NO134136B - - Google Patents
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- NO134136B NO134136B NO2860/72A NO286072A NO134136B NO 134136 B NO134136 B NO 134136B NO 2860/72 A NO2860/72 A NO 2860/72A NO 286072 A NO286072 A NO 286072A NO 134136 B NO134136 B NO 134136B
- Authority
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- Norway
- Prior art keywords
- nitrovin
- molecular complex
- growth
- bis
- neo
- Prior art date
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- 239000000203 mixture Substances 0.000 claims description 13
- 241001465754 Metazoa Species 0.000 claims description 9
- WHEQVHAIRSPYDK-UHFFFAOYSA-N 4,6-dimethyl-1h-pyrimidin-2-one Chemical compound CC1=CC(C)=NC(O)=N1 WHEQVHAIRSPYDK-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- 239000004135 Bone phosphate Substances 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 4
- -1 bis-(5-nitrofurfurylidene)-acetoneguanylhydrazone compound Chemical class 0.000 claims description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- XQCFHQBGMWUEMY-ZPUQHVIOSA-N Nitrovin Chemical compound C=1C=C([N+]([O-])=O)OC=1\C=C\C(=NNC(=N)N)\C=C\C1=CC=C([N+]([O-])=O)O1 XQCFHQBGMWUEMY-ZPUQHVIOSA-N 0.000 description 10
- 238000002360 preparation method Methods 0.000 description 7
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
- 235000013312 flour Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 241000287828 Gallus gallus Species 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
- 239000000969 carrier Substances 0.000 description 4
- 244000144972 livestock Species 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 229910000019 calcium carbonate Inorganic materials 0.000 description 3
- 235000013330 chicken meat Nutrition 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- XQCFHQBGMWUEMY-UHFFFAOYSA-N 2-[1,5-bis(5-nitrofuran-2-yl)penta-1,4-dien-3-ylideneamino]guanidine Chemical compound C=1C=C([N+]([O-])=O)OC=1C=CC(=NN=C(N)N)C=CC1=CC=C([N+]([O-])=O)O1 XQCFHQBGMWUEMY-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 240000008042 Zea mays Species 0.000 description 2
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 2
- 235000019730 animal feed additive Nutrition 0.000 description 2
- 235000009973 maize Nutrition 0.000 description 2
- 244000144977 poultry Species 0.000 description 2
- 235000013594 poultry meat Nutrition 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- LUWVSMYASMXSJY-UHFFFAOYSA-N 1,5-bis(5-nitrofuran-2-yl)penta-1,4-dien-3-one Chemical compound O1C([N+](=O)[O-])=CC=C1C=CC(=O)C=CC1=CC=C([N+]([O-])=O)O1 LUWVSMYASMXSJY-UHFFFAOYSA-N 0.000 description 1
- 241000272517 Anseriformes Species 0.000 description 1
- 241001474374 Blennius Species 0.000 description 1
- 241000283690 Bos taurus Species 0.000 description 1
- 240000007124 Brassica oleracea Species 0.000 description 1
- 235000003899 Brassica oleracea var acephala Nutrition 0.000 description 1
- 235000012905 Brassica oleracea var viridis Nutrition 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 235000019687 Lamb Nutrition 0.000 description 1
- 240000004658 Medicago sativa Species 0.000 description 1
- 235000017587 Medicago sativa ssp. sativa Nutrition 0.000 description 1
- JCXJVPUVTGWSNB-UHFFFAOYSA-N Nitrogen dioxide Chemical class O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 1
- 241001494479 Pecora Species 0.000 description 1
- 241000286209 Phasianidae Species 0.000 description 1
- 240000006394 Sorghum bicolor Species 0.000 description 1
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 1
- 241000282887 Suidae Species 0.000 description 1
- 235000009430 Thespesia populnea Nutrition 0.000 description 1
- 239000005862 Whey Substances 0.000 description 1
- 102000007544 Whey Proteins Human genes 0.000 description 1
- 108010046377 Whey Proteins Proteins 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 235000014590 basal diet Nutrition 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- UHZZMRAGKVHANO-UHFFFAOYSA-M chlormequat chloride Chemical compound [Cl-].C[N+](C)(C)CCCl UHZZMRAGKVHANO-UHFFFAOYSA-M 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012527 feed solution Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000007952 growth promoter Substances 0.000 description 1
- 150000004678 hydrides Chemical class 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- MXWHMTNPTTVWDM-NXOFHUPFSA-N mitoguazone Chemical compound NC(N)=N\N=C(/C)\C=N\N=C(N)N MXWHMTNPTTVWDM-NXOFHUPFSA-N 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 235000015099 wheat brans Nutrition 0.000 description 1
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- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Description
Dyrefor inneholdende et Animal feed containing a
vekstfremmende middel. growth promoter.
