KR950701654A - ADHESIVE AGENT CONTAINING POLYSILOXANE-GRAFTED POLYMER AND COSMETIC COMPOSITIONS THEREOF - Google Patents

ADHESIVE AGENT CONTAINING POLYSILOXANE-GRAFTED POLYMER AND COSMETIC COMPOSITIONS THEREOF

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Publication number
KR950701654A
KR950701654A KR1019940704063A KR19940704063A KR950701654A KR 950701654 A KR950701654 A KR 950701654A KR 1019940704063 A KR1019940704063 A KR 1019940704063A KR 19940704063 A KR19940704063 A KR 19940704063A KR 950701654 A KR950701654 A KR 950701654A
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South Korea
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weight
polysiloxane
vinyl
monomer
adhesive
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KR1019940704063A
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Korean (ko)
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마트 토거슨 피터
토마스 발츄나스 앤토니
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제이코버스 코넬리스 레이서
더 프록터 앤드 갬블 캄파니
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Publication of KR950701654A publication Critical patent/KR950701654A/en

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/02—Preparations for cleaning the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/08—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated side groups
    • C08F290/14—Polymers provided for in subclass C08G
    • C08F290/148—Polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J155/00—Adhesives based on homopolymers or copolymers, obtained by polymerisation reactions only involving carbon-to-carbon unsaturated bonds, not provided for in groups C09J123/00 - C09J153/00
    • C09J155/005—Homopolymers or copolymers obtained by polymerisation of macromolecular compounds terminated by a carbon-to-carbon double bond
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
    • C09J4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/04—Preparations for permanent waving or straightening the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/12—Preparations containing hair conditioners

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  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Medicinal Chemistry (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

(a) 전형적으로 유리 라디칼 중합에 의해 폴리실록산 함유 단량체 및 폴리실록산 비함유 단량체를 중합시켜 제조한 폴리실록산 그래프트된 중합체를 포함하고; (b) 약 20,000이상의 중량 평균 분자량을 갖고, 약 1 내지 약 50중량%의 폴리실록산 함유 단량체를 함유하고; (c) 미반응된 실리콘 단량체 및 폴리실록산 그래프트된 중합체로서 존재하는 전체 실리콘을 기준으로 25℃에서 약 10,000,000 센티스톡 미만의 점도를 갖는 실리콘 그래프트된 중합체 및 미반응된 폴리실록산 함유 단량체의 중량%가 약 15%이하인 중합체성 접착제를 개시한다. 또한 상기 접착제를 25℃에서 약 10,000,000 센티스톡 미만의 점도를 갖는 폴리실록산 그래프트된 중합체 및 미반응된 폴리실록산 함유 단량체를 약 4중량% 이하로 함유한다. 상기 접착제를 함유하는 화장료 조성물을 또한 개시한다.(a) typically comprising a polysiloxane grafted polymer prepared by polymerizing a polysiloxane containing monomer and a polysiloxane free monomer by free radical polymerization; (b) has a weight average molecular weight of at least about 20,000 and contains about 1 to about 50 weight percent polysiloxane containing monomers; (c) about 15% by weight of the silicone grafted polymer and the unreacted polysiloxane containing monomer having a viscosity of less than about 10,000,000 centistokes at 25 ° C. based on the total silicone present as the unreacted silicone monomer and the polysiloxane grafted polymer. A polymeric adhesive of less than or equal to% is disclosed. The adhesive also contains up to about 4% by weight of polysiloxane grafted polymer and unreacted polysiloxane containing monomer having a viscosity of less than about 10,000,000 centistokes at 25 ° C. Also disclosed is a cosmetic composition containing the adhesive.

Description

폴리실록산-그래프트된 중합체를 함유하는 접착제 및 그의 화장료 조성물(ADHESIVE AGENT CONTAINING POLYSILOXANE-GRAFTED POLYMER AND CONSMETIC COMPOSITIONS THEREOF)ADHESIVE AGENT CONTAINING POLYSILOXANE-GRAFTED POLYMER AND CONSMETIC COMPOSITIONS THEREOF

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

Claims (12)

