SA518391325B1 - عمليات لإنتاج حمض أسيتيك - Google Patents

عمليات لإنتاج حمض أسيتيك

Info

Publication number
SA518391325B1
SA518391325B1 SA518391325A SA518391325A SA518391325B1 SA 518391325 B1 SA518391325 B1 SA 518391325B1 SA 518391325 A SA518391325 A SA 518391325A SA 518391325 A SA518391325 A SA 518391325A SA 518391325 B1 SA518391325 B1 SA 518391325B1
Authority
SA
Saudi Arabia
Prior art keywords
acetic acid
lithium
withdrawn
vapor sidedraw
producing acetic
Prior art date
Application number
SA518391325A
Other languages
English (en)
Inventor
دي شافر رونالد
او سكاتس مارك
ليو ياو-هوا
Original Assignee
سيلانيز انترناشونال كوربوريشن
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by سيلانيز انترناشونال كوربوريشن filed Critical سيلانيز انترناشونال كوربوريشن
Publication of SA518391325B1 publication Critical patent/SA518391325B1/ar

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/445Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by steam distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/47Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08Acetic acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

يتعلق الكشف الحالي بعملية لإنتاج حمض اسيتيك acetic acid وفيها يتم سحب مخرج سحب جانبي بخاري vapor sidedraw من العمود الثاني second column في سلسلة التنقية الأولية primary purification train. يتضمن مخرج السحب الجانبي البخاري vapor sidedraw حمض اسيتيك acetic acid ومركبات تشتمل على ليثيوم lithium بتركيز لا يتعدى 100 جزء وزن لكل بليون Weight Parts Per Billion (wppb). كما يتم سحب تيار مواد مترسبة غني بمركبات تشتمل على الليثيوم lithium ، مثل اسيتات ليثيوم lithium acetate ، أو داي هيدرات اسيتات ليثيوم lithium acetate dihydrate ، من العمود الثاني second column. على نحو ملائم ، يتم تغذية مخرج السحب البخاري vapor sidedraw ، أو قسم مكثف منه، مباشرة إلى راتين resin تبادل أيوني ion يحدث به استبدال بفلز metal به مواقع تبادل كاتيوني حمضي acid cation للحصول على حمض اسيتيك منقى acetic acid. هذا يمنع استبدال الفلزات metals في راتينج التبادل الأيوني ion exchange resin. شكل 1.
SA518391325A 2015-11-13 2018-04-11 عمليات لإنتاج حمض أسيتيك SA518391325B1 (ar)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562255049P 2015-11-13 2015-11-13
US15/348,338 US9957216B2 (en) 2015-11-13 2016-11-10 Processes for producing acetic acid
PCT/US2016/061555 WO2017083668A1 (en) 2015-11-13 2016-11-11 Processes for producing acetic acid

Publications (1)

Publication Number Publication Date
SA518391325B1 true SA518391325B1 (ar) 2022-08-11

Family

ID=58689815

Family Applications (1)

Application Number Title Priority Date Filing Date
SA518391325A SA518391325B1 (ar) 2015-11-13 2018-04-11 عمليات لإنتاج حمض أسيتيك

Country Status (9)

Country Link
US (1) US9957216B2 (ar)
EP (1) EP3374342B1 (ar)
JP (1) JP7014365B2 (ar)
CN (1) CN108349865B (ar)
ES (1) ES2820571T3 (ar)
RS (1) RS60748B1 (ar)
SA (1) SA518391325B1 (ar)
SG (1) SG11201802063XA (ar)
WO (1) WO2017083668A1 (ar)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3392233B1 (en) * 2017-03-08 2020-07-22 Daicel Corporation Method for producing acetic acid
US10457622B2 (en) 2017-03-08 2019-10-29 Daicel Corporation Method for producing acetic acid

