KR200367389Y1 - Apparatus for multi-tube rotary evaporator with movable balls - Google Patents

Apparatus for multi-tube rotary evaporator with movable balls Download PDF

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Publication number
KR200367389Y1
KR200367389Y1 KR20-2004-0024030U KR20040024030U KR200367389Y1 KR 200367389 Y1 KR200367389 Y1 KR 200367389Y1 KR 20040024030 U KR20040024030 U KR 20040024030U KR 200367389 Y1 KR200367389 Y1 KR 200367389Y1
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South Korea
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rotary
raw material
outer cylinder
evaporation
rotary evaporator
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KR20-2004-0024030U
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Korean (ko)
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이종화
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이종화
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Priority to KR20-2004-0024030U priority Critical patent/KR200367389Y1/en
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Publication of KR200367389Y1 publication Critical patent/KR200367389Y1/en
Priority to PCT/KR2005/002771 priority patent/WO2006022507A1/en
Priority to CNA200580028036XA priority patent/CN101052447A/en
Priority to JP2007529689A priority patent/JP2008510613A/en

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/048—Purification of waste water by evaporation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
    • B01D1/222—In rotating vessels; vessels with movable parts
    • B01D1/228—In rotating vessels; vessels with movable parts horizontally placed cylindrical container or drum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/28—Evaporating with vapour compression
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/30—Accessories for evaporators ; Constructional details thereof
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/042—Prevention of deposits
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/10—Treatment of water, waste water, or sewage by heating by distillation or evaporation by direct contact with a particulate solid or with a fluid, as a heat transfer medium
    • C02F1/12—Spray evaporation

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)

Abstract

본 고안은 유동 세정구를 가진 다관(多管) 회전식 증발 농축 장치에 관한 것으로, 보다 자세하게는 다수개의 증발관 외표면에 돌출부, 내표면에는 핀을 형성하여 열전달 효율을 극대화하고, 전체 증발관에 그물망을 씌우고 그 속에 유동 세정구를 증발기와 같이 회전시켜 다량의 수분이 함유된 액체 원료의 순환 및 농축에 의해 증발관 외면에 부착된 고형물 및 스케일을 제거하여 증발관의 원료 증발 성능을 유지하도록 하는 증발 농축 장치에 관한 것이다.The present invention relates to a multi-pipe rotary evaporation concentrator with a flow scrubber, and more particularly, protrusions are formed on the outer surface of the plurality of evaporation tubes and fins are formed on the inner surface to maximize the heat transfer efficiency, Cover the net and rotate the flow cleaning device with the evaporator to remove the solids and scale attached to the outer surface of the evaporation tube by circulating and concentrating the liquid raw material containing a large amount of water to maintain the evaporation performance of the evaporation tube. An evaporation concentrator.

본 고안의 유동 세정구를 가진 다관(多管) 회전식 증발 농축 장치는 고정된 외부통; 상기 외부통으로부터 배출되는 수증기를 재압축시키는 증기재압축기; 상기 외부통 내부에서 회전하며 상기 증기재압축기에서 발생된 압축수증기에 의하여 가열되어 표면에 분사된 원료를 증발시키는 회전식 증발기; 상기 회전식 증발기를 경유하고 응축수 배출펌프를 통해 이송된 응축수의 열에 의하여 원료저장조로부터 여과기를 통과한 원료를 가열시키는 회전식 열교환기; 상기 회전식 열교환기를 통하여 가열되고, 펌프에 의하여 상기 외부통으로 압송되는 원료와 상기 외부통 하부에 모인 잔여물을 여과기로 여과한 원료를 함께 상기 회전식 증발기 표면으로 분사시키는 분사 파이프; 및 초기 수증기 공급과 운전중 손실된 열에너지 보충을 위한 히터로 이루어짐에 기술적 특징이 있다.The multi-pipe rotary evaporation concentrator having a flow cleaning device of the present invention comprises: a fixed outer cylinder; A steam recompressor for recompressing water vapor discharged from the outer cylinder; A rotary evaporator rotating inside the outer cylinder and evaporating the raw material sprayed on the surface by heating by compressed steam generated by the steam recompressor; A rotary heat exchanger for heating the raw material passing through the filter from the raw material storage tank by the heat of the condensate transferred through the rotary evaporator to the condensate discharge pump; An injection pipe heated through the rotary heat exchanger and injecting the raw material fed into the outer cylinder by a pump and the residue collected in the lower portion of the outer cylinder together with a filter to the surface of the rotary evaporator; And a heater for supplementing heat energy lost during initial steam supply and operation.

