MX2014002249A - Metodo para la conversion de mercaptopropionaldehido de metilo producido a partir de acroleina cruda y mercaptano de metilo crudo. - Google Patents

Metodo para la conversion de mercaptopropionaldehido de metilo producido a partir de acroleina cruda y mercaptano de metilo crudo.

Info

Publication number
MX2014002249A
MX2014002249A MX2014002249A MX2014002249A MX2014002249A MX 2014002249 A MX2014002249 A MX 2014002249A MX 2014002249 A MX2014002249 A MX 2014002249A MX 2014002249 A MX2014002249 A MX 2014002249A MX 2014002249 A MX2014002249 A MX 2014002249A
Authority
MX
Mexico
Prior art keywords
crude
methyl
conversion
produced
mercaptopropionaldehyde
Prior art date
Application number
MX2014002249A
Other languages
English (en)
Inventor
Hans Joachim Hasselbach
Martin Körfer
Martin Steffan
Harald Jakob
Jignesh Gangadwala
Original Assignee
Evonik Degussa Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Degussa Gmbh filed Critical Evonik Degussa Gmbh
Publication of MX2014002249A publication Critical patent/MX2014002249A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • C07C319/12—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by reactions not involving the formation of mercapto groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/26—Separation; Purification; Stabilisation; Use of additives
    • C07C319/28—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
    • C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/57—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C323/58—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups with amino groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D233/72—Two oxygen atoms, e.g. hydantoin
    • C07D233/76—Two oxygen atoms, e.g. hydantoin with substituted hydrocarbon radicals attached to the third ring carbon atom
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

La invención se refiere a una columna de rectificación reactiva para la conversión de metilmercaptopropionaldehído preparado a partir de acroleína cruda y mercaptano de metilo crudo a ácido 2-hidroxi-4-metilmercaptobutírico y/o metionina y al uso de los mismos en un método para la producción de ácido 2-hidroxi-4-metilmercaptobutírico y/o metionina.
MX2014002249A 2011-08-30 2012-08-23 Metodo para la conversion de mercaptopropionaldehido de metilo producido a partir de acroleina cruda y mercaptano de metilo crudo. MX2014002249A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102011081828A DE102011081828A1 (de) 2011-08-30 2011-08-30 Verfahren zur Umsetzung von Methylmercaptopropionaldehyd aus Roh-Acrolein und Roh-Methylmercaptan
PCT/EP2012/066376 WO2013030069A1 (de) 2011-08-30 2012-08-23 Verfahren zur umsetzung von methylmercaptopropionaldehyd aus roh-acrolein und roh-methylmercaptan

Publications (1)

Publication Number Publication Date
MX2014002249A true MX2014002249A (es) 2014-04-25

Family

ID=46724431

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2014002249A MX2014002249A (es) 2011-08-30 2012-08-23 Metodo para la conversion de mercaptopropionaldehido de metilo producido a partir de acroleina cruda y mercaptano de metilo crudo.

Country Status (12)

