KR20230097266A - Powder-type Cleansing Composition and Method for Producing Thereof - Google Patents
Powder-type Cleansing Composition and Method for Producing Thereof Download PDFInfo
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- KR20230097266A KR20230097266A KR1020210186232A KR20210186232A KR20230097266A KR 20230097266 A KR20230097266 A KR 20230097266A KR 1020210186232 A KR1020210186232 A KR 1020210186232A KR 20210186232 A KR20210186232 A KR 20210186232A KR 20230097266 A KR20230097266 A KR 20230097266A
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- KR
- South Korea
- Prior art keywords
- cleansing composition
- coating layer
- core
- gum
- powdery
- Prior art date
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- HTJNEBVCZXHBNJ-XCTPRCOBSA-H trimagnesium;(2r)-2-[(1s)-1,2-dihydroxyethyl]-3,4-dihydroxy-2h-furan-5-one;diphosphate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.OC[C@H](O)[C@H]1OC(=O)C(O)=C1O HTJNEBVCZXHBNJ-XCTPRCOBSA-H 0.000 description 1
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- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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Abstract
본 발명은 수분이 거의 없는 분말 타입의 클렌징 조성물 및 그 제조 방법에 관한 것으로, 구체적으로는, 장기 보관에 요구되는 강한 보존제 함량을 최소화하여 고유의 효능을 유지하고 피부 자극이나 트러블 등이 적으며, 즉석 용해시켜 액상 세정액을 형성할 수 있는 사용이 간편한 분말 타입의 세정 조성물과 그 제조방법을 제공한다.
이를 위하여, 본 발명은 물에 잘 용해되고 피부 자극이 적은 아미노산계 또는 이세치오네이트계 계면활성제를 높은 함량으로 포함하고, 산화방지제를 포함하며, 선택적으로 컨디셔닝제, 바인더, 색 첨가물질을 추가하여 제형이 안정한 파우더 타입의 세정 조성물을 제조하여 소비자들에게 세정 제품 사용 및 보관의 편의성과 함께 외관적인 심미감까지 제공한다.The present invention relates to a powder-type cleansing composition with little moisture and a method for manufacturing the same, and specifically, by minimizing the content of a strong preservative required for long-term storage to maintain inherent efficacy and to reduce skin irritation or trouble, Provided is an easy-to-use powder type cleaning composition capable of forming a liquid cleaning liquid by immediate dissolution and a manufacturing method thereof.
To this end, the present invention contains a high content of amino acid-based or isethionate-based surfactants that are well soluble in water and have little skin irritation, include antioxidants, and optionally add conditioning agents, binders, and color additives to By preparing a powder-type cleaning composition with a stable formulation, it provides consumers with external aesthetics as well as convenience in using and storing cleaning products.
Description
본 발명은 물에 잘 용해되는 분말 타입의 클렌징 조성물 및 제조 방법에 관한 것이다. 구체적으로, 본 발명은 파우더 형태로 형성된 클렌징 조성물로서, 장기 보관을 위한 강한 보존제 함량을 최소화하여 고유의 효능을 유지하고, 자연유래 성분을 이용하여 피부의 자극을 줄이며, 물에 쉽게 용해되어 사용이 매우 간편한 분말상 클렌징 조성물에 관한 것이다.The present invention relates to a water-soluble powder type cleansing composition and manufacturing method. Specifically, the present invention is a cleansing composition formed in the form of a powder, which maintains its own efficacy by minimizing the content of strong preservatives for long-term storage, reduces skin irritation by using natural-derived ingredients, and is easily soluble in water, making it easy to use. It relates to a very convenient powdery cleansing composition.
피부의 세정은 과도한 피지나 외부로부터 쌓이는 잔류물, 매일 사용하는 화장품의 잔류물 및 메이크업 제품이 피부의 주름에 축적되어 피부의 모공을 막을 수 있으며, 그 결과 반점의 출현을 초래할 수 있기 때문에 얼굴 및/또는 신체의 관리에서 매우 중요하다.The cleansing of the skin is important because excessive sebum or residues accumulated from the outside, residues of cosmetics and makeup products used daily can accumulate in the wrinkles of the skin and clog the pores of the skin, resulting in the appearance of spots. /or very important in the care of the body.
더불어 최근 세계적인 코로나 바이러스 전파로 인하여 피부 미용 및 청결 목적의 세정뿐만 아니라 오염물질, 바이러스 등의 저감을 위한 세정의 중요성도 높아지고 있다.In addition, due to the recent spread of the corona virus around the world, the importance of washing not only for skin care and cleaning purposes but also for reducing contaminants and viruses is increasing.
세정 제품은 액체 형태를 포함하는 다양한 형태로 제공된다. 일반적으로 액체 클렌징 형태가 매우 유용하고 효과적이지만, 누출 및 유출에 취약하며, 또한 병과 같은 대형 패키지를 필요로 한다. 이러한 이유로, 고체 클렌징 제품이 제시될 수 있다. 고체 클렌징 제품은 유체의 존재 하에서 용해가 가능하며, 제품의 부패를 방지하기 위해 사용되는 보존제, 방부제가 불필요하므로 액체 클렌징과 비교하여 화학물질에 의한 피부 자극을 줄일 수 있다.Cleaning products come in a variety of forms, including liquid forms. In general, liquid cleansing forms are very useful and effective, but are prone to leaks and spills, and also require large packages such as bottles. For this reason, solid cleansing products can be presented. Solid cleansing products can be dissolved in the presence of fluid and do not require preservatives or preservatives used to prevent product spoilage, so skin irritation caused by chemicals can be reduced compared to liquid cleansing products.
그러나, 고체 클렌저는 종종 물에 충분히 신속하게 용해되지 않으며 원하는 거품 안정성(foam stability)을 갖지 않고, 고체 상태로 흐르는 물에 바로 사용하는 파우더형 클렌저는 가루날림 등의 문제가 있었다. 또한 인체 세정용 화장료의 주성분인 계면활성제는 미세먼지 및 피부 노폐물의 제거나 메이크업에 따른 유기물의 제거에 우수한 세정력을 나타내지만 일부는 함량이 많을수록 피부 건조, 자극, 트러블 등이 유발될 가능성이 있다.However, solid cleansers often do not dissolve quickly enough in water and do not have desired foam stability, and powder type cleansers used directly in flowing water in a solid state have problems such as powder scattering. In addition, surfactants, which are the main components of cosmetics for washing the human body, show excellent detergency in removing fine dust and skin wastes or organic matter due to makeup, but some of them may cause skin dryness, irritation, and trouble as the content is high.
공개특허공보 제10-2018-0084378 호는 천연물질에 탈이온 증류수(Deionized distilled water) 또는 제1유기용매를 혼합하여 제조된 손 세정제 조성물을 제시하였다. 상기 발명은 항균 성능을 높이기 위하여 천연물질로서 상황버섯 또는 어성초로 이루어진 성분을 포함하고 있으나 액상으로 제조되기 때문에 정량의 보존제, 방부제가 필수적으로 필요하다.Publication No. 10-2018-0084378 discloses a hand sanitizer composition prepared by mixing deionized distilled water or a first organic solvent with a natural material. The above invention includes a component consisting of Phellinus linteus or Hoseongcho as a natural material in order to increase antibacterial performance, but since it is prepared in a liquid form, a quantitative preservative and preservative are essential.
공개특허공보 제10- 2019-0054560 호는 천연성분이 포함된 성분들의 수분이 모두 제거된 분말 형태로 제조되고 내부의 액상화 반응에 의한 부패를 억제하기 위하여 탄산수소나트륨을 포함하고, 밀봉 포장되는 클렌징 파우더용 조성물 및 그 제조 방법을 제시하였다. 그러나 상기의 발명은 성분들의 수분을 제거하는 단계와 탄산가스를 방출하는 단계를 필수적으로 포함하므로 공정이 비교적 복잡해지는 문제가 있다.Patent Publication No. 10-2019-0054560 is a cleansing product that is manufactured in the form of a powder from which all moisture of ingredients including natural ingredients has been removed, contains sodium bicarbonate to prevent decay due to an internal liquefaction reaction, and is sealed and packaged. A composition for powder and a manufacturing method thereof are presented. However, since the above invention essentially includes a step of removing moisture from components and a step of releasing carbon dioxide gas, there is a problem in that the process is relatively complicated.
이에 따라 본 발명은 상기와 같은 종래의 문제점을 개선하기 위한 것으로서, 본 발명의 목적은 종래 기술의 단점을 극복하고 제형이 차별화된 파우더 형상으로 제조되어 보관 및 이동이 간편한 분말 타입의 클렌징 조성물을 제공하는 것이다.Accordingly, the present invention is to improve the conventional problems as described above, and an object of the present invention is to overcome the disadvantages of the prior art and to provide a powder-type cleansing composition that is easy to store and move because the formulation is manufactured in a differentiated powder form. is to do
본 발명의 또다른 목적은 장기 보존을 위한 강한 보존제 등을 줄이고 천연유래의 성분들을 안정성 있게 캡슐레이션하여 피부 자극이나 트러블이 거의 없는 안전한 세정 조성물을 제공하는 것이다.Another object of the present invention is to provide a safe cleaning composition with little skin irritation or trouble by reducing strong preservatives for long-term preservation and stably encapsulating natural ingredients.
본 발명의 또다른 목적은 펌핑용기에 본 발명의 세정 파우더와 물을 혼합하고 몇 번 흔드는 것만으로 쉽게 용해되어, 사용시 가루날림을 방지하고, 세정 분말을 많이 쓰지 않아도 적당한 거품이 형성되어 클렌징의 과도한 사용을 줄이며, 장시간 방치해도 분리 석출 또는 침전되지 않아 오랫동안 사용할 수 있는 경제적인 세정 조성물을 제공하는 것이다.Another object of the present invention is to mix the cleaning powder of the present invention with water in a pumping container and dissolve it easily just by shaking it a few times, to prevent powder flying during use, and to form appropriate bubbles even without using a lot of cleaning powder, resulting in excessive cleansing. It is to provide an economical cleaning composition that can be used for a long time because it reduces use and does not separate or precipitate even when left for a long time.
본 발명의 또다른 목적은 제품 자체의 성능을 유지하고 외관으로부터 감성적 즐거움을 불러일으킬 수 있는 심미적 효과를 가진 세정 조성물을 제공하는 것이다.Another object of the present invention is to provide a cleaning composition having an aesthetic effect that can maintain the performance of the product itself and evoke emotional pleasure from its appearance.
본 발명이 이루고자 하는 기술적 과제는 이상에서 언급한 기술적 과제로 제한되지 않으며, 언급되지 않은 또 다른 기술적 과제들은 아래의 기재로부터 본 발명이 속하는 기술 분야에서 통상의 지식을 가진 자에게 명확하게 이해될 수 있을 것이다.The technical problem to be achieved by the present invention is not limited to the above-mentioned technical problem, and other technical problems not mentioned can be clearly understood by those skilled in the art from the description below. There will be.
