MX171749B - Proceso para la produccion de iminodiacetonitrilo a patir de glicolonitrilo y amoniaco o su sal - Google Patents
Proceso para la produccion de iminodiacetonitrilo a patir de glicolonitrilo y amoniaco o su salInfo
- Publication number
- MX171749B MX171749B MX023020A MX2302090A MX171749B MX 171749 B MX171749 B MX 171749B MX 023020 A MX023020 A MX 023020A MX 2302090 A MX2302090 A MX 2302090A MX 171749 B MX171749 B MX 171749B
- Authority
- MX
- Mexico
- Prior art keywords
- ammonia
- glycolonitrile
- salt
- iminodiacetonitrile
- production
- Prior art date
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title abstract 11
- 229910021529 ammonia Inorganic materials 0.000 title abstract 5
- LTYRAPJYLUPLCI-UHFFFAOYSA-N glycolonitrile Chemical compound OCC#N LTYRAPJYLUPLCI-UHFFFAOYSA-N 0.000 title abstract 4
- JMANVNJQNLATNU-UHFFFAOYSA-N glycolonitrile Natural products N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 title abstract 4
- BSRDNMMLQYNQQD-UHFFFAOYSA-N iminodiacetonitrile Chemical compound N#CCNCC#N BSRDNMMLQYNQQD-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 150000003839 salts Chemical class 0.000 title abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- 150000003863 ammonium salts Chemical class 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
- C07C255/24—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and singly-bound nitrogen atoms, not being further bound to other hetero atoms, bound to the same saturated acyclic carbon skeleton
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La presente invención se refiere a un proceso intermitente para formar iminodiacetonitrilo, caracterizado porque comprende hacer reaccionar el glicolonitrilo con amoníaco, sal de amonio no nocivas para la formación del iminodiacetonitrilo, o una mezcla de amoniaco y la sal de amonio, el amoníaco, la sal de amonio o una mezcla que se adiciona al glicolonitrilo en una relación en mol de glicolonitrilo a la porción de amoníaco de aproximadamente 1.5-2.5:1 y en una razón suficiente para mantener el pH durante la reacción en un rango de desde aproximadamente 5 hasta aproximadamente 7 mientras que se mantiene una temperatura de reacción de aproximadamente 40 a aproximadamente 150 grados C.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US42741489A | 1989-10-26 | 1989-10-26 | |
US07/597,247 US5187301A (en) | 1989-10-26 | 1990-10-11 | Preparation of iminodiacetonitrile from glycolonitrile |
Publications (1)
Publication Number | Publication Date |
---|---|
MX171749B true MX171749B (es) | 1993-11-11 |
Family
ID=27027389
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX023020A MX171749B (es) | 1989-10-26 | 1990-10-25 | Proceso para la produccion de iminodiacetonitrilo a patir de glicolonitrilo y amoniaco o su sal |
Country Status (9)
Country | Link |
---|---|
US (1) | US5187301A (es) |
EP (1) | EP0426394B1 (es) |
JP (1) | JPH04193854A (es) |
AU (1) | AU626144B2 (es) |
CA (1) | CA2028502A1 (es) |
DE (1) | DE69015776T2 (es) |
DK (1) | DK0426394T3 (es) |
ES (1) | ES2066153T3 (es) |
MX (1) | MX171749B (es) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2198867A1 (en) * | 2001-12-07 | 2010-06-23 | Vertex Pharmaceuticals, Inc. | Pyrimidine-based compounds useful as GSK-3 inhibitors |
US7445917B2 (en) * | 2004-12-22 | 2008-11-04 | E.I. Du Pont De Nemours And Company | Process for producing glycolic acid from formaldehyde and hydrogen cyanide |
EP1833784B1 (en) * | 2004-12-22 | 2010-10-20 | E.I. Dupont De Nemours And Company | Process for the synthesis of glycolonitrile |
EP1894910B1 (en) * | 2005-05-27 | 2015-02-25 | Asahi Kasei Chemicals Corporation | Method for producing glycolic acid |
CN1331844C (zh) * | 2006-03-30 | 2007-08-15 | 重庆紫光化工有限责任公司 | 亚氨基二乙腈的制备工艺 |
CN100558699C (zh) * | 2006-06-23 | 2009-11-11 | 北京紫光英力化工技术有限公司 | 一种以羟基乙腈为原料制备亚氨基二乙酸的方法 |
WO2008104578A1 (de) | 2007-03-01 | 2008-09-04 | Basf Se | Verfahren zur herstellung von ethylenaminen aus roh-aan |
JP5415286B2 (ja) * | 2007-03-01 | 2014-02-12 | ビーエーエスエフ ソシエタス・ヨーロピア | エチレンアミン混合物の製造方法 |
US8153845B2 (en) | 2007-03-01 | 2012-04-10 | Basf Se | Method for producing aminonitriles |
