PL442831A1 - Method of depositing thermal insulation layers on glass - Google Patents

Method of depositing thermal insulation layers on glass

Info

Publication number
PL442831A1
PL442831A1 PL442831A PL44283122A PL442831A1 PL 442831 A1 PL442831 A1 PL 442831A1 PL 442831 A PL442831 A PL 442831A PL 44283122 A PL44283122 A PL 44283122A PL 442831 A1 PL442831 A1 PL 442831A1
Authority
PL
Poland
Prior art keywords
sub
zinc
thermal insulation
aluminum
glass
Prior art date
Application number
PL442831A
Other languages
Polish (pl)
Inventor
Bartłomiej WITKOWSKI
Aleksandra Seweryn
Marek GODLEWSKi
Piotr Sybilski
Original Assignee
Instytut Fizyki Polskiej Akademii Nauk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Instytut Fizyki Polskiej Akademii Nauk filed Critical Instytut Fizyki Polskiej Akademii Nauk
Priority to PL442831A priority Critical patent/PL442831A1/en
Publication of PL442831A1 publication Critical patent/PL442831A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/30Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
    • C23C16/40Oxides
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/30Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
    • C23C16/40Oxides
    • C23C16/407Oxides of zinc, germanium, cadmium, indium, tin, thallium or bismuth

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Vapour Deposition (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób osadzania na szybach, metodą ALD, warstw termoizolacyjnych z tlenku cynku domieszkowanego glinem (AZO). W sposobie tym, oczyszczoną szybę, na której ma zostać nałożona warstwa termoizolacyjna umieszcza się w reaktorze ALD. Następnie wnętrze reaktora wraz z szybą podgrzewa do temperatury 50°C - 300°C i w tej temperaturze, w co najmniej 40 powtórzeniach sekwencji, gdzie po jednym cyklu glinowym (Al<sub>2</sub>O<sub>3</sub>) następuje 10 — 30 cykli cynkowych (ZnO) lub po 10 — 30 cyklach cynkowych (ZnO) następuje jeden cykl glinowy (Al<sub>2</sub>O<sub>3</sub>) prowadzi się wzrost warstwy termoizolacyjnej. Korzystnie jest jeżeli prekursorem glinowym jest TMA, prekursorem cynkowym jest DEZn — dietylocynk lub DMZn — dimetylocynk i jeżeli prekursorem tlenu jest woda lub ozon.The subject of the application is a method of depositing thermal insulating layers of zinc oxide doped with aluminum (AZO) on windows using the ALD method. In this method, the cleaned glass on which the thermal insulation layer is to be applied is placed in the ALD reactor. Then the interior of the reactor together with the glass is heated to a temperature of 50°C - 300°C and at this temperature, in at least 40 repetitions of the sequence, where after one aluminum cycle (Al<sub>2</sub>O<sub>3</sub >) 10 - 30 zinc cycles (ZnO) occur or after 10 - 30 zinc cycles (ZnO) one aluminum cycle occurs (Al<sub>2</sub>O<sub>3</sub>) the thermal insulation layer grows . It is preferable if the aluminum precursor is TMA, the zinc precursor is DEZn - diethyl zinc or DMZn - dimethyl zinc and if the oxygen precursor is water or ozone.

PL442831A 2022-11-15 2022-11-15 Method of depositing thermal insulation layers on glass PL442831A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL442831A PL442831A1 (en) 2022-11-15 2022-11-15 Method of depositing thermal insulation layers on glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL442831A PL442831A1 (en) 2022-11-15 2022-11-15 Method of depositing thermal insulation layers on glass

Publications (1)

Publication Number Publication Date
PL442831A1 true PL442831A1 (en) 2024-05-20

Family

ID=91128904

Family Applications (1)

Application Number Title Priority Date Filing Date
PL442831A PL442831A1 (en) 2022-11-15 2022-11-15 Method of depositing thermal insulation layers on glass

Country Status (1)

Country Link
PL (1) PL442831A1 (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103866269A (en) * 2012-12-11 2014-06-18 中国科学院微电子研究所 Method for preparing Te-N codoped zinc oxide film by atomic layer deposition
CN104195523A (en) * 2014-09-02 2014-12-10 嘉兴科民电子设备技术有限公司 Method for preparing aluminum-doped zinc oxide thin film through plasma-enhanced atomic layer deposition
US20150086709A1 (en) * 2013-09-26 2015-03-26 Mitchell Stewart Burberry Passivating ultra-thin azo with nano-layer alumina

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103866269A (en) * 2012-12-11 2014-06-18 中国科学院微电子研究所 Method for preparing Te-N codoped zinc oxide film by atomic layer deposition
US20150086709A1 (en) * 2013-09-26 2015-03-26 Mitchell Stewart Burberry Passivating ultra-thin azo with nano-layer alumina
CN104195523A (en) * 2014-09-02 2014-12-10 嘉兴科民电子设备技术有限公司 Method for preparing aluminum-doped zinc oxide thin film through plasma-enhanced atomic layer deposition

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