상기 기술적 과제를 달성하기 위하여, 본 발명의 일실시예에 따른 분말상 클렌징 조성물은 아미노산계 또는 이세치오네이트계 계면활성제와 산화방지제를 포함하여 구성된다.In order to achieve the above technical problem, the powdery cleansing composition according to an embodiment of the present invention is composed of an amino acid-based or isethionate-based surfactant and an antioxidant.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물은 상기 아미노산계 계면활성제는 소듐라우로일글루타메이트를 포함하고, 상기 산화방지제는 하이드록시아세토페논을 포함하여 구성될 수 있다.In addition, in the powdery cleansing composition according to an embodiment of the present invention, the amino acid-based surfactant may include sodium lauroyl glutamate, and the antioxidant may include hydroxyacetophenone.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물은, 코어; 상기 코어를 감싸는 코팅층;을 포함하여 캡슐 형태로 형성되며, 상기 코어는 아미노산계 계면활성제를 포함하고, 상기 코팅층은 산화방지제를 포함하도록 구성될 수 있다.In addition, the powdery cleansing composition according to an embodiment of the present invention, the core; It is formed in the form of a capsule including a coating layer surrounding the core, and the core may include an amino acid-based surfactant, and the coating layer may include an antioxidant.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물에서 상기 코어는, 소듐라우로일글루타메이트를 포함하고, 상기 코팅층은 하이드록시아세토페논, 아스코빅애씨드 및 그 염류, 비타민E, 토코페롤 에스터, 비타민 E와 비타민 C의 혼합물, 토코페롤 유도체 성분, 토코페솔란, 비타민 A, 유비퀴논, 알파리포애씨드, 카로티노이드, 비타민B, 로즈 방부제(Rose Preservative), 자몽 추출액(Grapefruit Seed Extract)중 어느 하나이상이 포함되어 구성될 수 있다.In addition, in the powdery cleansing composition according to an embodiment of the present invention, the core includes sodium lauroyl glutamate, and the coating layer is hydroxyacetophenone, ascorbic acid and its salts, vitamin E, tocopherol ester, vitamin E and a mixture of vitamin C, tocopherol derivatives, tocophersolan, vitamin A, ubiquinone, alpha lipoic acid, carotenoids, vitamin B, rose preservative, and grapefruit seed extract. can be configured.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물에서 상기 코팅층은 컨디셔닝제 및 바인더를 포함하며, 상기 컨디셔닝제는 천연 혹은 합성 추출물, 아미노산류 및 단백질, 당류, 천연 또는 합성 오일, 알코올류, 계면활성제로 구성된 군에서 적어도 하나 이상 포함하여 구성될 수 있다.In addition, in the powdery cleansing composition according to an embodiment of the present invention, the coating layer includes a conditioning agent and a binder, and the conditioning agent includes natural or synthetic extracts, amino acids and proteins, sugars, natural or synthetic oils, alcohols, and interfaces. It may be configured to include at least one or more from the group consisting of active agents.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물에서 상기 컨디셔닝제는 물에 쉽게 용해되지 않는 왁스, 지방알코올류, 미네랄 오일을 제외한 천연 혹은 합성 추출물, 아미노산류 및 단백질, 당류, 천연 또는 합성 오일, 알코올류, 계면활성제로 구성된 군에서 적어도 하나 이상 포함하여 구성될 수 있다.In addition, in the powdery cleansing composition according to an embodiment of the present invention, the conditioning agent is a wax that is not easily soluble in water, fatty alcohols, and natural or synthetic extracts other than mineral oil, amino acids and proteins, sugars, natural or synthetic oils , alcohols, and may be configured to include at least one or more from the group consisting of surfactants.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물에서 상기 코팅층의 바인더는 하이드록시프로필스타치포스페이트, 옥수수 전분, 쌀 전분, 카사바 전분, 감자 전분, 밀 전분, 수수 전분, 콩 전분, 펙틴, 아라비아검, 구아검, 로커스트콩검, 산탄검, 젤란검, 카라야검, 타라검, 타마린드검, 트라가칸스검, 천연검, 사일리움씨드검, 히드록실에틸셀룰로스, 히드록시프로필메틸셀룰로스로 구성된 군에서 적어도 하나 이상을 포함하여 구성될 수 있다.In addition, in the powdery cleansing composition according to an embodiment of the present invention, the binder of the coating layer is hydroxypropyl starch phosphate, corn starch, rice starch, cassava starch, potato starch, wheat starch, sorghum starch, soybean starch, pectin, arabic Group consisting of gum, guar gum, locust bean gum, xanthan gum, gellan gum, gum karaya, gum tara, gum tamarind, gum tragacanth, natural gum, psyllium seed gum, hydroxylethylcellulose, and hydroxypropylmethylcellulose It may be configured to include at least one or more in
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물은, 색조 효과를 주는 색 첨가물질을 더 포함하여 구성될 수 있다.In addition, the powdery cleansing composition according to an embodiment of the present invention may further include a color additive material giving a color effect.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물은, 아미노산계 계면활성제를 75 내지 84w% 이상 함유하고, 산화방지제는 15 내지 24w%를 포함하여 분말 형태로 제조될 수 있다.In addition, the powdery cleansing composition according to one embodiment of the present invention contains 75 to 84w% or more of an amino acid-based surfactant, and 15 to 24w% of an antioxidant may be prepared in a powder form.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물의 제조방법은, 아미노산계 계면활성제를 포함한 원료를 용매에 용해하여 과립입자를 형성하는 단계; 산화방지제를 포함한 원료를 용매에 용해하여 상기 과립입자에 도포하여 코팅 조성물을 형성하는 단계; 상기 코팅 조성물을 50 내지 65℃ 온도에서 건조하는 단계;를 포함하여 구성될 수 있다.In addition, the method for producing a powdery cleansing composition according to an embodiment of the present invention includes the steps of dissolving a raw material including an amino acid-based surfactant in a solvent to form granular particles; Forming a coating composition by dissolving a raw material including an antioxidant in a solvent and applying it to the granular particles; It may be configured to include; drying the coating composition at a temperature of 50 to 65 ℃.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물의 제조방법은, 입자형태의 코어를 준비하는 단계; 및 상기 코어의 표면을 코팅하여 코팅층을 형성하는 단계;를 포함하며, 상기 코어는 아미노산계 또는 이세치오네이트계 계면활성제를 포함하고, 상기 코팅층은 산화방지제를 포함하여 구성될 수 있다.In addition, the manufacturing method of the powdery cleansing composition according to an embodiment of the present invention, preparing a particulate core; and forming a coating layer by coating the surface of the core, wherein the core may include an amino acid-based or isethionate-based surfactant, and the coating layer may include an antioxidant.
또한, 본 발명의 일실시예에 따른 분말상 클렌징 조성물의 제조방법에서 상기 코어를 준비하는 단계는, 아미노산계 또는 이세치오네이트계 계면활성제가 포함된 코어 성분을 용해 및 분산한 후 유동층 공정에 의하여 입자형태의 코어를 형성하는 단계;를 포함하고, 상기 코팅층을 형성하는 단계는, 산화방지제가 포함된 제1 코팅성분을 용해 및 분산한 후 상기 코어의 표면에 유동층 공정에 의하여 코팅하여 제1 코팅층을 형성하는 단계;와 컨디셔닝제 또는 바인더가 포함된 제2 코팅성분을 용해 및 분산한 후 상기 코어의 표면에 유동층 공정에 의하여 코팅하여 제2 코팅층을 형성하는 단계;를 포함하여 구성될 수 있다.In addition, in the preparation method of the powdery cleansing composition according to an embodiment of the present invention, the step of preparing the core, after dissolving and dispersing the core component containing an amino acid-based or isethionate-based surfactant, particles by a fluidized bed process Including, forming a core of the form; in the forming of the coating layer, the first coating layer is formed by dissolving and dispersing the first coating component containing the antioxidant and then coating the surface of the core by a fluidized bed process. forming; and forming a second coating layer by dissolving and dispersing a second coating component including a conditioning agent or binder and then coating the surface of the core by a fluidized bed process.
상술한 과제의 해결 수단에 의하면, 본 발명에 따른 분말상 클렌징 조성물은 강한 보존제 등을 줄이고 재료 고유의 효능을 유지하여 세정력이 좋고 피부에는 덜 자극적인 세정 효과를 가질 수 있다.According to the means for solving the above problems, the powdery cleansing composition according to the present invention can have a good cleaning power and a less irritating cleaning effect on the skin by reducing the strong preservative and maintaining the inherent efficacy of the material.
또한 수분이 제거된 파우더 형태여서 휴대가 용이하고, 습식 세안제보다 산뜻한 느낌을 줄 수 있는 효과를 가진다.In addition, since it is in the form of a powder from which moisture has been removed, it is easy to carry and has an effect of giving a refreshing feeling compared to a wet face wash.
또한 실리카, 메티콘 같은 활택제를 사용하지 않아도 안정성 있게 캡슐레이션되어 제조공정 시간을 줄일 수 있는 효과를 가진다.In addition, it is stably encapsulated even without the use of lubricants such as silica and methicone, and thus has an effect of reducing manufacturing process time.
또한 세정 조성물 입자가 물에 쉽게 용해되어 펌핑 용기에 물과 혼합하여 준비하는 방식으로 쉽게 사용 가능하며, 가루 날림이 거의 없어 안정성이 우수하고, 잔여물 없이 투명성을 유지할 수 있는 심미적인 효과를 가진다.In addition, the cleaning composition particles are easily dissolved in water and can be easily used in a way that is prepared by mixing with water in a pumping container, has excellent stability due to almost no powder flying, and has an aesthetic effect of maintaining transparency without residue.
본 발명의 효과는 상기한 효과로 한정되는 것은 아니며, 본 발명의 상세한 설명 또는 특허청구범위에 기재된 발명의 구성으로부터 추론 가능한 모든 효과를 포함하는 것으로 이해되어야 한다.The effects of the present invention are not limited to the above effects, and should be understood to include all effects that can be inferred from the detailed description of the present invention or the configuration of the invention described in the claims.
도 1은 본 발명의 실시예를 이용한 미세먼지 모사체 흡착량에 대한 시험 그래프이다.
도 2는 본 발명의 실시예의 테스트에서 Folliscope를 이용한 미세먼지 모사체 세정력 결과에 대한 비교 그래프이다.
도 3은 본 발명의 실시예의 테스트 중 미세먼지 모사체 세정 개선율에 대한 비교 그래프이다.
도 4는 본 발명의 실시예의 모사체 세정력을 확인하기 위해 제품 사용전, 미세먼지 모사체 도포 후, 제품 사용 직후를 외관 비교한 이미지이다.
도 5는 본 발명의 일실시예에 따른 분말상 클렌징 조성물의 혼합액에서 혼합비율에 따른 투명도 등 외관 비교 이미지이다.
도 6은 본 발명의 일실시예에 따른 분말상 클렌징 조성물을 즉석에서 용해시켜 준비한 세정액의 세정력 실험 결과를 외관 비교한 이미지이다.1 is a test graph for the adsorption amount of fine dust mimics using an embodiment of the present invention.
Figure 2 is a comparison graph for the results of fine dust mimetic cleaning power using Folliscope in the test of the embodiment of the present invention.
Figure 3 is a comparison graph of the improvement rate of fine dust mimetic cleaning during the test of the embodiment of the present invention.
4 is an image comparing appearances before use of the product, after application of the fine dust mimetic, and immediately after use of the product in order to confirm the detergency of the parent body of the embodiment of the present invention.
Figure 5 is a comparison image of the appearance, such as transparency according to the mixing ratio in the mixed solution of the powdery cleansing composition according to an embodiment of the present invention.
Figure 6 is an image comparing the appearance of the results of the detergency test of the cleaning solution prepared by immediately dissolving the powdery cleansing composition according to an embodiment of the present invention.
이하에서는 첨부한 도면을 참조하여 본 발명을 설명하기로 한다. 그러나 본 발명은 여러 가지 상이한 형태로 구현될 수 있으며, 따라서 여기에서 설명하는 실시예로 한정되는 것은 아니다.Hereinafter, the present invention will be described with reference to the accompanying drawings. However, the present invention may be embodied in many different forms and, therefore, is not limited to the embodiments described herein.