폴리실록산-그래프트된 중합체 및 미반응된 폴리실록산 함유 단량체로서 존재하는 전체 실리콘을 기준으로 25℃에서 10,000,000 셀티스톡 미만의 점도를 갖는 폴리실록산-그래프트된 중합체 및 미반응된 폴리실록산 함유 단량체로서 존재하는 실리콘의 중량%가 15%이하임을 특징으로 하는, 20,000이상의 중량 평균 분자량을 갖고, 1 내지 50중량%의 폴리실록산 함유 단량체를 함유하며, 25℃에서 10,000,000 센티스톡 미만의 점도를 갖는 폴리실록산-그래프트된 중합체 및 미반응된 폴리실록산 함유 단량체를 4중량% 이하로 함유하는 폴리실록산 함유 단량체와 폴리실록산 비함유 단량체를 중합시킴으로써 제조된 폴리실록산-그래프트된 중합체를 포함하는 중합체성 접착제.Weight percent of silicone present as polysiloxane-grafted polymer and unreacted polysiloxane containing monomer at 25 ° C. based on total silicone present as polysiloxane-grafted polymer and unreacted polysiloxane containing monomer. Polysiloxane-grafted polymer and unreacted having a weight average molecular weight of 20,000 or more, containing 1 to 50% by weight of polysiloxane containing monomers, and having a viscosity of less than 10,000,000 centistokes at 25 ° C. A polymeric adhesive comprising a polysiloxane-grafted polymer prepared by polymerizing a polysiloxane containing monomer and a polysiloxane free monomer containing up to 4% by weight of a polysiloxane containing monomer. 제1항에 있어서, 상기 폴리실록산-그래프트된 중합체 및 미반응된 폴리실록산 함유 단량체로서 존재하는 전체 실리콘을 기준으로 25℃에서 10,000,000 셀티프톡 미만의 점도를 갖는 플리실록산-그래프트된 중합체 및 미반응된 폴리실록산 함유 단량체의 중량%가 10%이하, 바람직하게 5%이하이고, 25℃에서 10,000,000 센티스톡 미만의 점도를 갖는 폴리실폭산산-그래프트된 중합체 및 미반응된 폴리실폭산 함유 단량체를 3중량%이하, 바람직하게 1중량% 이하로 함유하는 접착제.The polysiloxane-grafted polymer and unreacted polysiloxane containing polysiloxane-grafted polymer and unreacted polysiloxane-containing monomer according to claim 1 having a viscosity of less than 10,000,000 Celtiftock at 25 ° C. based on total silicone present. Less than or equal to 3% by weight of the polysiloxanes-grafted polymer and unreacted polysiloxanes containing monomers having a viscosity of 10% or less, preferably 5% or less, and having a viscosity of 25.00 C. less than 10,000,000 centistokes at 25 ° C. To 1% by weight or less. 제1항 또는 제2항에 있어서, 상기 접착제의 중량 평균 분자량이 75,000이상, 바람직하게 100,000이상, 보다 바람직하게 100,000내지 750,000인 접착제.The adhesive according to claim 1 or 2, wherein the adhesive has a weight average molecular weight of at least 75,000, preferably at least 100,000, more preferably from 100,000 to 750,000. 제1항 내지 제3항중 어느 한 항에 있어서, 상기 중합체가 상기 접착제의 중량을 기준으로 50 내지 99중량%의 에틸렌형으로 불포화된 중합성 단량체, 및 1,000이상의 분자량을 갖는 하기 일반식의 폴리실록산 함유 단량체 1 내지 50중량%, 바람직하게 2 내지 25중량%를 포함하는 접착제 :The polymer according to any one of claims 1 to 3, wherein the polymer contains 50 to 99% by weight of an ethylenically unsaturated polymerizable monomer based on the weight of the adhesive, and a polysiloxane having a molecular weight of 1,000 or more. Adhesives comprising from 1 to 50%, preferably from 2 to 25%, by weight of monomers: X(Y)nSi(R)3-m(Z)m X (Y) n Si (R) 3-m (Z) m 상기식에서, X는 상기 A 및 B 단량체와 공중합가능한 비닐 그룹이고, Y는 2가의 결합 그룹이고, R은 수소, 하이드록시, 저급 알킬, 아릴, 알크아릴, 알킬아미노 또는 알콕시이고, Z는 500이상의 수 평균 분자량을 갖는 1가의 실록산 중합체성 잔기이고, 