따라서, 본 고안의 유동 세정구를 가진 다관(多管) 회전식 증발 농축 장치는다각적인 요소에서 증발 농축 장치의 효율을 극대화시킴으로써 원료 처리에 필요한 에너지를 최소화시켜 경제적인 효과를 거둘 수 있으며, 화학 처리용 약품을 사용하지 않고도 스케일을 제거하여 안정적인 장치 운용을 할 수 있는 기술적인 효과도 거둘 수 있다.Therefore, the multi-pipe rotary evaporation concentrator with the flow cleaning device of the present invention can maximize the efficiency of the evaporation concentrator in various elements, thereby minimizing the energy required for raw material treatment, and achieving economical effects. There is also a technical effect of stable scale operation by removing the scale without the use of chemicals.

Description

유동 세정구를 가진 다관(多管) 회전식 증발 농축 장치{Apparatus for multi-tube rotary evaporator with movable balls}Multi-tube rotary evaporator with movable balls {Apparatus for multi-tube rotary evaporator with movable balls}

본 고안은 유동 세정구를 가진 다관(多管) 회전식 증발 농축 장치에 관한 것으로, 보다 자세하게는 다수개의 증발관 외표면에 돌출부, 내표면에 핀을 형성하여 열전달 효율을 극대화하고, 전체 증발관에 그물망을 씌우고 그 속에 유동 세정구를 증발기와 함께 회전시켜 다량의 수분이 함유된 액체 원료의 순환 및 농축에 의해 증발관 외면에 부착된 고형물 및 스케일을 제거하여 증발관의 원료 증발 성능을 유지하도록 하는 증발 농축 장치에 관한 것이다.The present invention relates to a multi-pipe rotary evaporation concentrator having a flow cleaning device, and more particularly, protrusions are formed on the outer surface of a plurality of evaporation tubes and fins are formed on the inner surface to maximize heat transfer efficiency, and Cover the net and rotate the flow cleaning device with the evaporator to remove the solids and scale attached to the outer surface of the evaporation tube by circulating and concentrating the liquid raw material containing a large amount of water to maintain the evaporation performance of the evaporation tube. An evaporation concentrator.

기존의 수평관 회전식 증발 농축 장치의 원리를 보면 회전하는 수평관 표면에 분사되는 원료는 수평관의 내측으로 통과하는 고온의 증기에 의해 증발된 후 증기 압축기를 통해 수평관 내측으로 재공급되거나, 진공펌프에 의해 감압상태에서 수평관 외측에서 증발된 후 외부로 배출된다.According to the principle of the conventional horizontal tube rotary evaporator, the raw material sprayed on the rotating horizontal tube surface is evaporated by the hot steam passing through the inner side of the horizontal tube and then re-supplied into the horizontal tube through the steam compressor, or vacuum It is evaporated outside the horizontal tube by the pump under reduced pressure and then discharged outside.

