KR850003336A - 테레프탈산 제조 촉매의 회수 방법 - Google Patents
테레프탈산 제조 촉매의 회수 방법 Download PDFInfo
- Publication number
- KR850003336A KR850003336A KR1019830005365A KR830005365A KR850003336A KR 850003336 A KR850003336 A KR 850003336A KR 1019830005365 A KR1019830005365 A KR 1019830005365A KR 830005365 A KR830005365 A KR 830005365A KR 850003336 A KR850003336 A KR 850003336A
- Authority
- KR
- South Korea
- Prior art keywords
- terephthalic acid
- acetic acid
- production catalyst
- acid production
- recovery method
- Prior art date
Links
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 title claims 8
- 238000000034 method Methods 0.000 title claims 7
- 239000003054 catalyst Substances 0.000 title claims 3
- 238000011084 recovery Methods 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 12
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- 229940011182 cobalt acetate Drugs 0.000 claims 1
- QAHREYKOYSIQPH-UHFFFAOYSA-L cobalt(II) acetate Chemical compound [Co+2].CC([O-])=O.CC([O-])=O QAHREYKOYSIQPH-UHFFFAOYSA-L 0.000 claims 1
- 229940071125 manganese acetate Drugs 0.000 claims 1
- UOGMEBQRZBEZQT-UHFFFAOYSA-L manganese(2+);diacetate Chemical compound [Mn+2].CC([O-])=O.CC([O-])=O UOGMEBQRZBEZQT-UHFFFAOYSA-L 0.000 claims 1
- 239000011259 mixed solution Substances 0.000 claims 1
- 239000012452 mother liquor Substances 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 239000002699 waste material Substances 0.000 claims 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/40—Regeneration or reactivation
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (4)
- 초산 용매 중에서 초산코발트 및 초산망간 촉매 존재하에 p-크실렌을 산화시켜 테레프탈산을 제조함에 있어서, 그 반응 용액으로부터 공지의 방법으로 테레프탈산, 반응모액 및 용매를 분리한 반응폐액의 고형분에 대한 함수율을 25∼40%로 조정하여 800∼850℃에서 안전 소각 산화시켜 얻은 회분을 물 및 98% 초산의 혼합 용망에 용해한 다음 5∼35% 과산화수소와 반응시키는 제1공정과 이 반응액으로부터 미반응 물질을 제거하는 제2공정의 결합으로 구성된 것이 특징인 테레프탈산 제조촉매의 회수 방법.
- 제1항에 있어서, 물의 첨가량을 최종 초산의 농도가 5∼40%로 유지되는 양으로 하는 것이 특징인 방법.
- 제1항에 있어서, 초산과 과산화수소의 첨가비가 1 : 1 내지 10 : 1인 것이 특징인 방법.
- 제1항에 있어서, 제1공정을 30∼80℃ 근처에서 수행하는 것이 특징인 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019830005365A KR850001772B1 (ko) | 1983-11-11 | 1983-11-11 | 테레프탈산 제조 촉매의 회수 방법 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019830005365A KR850001772B1 (ko) | 1983-11-11 | 1983-11-11 | 테레프탈산 제조 촉매의 회수 방법 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR850003336A true KR850003336A (ko) | 1985-06-17 |
| KR850001772B1 KR850001772B1 (ko) | 1985-12-18 |
Family
ID=19230389
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019830005365A KR850001772B1 (ko) | 1983-11-11 | 1983-11-11 | 테레프탈산 제조 촉매의 회수 방법 |
Country Status (1)
| Country | Link |
|---|---|
| KR (1) | KR850001772B1 (ko) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107652177A (zh) * | 2017-10-28 | 2018-02-02 | 浙江上虞利星化工有限公司 | 一种钴或/和锰醋酸盐的制备方法 |
| CN107721847B (zh) * | 2017-10-28 | 2020-07-17 | 浙江上虞利星化工有限公司 | 利用回收钴锰制备醋酸钴锰水溶液的方法 |
-
1983
- 1983-11-11 KR KR1019830005365A patent/KR850001772B1/ko not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| KR850001772B1 (ko) | 1985-12-18 |
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| Date | Code | Title | Description |
|---|---|---|---|
| A201 | Request for examination | ||
| E902 | Notification of reason for refusal | ||
| G160 | Decision to publish patent application | ||
| E701 | Decision to grant or registration of patent right | ||
| GRNT | Written decision to grant | ||
| FPAY | Annual fee payment |
Payment date: 19961030 Year of fee payment: 12 |
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| LAPS | Lapse due to unpaid annual fee |