공중합 조건하에서 필수적으로 비반응성이며, 중합후에 상기 비닐 중합체성 주쇄의 펜던트가 되고, n은 0 또는 1이고, m은 1 내지 3의 정수이다.Wherein X is a vinyl group copolymerizable with the A and B monomers, Y is a divalent bonding group, R is hydrogen, hydroxy, lower alkyl, aryl, alkaryl, alkylamino or alkoxy and Z is 500 It is a monovalent siloxane polymeric moiety having a number average molecular weight or more, which is essentially non-reactive under copolymerization conditions, becomes a pendant of the vinyl polymeric main chain after polymerization, n is 0 or 1 and m is an integer of 1 to 3. . 제4항에 있어서, 상기 폴리실록산 비함유 단량체가 유리 라디칼 중합성 비닐인 접착제.The adhesive of claim 4 wherein said polysiloxane free monomer is free radically polymerizable vinyl. 제4항 또는 제5항에 있어서, 상기 폴리실록산 비함유 단량체가 C1-C18알콜의 아크릴산 에스테르 또는 C1-C18알콜의 메타크릴산 에스테르, 스티렌, 폴리스티렌 거대단량체, 비닐 아세테이트, 비닐 클로라이드, 비닐 프로피오네이트, 비닐리덴 클로라이드, 알파-메틸스티렌, t-부틸스티렌, 부타디엔, 사이클로헥사디엔, 에틸렌 프로필렌, 비닐 톨루엔, 아크릴산, 메타크릴산, N,N-디메틸아크릴아미드, 디메틸 아미노에틸 메타크릴레이트, 4급화된 디메틸아미노에틸 메타그릴레이트, 메타크릴아미드, N-t-부틸-아크릴아미드, 말렌산, 말렌산 무수물, 말렌산 무수물의 반 에스테르, 크로톤산, 아타콘산, 아크릴아미드, 아크릴레이트 알콜, 하이드록시 에틸 메타크릴레이트, 디아릴디메틸 암모늄 클로라이드, 비닐 필로리돈, 비닐 에테르, 말레이미드, 비닐 피리딘, 비닐 이마다졸, 스티렌 솔포네이트, 알릴 알콜, 비닐 카프로락탐, 및 이들의 혼합물로 이루어진 그룹중에서 선택된 소수성 단량체; 및 아크릴산, 메타크릴산, N,N-디메틸아크릴아미드, 디메틸아미노에틸 메타크릴레이트, 4급화된 디메틸아미노에틸 메타크릴레이트, 메타크릴아미드, N-t-부틸 아크릴아미드, 말렌산, 말렌산 무수물 및 그의 반 에스테르, 크로톤산, 아타콘산, 아크릴아미드, 아크릴레이트 알콜, 하이드록시에틸 메타크릴레이트, 디알릴디메틸 암모늄 클로라이드, 비닐 피롤리돈, 비닐 에테르, 말레이미드, 비닐 피리딘, 비닐 이미다졸, 기타 극성 비닐 헤테로사이클릭, 스티렌 설포네이트, 알릴 알콜, 비닐 알콜, 비닐 카프로락탐, 상기 산 및 아민의 염, 및 이들의 혼합물로 이루어진 그룹중에서 선택된 친수성 단량체로 이루어진 그룹중에서 선책된 친수성.Of claim 4 or claim 5, wherein the non-polysiloxane-containing monomers is C 1 -C 18 alcohol ester of acrylic acid or C 1 -C 18 alcohol esters of methacrylic acid, styrene, polystyrene macromer, vinyl acetate, vinyl chloride, Vinyl propionate, vinylidene chloride, alpha-methylstyrene, t-butylstyrene, butadiene, cyclohexadiene, ethylene propylene, vinyl toluene, acrylic acid, methacrylic acid, N, N-dimethylacrylamide, dimethyl aminoethyl methacryl Latex, quaternized dimethylaminoethyl methacrylate, methacrylamide, Nt-butyl-acrylamide, maleic acid, maleic anhydride, half ester of maleic anhydride, crotonic acid, ataconic acid, acrylamide, acrylate alcohol, Hydroxy ethyl methacrylate, diaryldimethyl ammonium chloride, vinyl pilolidone, vinyl ether, maleimide, vinyl pyridine Hydrophobic monomers selected from the group consisting of vinyl imidazole, styrene sulphonate, allyl alcohol, vinyl caprolactam, and mixtures thereof; And acrylic acid, methacrylic acid, N, N-dimethylacrylamide, dimethylaminoethyl methacrylate, quaternized dimethylaminoethyl methacrylate, methacrylamide, Nt-butyl acrylamide, maleic acid, maleic anhydride and their Half ester, crotonic acid, ataconic acid, acrylamide, acrylate alcohol, hydroxyethyl methacrylate, diallyldimethyl ammonium chloride, vinyl pyrrolidone, vinyl ether, maleimide, vinyl pyridine, vinyl imidazole, other polar vinyl Hydrophilicity selected from the group consisting of hydrophilic monomers selected from the group consisting of heterocyclic, styrene sulfonate, allyl alcohol, vinyl alcohol, vinyl caprolactam, salts of the acids and amines, and mixtures thereof. 