명세서 전체에서, 어떤 부분이 다른 부분과 "연결(접속, 접촉, 결합)"되어 있다고 할 때, 이는 "직접적으로 연결"되어 있는 경우뿐 아니라, 그 중간에 다른 부재를 사이에 두고 "간접적으로 연결"되어 있는 경우도 포함한다. 또한, 어떤 부분이 어떤 구성요소를 "포함"한다고 할 때, 이는 특별히 반대되는 기재가 없는 한 다른 구성요소를 제외하는 것이 아니라 다른 구성요소를 더 구비할 수 있다는 것을 의미한다.Throughout the specification, when a part is said to be "connected (connected, contacted, combined)" with another part, this is not only "directly connected", but also "indirectly connected" with another member in between. "Including cases where In addition, when a part "includes" a certain component, it means that it may further include other components without excluding other components unless otherwise stated.
본 명세서에서 사용한 용어는 단지 특정한 실시예를 설명하기 위해 사용된 것으로, 본 발명을 한정하려는 의도가 아니다. 단수의 표현은 문맥상 명백하게 다르게 뜻하지 않는 한, 복수의 표현을 포함한다. 본 명세서에서, "포함하다" 또는 "가지다" 등의 용어는 명세서상에 기재된 특징, 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것이 존재함을 지정하려는 것이지, 하나 또는 그 이상의 다른 특징들이나 숫자, 단계, 동작, 구성요소, 부품 또는 이들을 조합한 것들의 존재 또는 부가 가능성을 미리 배제하지 않는 것으로 이해되어야 한다.Terms used in this specification are only used to describe specific embodiments, and are not intended to limit the present invention. Singular expressions include plural expressions unless the context clearly dictates otherwise. In this specification, terms such as "include" or "have" are intended to indicate that there is a feature, number, step, operation, component, part, or combination thereof described in the specification, but one or more other features It should be understood that the presence or addition of numbers, steps, operations, components, parts, or combinations thereof is not precluded.
본 발명은 상온에서 고체형상이고, 물과 접촉시 쉽게 용해될 수 있는 분말 제형의 세정 조성물 및 상기 분말 제형의 세정 조성물을 제조하는 방법을 제공한다.The present invention provides a cleaning composition in a powder formulation that is in a solid state at room temperature and can be easily dissolved upon contact with water, and a method for preparing the cleaning composition in a powder formulation.
상기 분말 제형의 세정 조성물은 필수성분으로 계면활성제, 산화방지제 성분을 포함하여 제조되고, 선택적으로 바인더, 컨디셔닝제, 색 첨가물질 등이 코어 또는 코팅층에 포함되도록 유동층 시스템에 의해서 코팅된 캡슐 형태로 제조될 수 있다.The cleaning composition of the powder formulation is prepared in the form of capsules coated by a fluidized bed system to include surfactants and antioxidants as essential components, and optionally include binders, conditioners, color additives, etc. in the core or coating layer. It can be.
상기 계면활성제는 당업계에서 공지된 합성 계면활성제 혹은 천연 유래 계면활성제이며, 음이온성 계면활성제, 양쪽성 또는 쌍성 이온성 계면활성제, 양이온성 계면활성제 또는 비이온 계면활성제 등이 있다.The surfactant is a synthetic surfactant or a naturally derived surfactant known in the art, and includes an anionic surfactant, an amphoteric or zwitterionic surfactant, a cationic surfactant, or a nonionic surfactant.
본 발명의 일실시예에서는 물이 있는 환경에서 잘 용해되며, 피부 안전성과 함께 사용감이 좋은 성분을 사용하는 것이 좋고, 특히 저자극성 세안용 계면활성제로 널리 알려진 아미노산계 또는 이세치오네이트계 계면활성제가 바람직하다.In one embodiment of the present invention, it is good to use an ingredient that dissolves well in a water environment and has a good feeling of use with skin safety. desirable.
상기 아미노산계 계면활성제는 하기의 화학식을 만족하는 글루타믹애씨드 및 그 염을 포함하는 음이온 계면활성제가 바람직하다.The amino acid-based surfactant is preferably an anionic surfactant including glutamic acid and a salt thereof satisfying the following formula.
상기, M+는 일칼리 금속, 예를 들어 K 또는 Na의 금속이온이며, 상기 R1은 탄소 원자가 10 내지 18개, 바람직하게는 12개 내지 18개의 선형 또는 분지형의 포화 또는 불포화 탄화수소 사슬을 나타낸다.Wherein, M+ is a metal ion of a alkali metal, for example, K or Na, and R1 represents a linear or branched, saturated or unsaturated hydrocarbon chain having 10 to 18 carbon atoms, preferably 12 to 18 carbon atoms.
상기의 화학식을 만족하는 아미노산계 계면활성제로, 소듐라우로일글루타메이트, 소듐미리스토일글루타메이트, 포타슘라우로일글루타메이트, 포타슘미리스토일글루타메이트 등이 있으며, 바람직하게는, 소듐라우로일글루타메이트가 선택될 수 있다.Amino acid-based surfactants satisfying the above chemical formula include sodium lauroyl glutamate, sodium myristoyl glutamate, potassium lauroyl glutamate, potassium myristoyl glutamate, and the like, preferably, sodium lauroyl glutamate is selected. It can be.
상기 이세치오네이트계 계면활성제는 이세티오닉애씨드 유도체 및 그 염으로부터 선택되는 적어도 하나의 음이온성 계면활성제이며, 그 예로 암모늄 코코일 이세치오네이트, 소듐 코코일 이세치오네이트, 소듐 라우로일 이세치오네이트, 소듐 미리스토일 이세치오네이트 및 소듐 올레오일 이세치오네이트 중 어느 하나 이상을 포함할 수 있다.The isethionate-based surfactant is at least one anionic surfactant selected from isethionic acid derivatives and salts thereof, such as ammonium cocoyl isethionate, sodium cocoyl isethionate, and sodium lauroyl isethionate. nate, sodium myristoyl isethionate and sodium oleoyl isethionate.
상기 소듐라우로일글루타메이트는 코코넛 오일, 팜 오일 등에서 얻을 수 있는 글루탐산(아미노산), 라우르산 및 나트륨으로부터 유래된 음이온 계면활성제로서, 합성 계면활성제를 대체할 수 있는 식물성 성분으로 가볍고 부드러우며 촉촉한 느낌을 주는 천연 유래 계면활성제이다.The sodium lauroyl glutamate is an anionic surfactant derived from glutamic acid (amino acid), lauric acid, and sodium, which can be obtained from coconut oil, palm oil, etc., and is a vegetable ingredient that can replace synthetic surfactants, making it light, soft, and moist. It is a naturally derived surfactant that gives
본 발명의 일실시예에 따라 상기 소듐라우로일글루타메이트를 주성분으로 포함하여 제조할 시 일반적인 물에도 잘 녹고, 펌핑시 충분한 거품을 형성하며, 세정력과 사용감이 우수한 클렌징 조성물을 얻을 수 있다. 특히 소듐라우로일글루타메이트를 사용하여 파우더형 클렌징 조성물을 구성하는 경우에, 높은 함량으로 구성하여도 세정 조성물 분말이 물에 쉽게 용해되어 잔여물이 거의 없는 투명한 세정 혼합물을 형성할 수 있다.According to one embodiment of the present invention, when prepared by containing the sodium lauroyl glutamate as a main component, it is possible to obtain a cleansing composition that dissolves well in general water, forms sufficient foam when pumped, and has excellent cleaning power and feeling of use. In particular, in the case of constituting a powder type cleansing composition using sodium lauroyl glutamate, the powder of the cleaning composition is easily dissolved in water even if it is composed of a high content, so that a transparent cleaning mixture with little residue can be formed.
이러한 계면활성제의 함량은 전체 분말용 세정 조성물에서 75 w% 내지 84w%의 범위로 포함되는 것이 바람직하다. 만약 계면활성제가 상기 수치보다 적게 사용될 경우 세정 조성물로서의 세정 기능이 떨어지고, 충분한 거품형성이 되지 않는 문제가 있다.The content of such a surfactant is preferably included in the range of 75 w% to 84 w% in the total cleaning composition for powder. If the surfactant is used less than the above value, there is a problem in that the cleaning function as a cleaning composition is deteriorated and sufficient foaming is not formed.
본 발명의 분말상 클렌징 조성물의 필수성분으로 산화방지제가 포함된다. 산화방지제는 제품의 품질, 보존, 산화안정화를 위해 사용되는 성분으로, 고분자 대신 라디칼을 만들어 라디칼의 연쇄반응을 방지하고, 고분자를 안정화시키는 페놀계 또는 아민계의 산화방지제를 이용할 수 있다.An antioxidant is included as an essential component of the powdery cleansing composition of the present invention. Antioxidants are components used for product quality, preservation, and oxidation stabilization. A phenol-based or amine-based antioxidant can be used to prevent a chain reaction of radicals by creating radicals instead of polymers and to stabilize polymers.
본 발명의 분말상 클렌징 조성물은 건조 파우더형태여서 상기 필수성분 이외에 보관을 위한 방부제, 보존제, 정제수 등의 원료가 비필수적이므로 세정 목적을 가진 계면활성제 원료 함량을 높일 수 있으며, 세정시 적은 양의 분말을 사용하여도 세정력이 우수하고 충분한 거품이 형성되며, 이로 인하여 세정 분말의 과도한 사용을 예방하는 효과도 있다. 또한 세정 물질을 피부에 직접 접촉하여 흐르는 물에 세척하는 기존의 고형 세정 제품과 달리 본 발명의 세정 조성물은 디스펜서 용기에 물을 채우고 소정의 분말을 투입하여 용해시킨 형태로 임시 저장한 후 펌핑하는 방식으로 사용하는 형태여서 가루날림에 대한 염려를 줄일 수 있다.Since the powdery cleansing composition of the present invention is in the form of dry powder, raw materials such as preservatives, preservatives, and purified water for storage in addition to the above essential components are non-essential, so the content of surfactant raw materials for cleaning purposes can be increased, and a small amount of powder can be used during cleaning. Even when used, the cleaning power is excellent and sufficient bubbles are formed, thereby preventing excessive use of the cleaning powder. In addition, unlike conventional solid cleaning products in which cleaning materials are directly contacted with the skin and washed with running water, the cleaning composition of the present invention is temporarily stored in a form in which water is filled in a dispenser container, predetermined powder is injected, dissolved, and then pumped. As it is used in a form, it can reduce the concern about powder scattering.
본 발명의 일실시예에 따른 분말 제형의 클렌징 조성물은 추가로 컨디셔닝제를 포함할 수 있다. 상기 컨디셔닝제는 피부의 특성에 변화를 주는 성분으로 그 기능에 따라 보습제, 수분차단제, 유연제, 기타 등으로 나눌 수 있다. 보습제는 피부 외층의 수분보유를 증대시키기 위한 성분이고, 수분차단제(Skin conditioning agents-occlusive)는 피부표면으로부터 수분의 증발을 지연시키는 성분이다. 또한 유연제(Skin conditioning agents-emollient)는 피부를 부드럽고 유연하게 유지하는 데 도움을 주는 성분이며, 그 외에 기타 성분은 피부에 소정의 효과를 주기위한 성분으로서, 예를 들어, 건조하거나 손상된 피부를 개선, 피부탈락 감소, 피부 진정, 유연성 회복 등을 위해 사용할 수도 있다.The powdered cleansing composition according to an embodiment of the present invention may further include a conditioning agent. The conditioning agent is a component that changes the characteristics of the skin and can be divided into a moisturizer, a moisture blocker, a softener, and the like according to its function. Moisturizers are ingredients for increasing water retention in the outer layer of the skin, and skin conditioning agents (occlusive) are ingredients that delay evaporation of water from the skin surface. In addition, skin conditioning agents (emollient) are ingredients that help keep the skin soft and supple, and other ingredients are ingredients that give certain effects to the skin, such as improving dry or damaged skin. , It can also be used to reduce skin shedding, soothe skin, and restore flexibility.
