KR20140008906A - A phytoncide extraction method using chamaecyparis obtusa - Google Patents

A phytoncide extraction method using chamaecyparis obtusa Download PDF

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KR20140008906A
KR20140008906A KR1020120076557A KR20120076557A KR20140008906A KR 20140008906 A KR20140008906 A KR 20140008906A KR 1020120076557 A KR1020120076557 A KR 1020120076557A KR 20120076557 A KR20120076557 A KR 20120076557A KR 20140008906 A KR20140008906 A KR 20140008906A
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phytoncide
cypress
steam
heating
leaves
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KR101437221B1 (en
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오도윤
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오도윤
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/06—Production of fats or fatty oils from raw materials by pressing
    • C11B1/08—Production of fats or fatty oils from raw materials by pressing by hot pressing
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/02—Pretreatment
    • C11B1/04—Pretreatment of vegetable raw material
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/12—Production of fats or fatty oils from raw materials by melting out
    • C11B1/14—Production of fats or fatty oils from raw materials by melting out with hot water or aqueous solutions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention relates to a method for extracting phytoncide using cypress. The method minimizes the extraction time of phytoncide. That is, the method for extracting phytoncide using cypress softens cypress leaves by pressurizing and heating the cypress leaves for a predetermined time and supplying steam. Therefore, the method rapidly and easily produces phytoncide and extracts phytoncide with a small amounts of water by producing phytoncide by pressurizing and heating the cypress leaves and supplying steam. [Reference numerals] (110) Cold washing; (120) Sealed pressurizing and heating; (130) Heating and extracting phytoncide; (140) Separating and extracting the phytoncide

Description

편백나무를 이용한 피톤치드 추출방법{A phytoncide extraction method using Chamaecyparis obtusa}{Phytoncide extraction method using Chamaecyparis obtusa}

본 발명은 편백나무를 이용한 피톤치드 추출방법에 관한 것으로서, 더욱 상세하게는 편백나무를 이용한 피톤치드 추출방법에 있어서, 편백나무 잎을 일정시간 가압 가열하여 편백나무 잎의 조직을 연화시킨 후 증기를 공급하여서 피톤치드가 추출되게 함으로써 피톤치드의 추출 시간을 최소화할 수 있도록 함을 목적으로 한 것이다.
More particularly, the present invention relates to a method for extracting phytoncide from a cotton plant, and more particularly, to a method for extracting phytoncide from a cotton plant, So that the extraction time of the phytoncide can be minimized by allowing the phytoncide to be extracted.

일반적으로, 피톤치드(phytoncide)는 러시아어로 '식물의'라는 뜻의 'phyton'과 '죽이다'라는 뜻의 'cide'가 합해서 생긴 말로서, 식물이 병원균에 저항하기 위해 방출 또는 분비하는 물질을 말하는 것이다.In general, phytoncide is a mixture of 'phyton' (meaning 'plant') and 'cide' (meaning 'kill') in Russian and refers to a substance released or secreted by plants to resist pathogens .

이와 같은 피톤치드는 스트레스의 완화작용, 강력한 항균작용, 탈취작용, 피로의 진정작용, 알레르기 및 피부질환 개선작용 및 면역기능 증대 효과를 가지고 있는 것으로 알려져 있다.Such phytoncide has been known to have a stress relieving action, a strong antibacterial action, a deodorizing action, a soothing action of fatigue, an allergic and skin disease improving action, and an immune function increasing effect.

이처럼 다양한 기능을 지닌 피톤치드의 효과를 과학적으로 밝히기 위해 많은 연구가 진행되고 있으며, 특히 요즘에는 도시 공간에서도 손쉽게 삼림욕을 즐길 수 있도록 하기 위하여, 피톤치드 성분을 추출하여 만든 각종 방향제품이 판매되고 있는 실정이다.
Many researches have been conducted to scientifically clarify the effects of phytoncide having various functions. Recently, in order to enjoy the forest bath easily in the urban space, a variety of oriental products made by extracting phytoncide ingredients have been sold .

