MX2010009011A - Metodo para la produccion de (met) acrilatos de mezclas de alcohol de c10. - Google Patents

Metodo para la produccion de (met) acrilatos de mezclas de alcohol de c10.

Info

Publication number
MX2010009011A
MX2010009011A MX2010009011A MX2010009011A MX2010009011A MX 2010009011 A MX2010009011 A MX 2010009011A MX 2010009011 A MX2010009011 A MX 2010009011A MX 2010009011 A MX2010009011 A MX 2010009011A MX 2010009011 A MX2010009011 A MX 2010009011A
Authority
MX
Mexico
Prior art keywords
methylhexanol
meth
propyl
acrylates
alcohol mixtures
Prior art date
Application number
MX2010009011A
Other languages
English (en)
Inventor
Lothar Karrer
Reinhold Schwalm
Uwe Meisenburg
Frank Hoefer
Nick Gruber
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2010009011A publication Critical patent/MX2010009011A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04—Homopolymers or copolymers of esters
    • C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09D133/10—Homopolymers or copolymers of methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
    • C09J133/04—Homopolymers or copolymers of esters
    • C09J133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09J133/10—Homopolymers or copolymers of methacrylic acid esters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Paints Or Removers (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

Se describe un método para producir (met)acrilato de mezclas de alcoholes de C10 mediante la reacción del ácido (met)acrílico con una mezcla de isómeros de alcoholes de C10 que contiene 2-propilheptanol como el isómero principal y al menos uno de los alcoholes de C10 2-propil-4-metilhexanol, 2-propil-5-metilhexanol, 2-isopropilheptanol, 2-isopropil-4-metilhexanol, 2- isopropil-5-metilhexanol y/o 2-propil-4,4-dimetilpentanol en presencia de al menos un catalizador ácido y al menos un inhibidor de la polimerización y en presencia de un solvente que forma un azeótropo junto con agua, la separación del azeótropo por destilación y la condensación del mismo de modo que el condensado se descomponga en una fase acuosa y una orgánica. De acuerdo con el método, a) el proceso de esterificación se lleva a cabo en un reactor que comprende un evaporador de circulación, b) en presencia de un solvente, y c) el producto crudo se purifica en un proceso de destilación para purificación subsiguiente.
MX2010009011A 2008-02-27 2009-02-26 Metodo para la produccion de (met) acrilatos de mezclas de alcohol de c10. MX2010009011A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP08102070 2008-02-27
PCT/EP2009/052241 WO2009106550A1 (de) 2008-02-27 2009-02-26 Verfahren zur herstellung von (meth)acrylaten von c10-alkoholgemischen

Publications (1)

Publication Number Publication Date
MX2010009011A true MX2010009011A (es) 2010-09-09

Family

ID=40668441

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2010009011A MX2010009011A (es) 2008-02-27 2009-02-26 Metodo para la produccion de (met) acrilatos de mezclas de alcohol de c10.

Country Status (11)