본 발명의 일실시예에 따른 분말 제형의 클렌징 조성물은 선택적으로 바인더를 포함할 수 있다. 상기 바인더는 조성물 원료들을 서로 결합 또는 접착시키기 위해 사용되는 성분으로, 하이드록시프로필스타치포스페이트, 옥수수 전분, 쌀 전분, 감자 전분 등과 같은 전분류나 또는 한천, 카라게닌, 알기네이트, 펙틴, 젤라틴, 카제이네이트, 다당류, 검류 등과 같은 친수성 겔화제나 또는 셀룰로오스, 카보머 등을 사용하는 것이 좋으며, 특히 하이드록시프로필스타치포스페이트가 바람직하다.The powdered cleansing composition according to one embodiment of the present invention may optionally include a binder. The binder is a component used to bind or adhere the raw materials of the composition to each other, and may include starch such as hydroxypropyl starch phosphate, corn starch, rice starch, potato starch, etc., or agar, carrageenan, alginate, pectin, gelatin, It is preferable to use a hydrophilic gelling agent such as caseinate, polysaccharide, gum, or the like, or cellulose, carbomer, and the like, and hydroxypropyl starch phosphate is particularly preferable.
본 발명의 실시예에서 상기 분말 제형의 클렌징 조성물은 선택적으로 색 첨가물질을 포함할 수 있다. 상기 색 첨가물질은 조성물이나 완제품에 색조효과를 주기 위해 사용되는 성분으로 천연유래 착색제, 인공 착색제, 무기 안료 등을 포함하며, 특히 물에 잘 용해될 수 있는 성분이라면 한정하지 않는다.In an embodiment of the present invention, the powdered cleansing composition may optionally include a color additive. The color additive is a component used to give a color effect to a composition or finished product, and includes natural colorants, artificial colorants, inorganic pigments, and the like, and is not particularly limited as long as it is well soluble in water.
이외에도 본 발명의 실시예에서 부형제, 점증제, 금속이온 결합제, 향료 등을 더욱 추가하는 것도 가능하며, 그 예로서 만니톨, 자일리톨, 소르비톨, 셀룰로오스, 젤라틴, 펜테틱애씨드 및 그 염류, 이디티에이 등이 있다.In addition to the examples of the present invention, it is possible to further add excipients, thickeners, metal ion binders, flavoring agents, etc. Examples include mannitol, xylitol, sorbitol, cellulose, gelatin, pentetic acid and salts thereof, and EDTA. there is.
이하 본 발명에 대해 상세히 설명한다.Hereinafter, the present invention will be described in detail.
본 발명에서 분말, 캡슐, 파우더란 본 명세서에 기재된 제조 방법에 의해 완성되어 수분 함량이 6 % 이하이고, 입도가 0.71mm 이하인 입자를 의미한다.In the present invention, the powder, capsule, and powder mean particles having a water content of 6% or less and a particle size of 0.71 mm or less, which are completed by the manufacturing method described herein.
본 발명의 일실시예에서 상기 분말 제형의 클렌징 조성물은 계면활성제를 코어로 하여 유동층 시스템을 응용하여 제작될 수 있다. 즉, 유동층 시스템의 과립기 내부 아래에서 위로 향하는 공기로 인해 분말이 유동하고, 유동되는 분말은 아래로 뿌려지는 코팅 용액(분무액)에 의해 과립이 이루어지는 탑스프레이(Top Spray) 방식으로 제조되는 것이 바람직하다.In one embodiment of the present invention, the powdered cleansing composition may be prepared by applying a fluidized bed system using a surfactant as a core. That is, it is produced by a top spray method in which powder flows due to air directed upward from the inside of the granulator of the fluidized bed system, and the powder is granulated by a coating solution (spray liquid) sprayed downward. desirable.
본 발명에 의한 분말 형태의 클렌징 조성물의 제조 방법은,Method for producing a cleansing composition in powder form according to the present invention,
계면활성제가 포함되는 성분을 포함하여 코어를 제조하는 단계;와Preparing a core by including a component containing a surfactant; and
산화방지제를 포함하여 제1코팅층을 형성하는 단계를 포함하며,Including the step of forming a first coating layer including an antioxidant,
컨디셔닝제, 바인더, 색 첨가물질이 포함되는 성분을 제2코팅층으로 하여 캡슐을 제조하는 단계;를 선택적으로 추가 수행할 수 있다.A step of preparing a capsule by using components including a conditioning agent, a binder, and a color additive as a second coating layer may be optionally additionally performed.
구체적으로, (a) 단계는 본 발명의 필수성분인 계면활성제가 75w% 이상 84% 이하로 포함된 원료물질을 물 또는 에탄올 등의 용매에 용해한 후 적당한 크기의 과립입자로 성형하여 코어를 제조한다. 여기서 상기 계면활성제는 아미노산계 또는 이세치오네이트계 계면활성제가 바람직하다. 그리고 (b) 단계에서 산화방지제 원료물질을 물 또는 에탄올 등의 용매에 용해한 후 상기 코어에 도포하여 코팅층을 형성한 코팅 조성물을 50 내지 65℃ 온도 조건에서 건조하여 본 발명의 클렌징 조성물을 제조한다.Specifically, in step (a), a core is prepared by dissolving a raw material containing 75 wt% or more and 84% or less of a surfactant, which is an essential component of the present invention, in a solvent such as water or ethanol, and then molding it into granules of an appropriate size. . Here, the surfactant is preferably an amino acid-based or isethionate-based surfactant. And in step (b), the antioxidant raw material is dissolved in a solvent such as water or ethanol, and then applied to the core to form a coating layer, and the coating composition is dried at a temperature of 50 to 65 ° C to prepare a cleansing composition of the present invention.
(c) 단계는 비필수적인 공정으로서, 목적에 따라 부형제, 점증제, 금속이온 결합제, 향료 등을 더욱 추가하는 것도 가능하다.Step (c) is a non-essential process, and it is possible to further add an excipient, thickener, metal ion binder, flavoring agent, etc. according to the purpose.
일반적으로 원료를 캡슐레이션하여 제조하는 화장료 조성물은 과립형태의 형상을 유지하고, 서로 뭉치거나 점착되는 현상을 방지하기 위해 미네랄 활석 또는 규토, 지방 등의 성분을 활택제로 사용한다. 이러한 활택제는 가공 특성을 개선하기 위해 정제 및 캡슐 조성물에 소량으로 첨가되나, 조성물의 품질 및 사용감에 부정적인 영향을 주기도 한다.In general, cosmetic compositions prepared by encapsulating raw materials use ingredients such as mineral talc, silica, and fat as lubricants to maintain a granular shape and prevent aggregation or sticking together. These lubricants are added in small amounts to tablet and capsule compositions to improve processing properties, but they also negatively affect the quality and feel of the composition.
본 발명의 분말상 클렌징 조성물은 활택제 기능을 목적으로 하는 원료, 예를 들어, 실리카, 메티콘, 스테아르산 마그네슘, 셀룰로오스, 마이크로크리스탈린셀룰로오스, 실크가루, 징크미리스테이트, 징크스테아레이트, 알미늄실리케이트 등을 사용하지 않아도 장시간 보관이 가능하기 때문에 세정 조성물의 품질 저하 염려가 적고, 추가적인 후혼합 공정이 불필요하여 공정 시간을 절감할 수 있다.The powdery cleansing composition of the present invention is a raw material for the purpose of a lubricant function, for example, silica, methicone, magnesium stearate, cellulose, microcrystalline cellulose, silk powder, zinc myristate, zinc stearate, aluminum silicate, etc. Since it is possible to store for a long time without using, there is less concern about deterioration of the quality of the cleaning composition, and process time can be reduced because an additional post-mixing process is not required.
캡슐레이션되는 분말상 클렌징 조성물에 관하여 구체적으로 설명하면, 본 발명의 일실시예에서 캡슐형 분말상 클렌징 조성물은 코어; 및 제1 코팅층;을 포함하여 캡슐형태로 구성될 수 있다.In detail with respect to the powdery cleansing composition to be encapsulated, in one embodiment of the present invention, the capsule-type powdery cleansing composition includes a core; And a first coating layer; may be configured in the form of a capsule, including.
상기 코어는 캡슐의 중심이 되는 일정 크기의 시드 물질을 말하며, 크기를 조절하여 캡슐의 전체적인 평균 직경을 조절할 수 있다.The core refers to a seed material having a certain size that is the center of the capsule, and the overall average diameter of the capsule can be adjusted by adjusting the size.
본 발명의 일실시예에서, 상기 시드 물질은 소듐라우로일글루타메이트, 소듐 코코일 글루타메이트, 포타슘 라우로일 글루타메이트, 포타슘 미리스토일 글루타메이트, 암모늄 코코일 이세치오네이트, 소듐 코코일 이세치오네이트, 소듐 라우로일 이세치오네이트, 소듐 미리스토일 이세치오네이트 및 소듐 올레오일 이세치오네이트 등의 계면활성제로부터 하나 이상 선택될 수 있고, 바람직하게는 소듐라우로일글루타메이트로 구성될 수 있다.In one embodiment of the present invention, the seed material is sodium lauroyl glutamate, sodium cocoyl glutamate, potassium lauroyl glutamate, potassium myristoyl glutamate, ammonium cocoyl isethionate, sodium cocoyl isethionate, sodium It may be one or more selected from surfactants such as lauroyl isethionate, sodium myristoyl isethionate, and sodium oleoyl isethionate, and may be preferably composed of sodium lauroyl glutamate.
이러한 시드 물질의 함량은 하나의 분말형 클렌징 조성물을 기준으로 75 w% 이상 84 w% 이하의 범위에서 포함되는 것이 바람직하다.The content of such a seed material is preferably included in the range of 75 w% or more and 84 w% or less based on one powdery cleansing composition.
본 발명의 일실시예에서 상기 제1 코팅층은 산화방지제를 포함한다.In one embodiment of the present invention, the first coating layer includes an antioxidant.
상기 산화방지제는 하이드록시아세토페논, 아스코빅애씨드 및 그 염류, 비타민E, 토코페롤 에스터, 비타민 E (토코페롤)와 비타민 C (아스코빅애씨드)의 혼합물, 토코페롤 유도체 성분, 토코페솔란, 비타민 A(레티놀), 유비퀴논, 알파리포애씨드, 카로티노이드, 비타민B(판테놀), 로즈 방부제(Rose Preservative), 자몽 추출액(Grapefruit Seed Extract) 등을 사용할 수 있다.The antioxidant is hydroxyacetophenone, ascorbic acid and its salts, vitamin E, tocopherol ester, a mixture of vitamin E (tocopherol) and vitamin C (ascorbic acid), tocopherol derivative component, tocophersolane, vitamin A (retinol ), ubiquinone, alpha lipoic acid, carotenoids, vitamin B (panthenol), rose preservative, grapefruit seed extract, etc. can be used.