제6항에 있어서, 상기 소수성 단량체가 t-부틸 아크릴레이트, t-브틸 메타크릴레이트 및 이들의 혼합물로 이루어진 그룹중에서 선택된 친수성.7. Hydrophilic according to claim 6, wherein said hydrophobic monomer is selected from the group consisting of t-butyl acrylate, t-butyl methacrylate and mixtures thereof. 제6항 또는 7항에 있어서, 상기 친수성 단량체가 아크릴산, N-N-디메틸아크릴아미드, 디메틸아미노에틸 메타크릴레이트, 4급화된 디메틸아미노에틸 메타크릴레이트, 비닐 피롤리돈, 상기 산 및 아민의 염, 및 이들의 혼합물로 이루어진 그룹중에서 선택된 접착제.The method according to claim 6 or 7, wherein the hydrophilic monomer is acrylic acid, NN-dimethylacrylamide, dimethylaminoethyl methacrylate, quaternized dimethylaminoethyl methacrylate, vinyl pyrrolidone, salts of the acid and amine, And an adhesive selected from the group consisting of mixtures thereof. 제6항 내지 8항중 어느 한 항에 있어서, 0 내지 85중량%의 상기 소수성 단량체, 14 내지 95중량%의 상기 친수성 단량체, 및 1 내지 40중량%의 상기 폴리실록산 함유 단량체, 바람직하게 5 내지 70중량%의 상기 소수성 단량체, 29 내지 80중량%의 상기 친수성 단량체, 및 2 내지 25중량%의 상기 폴리실록산 함유 단량체를 포함하는 접착제.9 to 8% by weight of the hydrophobic monomer, 14 to 95% by weight of the hydrophilic monomer, and 1 to 40% by weight of the polysiloxane containing monomer, preferably 5 to 70% by weight. An adhesive comprising% of said hydrophobic monomer, 29 to 80% by weight of said hydrophilic monomer, and 2 to 25% by weight of said polysiloxane containing monomer. 제6항 내지 8항중 어느 한 항에 있어서, 0 내지 70중량%의 상기 소수성 단량체, 20 내지 80중량%의 상기 친수성 단량체, 및 1 내지 40중량%의 상기 폴리실록산 함유 단량체, 바람직하게 5 내지 70중량%의 상기 소수성 단량체, 29 내지 60중량%의 상기 친수성 단량체, 및 2 내지 25중량%의 상기 폴리실록산 함유 단량체를 포함하는 접착제.9 to 8% by weight of the hydrophobic monomer, 20 to 80% by weight of the hydrophilic monomer, and 1 to 40% by weight of the polysiloxane containing monomer, preferably 5 to 70% by weight. An adhesive comprising% of said hydrophobic monomer, 29 to 60% by weight of said hydrophilic monomer, and 2 to 25% by weight of said polysiloxane containing monomer. 제1항 내지 10항중 어느 한 항의 접착제 및 모발에 적응하기에 적합한 담체를 포함하는, 헤어 스타일링에 유용한 모발 보호 조성물.A hair care composition useful for hair styling, comprising the adhesive of any one of claims 1 to 10 and a carrier suitable for adapting to hair. 제11항에 있어서, 상기 담체가 물, C1-C61가 알콜 또는 이들의 혼합물을 포함하고, 모발에 스프레이로 적용시키기에 적합한 액체 형태의 모발 보호 조성물.The hair protection composition of claim 11, wherein the carrier comprises water, C 1 -C 6 monohydric alcohols or mixtures thereof and is suitable for spray application to the hair. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019940704063A 1992-05-15 1993-05-11 ADHESIVE AGENT CONTAINING POLYSILOXANE-GRAFTED POLYMER AND COSMETIC COMPOSITIONS THEREOF KR950701654A (en)

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