한편, 이상과 같은 피톤치드는 편백나무를 이용하여 피톤치드 제품을 얻은 사례가 있는데, 이는 알코올에 편백나무 잎을 갈아 넣고 이를 가열한 후, 여기에서 발생하는 증기를 포집하여 회수함으로써 피톤치드를 얻는 것이다. 이와 같이 얻은 피톤치드는 반드시 희석을 해서 사용을 하여야 하는데, 이때 제조과정에서 사용한 알코올로 인하여 정유가 물에 희석이 되지 않으므로, 인체에 유해한 화학물질인 유화제를 사용하여 희석을 시켜야 한다는 문제점이 있었다.
On the other hand, the above-mentioned phytoncide is a case of obtaining a phytoncide product using an untreated wood, which is obtained by heating an untreated wood leaf and then collecting the vapor generated therefrom and recovering the phytoncide. The phytoncide thus obtained must be diluted. In this case, since the essential oil is not diluted with water due to the alcohol used in the manufacturing process, dilution with an emulsifier which is a harmful chemical substance to the human body is required.

이에, 편백나무 잎을 이용하여 피톤치드를 추출함에 있어 알코올을 전혀 사용하지 않고, 대신 편백나무 잎과 물을 혼합한 후 이를 가열하여 증류수를 얻음으로써, 인체에 유해한 유화제를 사용하지 않은 피톤치드를 추출하였다.
Therefore, phytoncide which does not use harmful emulsifier is extracted by mixing distilled water with cotton seeds and heating it to obtain distilled water instead of using alcohol at all when extracting phytoncide using untreated leaves .

그러나, 상기한 바와 같은 종래의 피톤치드의 추출방법은 편백나무 잎 내부에 존재하는 피톤치드가 편백나무의 표피를 뚫고 배출되기가 용이하지 않아 많은 시간과 많은 양의 물이 사용되는 등 그 추출이 용이하지 않은 문제점이 있었다.
However, in the conventional method of extracting phytoncide as described above, since the phytoncide existing in the leaves of the perilla leaves is not easy to be discharged through the epidermis of the perilla trees, a lot of time and a large amount of water are used, .

이에, 본 발명은 상술한 바와 같이 종래 피톤치드 추출방법이 많은 시간과 많은 양의 물이 사용되는 등의 문제점을 해결할 수 있도록 한 것이다.
Accordingly, the present invention is capable of solving the problems of the conventional phytoncide extraction method, such as using a lot of time and a large amount of water, as described above.

즉, 본 발명은 편백나무를 이용한 피톤치드 추출방법에 있어서, 편백나무 잎을 일정시간 가압 가열하여 편백나무 잎의 조직을 연화시킨 후 증기를 공급하여 이루어지는 것이다.
That is, the present invention is a method for extracting phytoncide using a cottonwood, comprising heating softwood leaves for a certain period of time to soften the tissues of the softwood leaves, and then supplying the steam.

따라서, 본 발명은 편백나무 잎을 가압 가열한 후 증기를 공급하여 피톤치드를 생산함으로써 그 생산이 신속하고 용이하며 적은 양의 물을 이용하여 추출할 수 있는 것이다.
Accordingly, the present invention can produce the phytoncide by pressurizing and heating the unicorn tree leaf and supplying the steam, so that the production can be performed quickly, easily and with a small amount of water.

도 1 은 본 발명에 따른 공정도
도 2 는 본 발명의 따른 공정 중 가압 가열 과정의 상세도.
도 3 은 본 발명에 따른 제조 장치의 예시도.Figure 1 shows a process diagram according to the invention
2 is a detailed view of the pressurization heating process in the process according to the present invention.
3 is an illustration of an example of a manufacturing apparatus according to the present invention;

이하, 첨부된 도면에 의하여 상세히 설명하면 다음과 같다.Hereinafter, described in detail by the accompanying drawings as follows.

본 발명은 편백나무 잎을 이용한 피톤치드의 추출에 있어 신속하고 효율적으로 피톤치드를 추출할 수 있도록 한 것이다.The present invention enables rapid and efficient extraction of phytoncide in the extraction of phytoncide using a unicorn tree leaf.