Country Link
US (1) US9029597B2 (es)
EP (1) EP2750776A1 (es)
JP (1) JP6092218B2 (es)
KR (1) KR101945072B1 (es)
CN (1) CN103764239B (es)
BR (1) BR112014004538A2 (es)
DE (1) DE102011081828A1 (es)
MX (1) MX2014002249A (es)
MY (1) MY170459A (es)
RU (1) RU2615734C2 (es)
SG (1) SG2014014161A (es)
WO (1) WO2013030069A1 (es)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010064250A1 (de) 2010-12-28 2012-06-28 Evonik Degussa Gmbh Verfahren zur Herstellung von Methylmercaptopropionaldehyd
CN103347854B (zh) 2011-02-23 2017-04-26 赢创德固赛有限公司 由3‑(甲硫基)丙醛和氢氰酸制备2‑羟基‑4‑(甲硫基)丁腈的方法
WO2013030068A2 (de) * 2011-08-30 2013-03-07 Evonik Degussa Gmbh Verfahren zur herstellung eines methioninsalzes
EP2679579A1 (de) 2012-06-27 2014-01-01 Evonik Industries AG Integriertes Verfahren zur Herstellung von Acrolein und 3-Methylmercaptopropionaldehyd
EP2848607A1 (de) 2013-09-17 2015-03-18 Evonik Industries AG Verfahren zur Gewinnung von Methionin
KR102579625B1 (ko) 2014-09-24 2023-09-18 쉘 인터내셔날 리써취 마트샤피지 비.브이. 알킬렌 글리콜의 제조 방법 및 제조 장치
CN105061193B (zh) * 2015-08-10 2017-03-22 蓝星（北京）技术中心有限公司 蛋氨酸生产废水处理中回收有机物的方法
CN111491917B (zh) * 2017-12-19 2022-03-22 住友化学株式会社 甲硫氨酸的制造方法
WO2019131726A1 (ja) * 2017-12-28 2019-07-04 住友化学株式会社 メチオニンの製造方法
EP3656760A1 (de) * 2018-11-21 2020-05-27 Evonik Operations GmbH Lagerstabile form von 3-methylthiopropionaldehyd
CN114072214B (zh) * 2019-05-06 2023-09-12 沙特基础全球技术有限公司 具有不同直径的通孔的蒸馏塔板

