RU2004108028A - Горизонтальный химический ректор, в частности, для синтеза метанола - Google Patents
Горизонтальный химический ректор, в частности, для синтеза метанола Download PDFInfo
- Publication number
- RU2004108028A RU2004108028A RU2004108028/15A RU2004108028A RU2004108028A RU 2004108028 A RU2004108028 A RU 2004108028A RU 2004108028/15 A RU2004108028/15 A RU 2004108028/15A RU 2004108028 A RU2004108028 A RU 2004108028A RU 2004108028 A RU2004108028 A RU 2004108028A
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- Prior art keywords
- reactor according
- catalyst
- reactor
- gas
- supporting element
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Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
- F28D7/10—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being arranged one within the other, e.g. concentrically
- F28D7/12—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being arranged one within the other, e.g. concentrically the surrounding tube being closed at one end, e.g. return type
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
- B01J8/0085—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction promoting uninterrupted fluid flow, e.g. by filtering out particles in front of the catalyst layer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
- B01J8/0476—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds
- B01J8/0484—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds the beds being placed next to each other
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0496—Heating or cooling the reactor
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C07C29/152—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the reactor used
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
- F28D7/06—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits having a single U-bend
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00203—Coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/0053—Controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00796—Details of the reactor or of the particulate material
- B01J2208/00805—Details of the particulate material
- B01J2208/00814—Details of the particulate material the particulate material being provides in prefilled containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00796—Details of the reactor or of the particulate material
- B01J2208/00884—Means for supporting the bed of particles, e.g. grids, bars, perforated plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/18—Details relating to the spatial orientation of the reactor
- B01J2219/182—Details relating to the spatial orientation of the reactor horizontal
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F2280/00—Mounting arrangements; Arrangements for facilitating assembling or disassembling of heat exchanger parts
- F28F2280/02—Removable elements
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Thermal Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Fluid Mechanics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Claims (16)
1. Горизонтальный химический реактор, содержащий по меньшей мере один горизонтально расположенный в реакторе слой (5a-5d) катализатора с нижней газопроницаемой стенкой (6) для выхода газа и поддерживающий по меньшей мере один слой (5a-5d) катализатора элемент (2), отличающийся тем, что он имеет уплотнение (20) катализатора, содержащее несущий элемент (21), который крепится к поддерживающему элементу (2) ниже нижней газопроницаемой стенки (6), соединительный элемент (22), который одним концом (22а) крепится к несущему элементу (21), на промежуточный участок (22b) которого опирается боковой край нижней газопроницаемой стенки (6), и множество наполнителей (23) определенного размера, которые расположены между боковым краем нижней газопроницаемой стенки (6) и внутренней стенкой поддерживающего элемента (2), опорой которых служит участок (22с) соединительного элемента (22), расположенный между его промежуточным участком (22b) и внутренней стенкой поддерживающего элемента (2).
2. Реактор по п.1, отличающийся тем, что соединительный элемент (22) имеет Г-образную форму.
3. Реактор по п.1, отличающийся тем, что соединительный элемент (22) не крепится неподвижно к несущему элементу (21).
4. Реактор по п.3, отличающийся тем, что один край (33а) соединительного элемента (22) вставляется в прорезь (21а) несущего элемента (21).
5. Реактор по п.1, отличающийся тем, что наполнители (23) представляют собой шарики, изготовленные из инертного материала, например из керамики или металла.
6. Реактор по п.1, отличающийся тем, что наполнители (23) сверху закрыты проволочной сеткой (24).
7. Реактор по п.1, отличающийся тем, что поддерживающий элемент (2) представляет собой патрон, расположенный в корпусе реактора.
8. Реактор по п.1, отличающийся тем, что поддерживающий элемент (2) представляет собой наружный корпус (2) реактора, по существу, цилиндрической формы, в котором расположено по меньшей мере два горизонтальных примыкающих друг к другу слоя (5a-5d) катализатора с нижней газопроницаемой стенкой (6) для выхода газа, между которыми расположена по меньшей мере одна полость (10а-10с), доступ к которой возможен с внешней стороны корпуса (2), которая образует между слоями (5a-5d) катализатора канал для прохода газа, входящий в эту полость и выходящий из нее через соответствующее отверстие (12а, 13а...12с, 13с), в которой установлено съемное устройство (14) охлаждения, предназначенное для косвенного охлаждения протекающих между слоями (5a-5d) катализатора газов.
9. Реактор по п.8, отличающийся тем, что по меньшей мере два имеющихся в нем слоя (5a-5d) катализатора расположены рядом друг с другом.