즉, 본 발명은 편백나무를 이용한 피톤치드 추출방법에 있어서, 편백나무에서 취득한 편백나무 잎을 저온 세척하는 저온세척과정(110)과, 상기 저온세척과정(110)을 통하여 세척이 완료된 편백나무 잎이 연화되게 밀폐된 추출용기(10) 넣고 증기발생장치(40)에 의하여 증기를 공급하여 가압 가열하는 가압 가열과정(120)과, 상기 가압 가열과정(120)을 통하여 편백나무 잎을 연화시킨 상태에서 추출용기(10)로 증기를 주입하여 편백나무 잎에 함유된 피톤치드를 가열 용출시켜 피톤치드 증류수를 추출하는 피톤치드 가열 용출과정(130)과, 상기 피톤치드 가열 용출과정(130)을 통하여 용출된 피톤치드 증류수를 피톤치드오일(1)과 피톤치드수액(2)으로 분리하는 피톤치드 유분리추출과정(140)으로 이루어진 것이다.
That is, the present invention provides a method for extracting phytoncide using a cottonwood, comprising: a low-temperature washing process 110 for low-temperature washing the unbleached leaves obtained from the unbleached wood; A pressurizing and heating process 120 for supplying pressurized and heated steam into the brewed extraction container 10 and supplying the steam by the steam generator 40 and the pressurizing and heating process 120, A phytoncide heating elution process 130 in which steam is injected into the extraction vessel 10 to extract phytoncide distilled water by heating and dissolving the phytoncide contained in the senna tree leaves, and phytoncide distilled water eluted through the phytoncide heating elution process 130 And a phytoncide oil separation and extraction process 140 for separating the phytoncide oil (1) and the phytoncide sap (2).

여기서, 상기 저온세척과정(110)은 편백나무 잎에 함유되어 있은 피톤치드가 세척과정에 용출되지 않게 1~10℃의 세척수에 1~2시간 침수시킨 후 흐르는 1~10℃에 수세 세척하여 이루어지는 것이다.
The low-temperature washing step 110 is performed by immersing the phytoncide contained in the untwisted leaf for 1 to 2 hours in washing water at 1 to 10 ° C. so that the phytoncide does not dissolve in the washing process, and then rinsing at 1 to 10 ° C. .

그리고, 상기 가압 가열과정(120)은 밀폐된 추출용기(10)에 편백나무 잎을 넣고 1~2Kg/㎠의 압력으로 건증기를 증기발생장치(40)에서 20~30분간 공급하여 편백나무 잎의 표피가 균열손상되게 하는 건증기 가압가열과정(121)과, 상기 건증기 가압가열과정(121)을 통하여 표피가 균열된 편백나무 잎에 1~2Kg/㎠의 압력으로 습증기를 증기발생장치(40)에서 20~30분간 공급하여 균열된 표피를 통하여 수분이 침투되어 편백나무 잎의 내부 조직을 연화시키는 습증기 가압가열과정(122)으로 이루어지는 것이다.
The pressurizing and heating process 120 is carried out by inserting the unicorn tree leaves into the closed extraction container 10 and supplying the dry steam to the steam generator 40 for 20 to 30 minutes at a pressure of 1 to 2 Kg / A steam pressurization heating process 121 and a steam pressurization heating process 121 to cause the skin of the skin to be cracked and damaged by applying steam at a pressure of 1 to 2 kg / 40) for 20 to 30 minutes to permeate water through the cracked epidermis to soften the internal structure of the perilla leaf.

또한, 상기 피톤치드 가열 용출과정(130)은 추출용기(10)의 하부로 0.5Kg/㎠ 이하의 압력으로 증기를 증기발생장치(40)에서 공급하고 추출용기(10)의 상부 측에서 배출되는 증기를 냉각 응축기에서 응축하여 피톤치드증류수를 추출하는 것이다.
The phytoncide heating elution process 130 is a process in which steam is supplied from the steam generator 40 to the lower portion of the extraction vessel 10 at a pressure of 0.5 kg / cm 2 or less and the steam discharged from the upper side of the extraction vessel 10 Is condensed in a cooling condenser to extract the phytoncide distilled water.