CN101622223B (zh) * | 2007-03-01 | 2013-04-24 | 巴斯夫欧洲公司 | 制备亚乙基胺的方法 |
US7871802B2 (en) * | 2007-10-31 | 2011-01-18 | E.I. Du Pont De Nemours And Company | Process for enzymatically converting glycolonitrile to glycolic acid |
US7695945B2 (en) * | 2007-10-31 | 2010-04-13 | E. I. Du Pont De Nemours And Company | Immobilized microbial nitrilase for production of glycolic acid |
US7741088B2 (en) | 2007-10-31 | 2010-06-22 | E.I. Dupont De Nemours And Company | Immobilized microbial nitrilase for production of glycolic acid |
WO2009079861A1 (zh) * | 2007-12-25 | 2009-07-02 | Beijing Unis Insight Chemical Technology Co., Ltd. | 一种以羟基乙腈为原料制备亚氨基二乙酸的方法 |
CN101914037B (zh) * | 2010-09-14 | 2012-11-28 | 四川泸天化股份有限公司 | 生产高纯度亚氨基二乙腈的工艺 |
CN102633663B (zh) * | 2012-03-20 | 2015-03-25 | 石家庄杰克化工有限公司 | 清洁工艺生产氮川三乙酸 |
CN103787919B (zh) * | 2012-12-27 | 2016-06-29 | 三达膜科技(厦门)有限公司 | 一种亚氨基二乙腈的脱色方法 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR746641A (fr) * | 1931-12-31 | 1933-06-02 | Ig Farbenindustrie Ag | Procédé pour la préparation d'acides alpha-amino-carboxylique, d'acides imino-dicarboxyliques et de leurs sels |
US2442547A (en) * | 1946-05-07 | 1948-06-01 | Sinclair Refining Co | Method of producing iminodiacetonitrile |
US2511487A (en) * | 1946-08-08 | 1950-06-13 | Du Pont | Synthesis of iminodiacetonitrile |
GB744675A (en) * | 1952-03-12 | 1956-02-15 | Rohm & Haas | Improvements in or relating to new cyanoaminonitriles and process for their manufacture |
US2731490A (en) * | 1953-01-28 | 1956-01-17 | Barsky George | Method of making cyanohydrins |
US2752383A (en) * | 1953-10-19 | 1956-06-26 | Monsanto Chemicals | Production of formaldehyde cyanohydrin |
US2794044A (en) * | 1955-08-30 | 1957-05-28 | Du Pont | Synthesis of iminodiacetonitrile |
US3107581A (en) * | 1958-05-22 | 1963-10-22 | Ackerman Nathan | Hydropneumatic feed device |
US3167581A (en) * | 1962-04-12 | 1965-01-26 | American Cyanamid Co | Process for the preparation of n-methylene glycinonitrile |
US3167580A (en) * | 1962-04-12 | 1965-01-26 | American Cyanamid Co | Process for the preparation of iminodiacetonitrile |
US3412137A (en) * | 1965-10-14 | 1968-11-19 | Geigy Chemical Company | Process for the preparation of nitriles |
US3904668A (en) * | 1973-11-15 | 1975-09-09 | Grace W R & Co | Process for preparing iminodiacetonitrile and alkali metal iminodiacetates |
US3988360A (en) * | 1973-11-15 | 1976-10-26 | W. R. Grace & Co. | Process for preparing iminodiacetonitrile |
JPS5368725A (en) * | 1976-11-29 | 1978-06-19 | Showa Denko Kk | Preparation of glycollonitrile |
DE3242193A1 (de) * | 1982-11-15 | 1984-05-17 | Basf Ag, 6700 Ludwigshafen | Neue (alpha)-iminodiacetonitrile und verfahren zu ihrer herstellung |
US4661614A (en) * | 1986-03-06 | 1987-04-28 | Monsanto Company | Process for the preparation of iminodiacetonitrile |
US4895971A (en) * | 1988-10-31 | 1990-01-23 | W. R. Grace & Co.-Conn. | Process for the production of iminodiacetonitrile |
US4948909A (en) * | 1989-08-14 | 1990-08-14 | Monsanto Company | Process for the preparation of iminodiacetonitrile and iminodiacetic acid |
-
1990
- 1990-10-11 US US07/597,247 patent/US5187301A/en not_active Expired - Fee Related
- 1990-10-24 CA CA002028502A patent/CA2028502A1/en not_active Abandoned
- 1990-10-25 MX MX023020A patent/MX171749B/es unknown
- 1990-10-25 JP JP2286013A patent/JPH04193854A/ja active Pending
- 1990-10-26 DK DK90311768.7T patent/DK0426394T3/da active
- 1990-10-26 AU AU65541/90A patent/AU626144B2/en not_active Ceased
- 1990-10-26 DE DE69015776T patent/DE69015776T2/de not_active Expired - Fee Related
- 1990-10-26 EP EP90311768A patent/EP0426394B1/en not_active Expired - Lifetime
- 1990-10-26 ES ES90311768T patent/ES2066153T3/es not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE69015776T2 (de) | 1995-05-11 |
DK0426394T3 (da) | 1995-03-13 |
EP0426394B1 (en) | 1995-01-04 |
CA2028502A1 (en) | 1991-04-27 |
JPH04193854A (ja) | 1992-07-13 |
US5187301A (en) | 1993-02-16 |
AU6554190A (en) | 1991-05-02 |
ES2066153T3 (es) | 1995-03-01 |
EP0426394A1 (en) | 1991-05-08 |
DE69015776D1 (de) | 1995-02-16 |
AU626144B2 (en) | 1992-07-23 |
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