3334207A1 (de) 1983-09-22 1983-09-22 Neue n-(thio)carbamylarylcarboximido(thio)ester, verfahren zu ihrer herstellung, sie enthaltende mittel und ihre verwendung als schaedlingsbekaempfungsmittel

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SU1429922A3 true SU1429922A3 (ru) 1988-10-07

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US (1) US4769481A (ru)
EP (1) EP0135894B1 (ru)
JP (1) JPS6089465A (ru)
KR (1) KR850002463A (ru)
AT (1) ATE45729T1 (ru)
AU (1) AU561422B2 (ru)
BR (1) BR8404767A (ru)
CA (1) CA1234819A (ru)
DD (1) DD232422A5 (ru)
DE (2) DE3334207A1 (ru)
DK (1) DK452784A (ru)
ES (1) ES536086A0 (ru)
GR (1) GR80435B (ru)
HU (1) HU195636B (ru)
IL (1) IL73022A (ru)
MA (1) MA20235A1 (ru)
NZ (1) NZ209610A (ru)
OA (1) OA07821A (ru)
PH (1) PH19899A (ru)
PL (1) PL140688B1 (ru)
PT (1) PT79255A (ru)
SU (1) SU1429922A3 (ru)
TR (1) TR21974A (ru)
ZA (1) ZA847439B (ru)
ZW (1) ZW16284A1 (ru)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IE58417B1 (en) * 1984-04-27 1993-09-22 Ici Plc Chemical derivatives
EP0199945A3 (de) * 1985-03-23 1988-08-03 Hoechst Aktiengesellschaft Neue Carbamoylarylcarboximidsäureester, Verfahren zu ihrer Herstellung, sie enthaltende Mittel und ihre Verwendung als Schädlingsbekämpfungsmittel
DE3514450A1 (de) * 1985-04-22 1986-10-23 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von imidaten sowie neue arylsubstituierte imidate
DE3613062A1 (de) * 1986-04-18 1987-10-29 Hoechst Ag N-benzoyl-n'-phenyl(thio)harnstoffe, verfahren zu ihrer herstellung und ihre verwendung als schaedlingsbekaempfungsmittel
DE3711460A1 (de) * 1987-04-04 1988-10-13 Hoechst Ag Verfahren zur herstellung von ortho-substituierten arylcarboximido-estern
DE3741062A1 (de) * 1987-12-04 1989-08-31 Hoechst Ag (thio)benzoylharnstoffe und deren funktionelle derivate, verfahren zu ihrer herstellung, sie enthaltende mittel und ihre verwendung als schaedlingsbekaempfungsmittel
US5139785A (en) * 1988-03-26 1992-08-18 Hoechst Aktiengesellschaft Pesticides
AU2002360729A1 (en) 2001-12-21 2003-07-30 Pharmacia Corporation Aromatic thioether liver x-receptor modulators
EP1511723A1 (en) 2002-05-24 2005-03-09 Pharmacia Corporation Sulfone liver x-receptor modulators
MXPA04011691A (es) 2002-05-24 2005-09-12 Pharmacia Corp Moduladores del receptor x anilino hepaticos.
HUE059057T2 (hu) 2017-05-04 2022-10-28 Bayer Cropscience Ag 2-{[2-(feniloximetil)piridin-5-il]oxi}-etánamin-származékok és rokon vegyületek mint peszticidek, például növényvédelemre

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US3742000A (en) * 1969-06-03 1973-06-26 Grace W R & Co Imidoether and amidine derivatives of substituted fatty amides
EP0005944B1 (en) * 1978-06-02 1983-03-16 Imperial Chemical Industries Plc Substituted benzoylimidates, their preparation and compositions comprising them for insecticidal use
US4431667A (en) * 1981-12-04 1984-02-14 The Upjohn Company Imino ethers useful for controlling insect and arachnoid pests

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
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, За вка DE № 2123236, КЛ..С 07 С 127/16, опублик. 1971. Патент ША W 4200653, кл. С 07 С 127/19, опублик. 1980. *

Also Published As

Publication number Publication date
AU3341884A (en) 1985-03-28
DE3479496D1 (de) 1989-09-28
EP0135894B1 (de) 1989-08-23
US4769481A (en) 1988-09-06
HUT36086A (en) 1985-08-28
EP0135894A2 (de) 1985-04-03
ES8505648A1 (es) 1985-06-16
CA1234819A (en) 1988-04-05
IL73022A0 (en) 1984-12-31
DE3334207A1 (de) 1985-04-04
DK452784D0 (da) 1984-09-21
ES536086A0 (es) 1985-06-16
ZA847439B (en) 1985-05-29
BR8404767A (pt) 1985-08-13
OA07821A (fr) 1986-11-20
ZW16284A1 (en) 1985-04-10
DD232422A5 (de) 1986-01-29
HU195636B (en) 1988-06-28
JPS6089465A (ja) 1985-05-20
JPH0240064B2 (ru) 1990-09-10
PH19899A (en) 1986-08-13
IL73022A (en) 1991-03-10
NZ209610A (en) 1988-06-30
PT79255A (de) 1984-10-01
PL249691A1 (en) 1985-08-27
EP0135894A3 (en) 1985-12-18
PL140688B1 (en) 1987-05-30
MA20235A1 (fr) 1985-04-01
AU561422B2 (en) 1987-05-07
ATE45729T1 (de) 1989-09-15
KR850002463A (ko) 1985-05-13
DK452784A (da) 1985-03-23
GR80435B (en) 1985-01-21
TR21974A (tr) 1985-12-12

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