Foreliggende oppfinnelse angår dyrefor med nye molekylkomplekser som additiver. Mere spesielt angår oppfinn- The present invention relates to animal feed with new molecular complexes as additives. More particularly concerns invention-
elsen dyrefor som, som additiv inneholder' et molekylkompleks av et bis-(5-nitrofurfuryliden)-acetonguanylhydrazon eller et syreaddisjonssalt derav og 2-hydroksy-4,6-dimetylpyrimidin. the animal feed solution containing, as an additive, a molecular complex of a bis-(5-nitrofurfurylidene)-acetoneguanylhydrazone or an acid addition salt thereof and 2-hydroxy-4,6-dimethylpyrimidine.
De nye molekylkomplekser som i henhold til foreliggende oppfinnelse benyttes som dyreforadditiver er som så- The new molecular complexes which according to the present invention are used as animal feed additives are as follows
danne meget ønskelige. Tallrike additiver er benyttet i dyre-forsammensetninger i et forsøk på å aksellerere veksten av unge husdyr slik som f.eks. kveg, svin, sauer, kyllinger, kalkuner, form very desirable. Numerous additives are used in animal pre-compositions in an attempt to accelerate the growth of young livestock such as e.g. cattle, pigs, sheep, chickens, turkeys,
ender og lignende. Den hurtige veksthastighet for husdyr er av stor økonomisk viktighet på grunn av at jo hurtigere veksten er jo større er den del av foret som omdannes til kjøtt. Molekylkompleksene som benyttes i henhold til foreliggende oppfinnelse viser en overraskende høy aktivitet når de benyttes til å ducks and the like. The rapid growth rate of livestock is of great economic importance because the faster the growth, the greater the proportion of the feed that is converted into meat. The molecular complexes used according to the present invention show a surprisingly high activity when they are used to
fremme veksten av hysdyr. promote the growth of livestock.
Bis-(5-nitrofurfuryliden)-acetonguanylhydrazon og Bis-(5-nitrofurfurylidene)-acetoneguanylhydrazone and
dets addisjonssalter er benyttet som dyreforadditiver slik som det er beskrevet i US-patent nr3;264 .112...Teknikkens stand beskriver imidlertid'ikke de''molekylkomplekser som benyttes i ''its addition salts are used as animal feed additives as described in US patent no. 3;264.112...However, the state of the art does not describe the "molecular complexes used in"
henhold til foreliggende oppfinnelse, eller deres overraskende according to the present invention, or their surprising
høye aktivitet for fremming av.vekst av husdyr. vv. high activity for promoting the growth of livestock. etc.
Det er derfor.en'gjenstand'for•foreliggende oppfinnelse å frembringe dyrefor inneholdende' nye additiver. It is therefore an object of the present invention to produce animal feed containing new additives.
Oppfinnelsen angår således et' dyrefor og dette karakteriseres ved at det som vekstfremmende bestanddel innehol- The invention thus relates to an animal feed and this is characterized by the fact that as a growth-promoting ingredient it contains
der 1-20 g/tonn, beregnet'på den totale sammensetning, av et molekylkompleks 'omfattende where 1-20 g/tonne, calculated on the total composition, of a molecular complex comprising
a) en bis-(5-nitrofurfuryliden)-acetonguanylhydrazon-forbindelse med;formelen: , .....<•■ eller med formelen : a) a bis-(5-nitrofurfurylidene)-acetoneguanylhydrazone compound with the formula: , .....<•■ or with the formula :
der X .er ien.-mpno-, di-; ■ eller .tribasisk syre og n=lhvis-X er mono.basisk^ -n=l eller. -2 hvis .X er dibasisk. og n=l, 2 eller- 3 hvis X er tribasisk, og where X is ien.-mpno-, di-; ■ or .tribasic acid and n=lhif-X is mono.basic^ -n=l or. -2 if .X is dibasic. and n=1, 2 or- 3 if X is tribasic, and
b) .-. • ■ . '2-hydr6ksy-4,6-dimetylpyrimidin. b) .-. • ■ . 2-hydroxy-4,6-dimethylpyrimidine.