또한, 상기 피톤치드 유분리추출과정(140)은 상기 피톤치드 가열 용출과정(130)을 통하여 배출된 피톤치드증류수를 유분리용기(30)에 공급하여 유분리용기(30)의 하부 측에서는 수분상태의 피톤치드수액(1)을 분리하고, 상부에서는 비중이 가벼워 물에 떠 있는 피톤치드오일(2)을 분리하는 것이다.
The phytoncide oil extraction and extraction process 140 may be performed by supplying the phytoncide distilled water discharged through the phytoncide heating elution process 130 to the oil separation container 30 so that the phytoncide water solution (1) is separated, and the phytoncide oil (2) floating in the water is separated from the upper portion at a light specific gravity.

이상과 같이 저온세척과정(110)과 가압 가열과정(120), 피톤치드 가열 용출과정(130) 및 피톤치드 유분리추출과정(140)으로 이루어진 본 발명에 따른 편백나무를 이용한 피톤치드 추출방법에 따라 피톤치드오일(1)과 피톤치드수액(2)을 추출하게 되면, 종래와 같은 증류수에 의한 추출과정보다 많은 양의 피톤치드오일(1)이 추출되는 것이다.
According to the method of extracting phytoncide from the cotton wool according to the present invention comprising the low-temperature washing process 110, the pressurization heating process 120, the phytoncide heating elution process 130 and the phytoncide oil separation and extraction process 140, (1) and the phytoncide sap (2) are extracted, a larger amount of phytoncide oil (1) is extracted than in the conventional extraction process using distilled water.

한편, 편백나무 잎을 저온세척과정(110)을 통하여 편백나무 잎을 세척하여 실시하게 되면, 편백나무 잎에 함유된 피톤치드오일이 응결된 상태를 유지하여 세척과정에 있어 편백나무 잎으로부터의 피톤치드 유실이 최소화되는 것이다.
On the other hand, when the untwisted leaves are washed through the low-temperature washing process 110, the phytoncide oil contained in the untwisted leaves is kept in a frozen state, Is minimized.

또한, 편백나무 잎을 건증기 가압가열과정(121)과 습증기 가압가열과정(122)으로 이루어진 가압 가열과정(120)을 실시하게 되면 편백나무 잎의 표피가 건증기에 의하여 균열되고 습증기가 편백나무 잎 내부로 침투되어서 편백나무 잎의 조직이 부피 팽창되며 피톤치드의 추출이 가장 용이한 상태로 연화되는 것이다.
In addition, when the pressurization heating process 120 comprising the steam pressurization heating process 121 and the wet steam pressurization heating process 122 is performed, the epidermis of the perilla leaf is cracked by the dry steam, It is infiltrated into the leaf, and the tissue of the unicorn tree leaves is expanded to volume, and the phytoncide is easily extracted and softened.

또한, 가압 가열과정(120)을 통하여 연화된 편백나무 잎에 피톤치드 가열 용출과정(130)을 통하여 추출용기(10)의 하부에 증기를 공급하게 되면, 상기 증기가 추출용기에 저장된 편백나무 잎을 통과하면서 피톤치드를 기화시켜서 추출용기의 상부로 배출되게 하며, 상기 추출용기(10)의 상부로 배출된 증기는 냉각응축기(20)에서 냉각되어서 피톤치드증류수가 추출되는 것이다.
When steam is supplied to the lower portion of the extraction vessel 10 through the phytoncide heating and eluting process 130 through the softening process 120 by the softening process, And the vapor discharged to the upper portion of the extraction vessel 10 is cooled in the cooling condenser 20 to extract the phytoncide distilled water.

또한, 상기 피톤치드 가열 용출과정(130)을 통하여 추출된 피톤치드증류수는 피톤치드 유분리추출과정(140)을 통하여 피톤치드수액과 피톤치드오일을 분리 저장되는 것이다.The phytoncide distilled water extracted through the phytoncide heating elution process 130 is separated and stored in the phytoncide oil and phytoncide oil through the phytonide oil extraction and extraction process 140.

한편, 상기한 바와 같은 과정을 통하여 피톤치드가 추출된 편백나무 잎은 건조과정과 분쇄과정을 통하여 미용비누 및 입욕제 등으로 사용할 수 있는 것이다.
On the other hand, the unicorn tree leaves extracted with phytoncide through the above-described process can be used as a cosmetic soap and a bathing agent through a drying process and a pulverizing process.

