KR960000854A - Method for preparing tertiary amine - Google Patents

Method for preparing tertiary amine Download PDF

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Publication number
KR960000854A
KR960000854A KR1019940015520A KR19940015520A KR960000854A KR 960000854 A KR960000854 A KR 960000854A KR 1019940015520 A KR1019940015520 A KR 1019940015520A KR 19940015520 A KR19940015520 A KR 19940015520A KR 960000854 A KR960000854 A KR 960000854A
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KR
South Korea
Prior art keywords
amine compound
amine
tertiary amine
preparing
salt effect
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Application number
KR1019940015520A
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Korean (ko)
Inventor
김윤철
박인수
Original Assignee
하기주
코오롱 주식회사
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Publication date
Application filed by 하기주, 코오롱 주식회사 filed Critical 하기주
Priority to KR1019940015520A priority Critical patent/KR960000854A/en
Publication of KR960000854A publication Critical patent/KR960000854A/en

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Abstract

본 발명은 경질, 연질 폴리우레탄 발포 및 엘라스토머 등의 발포촉매로 사용되는 트리아민구조를 갖는 아래구조식(I)로 표시되는 3차아민의 제조방법에 관한 것으로,The present invention relates to a method for preparing a tertiary amine represented by the following structural formula (I) having a triamine structure used as a foaming catalyst such as hard, flexible polyurethane foam and elastomer,

위 식에서, n=1~5의 정수이다. 1차아민, 2차아민 혹은 고리구조를 갖는 아민화합물을 메틸화시켜 일반식 (I)의 3차아민 화합물을 제조함에 있어서, 상기 아민화합물을 포름산 및 파라포름알데히드와 반응시킨 후 가성소다 수용액으로 중화하여 염효과에 의해 층분리를 하여 제조한다.In the above formula, n = 1-5. In preparing a tertiary amine compound of general formula (I) by methylating a primary amine, a secondary amine or an amine compound having a ring structure, the amine compound is reacted with formic acid and paraformaldehyde and neutralized with an aqueous solution of caustic soda. To prepare a layer by the salt effect.

본 발명의 방법은 부반응이 거의 없고 정량적으로 반응이 진행되며 염효과에 의하여 펜타메틸디에틸렌트리아민이 물층과 분리되어 그 정제법이 간편한 새로운 제조방법이다.In the method of the present invention, there is almost no side reaction, the reaction proceeds quantitatively, and pentamethyldiethylenetriamine is separated from the water layer by the salt effect, and thus the purification method is simple.

Description

3차아민의 제조방법Method for preparing tertiary amine

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음As this is a public information case, the full text was not included.

Claims (1)

1차아민, 2차아민 혹은 고리구조를 갖는 아민화합물을 메틸화시켜 일반식 (I)의 3차아민 화합물을 제조함에 있어서, 상기 아민화합물을 포름산 및 파라포름알데히드와 반응시킨 후 가성소다 수용액으로 중화하여 염효과에 의해 층분리함을 특징으로 하는 일반식(I)의 3차아민화합물의 제조방법.In preparing a tertiary amine compound of general formula (I) by methylating a primary amine, a secondary amine or an amine compound having a ring structure, the amine compound is reacted with formic acid and paraformaldehyde and neutralized with an aqueous solution of caustic soda. To separate the layers by the salt effect. 위 식에서, n=1~5의 정수이다.In the above formula, n = 1-5. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019940015520A 1994-06-30 1994-06-30 Method for preparing tertiary amine KR960000854A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019940015520A KR960000854A (en) 1994-06-30 1994-06-30 Method for preparing tertiary amine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019940015520A KR960000854A (en) 1994-06-30 1994-06-30 Method for preparing tertiary amine

Publications (1)

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KR960000854A true KR960000854A (en) 1996-01-25

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KR1019940015520A KR960000854A (en) 1994-06-30 1994-06-30 Method for preparing tertiary amine

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5985993A (en) * 1996-08-01 1999-11-16 Cheil Industries, Inc. Method for preparing polybutadiene latex
KR100352551B1 (en) * 1995-12-27 2003-04-21 주식회사 코오롱 Process for preparing tertiary amines
US20210388199A1 (en) * 2018-08-27 2021-12-16 Zeon Corporation Styrene-based block copolymer latex

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100352551B1 (en) * 1995-12-27 2003-04-21 주식회사 코오롱 Process for preparing tertiary amines
US5985993A (en) * 1996-08-01 1999-11-16 Cheil Industries, Inc. Method for preparing polybutadiene latex
US6365669B1 (en) 1996-08-01 2002-04-02 Cheil Industries Inc. Method for preparing polybutadiene latex
US20210388199A1 (en) * 2018-08-27 2021-12-16 Zeon Corporation Styrene-based block copolymer latex
US11958969B2 (en) * 2018-08-27 2024-04-16 Zeon Corporation Styrene-based block copolymer latex

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