Country Link
US (1) US8318970B2 (es)
EP (1) EP2257519B1 (es)
JP (1) JP5506700B2 (es)
KR (1) KR101653843B1 (es)
CN (1) CN101959838B (es)
AT (1) ATE522492T1 (es)
BR (1) BRPI0908521A2 (es)
CA (1) CA2715712A1 (es)
ES (1) ES2369339T3 (es)
MX (1) MX2010009011A (es)
WO (1) WO2009106550A1 (es)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009001577A1 (de) * 2009-03-16 2010-09-23 Evonik Röhm Gmbh Für eine Aufreinigung stabilisierte Zusammensetzung und Verfahren zur Aufreinigung und zur Herstellung von Hydroxyalkyl(meth)acrylaten
DE102009047228A1 (de) * 2009-11-27 2011-06-01 Basf Se Verfahren zur Herstellung von (Meth)acrylaten von C17-Alkoholgemischen
GB0922255D0 (en) * 2009-12-21 2010-02-03 Lucite Int Uk Ltd Method of producing acrylic and methacrylic acid
CN102229529B (zh) * 2011-05-11 2013-12-04 华诺森（武汉）生物医药技术有限公司 一种(甲基)丙烯酸苯乙醇酯类化合物的制备方法
ES2720326T3 (es) 2011-08-03 2019-07-19 Cognis Ip Man Gmbh Procedimiento para preparar ésteres de ácido (met)acrílico de polioles
CN103827244B (zh) * 2011-09-26 2016-02-03 3M创新有限公司 具有使用(甲基)丙烯酸(2-异丙基-5-甲基)己酯制备的基于(甲基)丙烯酸的弹性体材料的压敏粘合剂
DE102012217943A1 (de) 2012-10-01 2014-05-15 Basf Se Kontinuierliches Verfahren zur Herstellung von (Meth)acrylaten von C10-Alkoholgemischen
US9388118B2 (en) * 2012-10-01 2016-07-12 Basf Se Continuous process for preparing (meth)acrylates of C10-alcohol mixtures
EP2735595A1 (en) 2012-11-23 2014-05-28 3M Innovative Properties Company Multilayer pressure-sensitive adhesive assembly
FR3002771B1 (fr) * 2013-03-01 2015-02-27 Arkema France Procede de production d'acrylate de 2-propyl heptyle par transesterefication
EP2803712A1 (en) 2013-05-17 2014-11-19 3M Innovative Properties Company Multilayer Pressure Sensitive Adhesive Assembly
EP2803711B1 (en) 2013-05-17 2018-06-27 3M Innovative Properties Company Pressure sensitive adhesive assembly comprising filler material
US20160090348A1 (en) 2014-09-30 2016-03-31 Basf Se Preparation of c8-c24 alkyl (meth)acrylates
WO2016071052A1 (de) 2014-11-05 2016-05-12 Basf Se Verfahren zur herstellung von c8-c22-alkyl(meth)acrylaten
WO2024090423A1 (ja) * 2022-10-24 2024-05-02 株式会社日本触媒 （メタ）アクリレート含有組成物

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3134347B2 (ja) * 1990-08-10 2001-02-13 日本合成化学工業株式会社 アクリル酸デシルエステル組成物
JP3149474B2 (ja) * 1991-09-13 2001-03-26 チッソ株式会社 新規メタクリレート
JPH0570404A (ja) 1991-09-13 1993-03-23 Chisso Corp 新規アクリレート
DE19604253A1 (de) 1996-02-06 1997-08-07 Basf Ag Verfahren zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure
DE19604267A1 (de) 1996-02-06 1997-08-07 Basf Ag Verfahren zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure
DE19941136A1 (de) 1999-08-30 2001-03-01 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
DE10036879A1 (de) 2000-07-28 2001-09-20 Basf Ag Verfahren zur Herstellung von Estern der (Meth)acrylsäure
DE10063175A1 (de) * 2000-12-18 2002-06-20 Basf Ag Verfahren zur Herstellung von höheren (Meth)acrylsäureestern
WO2002055472A1 (de) 2000-12-18 2002-07-18 Basf Aktiengesellschaft Verfahren zur herstellung von höheren (meth)acrylsäureestern
DE10154714A1 (de) * 2001-11-09 2002-11-07 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
DE102007001540A1 (de) 2006-02-02 2007-08-09 Basf Ag C10/C6-Estergemische auf Basis 2-Propylheptanol

Also Published As

Publication number Publication date
KR101653843B1 (ko) 2016-09-02
US8318970B2 (en) 2012-11-27
US20100317887A1 (en) 2010-12-16
WO2009106550A1 (de) 2009-09-03
ATE522492T1 (de) 2011-09-15
ES2369339T3 (es) 2011-11-29
BRPI0908521A2 (pt) 2015-09-29
CA2715712A1 (en) 2009-09-03
JP5506700B2 (ja) 2014-05-28
EP2257519A1 (de) 2010-12-08
KR20100133386A (ko) 2010-12-21
EP2257519B1 (de) 2011-08-31
CN101959838A (zh) 2011-01-26
JP2011513275A (ja) 2011-04-28
CN101959838B (zh) 2015-05-13
WO2009106550A9 (de) 2009-11-12

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