10. Реактор по п.8, отличающийся тем, что он имеет несколько свободных зон (9a-9h) для прохода газов из слоя катализатора и в слой катализатора (5a-5d), расположенных между внутренней стенкой корпуса (2) и противоположными верхней и нижней поверхностями (7, 6) слоев катализатора.
11. Реактор по п.10, отличающийся тем, что отверстия (12а, 13а...12с, 13с) для входа и выхода газов по меньшей мере из одной полости (10а-10с) соединяют эту полость с соответствующей свободной зоной (9a-9h).
12. Реактор по п.8, отличающийся тем, что по меньшей мере одна расположенная между соседними слоями катализатора полость (10а-10с) имеет, по существу, цилиндрическую форму.
13. Реактор по п.8, отличающийся тем, что устройство охлаждения содержит по меньшей мере один котел (14), предназначенный для получения водяного пара высокого давления.
14. Реактор по п.8, отличающийся тем, что котел (14) выполнен в виде трубчатого теплообменника с пучком труб и трубной решеткой или в виде теплообменника байонетного типа.
15. Реактор по п.14, отличающийся тем, что котел (14) выполнен в виде теплообменника с естественной или принудительной циркуляцией.
16. Реактор по п.8, отличающийся тем, что устройство охлаждения содержит по меньшей мере один газовый теплообменник (14).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN03107444 | 2003-03-20 | ||
CN03107444.8 | 2003-03-20 |
Publications (1)
Publication Number | Publication Date |
---|---|
RU2004108028A true RU2004108028A (ru) | 2005-09-10 |
Family
ID=32831754
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
RU2004108028/15A RU2004108028A (ru) | 2003-03-20 | 2004-03-19 | Горизонтальный химический ректор, в частности, для синтеза метанола |
Country Status (7)
Country | Link |
---|---|
US (1) | US7279138B2 (ru) |
EP (1) | EP1464384B1 (ru) |
AT (1) | ATE302057T1 (ru) |
AU (1) | AU2004201132A1 (ru) |
DE (1) | DE602004000055T2 (ru) |
DK (1) | DK1464384T3 (ru) |
RU (1) | RU2004108028A (ru) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6983852B2 (en) * | 2002-10-10 | 2006-01-10 | Specialized Tech Inc. | Desanding apparatus and system |
EP2292326A1 (en) * | 2009-09-02 | 2011-03-09 | Methanol Casale S.A. | Vertical isothermal shell-and-tube reactor |
WO2012077143A1 (en) | 2010-12-09 | 2012-06-14 | Provides Metalmeccanica S.R.L. | Heat exchanger |
US9938812B2 (en) | 2012-02-13 | 2018-04-10 | Specialized Desanders Inc. | Desanding apparatus and a method of using same |
US9327214B2 (en) | 2012-02-13 | 2016-05-03 | Specialized Desanders Inc. | Desanding apparatus and a method of using same |
US9909405B2 (en) | 2012-02-13 | 2018-03-06 | Specialized Desanders Inc. | Desanding apparatus and a method of using same |
CA2836437A1 (en) | 2013-12-16 | 2015-06-16 | Specialized Desanders Inc. | An desanding apparatus and a method of using the same |
EP2957339A1 (en) | 2014-06-17 | 2015-12-23 | Casale SA | Radial flow horizontal catalytic reactor |
US10076739B1 (en) | 2014-07-22 | 2018-09-18 | Precision Combustion, Inc. | Chemical reactor for use with overly reactive chemicals |
EP3400098B1 (en) | 2016-01-07 | 2019-12-04 | Total Raffinage Chimie | Supported indium oxide catalyst and process for methanol synthesis using the same |
WO2017118573A1 (en) | 2016-01-07 | 2017-07-13 | Total Research & Technology Feluy | Process for methanol synthesis using an indium oxide based catalyst |
DE102017203058A1 (de) * | 2017-02-24 | 2018-08-30 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Wärmeübertrager und Reaktor |
WO2018210826A1 (en) | 2017-05-17 | 2018-11-22 | Total Research & Technology Feluy | Process for ethylene aromatisation from diluted stream |
EP3404005A1 (en) | 2017-05-17 | 2018-11-21 | Total Research & Technology Feluy | Process for ethylene oligomerisation from diluted stream |
WO2018210827A1 (en) | 2017-05-17 | 2018-11-22 | Total Research & Technology Feluy | Mto-ocp upgrading process to maximize the selectivity to propylene |
