NO129956B - - Google Patents

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Info

Publication number: NO129956B
Authority: NO; Norway
Prior art keywords: chamber; reaction; reacting substances; gas; burner
Prior art date: 1962-02-28

Application number

NO00147431A

Other languages

English (en)

Norwegian (no)

Inventor

B Sjoeberg

B Ekstroem

Original Assignee

Beecham Group Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1962-02-28

Filing date

1963-02-06

Publication date

1974-06-17

1963-02-06 Application filed by Beecham Group Ltd filed Critical Beecham Group Ltd

1974-06-17 Publication of NO129956B publication Critical patent/NO129956B/no

Links

238000000034 method Methods 0.000 claims abstract description 21
238000006243 chemical reaction Methods 0.000 claims description 66
239000007789 gas Substances 0.000 claims description 61
239000000126 substance Substances 0.000 claims description 36
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 28
239000001301 oxygen Substances 0.000 claims description 28
229910052760 oxygen Inorganic materials 0.000 claims description 28
239000007795 chemical reaction product Substances 0.000 claims description 13
150000004820 halides Chemical class 0.000 claims description 12
230000003647 oxidation Effects 0.000 claims description 10
238000007254 oxidation reaction Methods 0.000 claims description 10
239000012808 vapor phase Substances 0.000 claims description 7
229930182555 Penicillin Natural products 0.000 abstract 3
JGSARLDLIJGVTE-MBNYWOFBSA-N Penicillin G Chemical compound N([C@H]1[C@H]2SC([C@@H](N2C1=O)C(O)=O)(C)C)C(=O)CC1=CC=CC=C1 JGSARLDLIJGVTE-MBNYWOFBSA-N 0.000 abstract 2
229940049954 penicillin Drugs 0.000 abstract 2
NGHVIOIJCVXTGV-UHFFFAOYSA-N 6beta-amino-penicillanic acid Natural products OC(=O)C1C(C)(C)SC2C(N)C(=O)N21 NGHVIOIJCVXTGV-UHFFFAOYSA-N 0.000 abstract 1
230000010933 acylation Effects 0.000 abstract 1
238000005917 acylation reaction Methods 0.000 abstract 1
125000003277 amino group Chemical group 0.000 abstract 1
239000003242 anti bacterial agent Substances 0.000 abstract 1
125000001584 benzyloxycarbonyl group Chemical group C(=O)(OCC1=CC=CC=C1)* 0.000 abstract 1
239000003054 catalyst Substances 0.000 abstract 1
238000005984 hydrogenation reaction Methods 0.000 abstract 1
229910000510 noble metal Inorganic materials 0.000 abstract 1
125000001181 organosilyl group Chemical group [SiH3]* 0.000 abstract 1
125000006239 protecting group Chemical group 0.000 abstract 1
XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 19
239000011449 brick Substances 0.000 description 11
VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 7
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 7
229910052801 chlorine Inorganic materials 0.000 description 7
239000000460 chlorine Substances 0.000 description 7
239000002245 particle Substances 0.000 description 7
239000005049 silicon tetrachloride Substances 0.000 description 7
229910021578 Iron(III) chloride Inorganic materials 0.000 description 6
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 6
239000007787 solid Substances 0.000 description 6
238000010438 heat treatment Methods 0.000 description 5
239000000463 material Substances 0.000 description 5
239000000047 product Substances 0.000 description 5
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 5
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
239000000203 mixture Substances 0.000 description 4
230000001590 oxidative effect Effects 0.000 description 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
229910000831 Steel Inorganic materials 0.000 description 3
238000002485 combustion reaction Methods 0.000 description 3
230000000694 effects Effects 0.000 description 3
229910001507 metal halide Inorganic materials 0.000 description 3
150000005309 metal halides Chemical class 0.000 description 3
229910052710 silicon Inorganic materials 0.000 description 3
239000010703 silicon Substances 0.000 description 3
239000000377 silicon dioxide Substances 0.000 description 3
229910001220 stainless steel Inorganic materials 0.000 description 3
239000010935 stainless steel Substances 0.000 description 3
239000010959 steel Substances 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
239000004568 cement Substances 0.000 description 2
239000012530 fluid Substances 0.000 description 2
238000009413 insulation Methods 0.000 description 2
239000000376 reactant Substances 0.000 description 2
239000012265 solid product Substances 0.000 description 2
CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 1
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical class [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
229910052770 Uranium Inorganic materials 0.000 description 1
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
238000007792 addition Methods 0.000 description 1
239000004411 aluminium Substances 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
238000009835 boiling Methods 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
150000001805 chlorine compounds Chemical class 0.000 description 1
229910052804 chromium Inorganic materials 0.000 description 1
239000011651 chromium Substances 0.000 description 1
230000007423 decrease Effects 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
239000012467 final product Substances 0.000 description 1
239000000446 fuel Substances 0.000 description 1
239000002737 fuel gas Substances 0.000 description 1
229910052736 halogen Inorganic materials 0.000 description 1
150000002367 halogens Chemical class 0.000 description 1
XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
239000000155 melt Substances 0.000 description 1
229910044991 metal oxide Inorganic materials 0.000 description 1
150000004706 metal oxides Chemical class 0.000 description 1
229910052752 metalloid Inorganic materials 0.000 description 1
150000002738 metalloids Chemical class 0.000 description 1
239000010955 niobium Substances 0.000 description 1
229910052758 niobium Inorganic materials 0.000 description 1
GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 1
235000020030 perry Nutrition 0.000 description 1
239000012071 phase Substances 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
238000010992 reflux Methods 0.000 description 1
235000012239 silicon dioxide Nutrition 0.000 description 1
-1 silicon halide Chemical class 0.000 description 1
235000002639 sodium chloride Nutrition 0.000 description 1
229910052718 tin Inorganic materials 0.000 description 1
239000010936 titanium Substances 0.000 description 1
229910052719 titanium Inorganic materials 0.000 description 1
238000011144 upstream manufacturing Methods 0.000 description 1
JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 description 1
229910052720 vanadium Inorganic materials 0.000 description 1
LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 1
239000002699 waste material Substances 0.000 description 1
229910052726 zirconium Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D499/00—Heterocyclic compounds containing 4-thia-1-azabicyclo [3.2.0] heptane ring systems, i.e. compounds containing a ring system of the formula:, e.g. penicillins, penems; Such ring systems being further condensed, e.g. 2,3-condensed with an oxygen-, nitrogen- or sulfur-containing hetero ring
- C07D499/21—Heterocyclic compounds containing 4-thia-1-azabicyclo [3.2.0] heptane ring systems, i.e. compounds containing a ring system of the formula:, e.g. penicillins, penems; Such ring systems being further condensed, e.g. 2,3-condensed with an oxygen-, nitrogen- or sulfur-containing hetero ring with a nitrogen atom directly attached in position 6 and a carbon atom having three bonds to hetero atoms with at the most one bond to halogen, e.g. an ester or nitrile radical, directly attached in position 2
- C07D499/44—Compounds with an amino radical acylated by carboxylic acids, attached in position 6
- C07D499/48—Compounds with an amino radical acylated by carboxylic acids, attached in position 6 with a carbon chain, substituted by hetero atoms or by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, attached to the carboxamido radical
- C07D499/58—Compounds with an amino radical acylated by carboxylic acids, attached in position 6 with a carbon chain, substituted by hetero atoms or by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, attached to the carboxamido radical substituted in alpha-position to the carboxamido radical
- C07D499/64—Compounds with an amino radical acylated by carboxylic acids, attached in position 6 with a carbon chain, substituted by hetero atoms or by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, attached to the carboxamido radical substituted in alpha-position to the carboxamido radical by nitrogen atoms