Family Cites Families (63)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3769329A (en) 1970-03-12 1973-10-30 Monsanto Co Production of carboxylic acids and esters
BE791577A (fr) 1971-11-19 1973-05-17 Monsanto Co Purification de courants d'acide carboxylique
US4302432A (en) 1980-11-21 1981-11-24 Eastman Kodak Company Preparation of hydrogen iodide, lithium iodide and methyl iodide
DE3107731A1 (de) 1981-02-28 1982-09-16 Basf Ag, 6700 Ludwigshafen Verfahren zur abtrennung organischer jod-verbindungen von carbonylierungsprodukten des methanols, methylacetates und dimethylethers
NZ203226A (en) 1982-02-13 1985-08-30 Bp Chemical Ltd Production of acetic anhydride from methanol and carbon monoxide
US4792620A (en) 1983-10-14 1988-12-20 Bp Chemicals Limited Carbonylation catalysts
US5026908A (en) 1984-05-03 1991-06-25 Hoechst Celanese Corporation Methanol carbonylation process
CA1228867A (en) 1984-05-03 1987-11-03 G. Paull Torrence Methanol carbonylation process
US5001259A (en) 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
US5144068A (en) 1984-05-03 1992-09-01 Hoechst Celanese Corporation Methanol carbonylation process
US4615806B1 (en) 1985-03-07 1994-05-03 Hoechst Co American Removal of iodide compounds from non-aqueous organic media
US4894477A (en) 1986-10-14 1990-01-16 Hoechst Celanese Corporation Process for regenerating a carbonylation catalyst solution to remove corrosion metals and carbonylation of methanol to acetic acid
US5220058A (en) 1991-09-30 1993-06-15 Union Carbide Chemicals & Plastics Technology Corporation Iodide removal process
GB9122168D0 (en) * 1991-10-18 1991-11-27 Bp Chem Int Ltd Process
GB9211671D0 (en) 1992-06-02 1992-07-15 Bp Chem Int Ltd Process
US5672743A (en) 1993-09-10 1997-09-30 Bp Chemicals Limited Process for the production of acetic acid
JP3377555B2 (ja) 1993-05-31 2003-02-17 ダイセル化学工業株式会社 カルボニル化反応生成物に含有されるヨウ素化合物の除去方法
JP3244385B2 (ja) 1994-06-15 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
JP3306227B2 (ja) 1994-07-06 2002-07-24 ダイセル化学工業株式会社 酢酸および/または無水酢酸の製造法
SG44317A1 (en) 1994-06-15 1997-12-19 Daicel Chem Process for producing high purity acetic acid
US5696284A (en) 1995-06-21 1997-12-09 Bp Chemicals Limited Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof
AU702225B2 (en) * 1995-10-27 1999-02-18 Hoechst Celanese Corporation Process for improving productivity of a carbonylation catalyst solution by removing corrosion metals
US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
IN192600B (ar) 1996-10-18 2004-05-08 Hoechst Celanese Corp
GB9625335D0 (en) 1996-12-05 1997-01-22 Bp Chem Int Ltd Process
GB9626429D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626428D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626317D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
US6066762A (en) 1996-12-30 2000-05-23 Chiyoda Corporation Process for the production of carbonyl compound
JPH10231267A (ja) 1997-02-19 1998-09-02 Chiyoda Corp 有機カルボン酸の製造方法
US5962735A (en) 1998-03-06 1999-10-05 Uop Llc Method for treating an organic liquid contaminated with an iodide compound
US6303813B1 (en) 1999-08-31 2001-10-16 Celanese International Corporation Rhodium/inorganic iodide catalyst system for methanol carbonylation process with improved impurity profile
US6323364B1 (en) 1999-08-31 2001-11-27 Celanese International Corporation Rhodium/inorganic iodide catalyst system for methanol carbonylation process with improved impurity profile