- •-. Det foretrukkede bis-(5-nitrofurfuryliden)-aceton- ' -•-. The preferred bis-(5-nitrofurfurylidene)-acetone-'
guanylhydrazon-syreaddisjonssalt er det hydroklorid-som er kommersielt tilgjengelig under "Nitrovin". guanylhydrazone acid addition salt is the hydrochloride which is commercially available under "Nitrovin".
;•.. ' En foretrukket fremgangsmåte-til - fremstilling av molekylkompleksene som "benyttes omfatter oppløsning av aminet "i et egnet' oppløsningsmiddél, f.eks. metanol'og deretter tilsetning av bis-.('5-nitrofurfuryliden)-actonguany-lhyd-razoriet eller dettes-syreaddisjonssalt. -Den resulterende blanding'..omrøres ved romtemperatur i omkring 16 :t'imér-og det--resulterende produkt filt- ":-reres'deretter/f. eks . ved sug, - vaskes 'og ^tørkes ■ f or å gi det ønskede mdlekylkompleks .'".^X.;/^' ;•.. ' A preferred method-for - preparation of the molecular complexes which are used comprises dissolving the amine in a suitable solvent, e.g. methanol' and then addition of the bis-(5-nitrofurfurylidene)-actonguanyyl hydride or its acid addition salt. The resulting mixture is stirred at room temperature for about 16 hours and the resulting product is then filtered, e.g. by suction, washed and dried before give the desired mdlecyl complex .'".^X.;/^'
' : ■ Molékylkompleksforbindelsene -kan tilsettes grunn-foret'.som sådanne eller blandet med egnede bærere •■ De kan be- ""-nyttes med' enten sureeller alkaliske bærere;på grunn av derés ' : ■ The molecular complex compounds can be added to the base as such or mixed with suitable carriers • They can be used with either acidic or alkaline carriers because of their
ekstreme stabilitet. Forskjellige bærere 'er tilgjengelige,- og bæreren velges -vanligvis på basis av -kostnadene-, inertheten over-for molekylkomplekset'og toleransen for det spesielle dyr. • Den følgende liste omfatter kun noen av de næringsstoffer som er extreme stability. Various carriers are available, and the carrier is usually selected on the basis of cost, inertness to the molecular complex, and tolerance of the particular animal. • The following list includes only some of the nutrients that are
brukt eller som kan brukes'som..bærere: maismel, maiskolbemel, used or which can be used'as..carriers: maize flour, maize cob flour,
milo, soyabønnoljemel,. ,alfalfamelY.\tørket myse,' tørkede oppløs-,\eligeVstof fer fra destillerier';^ kale it, f jær-febiprodukter, hvetekliy.<Æ>éks^^ tang, lin-oljemel, rugmel,'.'.tørket,' milo, soybean oil flour,. Alfalfa flour, dried whey, dried solubles from distilleries, kale, lamb byproducts, wheat bran, seaweed, linseed oil flour, rye flour, dried '
En, forblanding^fremstille^s "Vanligvis slik at den -:' ./('■' inneholder 8 g komp 1 eks / kg •; imid ler,t id kan'}.' f orb landinger av f ler-';;: dobbelt styrke,-;(f .eks. ''de'; sbm^inVéholder'l6^24,<*>:,32>f<!>i8, 64 og 128 g molekylkompleks/kg fremstilles og benyttes. • Porblandingen kan deretter kombineres med andre bestanddeler slik at det dannes et komplett for, f.eks. vil omkring.100. g fqrblanding sammen med. omkring 1 tonn andre bestanddeler danne et komplett kyllingfor. Komplette f6r for andre' dyr"karr'formuleres på lignende måte. En komplett forsammensetning kan. også fremstilles direkte slik at den inneholder fra omkring 1 g til omkring 2 g av det ønskede molekylkompleks/tonn sammensetning uten bruk av forblandings-preparatet. A, premix^produce^s "Usually so that it -:' ./('■' contains 8 g comp 1 ex / kg •; imid ler,t id kan'}.' f orb landings of f ler-'; ;: double strength,-;(e.g. "de"; sbm^inVéholder'l6^24,<*>:,32>f<!>i8, 64 and 128 g molecular complex/kg are produced and used. • The pore mixture can then be combined with other ingredients so that a complete feed is formed, for example about 100 g of feed mixture together with about 1 tonne of other ingredients will form a complete chicken feed. Complete feeds for other animals are formulated on A complete pre-composition can also be prepared directly so that it contains from about 1 g to about 2 g of the desired molecular complex/ton of composition without the use of the pre-mix preparation.
