KR960034120A - Manufacturing method of carbon / carbon composite material of high density structure - Google Patents

Manufacturing method of carbon / carbon composite material of high density structure Download PDF

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Publication number
KR960034120A
KR960034120A KR1019950004899A KR19950004899A KR960034120A KR 960034120 A KR960034120 A KR 960034120A KR 1019950004899 A KR1019950004899 A KR 1019950004899A KR 19950004899 A KR19950004899 A KR 19950004899A KR 960034120 A KR960034120 A KR 960034120A
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South Korea
Prior art keywords
carbon
composite material
producing
carbon composite
added
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KR1019950004899A
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Korean (ko)
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KR970010311B1 (en
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박수진
이재락
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유현식
제일모직 주식회사
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Priority to KR1019950004899A priority Critical patent/KR970010311B1/en
Publication of KR960034120A publication Critical patent/KR960034120A/en
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Publication of KR970010311B1 publication Critical patent/KR970010311B1/en

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/71Ceramic products containing macroscopic reinforcing agents
    • C04B35/78Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
    • C04B35/80Fibres, filaments, whiskers, platelets, or the like
    • C04B35/83Carbon fibres in a carbon matrix
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/62645Thermal treatment of powders or mixtures thereof other than sintering
    • C04B35/6267Pyrolysis, carbonisation or auto-combustion reactions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52Constituents or additives characterised by their shapes
    • C04B2235/5208Fibers
    • C04B2235/5212Organic
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6562Heating rate
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74Physical characteristics
    • C04B2235/77Density

Abstract

본 발명은 탄소/탄소 복합재료의 제조에 있어서, 신속한 열처리 속도와 냉각속도를 유지케 하고, 계속되어지는 재함침/재탄화에 따라 점진적인 밀도 증가와 기공율 감소를 가져오게 하여 탄소/탄소 복합재료의 기계적 강도와 탄성률, 열적 안정성을 높이기 위한 것으로, 한 종류 이상의 강화 섬유 수단 및 한 종류 이상의 수지를 포함하는 탄소 모체를 그 기본 성분으로 하여 탄소/탄소 복합재료 제조시에, 전체적인 또는 부분적인 보강섬유의 방향성 구조를 가지게 하여, 경화와 탄화과정 중 열분해 발생 기체가 방출 방향성을 가지게 함을 특징으로 한다.The present invention is to maintain a rapid heat treatment rate and cooling rate in the production of carbon / carbon composites, and to increase the density and decrease the porosity of the carbon / carbon composite material with the subsequent re-impregnation / recarbonization In order to improve the mechanical strength, elastic modulus and thermal stability, the carbon matrix containing at least one kind of reinforcing fiber means and at least one kind of resin is used as a base component. It has a directional structure, characterized in that the pyrolysis generating gas has a release direction during the curing and carbonization process.

Description

고밀도 구조의 탄소/탄소 복합재료의 제조방법Manufacturing method of carbon / carbon composite material of high density structure

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

Claims (7)

한 종류 이상의 강화섬류 및한 종류 이상의 수지를 포함하는 탄소 모체를 그 기본 성분으로 하며, 이를 열처리하여 경화 및 탄화시키는 탄소/탄소 복합재료 제조에 있어서, 전체적으로 또는 부분적으로 보상섬유를 방향성 구조를 가지게 함으로써 경화 및 탄화과정 중 발생되는 열분해 기체가 방풀 방향성을 가지게 하는 것을 특징으로 하는 고밀도 구조의 탄소/탄소 복합재료의 제조방법.A carbon matrix comprising at least one type of reinforcing island and at least one type of resin is used as a basic component, and in the production of a carbon / carbon composite material which is cured and carbonized by heat treatment, the compensation fiber has a directional structure in whole or in part. A method of producing a carbon / carbon composite material having a high density structure, characterized in that the pyrolysis gas generated during the curing and carbonization process has a directional pooling. 제1항에 있어서, 열처리 속도는 시간당 50~300℃인 것을 특징으로 하는 고밀도 구조의 탄소/탄소 복합재료의 제조방법.The method of claim 1, wherein the heat treatment rate is 50 ~ 300 ℃ per hour. 제1항에 있어서, 녹는점이 2000℃ 이상인 초고내열성 탄소질계의 충진제를 약 1~5중량% 첨가하는 것을 특징으로 하는 고밀도 구조의 탄소/탄소 복합재료의 제조방법.The method for producing a carbon / carbon composite material according to claim 1, wherein about 1 to 5% by weight of an ultra high heat resistant carbonaceous filler having a melting point of 2000 ° C. or more is added. 제3항에 있어서, 첨가되는 충진제의 입경이 사용된 섬유 직경보다 작은 것을 특징으로 하는 고밀도 구조의 탄소/탄소 복합재료의 제조방법.4. A method for producing a carbon / carbon composite material according to claim 3, wherein the particle diameter of the filler to be added is smaller than the fiber diameter used. 제3항 또는 제4항에 있어서, 첨가되는 충진제의 입경이 사용된 섬유 직경보다 ⅓이하의 작은 것을 특징으로 하는 고밀도 구조의 탄소/탄소 복합재료의 제조방법.The method for producing a carbon / carbon composite material according to claim 3 or 4, wherein the particle diameter of the filler to be added is smaller than or equal to the fiber diameter used. 제1항에 있어서, 분말첨가제 또는 섬유코팅제를 첨가하는 것을 특징으로 하는 고밀도 구조의 탄소/탄소 복합재료의 제조방법.The method for producing a carbon / carbon composite material according to claim 1, wherein a powder additive or a fiber coating agent is added. 제6항에 있어서, 분말첨가제 또는 섬유코팅제를 복합재료의 열처리온도 보다 높은 녹는 점을 가지는 것을 특징으로 하는 고밀도 구조의 탄소/탄소 복합재료의 제조방법.The method of claim 6, wherein the powder additive or the fiber coating agent has a melting point higher than the heat treatment temperature of the composite material. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019950004899A 1995-03-10 1995-03-10 Process for the preparation of composite material of carbon/carbon KR970010311B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019950004899A KR970010311B1 (en) 1995-03-10 1995-03-10 Process for the preparation of composite material of carbon/carbon

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019950004899A KR970010311B1 (en) 1995-03-10 1995-03-10 Process for the preparation of composite material of carbon/carbon

Publications (2)

Publication Number Publication Date
KR960034120A true KR960034120A (en) 1996-10-22
KR970010311B1 KR970010311B1 (en) 1997-06-25

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KR1019950004899A KR970010311B1 (en) 1995-03-10 1995-03-10 Process for the preparation of composite material of carbon/carbon

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KR970010311B1 (en) 1997-06-25

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