1 : 피톤치드오일 2 : 피톤치드수액
10 : 추출용기 20 : 냉각응축기
30 : 유분리용기 40 : 증기발생장치
110 : 저온세척과정
120 : 가압 가열과정
121 : 건증기 가압가열과정
122 : 습증기 가압가열과정
130 : 피톤치드 가열 용출과정
140 : 피톤치드 유분리추출과정1: Phytoncide oil 2: Phytoncide sap
10: Extraction vessel 20: Refrigerated condenser
30: Oil separation vessel 40: Steam generator
110: Low-temperature cleaning process
120: Pressure heating process
121: Steam pressure heating process
122: Wet steam heating process
130: Phytoncide heat elution process
140: Phytoncide oil extraction extraction process

Claims (2)

편백나무를 이용한 피톤치드 추출방법에 있어서;
편백나무에서 취득한 편백나무 잎을 저온 세척하는 저온세척과정과, 상기 저온세척과정을 통하여 세척이 완료된 편백나무 잎이 연화되게 밀폐된 추출용기 넣고 증기발생장치에 의하여 증기를 공급하여 가압 가열하는 가압 가열과정과, 상기 가압 가열과정을 통하여 편백나무 잎을 연화시킨 상태에서 추출용기로 증비발생장치에 의하여 증기를 주입하며 편백나무 잎에 함유된 피톤치드를 가열 용출하는 피톤치드 증류수를 추출하는 피톤치드 가열 용출과정과, 상기 피톤치드 가열 용출과정을 통하여 용출된 피톤치드 증류수를 피톤치드오일과 피톤치드수액으로 분리하는 피톤치드 유분리추출과정으로 이루어진 것을 특징으로 하는 편백나무를 이용한 피톤치드 추출방법.
A method for extracting phytoncide from a cottonwood;
Pressurized heating for low-temperature washing of cypress leaves obtained from cypress, and an extraction vessel sealed to soften the cypress leaves, which have been washed through the low-temperature washing, to supply steam by a steam generator and pressurized heating. And a phytoncide heating elution process for extracting phytoncide distilled water which injects steam by the enrichment generating device into the extraction container in the state of softening the cypress leaf through the pressurized heating process and heat eluting the phytoncide contained in the cypress leaf; And a phytoncide oil separation extraction process for separating phytoncide distilled water eluted through the phytoncide heating elution process into phytoncide oil and phytoncide sap.
제 1 항에 있어서;
상기 저온세척과정은 편백나무 잎에 함유되어 있은 피톤치드가 세척과정에 용출되지 않게 1~10℃의 세척수에 1~2시간 침수시킨 후 흐르는 1~10℃에 수세 세척하여 이루어지며,
상기 가압 가열과정은 밀폐된 추출용기에 편백나무 잎을 넣고 1~2Kg/㎠의 압력으로 건증기를 증기발생장치에 의하여 20~30분간 공급하여 편백나무 잎의 표피가 균열손상되게 하는 건증기 가압가열과정과, 상기 건증기 가압가열가정을 통하여 표피가 균열된 편백나무 잎에 1~2Kg/㎠의 압력으로 습증기를 증기발생장치에 의하여 20~30분간 공급하여 균열된 표피를 통하여 수분이 침투되어 편백나무 잎의 내부 조직을 연화시키는 습증기 가압가열과정으로 이루어진 것을 특징으로 하는 편백나무를 이용한 피톤치드 추출방법.
The method of claim 1, further comprising:
The low temperature washing process is performed by immersing the phytoncide contained in the cypress leaves in the washing water at 1 ~ 10 ℃ for 1 to 2 hours so as not to be eluted during the washing process, washing with water at 1 ~ 10 ℃ flowing,
The pressurized heating process puts the cypress leaves into a sealed extraction container and supplies dry steam at a pressure of 1 ~ 2Kg / ㎠ for 20-30 minutes by steam generating device to pressurize the dry steam so that the skin of the cypress leaves is cracked. Moisture penetrates through the cracked epidermis by supplying wet steam for 20-30 minutes by steam generator at a pressure of 1 ~ 2Kg / ㎠ to the cracked cypress leaf through the heating process and the dry steam pressurized heating. Phytoncide extracting method using a cypress, characterized in that the wet steam pressurized heating process to soften the internal structure of the cypress leaves.
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