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Preparation Of Compounds By Using Micro-Organisms (AREA)
Lubricants (AREA)

NO00147431A 1962-02-28 1963-02-06 NO129956B (pt)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
GB775162A GB959853A (en)	1962-02-28	1962-02-28	Penicillins
GB775262		1962-02-28

Publications (1)

Publication Number	Publication Date
NO129956B true NO129956B (pt)	1974-06-17

Family

ID=26241643

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO00147431A NO129956B (pt)	1962-02-28	1963-02-06

Country Status (9)

Country	Link
AT (1)	AT275732B (pt)
BR (1)	BR6346795D0 (pt)
CH (1)	CH446336A (pt)
DK (1)	DK132412C (pt)
ES (1)	ES285236A1 (pt)
FI (1)	FI41652C (pt)
GB (1)	GB959853A (pt)
NO (1)	NO129956B (pt)
SE (1)	SE320369B (pt)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
IL37124A (en) *	1970-07-03	1974-10-22	Chinoin Gyogyszer Es Vegyeszet	Chlorocarbonyl history of penicillin and their preparation
US3678037A (en) *	1970-08-10	1972-07-18	American Home Prod	Process for producing {60 -amino penicillin intermediates
US4182709A (en) *	1976-01-15	1980-01-08	Glaxo Group Limited	Manufacture of semi-synthetic penicillin antibiotics
US4278600A (en)	1979-03-19	1981-07-14	Bristol-Myers Company	Production of penicillins
US4310458A (en)	1979-03-19	1982-01-12	Bristol-Myers Company	Production of penicillins
US7230097B2 (en)	2003-03-10	2007-06-12	Lupin Ltd.	Process for preparation of 7-[α-Amino (4-hydroxyphenyl) acetamido]-3-substituted-3-cephem-4-carboxylic acid

1962
- 1962-02-28 GB GB775162A patent/GB959853A/en not_active Expired
1963
- 1963-02-06 NO NO00147431A patent/NO129956B/no unknown
- 1963-02-08 BR BR14679563A patent/BR6346795D0/pt unknown
- 1963-02-18 ES ES285236A patent/ES285236A1/es not_active Expired
- 1963-02-20 CH CH213663A patent/CH446336A/de unknown
- 1963-02-22 SE SE197763A patent/SE320369B/xx unknown
- 1963-02-22 AT AT139563A patent/AT275732B/de active
- 1963-02-26 FI FI37563A patent/FI41652C/fi active
- 1963-02-28 DK DK92263A patent/DK132412C/da active

Also Published As

Publication number	Publication date
AT275732B (de)	1969-11-10
SE320369B (pt)	1970-02-09
GB959853A (en)	1964-06-03
FI41652B (pt)	1969-09-30
ES285236A1 (es)	1963-06-01
DK132412B (da)	1975-12-01
CH446336A (de)	1967-11-15
DK132412C (da)	1976-05-03
BR6346795D0 (pt)	1973-07-19
FI41652C (fi)	1973-03-23

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US4595573A (en)	1986-06-17	Chlorinator furnace and method for producing tetrachloride of such metals as titanium and zirconium
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US2834655A (en)	1958-05-13	Production of elemental sulfur
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US3305309A (en)	1967-02-21	Production and recovery of hydrogen halides
US3689039A (en)	1972-09-05	Method of heating oxygen-containing gases
CA1077677A (en)	1980-05-20	Process for preparing sulfur dioxide from sulfur and oxygen
US3955552A (en)	1976-05-11	Heater for large flows at low pressure losses
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