De følgende eksempler vil illustrere oppfinnelsen nærmere. The following examples will illustrate the invention in more detail.
Eksempel I Example I
1,98 g (0,016 mol) 2-hydroksy-4,6-dimetylpyrimidin ble oppløst i 10 ml metanol og under kontinuerlig omrøring ble 3,97 g (0,01 mol) "Nitrovin" tilsatt langsomt i små mengder. 1.98 g (0.016 mol) of 2-hydroxy-4,6-dimethylpyrimidine was dissolved in 10 ml of methanol and, with continuous stirring, 3.97 g (0.01 mol) of "Nitrovin" was added slowly in small amounts.
Den resulterende blanding ble omrørt ved romtemperatur i et The resulting mixture was stirred at room temperature in a
tidsrom på 16 timer og deretter sugfiltrert på et glass-sintret filter. Det filtrerte produkt ble deretter vasket med en liten period of 16 hours and then suction-filtered on a glass-sintered filter. The filtered product was then washed with a small
mengde etanol og tørket ved omkring 40°C, noe som ga 4,85 g av et oransje-brunt pulver.. Analyser av produktet bekreftet at strukturen"'var den til det ønskede "molekylkompleks. amount of ethanol and dried at about 40°C, yielding 4.85 g of an orange-brown powder. Analysis of the product confirmed that the structure was that of the desired molecular complex.
Eksempel" II - ■- •■ Example" II - ■- •■
1,98 g (0,016 mol) 2-hydroksy-4,6-dimétylpyrimidin ble oppløst i 10 ml metanol og under kontinuerlig omrøring ble 3,6l g . (0, Olj'mol) bis-( 5-nitrofurfurylidé'n)1-acetonguanylhydrazon tilsatt langsomt i små andeler'.'''". Den;resulterende"'blanding ble omrørt ved romtemperatur i et. tidsrom på 16'timer"og deretter sugfiltrert på et glass-sintret - f ilter".V Det filtrerte produkt ble deretter vasket med en liten mengde.metanol og tørket ved •:>'<.. /omkring 40°C, noe som ga(4,4o'g av et sort-fiolett' pulver. Analyser av produktet bekreftet at strukturen var det ønsekde 1.98 g (0.016 mol) of 2-hydroxy-4,6-dimethylpyrimidine was dissolved in 10 ml of methanol and, with continuous stirring, 3.6 l g . (0.Olj'mol) bis-(5-nitrofurfurylide'n)1-acetoneguanylhydrazone was added slowly in small portions'.'''". The "resulting"' mixture was stirred at room temperature in a period of 16 hours" and then suction filtered on a glass sintered filter". The filtered product was then washed with a small amount of methanol and dried at about 40°C, which gave (4.4o'g of a black-violet' powder. Analyzes of the product confirmed that the structure was the desired
molekylkompleks. molecular complex.
Eksempel III Example III
Et f6r-forblandingspreparat ble fremstilt ved A f6r premix preparation was prepared by
blanding av de nedenfor angitte bestanddeler. mixture of the components listed below.
Et i det vesentlige likt f6r-forblandingspreparat fremstilles når molekylkomplekset i henhold til eks. II benyttes på samme vektbasis i stedet for molekylkomplekset i henhold til eks. I i det ovenfor angitte preparat. An essentially similar f6r premix preparation is produced when the molecular complex according to e.g. II is used on the same weight basis instead of the molecular complex according to ex. In the preparation indicated above.