상기 아스코빅애씨드 및 그 염류는 예를 들어, 칼슘아스코베이트, 마그네슘아스코베이트, 마그네슘아스코빌포스페이트, 소듐아스코베이트 및 소듐아스코빌포스페이트 등을 사용할 수 있으며, 상기 토코페롤 에스터는 토코페릴아세테이트(토코페롤의 아세틱애씨드에스터), 토코페릴리놀리에이트 (토코페롤의 리놀레익애씨드에스터), 토코페릴리놀리에이트/올리에이트 (토코페롤의 리놀레익애씨드에스터와 올레익애씨드에스터의 혼합물), 토코페릴니코티네이트 (토코페롤의 니코티닉애씨드에스터) 및 토코페릴석시네이트 (토코페롤의 석시닉애씨드에스터)가 포함된다. 상기 비타민 E (토코페롤)와 비타민 C (아스코빅애씨드)의 혼합물은 포타슘아스코빌토코페릴포스페이트를 포함하며, 토코페롤 유도체 성분은 다이올레일토코페릴메틸실란올 (메틸실란에트리올과 토코페릴아세테이트모노에터의 다이올레일에터)과 토코페솔란 (토코페릴폴리에틸렌글리콜1000석시네이트를 포함하고, 상기 토코페솔란은 석시닉애씨드와 평균 22 개의 에틸렌옥사이드기를 토코페롤에 첨가하는 것으로 토코페롤의 수용성 형태인 토코페솔란을 만들 수 있다.Examples of the ascorbic acid and salts thereof include calcium ascorbate, magnesium ascorbate, magnesium ascorbyl phosphate, sodium ascorbate and sodium ascorbyl phosphate, and the tocopherol ester is tocopheryl acetate (tocopheryl acetate). tic acid ester), tocopheryl linoleate (linoleic acid ester of tocopherol), tocopheryl linoleate/oleate (mixture of linoleic acid ester and oleic acid ester of tocopherol), tocopheryl nicotinate (tocopherol nicotinic acid ester) and tocopheryl succinate (succinic acid ester of tocopherol). The mixture of vitamin E (tocopherol) and vitamin C (ascorbic acid) includes potassium ascorbyl tocopheryl phosphate, and the tocopherol derivative component is dioleyl tocopheryl methylsilanol (methylsilane triol and tocopheryl acetate mono dioleyl ether of ether) and tocophersolane (tocopheryl polyethylene glycol 1000 succinate, wherein tocophersolane is a water-soluble form of tocopherol by adding succinic acid and an average of 22 ethylene oxide groups to tocopherol. Tocofesolan can be made.
이러한 산화방지 물질의 함량은 하나의 분말형 클렌징 조성물을 기준으로 15 w% 이상 24 w% 이하의 범위에서 포함되는 것이 바람직하다.The content of these antioxidants is preferably included in the range of 15 w% or more and 24 w% or less based on one powder type cleansing composition.
본 발명의 일실시예에서 상기 제2코팅층은 컨디셔닝제를 포함할 수 있다.In one embodiment of the present invention, the second coating layer may include a conditioning agent.
상기 컨디셔닝제는 피부에 보습, 윤기, 유연성을 주거나 손상된 피부를 개선하는 등의 목적을 위해 사용되는 원료를 말하며, 본 발명에서는 보습제, 수분차단제, 유연제 등의 원료를 포함하는 컨디셔닝제를 사용하되, 바람직하게는 물에 쉽게 용해되지 않는 왁스, 지방알코올류, 미네랄 오일을 제외한 컨디셔닝제를 어느 하나 이상 선택하여 사용할 수 있다.The conditioning agent refers to a raw material used for the purpose of providing moisture, shine, flexibility to the skin or improving damaged skin. Preferably, at least one conditioning agent other than waxes, fatty alcohols, and mineral oils that are not easily soluble in water may be selected and used.
상기 컨디셔닝제는 천연 혹은 합성 추출물, 아미노산류 및 단백질, 당류, 천연 또는 합성 오일, 알코올류, 계면활성제 등을 포함하며, 그 예로 히비스커스꽃추출물, 비터오렌지꽃추출물, 연꽃추출물, 에델바이스꽃/잎/줄기추출물, 부틸렌글라이콜, 1,2-헥산다이올, 글리세린, 엘더꽃추출물, 개똥쑥추출물, 포트마리골드꽃추출물, 라벤더꽃추출물, 헥실렌글라이콜, 에톡시다이클라이콜, 다이프로필렌글라이콜, 꿀, 소듐피씨에이액, 소르비톨, 스쿠알란, 스테아릴스테아레이트, 스테아릴헵타노에이트, 식물성스쿠알란, 글리세릴로지네이트, 소듐폴리아크릴레이트, 알로에추출물, C12-15알코올스벤조에이트, 아세틸레이티드라놀린 등으로 이루어진 어느 하나 이상의 군에서 선택할 수 있으며, 바람직하게 히비스커스꽃추출물, 비터오렌지꽃추출물, 연꽃추출물, 에델바이스꽃/잎/줄기추출물을 포함할 수 있다.The conditioning agent includes natural or synthetic extracts, amino acids and proteins, sugars, natural or synthetic oils, alcohols, surfactants, etc., for example, hibiscus flower extract, bitter orange flower extract, lotus flower extract, edelweiss flower / leaf / Stem extract, butylene glycol, 1,2-hexanediol, glycerin, elder flower extract, artemisia extract, port marigold flower extract, lavender flower extract, hexylene glycol, ethoxydiglycol, dipropylene Glycol, Honey, Sodium PCA, Sorbitol, Squalane, Stearyl Stearate, Stearyl Heptanoate, Vegetable Squalane, Glyceryl Loginate, Sodium Polyacrylate, Aloe Extract, C12-15 Alcohols Benzoate, It may be selected from any one or more groups consisting of acetylated lanolin, etc., and may preferably include hibiscus flower extract, bitter orange flower extract, lotus flower extract, and edelweiss flower/leaf/stem extract.
이러한 컨디셔닝제의 함량은 0.1w% 내지 2w% 범위에서 사용될 수 있다. 만약 컨디셔닝제의 원료가 물에 잘 녹지 않는 지용성일 경우 다량 사용시 딱딱한 이물감을 발생시킬 수 있으므로 본 발명에서는 물에 쉽게 용해되지 않는 왁스, 지방알코올류, 미네랄 오일을 제외하여 제조하는 것도 가능하다.The amount of this conditioning agent may be used in the range of 0.1w% to 2w%. If the conditioning agent is fat-soluble and does not dissolve well in water, it may cause a hard foreign body sensation when used in large amounts. In the present invention, it is also possible to manufacture excluding waxes, fatty alcohols, and mineral oils that are not easily soluble in water.
이외에도 컨디셔닝제는 본 발명의 목적과 효능을 해치지 않는 범위에서 다양하게 선택할 수 있다.In addition, the conditioning agent may be variously selected within a range that does not impair the purpose and efficacy of the present invention.
상기 제2 코팅층은 바인더를 포함할 수 있다. 바인더는 원료를 원하는 제형으로 성형할 때 입자끼리 점착될 수 있도록 접착제 역할을 하는 성분을 의미한다.The second coating layer may include a binder. Binder refers to a component that acts as an adhesive so that particles can be adhered to each other when molding raw materials into a desired formulation.
이러한 바인더의 종류로 변성 전분이나 천연 유래 전분, 다당류, 셀룰로오스 등을 사용할 수 있으며, 그 예로 하이드록시프로필스타치포스페이트, 옥수수 전분, 쌀 전분, 카사바 전분, 감자 전분, 밀 전분, 수수 전분, 콩 전분, 펙틴, 아라비아검, 구아검, 로커스트콩검, 산탄검, 젤란검, 카라야검, 타라검, 타마린드검, 트라가칸스검, 천연검, 사일리움씨드검, 히드록실에틸셀룰로스, 히드록시프로필메틸셀룰로스 등이 있다. 이외에도 바인더는 비슷한 기능을 가진 다른 물질로 대체하거나 추가하여 사용할 수 있고, 바람직하게는 하이드록시프로필스타치포스페이트가 좋다.Modified starch, naturally derived starch, polysaccharide, cellulose, etc. may be used as the binder, and examples thereof include hydroxypropyl starch phosphate, corn starch, rice starch, cassava starch, potato starch, wheat starch, sorghum starch, and soybean starch , pectin, gum arabic, guar gum, locust bean gum, xanthan gum, gellan gum, gum karaya, gum tara, gum tamarind, gum tragacanth, natural gum, psyllium seed gum, hydroxyethylcellulose, hydroxypropylmethyl cellulose, etc. In addition, the binder may be used by replacing or adding another material having a similar function, preferably hydroxypropyl starch phosphate.
상기 제2 코팅층은 색 첨가물질을 포함할 수 있다.The second coating layer may include a color additive material.
상기 색 첨가물질은 색조 효과를 주는 화장품 원료라면 한정하지 않으며, 그 예로, 시아노코발라민, 해바라기씨오일, 알칸나뿌리추출물, 울금추출물, 알루미늄가루, 울트라마린핑크처리폴리에칠렌가루, 티타늄옥사이드블랙, 코발트알루미늄옥사이드, 크로뮴옥사이드그린 등이 있고, 바람직하게 시아노코발라민이 좋다.The color additive material is not limited as long as it is a cosmetic raw material that gives a color effect, for example, cyanocobalamin, sunflower seed oil, alkanna root extract, turmeric extract, aluminum powder, ultramarine pink treated polyethylene powder, titanium oxide black, cobalt There are aluminum oxide, chromium oxide green, etc., Preferably cyanocobalamin is good.
상기 색 첨가 물질의 함량은 하나의 분말용 클렌징 조성물에서 0.01w% 이하의 범위가 좋다.The content of the color additive is preferably in the range of 0.01w% or less in one powder cleansing composition.
본 발명의 일실시예에서 상기 코어 입자를 베이스로 하여 컨디셔닝제, 바인더, 색 첨가물질을 포함한 물질을 유동층 공정기에 투입한 후 분사하면서 건조하는 것으로 제2 코팅층이 포함된 입자를 제조할 수 있으며, 제2 코팅층까지 도포가 완료된 물질은 유동층 시스템 내에서 50℃ 내지 65℃의 온도로 건조되어진다.In one embodiment of the present invention, particles including a second coating layer can be prepared by injecting materials including a conditioning agent, binder, and color additives into a fluidized bed process machine based on the core particles, and drying while spraying, The material applied to the second coating layer is dried at a temperature of 50° C. to 65° C. in a fluidized bed system.
이하 구체적인 실시예를 통하여 본 발명의 구성 및 효과를 보다 상세하게 설명하되, 이들 실시예는 단지 본 발명을 보다 명확하게 이해시키기 위한 것일 뿐, 본 발명의 청구범위를 한정하고자 하는 것은 아니다.Hereinafter, the configuration and effects of the present invention will be described in more detail through specific examples, but these examples are only intended to more clearly understand the present invention, and are not intended to limit the scope of the present invention.
실시예 : 분말형 세정 조성물Example: Powder type cleaning composition
하기의 표 1의 성분들을 아래의 단계 a 내지 e에 따라 진행하여 분말형 세정 조성물을 제조하였다. 각 성분의 함량은 중량%에 따른다.The ingredients of Table 1 below were proceeded according to steps a to e below to prepare a powder type cleaning composition. The content of each component is according to weight %.
