MY148448A - Method for producing ?-sulfofatty acid alkyl ester salt - Google Patents

Method for producing ?-sulfofatty acid alkyl ester salt

Info

Publication number
MY148448A
MY148448A MYPI20090332A MY148448A MY 148448 A MY148448 A MY 148448A MY PI20090332 A MYPI20090332 A MY PI20090332A MY 148448 A MY148448 A MY 148448A
Authority
MY
Malaysia
Prior art keywords
alkyl ester
temperature
acid alkyl
producing
product
Prior art date
Application number
Inventor
Ishikawa Tsutomu
Nishio Taku
Ichitani Go
Negishi Daisuke
Syogase Nobukazu
Matsushita Ryuichi
Original Assignee
Lion Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lion Corp filed Critical Lion Corp
Publication of MY148448A publication Critical patent/MY148448A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/32—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of salts of sulfonic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C07C303/06—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A METHOD FOR PRODUCING AN ?-SULFOFATTY ACID ALKYL ESTER SALT, THE METHOD INCLUDING A SULFONATION STEP IN WHICH A FATTY ACID ALKYL ESTER IS SULFONATED, AN AGING STEP IN WHICH THE SULFONATED PRODUCT OBTAINED IN THE SULFONATION STEP IS AGED, AN ESTERIFICATION STEP IN WHICH THE SULFONATED PRODUCT OBTAINED IN THE AGING STEP IS ESTERIFIED WITH AN ALCOHOL HAVING 1 TO 6 CARBON ATOMS, A NEUTRALIZATION STEP IN WHICH THE ESTERIFIED PRODUCT OBTAINED IN THE ESTERIFICATION STEP IS NEUTRALIZED TO OBTAIN A NEUTRALIZATION PRODUCT, AND A BLEACHING STEP IN WHICH THE NEUTRALIZATION PRODUCT IS BLEACHED TO OBTAIN A BLEACHED PRODUCT, IN WHICH IN THE BLEACHING STEP, THE INITIATION TEMPERATURE OF THE BLEACHING REACTION IS SET AT 55 TO 80�C, AND THE TEMPERATURE IS RAISED FROM THE INITIATION TEMPERATURE TO A MAXIMUM TEMPERATURE OF 85 TO 100�C OVER A PERIOD OF 20 TO 240 MINUTES AFTER THE REACTION INITIATION, KEPT AT THE MAXIMUM TEMPERATURE FOR 20 TO 360 MINUTES, AND THEN LOWERED TO A REACTION TERMINATION TEMPERATURE OF 55 TO 80�C.
MYPI20090332 2006-07-24 2007-07-24 Method for producing ?-sulfofatty acid alkyl ester salt MY148448A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2006201073 2006-07-24

Publications (1)

Publication Number Publication Date
MY148448A true MY148448A (en) 2013-04-30

Family

ID=38981485

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI20090332 MY148448A (en) 2006-07-24 2007-07-24 Method for producing ?-sulfofatty acid alkyl ester salt

Country Status (3)

Country Link
JP (1) JP5193865B2 (en)
MY (1) MY148448A (en)
WO (1) WO2008013174A1 (en)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5587500A (en) * 1993-09-17 1996-12-24 The Chemithon Corporation Sulfonation of fatty acid esters
JP2000128852A (en) * 1998-10-21 2000-05-09 Lion Corp Production of light-colored alpha-sulfofatty acid alkyl ester salt
JP2000319685A (en) * 1999-05-07 2000-11-21 Lion Corp Production of surfactant

Also Published As

Publication number Publication date
JP5193865B2 (en) 2013-05-08
WO2008013174A1 (en) 2008-01-31
JPWO2008013174A1 (en) 2009-12-17

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MY148448A (en) Method for producing ?-sulfofatty acid alkyl ester salt