Family Cites Families (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL6706022A (es) 1966-04-30 1967-10-31
DE2640592A1 (de) * 1976-09-09 1978-03-16 Hoechst Ag Entgasungskolonne
DE3335218A1 (de) * 1983-09-29 1985-04-11 Degussa Ag, 6000 Frankfurt Verfahren zur hydrolyse von 5-(ss-methylmercaptoethyl) -hydantoin
SU1360753A1 (ru) * 1986-07-14 1987-12-23 Киевский Технологический Институт Пищевой Промышленности Тепломассообменный аппарат
JP2517796B2 (ja) * 1990-12-27 1996-07-24 昭和電工株式会社 アリルアルコ―ルの精製法
DE4235295A1 (de) * 1992-10-20 1994-04-21 Degussa Kontinuierlich durchführbares Verfahren zur Herstellung von Methionin oder Methioninderivaten
US5905171A (en) 1995-06-22 1999-05-18 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
DE19547236A1 (de) * 1995-12-18 1997-07-03 Degussa Verfahren zur Herstellung von D,L-Methionin oder dessen Salz
DE19548538C2 (de) 1995-12-23 1997-12-18 Degussa Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
US6057481A (en) 1996-04-01 2000-05-02 Union Carbide Chemicals & Plastics Technology Corporation Processes for the manufacture of methylmercaptopropanal
DE19716373A1 (de) * 1997-04-18 1998-10-22 Basf Ag Kolonne und Verfahren zur Desodorierung von Dispersionen
BR9709367A (pt) * 1996-05-24 1999-08-10 Basf Ag Coluna de contracorrente para abaixar o nível de voláteis residuais em dispersões aparelho para preparar dispersões de polímero processo para preparar dispers es dispersão e uso de dispers es de polímero
DE19707380A1 (de) 1997-02-25 1998-08-27 Degussa Verfahren zur Herstellung eines rieselfähigen Tierfuttermittelsupplements auf Methioninsalzbasis und das so erhältliche Granulat
DE19735332A1 (de) 1997-08-14 1999-02-18 Degussa Aliphatische Alkanale mit verbesserter Lagerstabilität und Verfahren zur Verbesserung der Lagerstabilität
DE19822099A1 (de) 1998-05-16 1999-11-18 Degussa Verfahren zur Herstellung von wäßrigen Natriummethioninat-Lösungen und Verwendung dieser Lösungen zur Herstellung eines Granulats
RU2150314C1 (ru) * 1999-06-10 2000-06-10 Асадов Георгий Арменакович Установка для тепломассообменных процессов с горизонтальным противотоком газа и жидкости
WO2001060788A1 (en) * 2000-02-15 2001-08-23 Rhone-Poulenc Animal Nutrition Process for the production of methionine
JP2003119557A (ja) * 2001-10-12 2003-04-23 Sumitomo Chem Co Ltd 耐食性部材、耐食性部材の製造方法およびメチオニンの製造装置
DE10160358A1 (de) 2001-12-08 2003-06-18 Degussa Verfahren zur Herstellung von Methionin
DE10238212A1 (de) * 2002-08-21 2004-03-04 Degussa Ag Verfahren zur Herstellung von α-Aminosäuren durch Hydrolyse von Hydantoinen bei erhöhtem Druck und erhöhter Temperatur
DE10359636A1 (de) 2003-12-18 2005-07-28 Degussa Ag Verfahren zur Abtrennung von Methylmercaptan aus Reaktionsgemischen
ES2365849T3 (es) 2004-02-14 2011-10-11 Evonik Degussa Gmbh Procedimiento para producir metionina.
DE102004035465A1 (de) * 2004-07-22 2006-02-16 Degussa Ag Verfahren zur Reinigung von CO2-Gasströmen
JP4792754B2 (ja) * 2005-01-31 2011-10-12 住友化学株式会社 アンモニウム塩を含有する溶液からアンモニアを除去する方法
CN101341109B (zh) * 2005-12-21 2011-12-28 旭化成化学株式会社 碳酸二烷基酯和二醇类的工业制备方法
TWI327998B (en) * 2006-01-26 2010-08-01 Asahi Kasei Chemicals Corp Industrial process for production of diol
JP2007254442A (ja) * 2006-03-27 2007-10-04 Sumitomo Chemical Co Ltd メチオニンの製造方法
JP2009292795A (ja) 2008-06-09 2009-12-17 Sumitomo Chemical Co Ltd メチオニンの製造方法
DE102008040544A1 (de) 2008-07-18 2010-01-21 Evonik Degussa Gmbh Reaktionsbehälter und Verfahren zur Verwendung
FR2938535B1 (fr) * 2008-11-20 2012-08-17 Arkema France Procede de fabrication de methylmercaptopropionaldehyde et de methionine a partir de matieres renouvelables
DE102010064250A1 (de) 2010-12-28 2012-06-28 Evonik Degussa Gmbh Verfahren zur Herstellung von Methylmercaptopropionaldehyd
ES2526165T3 (es) 2011-02-23 2015-01-07 Evonik Degussa Gmbh Nitrilo del ácido 2-hidroxi-4-(metiltio)butírico estable al almacenamiento
CN103347854B (zh) 2011-02-23 2017-04-26 赢创德固赛有限公司 由3‑(甲硫基)丙醛和氢氰酸制备2‑羟基‑4‑(甲硫基)丁腈的方法
WO2013030068A2 (de) * 2011-08-30 2013-03-07 Evonik Degussa Gmbh Verfahren zur herstellung eines methioninsalzes

Also Published As

Publication number Publication date
MY170459A (en) 2019-08-02
SG2014014161A (en) 2014-10-30
RU2014111965A (ru) 2015-11-10
US20130245318A1 (en) 2013-09-19
WO2013030069A1 (de) 2013-03-07
CN103764239A (zh) 2014-04-30
CN103764239B (zh) 2016-05-18
DE102011081828A1 (de) 2013-02-28
JP2014529616A (ja) 2014-11-13
KR101945072B1 (ko) 2019-04-17
BR112014004538A2 (pt) 2017-03-28
US9029597B2 (en) 2015-05-12
EP2750776A1 (de) 2014-07-09
RU2615734C2 (ru) 2017-04-10
JP6092218B2 (ja) 2017-03-08
KR20140068030A (ko) 2014-06-05

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