본 발명의 실시예에 따른 캡슐형 세정 조성물의 제조방법은 다음과 같다.The manufacturing method of the capsule-type cleaning composition according to an embodiment of the present invention is as follows.
a) 상기 표의 코어 시드 성분으로 코어를 형성한다. 이러한 코어는 분말 형태로 하기 유동층 공정 시스템에 도입된다.a) Form a core with the core seed ingredients in the table above. These cores are introduced in the following fluidized bed processing system in powder form.
b) 상기 표의 제1 코팅층의 성분들을 물에 용해 및 분산한 후, 유동층 공정 시스템에 도입하여 약 1000ml/h 속도로 상기 분말 형태의 코어에 1차 코팅을 수행한다.b) After dissolving and dispersing the components of the first coating layer in the above table in water, first coating is performed on the powder core at a speed of about 1000 ml/h by introducing the fluidized bed process system.
c) 상기 표의 제2 코팅층의 성분들을 물에 용해 및 분산한 후, 유동층 공정 시스템에 도입하여 약 1000ml/h 속도로 상기 분말 형태의 입자에 2차 코팅을 수행한다c) After dissolving and dispersing the components of the second coating layer in the above table in water, a second coating is performed on the powdery particles at a rate of about 1000 ml/h by introducing them into a fluidized bed process system
d) 수득된 입자는 유동층 공정 시스템에서 50 내지 65℃의 온도로 약 10분 동안 건조 과정을 거친다.d) The obtained particles are subjected to a drying process for about 10 minutes at a temperature of 50 to 65° C. in a fluidized bed process system.
e) 건조된 과립 입자는 분류(Sieving) 과정을 거쳐 대략 200Mesh 내지 25Mesh 또는 75μm 내지 710μm 크기를 갖는 캡슐 형태의 분말상 세정 조성물로 수득된다.e) The dried granular particles are obtained as a powdery cleaning composition in the form of capsules having a size of approximately 200Mesh to 25Mesh or 75μm to 710μm through a sieving process.
한편, 상기 캡슐형 세정 조성물을 제조하기 위한 상기 세부 함량은 소듐라우로일글루타메이트(SLG) 75~84w%, 하이드록시아세토페논 15~24w%, 히비스커스꽃추출물 0.05~0.2w%, 비터오렌지꽃추출물 0.05~0.3w%, 연꽃추출물0.05~0.4w%, 에델바이스꽃/잎/줄기추출물 0.05~0.5w%, 시아노코발라민 0.0001~0.01w%의 조성비에서 선택되는 것이 바람직하다.On the other hand, the detailed content for preparing the capsule type cleaning composition is sodium lauroyl glutamate (SLG) 75 ~ 84w%, hydroxyacetophenone 15 ~ 24w%, hibiscus flower extract 0.05 ~ 0.2w%, bitter orange flower extract It is preferably selected from a composition ratio of 0.05 to 0.3w%, lotus extract 0.05 to 0.4w%, edelweiss flower/leaf/stem extract 0.05 to 0.5w%, and cyanocobalamin 0.0001 to 0.01w%.
다음으로, 상기 실시예에서 수득된 분말상 클렌징 조성물을 이용하여 미세먼지 모사체 차단제 세정력에 대해 수행하여 인체 효능 평가를 확인한 결과는 다음과 같다.Next, the results of confirming the human body efficacy evaluation by performing the cleaning power of the fine dust mimetic blocker using the powdery cleansing composition obtained in the above example are as follows.
시험 개요 및 피험자 선정기준Trial overview and subject selection criteria
상기 인체 효능 평가는 만 20~60세의 성인을 대상으로 시험을 진행하였으며, 시험 제품은 사용방법에 따라 시험 부위에 사용하였다. 또한 평가는 관련 표준시험방법(SOP)에 준하여 성실히 수행하였다. 피험자의 선정기준은 만 20~60세의 건강한 성인 남녀이며, 선정기준에 부합되는 20명을 선정하여 평가하였다.The human efficacy evaluation was conducted on adults aged 20 to 60 years old, and the test product was used in the test site according to the method of use. In addition, the evaluation was faithfully performed according to the relevant standard test method (SOP). The selection criteria for subjects were healthy adult men and women aged 20 to 60 years, and 20 subjects who met the selection criteria were selected and evaluated.
측정 개요Measurement overview
시험은 피험자의 전박부에 적당량 도포하여 사용하였고, 측정 시기는 제품 사용 전, 미세먼지 모사체 도포 후, 제품 사용 직후에 측정을 실시하였다. 측정 환경은 피험자들의 측정 조건을 동일하게 하고자 시험 부위를 깨끗하고 마른 상태로 유지하였으며, 공기의 이동과 직사광선이 없는 항온 항습 조건(실내온도20~24℃, 습도 40~60%)에서 진행하였다.The test was used by applying an appropriate amount to the forearm of the subject, and the measurement time was measured before using the product, after applying the fine dust mimetic, and immediately after using the product. For the measurement environment, the test site was kept clean and dry in order to make the measurement conditions of the subjects the same, and it was conducted under constant temperature and humidity conditions (room temperature 20 ~ 24 ℃, humidity 40 ~ 60%) without air movement and direct sunlight.
측정measurement
미세먼지 모세체 세정력 측정은 모발측정기(Folliscope 5.0, Lead M Co.Korea)을 이용하였다. 상기 Folliscope 5.0 (Lead M Co.Korea)은 Folliscope 를 이용하여 제공된 소프트웨어 소프트웨어 프로그램인 Folliscope(Phototrichogram)가 장착된 컴퓨터를 통해 이미지를 촬영한 후, 분석프로그램(Image-Pro, Media Cybernetics, USA)를 이용하여 Intensity(명도)값을 분석하였으며, 시험군, 비누 처치군, 물 세정군의 제품 사용 전, 미세먼지 모사체 도포 후, 제품 사용 직후 변화를 비교 평가하였다. 분석값은 Intensity(명도)값으로, 값이 증가할수록 세정 효과가 있다고 판단한다.Fine dust capillary cleaning power was measured using a hair measuring instrument (Folliscope 5.0, Lead M Co. Korea). The Folliscope 5.0 (Lead M Co.Korea) takes images through a computer equipped with Folliscope (Phototrichogram), a software program provided using Folliscope, and then uses an analysis program (Image-Pro, Media Cybernetics, USA) Intensity values were analyzed, and changes in the test group, soap treatment group, and water washing group were compared and evaluated before product use, after application of fine dust mimics, and immediately after product use. The analysis value is the Intensity value, and as the value increases, it is judged that there is a cleaning effect.
설문 평가survey evaluation
시험대상자는 시험 제품 사용 후 주관적 평가 및 제품 기호도 평가에 대하여 평가하였다. 아주 좋음 - 좋음 - 보통 - 나쁨 - 아주 나쁨의 총 5단계로 나누어 답하게 하였고, 결과는 합산하여 백분율로 나타내었다.Subjects were evaluated for subjective evaluation and product preference after using the test product. Very good - good - average - bad - very bad were divided into five levels, and the results were summed and expressed as a percentage.
안전성 평가(이상반응 및 병용약물 평가)Safety evaluation (adverse reactions and concomitant drug evaluation)
시험대상자는 피부 반응에 영향을 미칠 수 있는 병용약물 사용 및 제품 사용 전, 제품사용 직후의 이상반응 여부를 확인하였다. 이상반응 평가는 피험자가 매회 방문할 때마다 육안으로 이상반응 (홍반(Erythema), 부종(Edema), 인설(Scaling), 가려움(Itching), 자통(Stinging), 작열감(Burning), 뻣뻣함(Tightness), 따끔거림(Prickling) 및 다른 이상반응)이 발생하는 지의 여부를 면밀히 관찰하고 평가하였다. 이상 반응 여부 및 등급 분류표는 다음과 같다.Subjects were checked for concomitant drug use that may affect skin reactions, and for adverse reactions before and after product use. Adverse reaction evaluation was performed by the subject at each visit, with the naked eye examining adverse reactions (erythema, edema, scaling, itching, stinging, burning, and tightness). , prickling and other adverse reactions) were closely observed and evaluated. The adverse reaction status and classification table are as follows.
이상반응 여부의 평가 종류 및 등급 분류 기준Types of evaluation of adverse reactions and criteria for grading
홍반Erythema
erythema
부종Edema
edema
인설Scaling
scale
가려움Itching
itch
자통Stinging
sting
작열감Burning
burning sensation
뻣뻣함Tightness
stiffness
따끔거림Prickling
tingling
0:none(이상반응 없음), 1:mild, 2:severe, 3:very severe(심각한 이상반응)
0:none (no adverse reaction), 1:mild, 2:severe, 3:very severe (severe adverse reaction)
미세먼지 모사체 세정력의 측정 결과 분석Analysis of the measurement result of fine dust mimetic detergency
상기 모발측정기(Folliscope 5.0, Lead M Co., Korea)를 이용하여 시험 부위의 미세먼지 모사체 세정력을 측정하였다. 평가는 제품 사용 전, 미세먼지 모사체 도포 후, 제품 사용 직후에 전박 부위 촬영 이미지 및 데이터를 분석하였다. 세정력 및 개선율은 아래와 같이 계산하였다.The cleaning power of the fine dust mimetic at the test site was measured using the hair measuring device (Folliscope 5.0, Lead M Co., Korea). For evaluation, images and data taken in the forearm area were analyzed before product use, after application of the fine dust mimic, and immediately after product use. The cleaning power and improvement rate were calculated as follows.
- 세정력(%) 및 개선율(%) 계산식- Calculation formula for detergency (%) and improvement rate (%)
통계적 분석statistical analysis
통계프로그램(데이터 솔루션의 SPSS statistics)을 사용하여 분석하였으며, 시험 결과는 정규성 검정을 실시한 후 통계분석을 실시하였다. 분석 결과 95%의 신뢰구간에서 유의확률p<0.05일 때, 시험제품 사용에 의해 개선 효과가 있다고 판단하였다. 통계분석법으로는 모수적 방법을 이용한 경우에는 Paired samples t-test, 비모수적 방법을 이용한 경우 Wilcoxon signed rank test를 사용하여 분석하였다. 군간 비교는 변화량으로 비교하였으며, 모수적 통계 방법으로 Independent samples t-test, 비모수적인 통계 방법으로는 Mann-Whitney 검정을 사용하였다.It was analyzed using a statistical program (SPSS statistics of data solution), and the test results were subjected to statistical analysis after normality test. As a result of the analysis, when the significance probability p<0.05 in the 95% confidence interval, it was judged that there was an improvement effect by using the test product. For statistical analysis, paired samples t-test was used in case of using parametric method, and Wilcoxon signed rank test was used in case of using non-parametric method. Comparison between groups was compared by the amount of change, and the independent samples t-test was used as a parametric statistical method, and the Mann-Whitney test was used as a non-parametric statistical method.
시험결과Test result
피험자 정보Subject information
본 인체적용시험에 참가한 인원은 20 명이며, 시험 도중 이상반응, 병용약물 및 그 외 이유로 탈락한 피험자는 없으므로 전체 시험에 참여한 총 피험자는 20 명이다. 피험자의 평균 연령은 42.0 세, 표준 편차는 6.9 이었다.The number of subjects who participated in this human application test was 20, and there were no subjects who dropped out due to adverse reactions, concomitant drugs, or other reasons during the test, so the total number of subjects who participated in the entire test was 20. The mean age of the subjects was 42.0 years, and the standard deviation was 6.9.
측정 결과measurement result
미세먼지 모사체 세정력Fine dust matrix detergency
Folliscope를 이용한 미세먼지 모사체 세정력 측정결과 및 통계학적 분석결과, 세정력 및 개선율은 다음 표과 같다.The results of measuring and statistically analyzing the cleaning power of fine dust mimics using the Folliscope, cleaning power and improvement rate are shown in the following table.
미세먼지 모사체 흡착량Adsorption amount of fine dust mimetic
3.20274.07 ±
3.202
7.00365.31 ±
7.003
4.34075.90 ±
4.340
8.30755.70±
8.307
4.04176.04±
4.041
5.88319.09±
5.883
(1) 미세먼지 모사체 도포 후vs제품 사용 직후 by Paired samples t-test, p<0.05(1) After application of fine dust mimetic vs. immediately after product use by Paired samples t-test, p<0.05
(2) 시험군 흡착량 변화량(Δ)vs비누 처치군 흡착량 변화량(Δ) by Independent samples t-test, p<0.05(2) Change in adsorption amount in the test group (Δ) vs. change in adsorption amount in the soap-treated group (Δ) by Independent samples t-test, p<0.05
상기 표4에 의한 결과는 미세먼지 모사체 흡착량에 대한 도면(도 1)과 미세먼지 모사체 세정력에 대한 도면(도 2)과 미세먼지 모사체 세정 개선율에 대한 도면(도 3)에서 그래프로 확인할 수 있다.The results according to Table 4 are graphed in the graph for the amount of adsorption of the fine dust matrix (Fig. 1), the figure for the cleaning power of the fine dust matrix (Fig. 2), and the figure for the cleaning improvement rate of the fine dust matrix (Fig. 3). You can check.