EP3593900A1 (en) | 2018-07-10 | 2020-01-15 | Total Raffinage Chimie | Copper-iron-based catalytic composition for the conversion of syngas to higher alcohols and process using such catalyst composition |
US11491468B2 (en) | 2018-09-06 | 2022-11-08 | Total Se | Noble metal promoted supported indium oxide catalyst for the hydrogenation of CO2 to methanol and process using said catalyst |
WO2020157049A1 (en) | 2019-02-01 | 2020-08-06 | Total S.A. | Process using catalytic composition for the conversion of syngas to higher alcohols |
WO2020157057A1 (en) | 2019-02-01 | 2020-08-06 | Total S.A. | Copper-iron-based catalytic composition comprising zeolites, method for producing such catalytic composition and process using such catalytic composition for the conversion of syngas to higher alcohols |
CN116457325B (zh) | 2020-11-17 | 2024-07-02 | 道达尔能源一技术 | 用于由富co2合成气合成甲醇的工艺 |
DE102022131061A1 (de) | 2022-11-23 | 2024-05-23 | PACE-Tec GmbH | Vorrichtung zum Behandeln, Spülvorrichtung zum Spülen und Trocknungsvorrichtung zum Trocknen von partikelförmigen Feststoffen sowie Verfahren zum Behandeln, Spülen und/oder Trocknen von derartigen Feststoffen |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2483178A (en) * | 1946-07-29 | 1949-09-27 | Phillips Petroleum Co | Catalyst vessel |
US2505850A (en) * | 1946-08-20 | 1950-05-02 | Phillips Petroleum Co | Seal slot for catalyst bed screens in catalyst chambers |
GB670299A (en) | 1948-11-02 | 1952-04-16 | Metallgesellschaft Ag | Process of and apparatus for producing hydrocarbons |
AT306745B (de) | 1971-05-24 | 1973-04-25 | Chemie Linz Ag | Vorrichtung zur Durchführung von Hochdrucksynthesen, beispielsweise der Ammoniaksynthese |
RO58713A2 (ro) | 1972-04-24 | 1975-08-26 | Inst De Proiectare Tehnologica | Aparat multifunctional pentru materiale pulverulente |
DE2449789B1 (de) | 1974-10-19 | 1976-03-11 | Deggendorfer Werft Eisenbau | Mehrstufiger Horden-Reaktor |
DE3310772A1 (de) | 1983-03-24 | 1984-09-27 | Interatom Internationale Atomreaktorbau Gmbh, 5060 Bergisch Gladbach | Methanol-synthese-reaktor mit niedrig siedendem kuehlmittel |
US4919909A (en) * | 1984-12-03 | 1990-04-24 | Societe Chimique De La Grande Paroisse | Reactor for catalytic synthesis and process for using the reactor |
US4696799A (en) | 1986-07-15 | 1987-09-29 | The M. W. Kellogg Company | Ammonia synthesis converter |
WO1995024961A1 (en) * | 1994-03-14 | 1995-09-21 | Methanol Casale S.A. | Horizontal reactor for heterogeneous exothermic synthesis, in particular for methanol synthesis |
ZA955492B (en) * | 1994-07-18 | 1996-02-13 | Methanol Casale Sa | Catalyst-seal support device in particular for exothermic heterogeneous catalytic synthesis reactors |
GB2329597B (en) * | 1995-02-15 | 1999-08-11 | Air Liquide | Arrangement of a retaining grille of an active material in a vessel,and a vessel so equipped |
US6132687A (en) * | 1998-05-21 | 2000-10-17 | Kellogg Brown & Root, Inc. | Horizontal ammonia converter adapted for high activity catalyst |
-
2004
- 2004-03-16 DE DE602004000055T patent/DE602004000055T2/de not_active Expired - Lifetime
- 2004-03-16 EP EP04006216A patent/EP1464384B1/en not_active Expired - Lifetime
- 2004-03-16 AT AT04006216T patent/ATE302057T1/de not_active IP Right Cessation
- 2004-03-16 DK DK04006216T patent/DK1464384T3/da active
- 2004-03-19 RU RU2004108028/15A patent/RU2004108028A/ru not_active Application Discontinuation
- 2004-03-19 AU AU2004201132A patent/AU2004201132A1/en not_active Abandoned
- 2004-03-19 US US10/804,896 patent/US7279138B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
DK1464384T3 (da) | 2005-12-27 |
US20040184976A1 (en) | 2004-09-23 |
EP1464384B1 (en) | 2005-08-17 |
DE602004000055D1 (de) | 2005-09-22 |
EP1464384A1 (en) | 2004-10-06 |
DE602004000055T2 (de) | 2006-06-29 |
US7279138B2 (en) | 2007-10-09 |
ATE302057T1 (de) | 2005-09-15 |
AU2004201132A1 (en) | 2004-10-07 |
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