US6225498B1 (en) 2000-03-24 2001-05-01 Celanese International Corporation Method of removing organic iodides from organic media
CN1117628C (zh) 2000-10-24 2003-08-13 中国科学院化学研究所 均相甲醇羰基化反应双金属催化剂及其制法
US6657078B2 (en) 2001-02-07 2003-12-02 Celanese International Corporation Low energy carbonylation process
US6677480B2 (en) 2002-01-28 2004-01-13 Celanese International Corporation Process control in production of acetic acid via use of heavy phase density measurement
GB0213485D0 (en) 2002-06-12 2002-07-24 Bp Chem Int Ltd Process
JP2004131389A (ja) 2002-10-08 2004-04-30 Daicel Chem Ind Ltd カルボン酸の製造方法及び製造システム
US7005541B2 (en) 2002-12-23 2006-02-28 Celanese International Corporation Low water methanol carbonylation process for high acetic acid production and for water balance control
CN1270825C (zh) 2004-01-09 2006-08-23 中国科学院化学研究所 一种正负离子型双金属催化剂及制备方法和应用
US7223883B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7223886B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
JP5075336B2 (ja) 2004-12-20 2012-11-21 株式会社ダイセル 酢酸の製造方法
JP4526381B2 (ja) * 2004-12-27 2010-08-18 ダイセル化学工業株式会社 酢酸の製造方法
US7855306B2 (en) 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
CN101223124B (zh) 2005-07-14 2011-05-04 大赛璐化学工业株式会社 生产羧酸的方法
CN100411738C (zh) 2006-04-10 2008-08-20 中国科学院化学研究所 有机金属锂盐为配体的铑催化剂
US20090156859A1 (en) * 2007-05-21 2009-06-18 Scates Mark O Control of impurities in product glacial acetic acid of rhodium-catalyzed methanol carbonylation
US20090187043A1 (en) 2007-05-21 2009-07-23 Scates Mark O Control of impurities in product glacial acetic acid of rhodium-catalyzed methanol carbonylation
US20090209786A1 (en) * 2007-05-21 2009-08-20 Scates Mark O Control of impurities in product glacial acetic acid of rhodium-catalyzed methanol carbonylation
US7884237B2 (en) 2008-11-07 2011-02-08 Celanese International Corp. Methanol carbonylation with improved aldehyde removal
US8168822B2 (en) 2009-07-07 2012-05-01 Celanese International Corporation Acetic acid production by way of carbonylation with enhanced reaction and flashing
US8889904B2 (en) 2010-05-18 2014-11-18 Celanese International Corporation Processes for producing acetic acid
WO2012014393A1 (en) 2010-07-26 2012-02-02 Daicel Chemical Industries, Ltd. Process for producing acetic acid
MY160523A (en) 2010-10-06 2017-03-15 Daicel Corp Process for producing acetic acid
MX340955B (es) 2010-12-15 2016-07-29 Daicel Corp Procedimiento para producir acido acetico.
MX340954B (es) 2010-12-15 2016-07-29 Daicel Corp Procedimiento para producir acido acetico.
EP2653458B2 (en) 2010-12-15 2021-03-17 Daicel Corporation Process for producing acetic acid
US9776944B2 (en) 2010-12-24 2017-10-03 Daicel Corporation Process for producing acetic acid
TWI547477B (zh) 2012-03-14 2016-09-01 大賽璐股份有限公司 醋酸之製造方法
AR094541A1 (es) 2013-01-25 2015-08-12 Daicel Corp Procedimiento para producir ácido carboxílico
CN104689854B (zh) 2015-01-07 2017-05-24 江苏索普(集团)有限公司 一种甲醇羰基化合成醋酸的催化剂体系及其应用

Also Published As

Publication number Publication date
CN108349865A (zh) 2018-07-31
KR20180081707A (ko) 2018-07-17
SG11201802063XA (en) 2018-05-30
ES2820571T3 (es) 2021-04-21
US20170137361A1 (en) 2017-05-18
CN108349865B (zh) 2021-05-11
JP7014365B2 (ja) 2022-02-01
EP3374342B1 (en) 2020-07-08
RS60748B1 (sr) 2020-10-30
US9957216B2 (en) 2018-05-01
WO2017083668A1 (en) 2017-05-18
JP2018535220A (ja) 2018-11-29
EP3374342A1 (en) 2018-09-19

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