- 본 발명의 클렌징 조성물의 미세먼지 모사체 흡착량 Intensity 분석 결과, 제품 사용 전 119.90, 미세먼지 모사체 도포 후 45.83, 제품 사용 직후 111.14로 통계적으로 유의한 수준으로 미세먼지 모사체 흡착량이 감소하였으며, 미세먼지 모사체 도포 후 대비 제품 사용 직후 88.1%의 세정력을 나타내었다(p<0.05).- As a result of the intensity analysis of the fine dust matrix adsorption amount of the cleansing composition of the present invention, the amount of fine dust matrix adsorption decreased to a statistically significant level: 119.90 before using the product, 45.83 after application of the fine dust matrix, and 111.14 immediately after using the product, It showed 88.1% of cleaning power immediately after using the product compared to after application of the fine dust mimic (p<0.05).
- 미세먼지 모사체 도포 후 대비 제품 사용 직후 흡착량 변화량(Δ) 비교 결과, 시험군은 65.31, 비누 처치군은 55.70로 비누 처치군에 비해 시험군이 통계적으로 유의한 수준으로 미세먼지 모사체 흡착량 변화량(Δ)이 높았다(p<0.05).- As a result of comparing the change in adsorption amount (Δ) immediately after product use compared to after application of the fine dust mimetic, the test group was 65.31 and the soap-treated group was 55.70, which is a statistically significant level of adsorption of the fine dust mimetic compared to the soap-treated group. The amount change (Δ) was high (p<0.05).
- 시험군과 비누 처치군의 군간 비교 분석 결과, 시험군의 개선율은 73.4%, 비누 처치군의 개선율은 56.5%로 비누 처치군에 비해 시험군이 통계적으로 유의한 수준으로 개선율이 높았다(p<0.05).- As a result of the comparative analysis between the test group and the soap-treated group, the improvement rate of the test group was 73.4% and the soap-treated group was 56.5%, showing a statistically significant improvement in the test group compared to the soap-treated group (p < 0.05).
피험자의 미세먼지 모사체 세정력 외형 비교Comparison of the external appearance of the fine dust mimetic cleaning power of the subjects
다음으로, 피험자 중 일부의 모사체 세정력을 확인하기 위해 제품 사용전, 미세먼지 모사체 도포 후, 제품 사용 직후를 외형 비교한 이미지(도 4)를 보면, 미세먼지 모사체가 도포된 상태에서 본 발명의 세정 조성물을 사용할 경우 미세먼지가 깨끗이 지워진 것을 확인할 수 있다Next, looking at the image (FIG. 4) comparing the appearance of the product before use, after application of the fine dust mimetic, and immediately after using the product to confirm the detergency of the mimetic body of some of the subjects, in the state in which the mimetic fine dust is applied, the present invention When using the cleaning composition, it can be confirmed that the fine dust is completely removed.
안전성 평가safety assessment
시험 제품 적용 후 전체 20명의 시험대상자 중 20명이 증상 없음에 답하였다.After application of the test product, 20 out of 20 subjects answered no symptoms.
이상반응 확인Adverse reaction confirmation
설문평가Survey evaluation
시험 제품 사용 후 시험 제품에 대한 주관적 설문 평가 및 제품 기호도 평가를 실시하여 다음과 같은 결과를 얻었다.After using the test product, subjective questionnaire evaluation and product preference evaluation were conducted on the test product, and the following results were obtained.
시험대상자의 제품 만족도 설문평가Product satisfaction survey evaluation of test subjects
5점very good
5 points
4점good
4 points
3점commonly
3 points
2점bad
2 points
1점very bad
1 point
(25.0%)5
(25.0%)
(50.0%)10
(50.0%)
(25.0%)5
(25.0%)
(0.0%)0
(0.0%)
(0.0%)0
(0.0%)
※ 5점: 아주 좋음, 4점: 좋음, 3점: 보통, 2점: 나쁨, 1점: 아주 나쁨※ 5 points: very good, 4 points: good, 3 points: average, 2 points: bad, 1 point: very bad
기호도 설문평가Preference survey evaluation
※ 5점: 아주 좋음, 4점: 좋음, 3점: 보통, 2점: 나쁨, 1점: 아주 나쁨※ 5 points: very good, 4 points: good, 3 points: average, 2 points: bad, 1 point: very bad
정리 및 요약Organize and summarize
상기 평가에서 본 발명의 세정 조성물을 통해 미세먼지 모사체, 자외선 차단제 세정력 시험에 대한 인체적용시험을 실시하여 다음과 같은 결론을 얻었다.In the above evaluation, a human application test was conducted on the cleaning power of the fine dust mimetic and sunscreen using the cleaning composition of the present invention, and the following conclusions were obtained.
1. 만20~60세의 시험대상자(평균나이 42.0 ± 6.9세)를 대상으로 시험을 실시하였고, 최종 20명(중도탈락: 0명)이 시험을 종료하였다.1. The test was conducted on subjects between the ages of 20 and 60 (average age: 42.0 ± 6.9 years), and the final 20 (dropout: 0) completed the test.
2. 미세먼지 모사체 세정력 시험군 군내 비교(전후 비교)2. Comparison within the fine dust matrix detergency test group (before and after comparison)
- 미세먼지 모사체 흡착량 Intensity 분석 결과, 제품 사용 전 119.90, 미세먼지 모사체 도포 후 45.83, 제품 사용 직후 111.14로 통계적으로 유의한 수준으로 미세먼지 모사체 흡착량이 감소하였으며, 미세먼지 모사체 도포 후 대비 제품 사용 직후 88.1%의 세정력을 나타내었다(p<0.05).- As a result of the intensity analysis of the adsorption amount of fine dust mimetic, it was 119.90 before using the product, 45.83 after application of the fine dust mimetic, and 111.14 immediately after using the product. Immediately after using the contrast product, 88.1% of cleaning power was shown (p<0.05).
3. 미세먼지 모사체 세정력 군간 비교3. Comparison of fine dust matrix detergency between groups
- 미세먼지 모사체 도포 후 대비 제품 사용 직후 흡착량 변화량(Δ) 비교 결과, 시험군은 65.31, 비누 처치군은 55.70로 비누 처치군에 비해 시험군 미세먼지 모사체 흡착량 변화량(Δ)이 통계적으로 유의한 수준을 나타내었다(p<0.05).- As a result of comparing the change in adsorption amount (Δ) immediately after using the product compared to after application of the fine dust mimetic, the test group was 65.31 and the soap treatment group was 55.70. showed a significant level (p<0.05).
- 시험군과 비누 처치군의 군간 비교 분석 결과, 시험군의 개선율은 73.4%, 비누 처치군의 개선율은 56.5%로 비누 처치군에 비해 시험군의 개선율이 통계적으로 유의한 수준을 나타내었다(p<0.05).- As a result of comparative analysis between the test group and the soap-treated group, the improvement rate of the test group was 73.4%, and the soap-treated group was 56.5%, showing a statistically significant improvement rate compared to the soap-treated group (p <0.05).
상기의 내용을 요약하면, 인체적용시험 결과를 통해볼 때, 본 발명에 의한 분말상 클렌징 조성물은 미세먼지 모사체 세정력 시험에 도움을 주는 것을 확인할 수 있다. 또한, 평가 기간 동안 특별한 피부 이상반응을 나타내지 않았다.Summarizing the above, when viewed through the human body application test results, it can be confirmed that the powdery cleansing composition according to the present invention helps in the fine dust mimetic cleaning power test. Also, during the evaluation period, no specific skin adverse reaction was shown.
다음으로, 본 발명의 실시예에서 중금속/유기물 및 미생물 시험을 수행한 결과는 다음과 같다.Next, the results of heavy metal/organic and microbial tests in Examples of the present invention are as follows.
중금속/유기물 시험결과Heavy metal/organic test results
미생물 시험결과Microbial test result
본 발명의 세정 조성물은 식품의약품안전처고시에 의한 중금속/유기물 평가에서 “검출안됨”의 결과를 얻었으며, 미생물 평가에서 세균수, 진균수는 허용 기준치 미만의 결과가 검출되고, 대장균, 녹공균, 황색포도상구균은 “검출안됨”의 결과를 얻었다.The cleaning composition of the present invention obtained the result of “not detected” in the evaluation of heavy metals/organic substances according to the Ministry of Food and Drug Safety, and in the evaluation of microorganisms, the number of bacteria and fungi were less than the acceptable standard, and E. coli and Pseudomonas were detected. , Staphylococcus aureus obtained a result of “not detected”.
다음으로, 상기 실시예에서 수득된 세정 조성물을 물과 혼합하여 그 함량에 따른 용해도, 제품 안정성 등을 확인하기 위해 투명한 디스펜서에 세정 조성물을 0.5% 1%, 1.5%, 2.5%, 5% 함유한 혼합액을 넣어 육안으로 관찰하였다. 이때 본 발명을 사용할 소비자의 편의를 고려하여 용매는 상온의 일반 수돗물을 이용하였으며, 용매와 용질의 총 질량은 200g으로 고정하였다.Next, the cleaning composition obtained in the above example was mixed with water to check the solubility and product stability according to the content thereof. The mixed solution was added and observed with the naked eye. At this time, in consideration of the convenience of consumers who will use the present invention, ordinary tap water at room temperature was used as the solvent, and the total mass of the solvent and solute was fixed at 200 g.
그 결과, 0.5% 혼합액은 용질이 거의 녹아 투명한 액체로 관찰되었고, 1% 혼합액, 1.5% 혼합액, 2.5% 혼합액은 전체적으로 옅은 핑크색을 띄고 있으나 여전히 투명한 액체 형상을 유지하고, 5% 혼합물은 약간의 부유물이 육안으로 발견되었다.(도 5 참고)As a result, the 0.5% mixed solution was observed as a transparent liquid with almost dissolved solute, and the 1% mixed solution, 1.5% mixed solution, and 2.5% mixed solution had a pale pink color as a whole, but still maintained a transparent liquid shape, and the 5% mixture had some floating matter. This was found with the naked eye. (See Fig. 5)
제품 안정성에 있어서, 0.5% 1%, 1.5%, 2.5%, 5% 혼합물 모두 풍성한 거품 형성과 충분한 세정력이 있음을 관찰하였고, 상기 혼합액을 대략 30일 동안 상온에서 보관하여도 용매 및 원료들의 분리현상이나 세정 능력 저하 등의 문제없이 사용이 가능하였다.In terms of product stability, it was observed that all 0.5%, 1%, 1.5%, 2.5%, and 5% mixtures had abundant foam formation and sufficient detergency, and separation of solvents and raw materials even when the mixture was stored at room temperature for about 30 days. It was possible to use without problems such as deterioration of cleaning ability.