Eksempel IV Example IV
Et fjærfeforpreparat fremstilles ved blanding av A poultry pre-preparation is produced by mixing
de nedenfor viste bestanddeler. the components shown below.
Et i det vesentlige likt fjærfepreparat fremstilles hvis molekylkomplekset i henhold til eks. II benyttes på samme vektbasis i stedet for molekylkomplekset i' eks. I i den ovenfor gitte sammensetning. A substantially similar poultry preparation is produced if the molecular complex according to e.g. II is used on the same weight basis instead of the molecular complex i' ex. In the composition given above.
De karakteristiske trekk for molekylkomplekset av Nitrovin og 2-hydroksy-4,6-dimetylpyrimidin, heretter kalt neo-Nitrovin, sammenlignet med de karakteristiske trekk for Nitrovin slik som følger: The characteristic features of the molecular complex of Nitrovin and 2-hydroxy-4,6-dimethylpyrimidine, hereinafter called neo-Nitrovin, compared to the characteristic features of Nitrovin as follows:
Por å vise den forbedrede aktivitet for neo-Nitrovin sammenlignet med Nitrovin, ble det gjennomført forsøk hvori grupper av broilere ble matet med en basisdiett i 8 uker for å bestemme mengden for som er nødvendig for å frembringe en vekt på 1 kg ved 8 ukersalderen. Sammensetningen av basisrasjonen var som følger: In order to demonstrate the improved activity of neo-Nitrovin compared to Nitrovin, experiments were conducted in which groups of broilers were fed a basal diet for 8 weeks to determine the amount of feed required to produce a weight of 1 kg at 8 weeks of age. The composition of the basic ration was as follows:
Forskjellige grupper kyllinger ble matet med basisrasj onen, med basisrasjonen blandet med forskjellige mengder Nitrovin og basisrasj onen blandet med forskjellige meng;der neo- Different groups of chickens were fed with the basic ration, with the basic ration mixed with different amounts of Nitrovin and the basic ration mixed with different amounts; where neo-
Nitrovin. Resultatene var som følger: Nitro wine. The results were as follows:
Da de angitte resultater er på statistisk basis er As the stated results are on a statistical basis are
det klart at de resultater som er oppnådd med lavere nivåer, dvs. it is clear that the results obtained with lower levels, i.e.
5 og 11 ppm, av neo-Nitrovin er betraktelig bedre enn de som er 5 and 11 ppm, of neo-Nitrovin are considerably better than those that are
oppnådd uten noe supplement og med Nitrovin. achieved without any supplement and with Nitrovin.
Forsøk som ble utført for å sammenligne stabili- Experiments carried out to compare the stability of
teten av Nitrovin og neo-Nitrovin på en vanlig brukt bærer, kalsiumkarbonat, viste at neo-Nitrovin er overlegen. Således ble separate mengder Nitrovin blandet med kalsiumkarbonat og neo- test of Nitrovin and neo-Nitrovin on a commonly used carrier, calcium carbonate, showed that neo-Nitrovin is superior. Thus, separate quantities of Nitrovin were mixed with calcium carbonate and neo-
Nitrovin blandet med kalsiumkarbonat fremstillet, og disse meng- Nitrovin mixed with calcium carbonate produced, and these mix-
der ble lagret i et kammer ved 20°C og 75% relativ fuktighet. there was stored in a chamber at 20°C and 75% relative humidity.
Resultatene var som følger: The results were as follows:
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NO2860/72A NO134136C (en) | 1970-11-06 | 1972-08-10 |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US8763270A | 1970-11-06 | 1970-11-06 | |
NO4066/71A NO135287C (en) | 1970-11-06 | 1971-11-03 | |
NO2860/72A NO134136C (en) | 1970-11-06 | 1972-08-10 |
Publications (2)
Publication Number | Publication Date |
---|---|
NO134136B true NO134136B (en) | 1976-05-18 |
NO134136C NO134136C (en) | 1976-09-08 |
Family
ID=27352619
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO2860/72A NO134136C (en) | 1970-11-06 | 1972-08-10 |
Country Status (1)
Country | Link |
---|---|
NO (1) | NO134136C (en) |
-
1972
- 1972-08-10 NO NO2860/72A patent/NO134136C/no unknown
Also Published As
Publication number | Publication date |
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NO134136C (en) | 1976-09-08 |
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