실험예 : 분말형 세정 조성물의 세정력Experimental Example: Cleaning Power of Powdered Cleaning Composition
상기 실시예에서 제조된 분말형 세정 조성물의 세정력을 평가하기 위해서 실험대상자의 하박부 피부에 메이크업 화장료를 묻히고, 물(일반 수돗물)만 사용(A)했을 때와, 본 발명에 의한 세정 조성물(B)의 혼합액을 사용했을 때의 세정 효과를 관찰하였다. 이때 본 발명의 세정 조성물의 혼합액은 디스펜서에 물 198g과 상기 실시예의 세정 조성물 2g을 혼합한 1% 혼합액을 사용하였고, 펌핑 횟수는 1회로 제한하여 관찰하였다.In order to evaluate the cleaning power of the powder type cleaning composition prepared in the above example, makeup cosmetics were applied to the skin of the lower part of the test subject and only water (normal tap water) was used (A), and the cleaning composition according to the present invention (B) ), the cleaning effect was observed when the mixed solution was used. At this time, the liquid mixture of the cleaning composition of the present invention was a 1% liquid mixture obtained by mixing 198 g of water and 2 g of the cleaning composition of the above example in a dispenser, and the number of pumping was limited to one time and observed.
평가는 피부에 남아있는 화장료의 흔적을 육안으로 관찰하여 화장료가 모두 지워진 것을 우수(◎), 1/2 이하로 남아있는 것을 보통(△), 1/2 이상 남아있는 것을 불량(Ⅹ)으로 평가하였다. 그 결과는 하기 표 10 및 도 6에 나타내었다.In the evaluation, traces of cosmetics remaining on the skin are observed with the naked eye, and those with all cosmetics removed are evaluated as excellent (◎), those with less than 1/2 remaining are evaluated as normal (△), and those with more than 1/2 remaining as poor (X). did The results are shown in Table 10 and FIG. 6 below.
이 외에도 전술한 본 발명의 설명은 예시를 위한 것이며, 본 발명이 속하는 기술분야의 통상의 지식을 가진 자는 본 발명의 기술적 사상이나 필수적인 특징을 변경하지 않고서 다른 구체적인 형태로 쉽게 변형이 가능하다는 것을 이해할 수 있을 것이다. 그러므로 이상에서 기술한 실시예들은 모든 면에서 예시적인 것이며 한정적이 아닌 것으로 이해해야만 한다. 예를 들어, 단일형으로 설명되어 있는 각 구성 요소는 분산 또는 분할되어 실시될 수도 있으며, 마찬가지로 분산 또는 분할된 것으로 설명되어 있는 구성 요소들도 통상의 기술자가 이해하는 범위 안에서 결합된 형태로 실시될 수 있다. 또한, 방법의 단계는 단독으로 복수회 실시되거나 혹은 적어도 다른 어느 한 단계와 조합으로 복수회 수행되는 형태로 실시될 수 있다.In addition to this, the description of the present invention described above is for illustrative purposes, and those skilled in the art will understand that it can be easily modified into other specific forms without changing the technical spirit or essential features of the present invention. You will be able to. Therefore, the embodiments described above should be understood as illustrative in all respects and not limiting. For example, each component described as a single type may be implemented in a distributed or divided manner, and likewise, components described as distributed or divided may be implemented in a combined form within the understanding of a person skilled in the art. there is. Further, a method step may be performed alone or multiple times or in combination with at least one other step.
본 발명의 범위는 후술하는 특허청구범위에 의하여 나타내어지며, 특허청구범위의 의미 및 범위 그리고 그 균등 개념으로부터 도출되는 모든 변경 또는 변형된 형태가 본 발명의 범위에 포함되는 것으로 해석되어야 한다.The scope of the present invention is indicated by the following claims, and all changes or modifications derived from the meaning and scope of the claims and equivalent concepts should be interpreted as being included in the scope of the present invention.
Claims (12)
A powdery cleansing composition comprising an amino acid-based or isethionate-based surfactant; and an antioxidant.
상기 아미노산계 계면활성제는 소듐라우로일글루타메이트를 포함하고,
상기 산화방지제는 하이드록시아세토페논을 포함하는 것을 특징으로 하는 분말상 클렌징 조성물.
According to claim 1,
The amino acid-based surfactant includes sodium lauroyl glutamate,
The antioxidant is a powdery cleansing composition, characterized in that it comprises hydroxyacetophenone.
상기 코어는 아미노산계 계면활성제를 포함하고,
상기 코팅층은 산화방지제를 포함하는 것을 특징으로 하는 분말상 클렌징 조성물.
core; And, it is formed in the form of a capsule, including; a coating layer surrounding the core,
The core includes an amino acid-based surfactant,
The powdery cleansing composition, characterized in that the coating layer contains an antioxidant.
상기 코어는 소듐라우로일글루타메이트를 포함하고,
상기 코팅층은 하이드록시아세토페논, 아스코빅애씨드 및 그 염류, 비타민E, 토코페롤 에스터, 비타민 E와 비타민 C 의 혼합물, 토코페롤 유도체 성분, 토코페솔란, 비타민 A, 유비퀴논, 알파리포애씨드, 카로티노이드, 비타민B, 로즈 방부제(Rose Preservative), 자몽 추출액(Grapefruit Seed Extract)중 어느 하나이상이 포함되는 것을 특징으로 하는 분말상 클렌징 조성물.
According to claim 3,
The core contains sodium lauroyl glutamate,
The coating layer is hydroxyacetophenone, ascorbic acid and its salts, vitamin E, tocopherol ester, a mixture of vitamin E and vitamin C, tocopherol derivatives, tocophersolane, vitamin A, ubiquinone, alpha lipoic acid, carotenoids, vitamins B, a powdery cleansing composition comprising at least one of Rose Preservative and Grapefruit Seed Extract.
상기 코팅층은 컨디셔닝제 및 바인더를 포함하며,
상기 컨디셔닝제는 천연 혹은 합성 추출물, 아미노산류 및 단백질, 당류, 천연 또는 합성 오일, 알코올류, 계면활성제로 구성된 군에서 적어도 하나 이상 포함하는 것을 특징으로 하는 분말상 클렌징 조성물.
According to claim 3,
The coating layer includes a conditioning agent and a binder,
The conditioning agent powdery cleansing composition, characterized in that it comprises at least one or more from the group consisting of natural or synthetic extracts, amino acids and proteins, sugars, natural or synthetic oils, alcohols, surfactants.
상기 컨디셔닝제는 물에 쉽게 용해되지 않는 왁스, 지방알코올류, 미네랄 오일을 제외한 천연 혹은 합성 추출물, 아미노산류 및 단백질, 당류, 천연 또는 합성 오일, 알코올류, 계면활성제로 구성된 군에서 적어도 하나 이상 포함하는 것을 특징으로 하는 분말상 클렌징 조성물.
According to claim 5,
The conditioning agent includes at least one from the group consisting of natural or synthetic extracts, amino acids and proteins, sugars, natural or synthetic oils, alcohols, and surfactants excluding waxes, fatty alcohols, and mineral oils that are not easily soluble in water. Powdery cleansing composition, characterized in that the.
상기 코팅층의 바인더는 하이드록시프로필스타치포스페이트, 옥수수 전분, 쌀 전분, 카사바 전분, 감자 전분, 밀 전분, 수수 전분, 콩 전분, 펙틴, 아라비아검, 구아검, 로커스트콩검, 산탄검, 젤란검, 카라야검, 타라검, 타마린드검, 트라가칸스검, 천연검, 사일리움씨드검, 히드록실에틸셀룰로스, 히드록시프로필메틸셀룰로스로 구성된 군에서 적어도 하나 이상을 포함하는 것을 특징으로 하는 분말상 클렌징 조성물.
According to any one of claims 5 or 6,
The binder of the coating layer is hydroxypropyl starch phosphate, corn starch, rice starch, cassava starch, potato starch, wheat starch, sorghum starch, soybean starch, pectin, gum arabic, guar gum, locust bean gum, xanthan gum, gellan gum, A powdery cleansing composition comprising at least one from the group consisting of karaya gum, tara gum, tamarind gum, tragacanth gum, natural gum, psyllium seed gum, hydroxylethylcellulose, and hydroxypropylmethylcellulose .
색조 효과를 주는 색 첨가물질을 포함하는 것을 특징으로 하는 분말상 클렌징 조성물.
According to any one of claims 1 to 6,
A powdery cleansing composition comprising a color additive providing a color effect.
아미노산계 계면활성제를 75 내지 84w% 함유하고, 산화방지제는 15 내지 24w%를 포함하여 분말 형태로 제조되는 것을 특징으로 하는 분말상 클렌징 조성물.
According to claim 8,
A powdery cleansing composition comprising 75 to 84w% of an amino acid-based surfactant and 15 to 24w% of an antioxidant, characterized in that it is prepared in powder form.
아미노산계 계면활성제를 포함한 원료를 용매에 용해하여 과립입자를 형성하는 단계; 및,
산화방지제를 포함한 원료를 용매에 용해하여 상기 과립입자에 도포하여 코팅 조성물을 형성하는 단계;
상기 코팅 조성물을 50 내지 65℃ 온도에서 건조하는 단계;를 포함하여 제조되는 것을 특징으로 하는 분말상 클렌징 조성물의 제조방법.
In the method for producing a powdery cleansing composition,
Forming granular particles by dissolving a raw material including an amino acid-based surfactant in a solvent; and,
Forming a coating composition by dissolving a raw material including an antioxidant in a solvent and applying it to the granular particles;
Drying the coating composition at a temperature of 50 to 65 ° C. Method for producing a powdery cleansing composition, characterized in that produced including.
입자형태의 코어를 준비하는 단계; 및,
상기 코어의 표면을 코팅하여 코팅층을 형성하는 단계;를 포함하며,
상기 코어는 아미노산계 또는 이세치오네이트계 계면활성제를 포함하고,
상기 코팅층은 산화방지제를 포함하는 것을 특징으로 하는 분말상 클렌징 조성물의 제조방법.
In the method for producing a powdery cleansing composition,
preparing a particulate core; and,
Forming a coating layer by coating the surface of the core; includes,
The core includes an amino acid-based or isethionate-based surfactant,
The method for producing a powdery cleansing composition, characterized in that the coating layer contains an antioxidant.
상기 코어를 준비하는 단계는,
아미노산계 또는 이세치오네이트계 계면활성제가 포함된 코어 성분을 용해 및 분산한 후 유동층 공정에 의하여 입자형태의 코어를 형성하는 단계;를 포함하고,
상기 코팅층을 형성하는 단계는,
산화방지제가 포함된 제1 코팅성분을 용해 및 분산한 후 상기 코어의 표면에 유동층 공정에 의하여 코팅하여 제1 코팅층을 형성하는 단계;와
컨디셔닝제 또는 바인더가 포함된 제2 코팅성분을 용해 및 분산한 후 상기 제1코팅층의 표면에 유동층 공정에 의하여 코팅하여 제2코팅층을 형성하는 단계;를 포함하여 구성된 것을 특징으로 하는 분말상 클렌징 조성물의 제조방법.
According to claim 11,
Preparing the core is
Forming a particle-shaped core by a fluidized bed process after dissolving and dispersing a core component containing an amino acid-based or isethionate-based surfactant; including,
Forming the coating layer,
Forming a first coating layer by dissolving and dispersing a first coating component containing an antioxidant and then coating the surface of the core by a fluidized bed process; and
Forming a second coating layer by dissolving and dispersing a second coating component including a conditioning agent or a binder and then coating the surface of the first coating layer by a fluid bed process to form a powdery cleansing composition manufacturing method.
Priority Applications (1)
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KR102610628B1 (en) * | 2023-08-30 | 2023-12-07 | (주)프랜드 | Granular antioxidant foaming cleansing composition containing high concentration of vitamins and method for preparing the same |
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KR102610628B1 (en) * | 2023-08-30 | 2023-12-07 | (주)프랜드 | Granular antioxidant foaming cleansing composition containing high concentration of vitamins and method for preparing the same |
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