이때 원료 중에 용존되어 있거나 부유되어 있는 오염물질은 수평관 외측에 스케일을 형성하여 스팀과 원료간의 열전달을 방해하여 열교환 성능을 떨어트리기 때문에 시스템의 안정된 운전을 위하여 주기적인 세정이 필요하다. 세정방법으로는 화학약품에 의한 세정방법이 일반적이나 이와 같은 화학적 세정방법은 세정액에 의한 2차적 오염물질을 야기시킬 뿐만 아니라 완벽한 세정이 이루어지지 않아 효율이 떨어진다. 다른 방법으로는 주기적으로 수평관을 교체하거나 청소하는 방법이 있지만 유지비가 많이 드는 등의 문제가 발생한다.At this time, the pollutants dissolved or suspended in the raw materials form scales on the outside of the horizontal pipe to prevent heat transfer between the steam and the raw materials, thereby degrading heat exchange performance. Therefore, periodic cleaning is necessary for stable operation of the system. As a cleaning method, a chemical cleaning method is common, but such a chemical cleaning method not only causes secondary pollutants by the cleaning liquid, but also does not perform perfect cleaning, resulting in poor efficiency. Another method is to replace or clean the horizontal pipe periodically, but it causes a problem such as high maintenance costs.

또한, 기존의 수평관은 원통형의 단일 튜브로 형성되기 때문에 표면에 분사되는 원료와의 열전달 면적이 적어 에너지 소비가 클 뿐만 아니라 원료 증발효율이 낮은 문제점이 있다.In addition, since the conventional horizontal tube is formed of a single cylindrical tube, the heat transfer area with the raw material sprayed on the surface is small, so that the energy consumption is large and the raw material evaporation efficiency is low.

따라서, 본 고안은 상기와 같은 종래기술의 문제점을 해결하기 위한 것으로, 증발관의 열전달 면적을 최대한 크게하여 열전달 효율을 극대화하고, 증발관 표면에 형성되는 스케일을 제거하며, 원료 예열을 위한 열교환장치에서 원료를 적정온도로 예열시켜 유동 세정구를 가진 다관(多管) 회전식 증발 농축 장치의 효율을 극대화시켜 소모되는 에너지량을 최소화하는데 본 고안의 목적이 있다.Therefore, the present invention is to solve the problems of the prior art as described above, to maximize the heat transfer efficiency by maximizing the heat transfer area of the evaporator tube, to remove the scale formed on the surface of the evaporator tube, heat exchanger for raw material preheating The purpose of the present invention is to minimize the amount of energy consumed by maximizing the efficiency of a multi-pipe rotary evaporator with a flow scrubber by preheating the raw material to an appropriate temperature.

도 1은 본 고안에 따른 유동 세정구를 가진 다관 회전식 증발 농축 장치를 나타낸 개략적인 전체 구성도.1 is a schematic overall configuration diagram showing a multi-tube rotary evaporation concentrator having a flow cleaning device according to the present invention.

도 2는 본 고안에 따른 회전식 증발기의 입체도.Figure 2 is a three-dimensional view of the rotary evaporator according to the present invention.

도 3은 본 고안에 따른 증발관의 입체도.3 is a three-dimensional view of the evaporation tube according to the present invention.

도 4는 본 고안에 따른 회전식 증발기의 횡단면도.4 is a cross-sectional view of a rotary evaporator according to the present invention.

도 5는 도 4의 A-A' 단면도.5 is a cross-sectional view taken along line AA ′ of FIG. 4.

<도면의 주요부분에 대한 부호의 설명><Description of the symbols for the main parts of the drawings>

10 : 외부통 20 : 증기재압축기10: outer cylinder 20: steam recompressor

30 : 회전식 증발기 31 : 증발관30: rotary evaporator 31: evaporator tube

32 : 돌출부 33 : 핀(fin)32: protrusion 33: fin

34 : 그물망 35 : 유동 세정구34: mesh 35: flow washing hole

40 : 응축배출수펌프 41 : 원료순환펌프40: condensate discharge water pump 41: raw material circulation pump

42 : 원료압송펌프 50 : 원료저장조42: raw material pressure pump 50: raw material storage tank

60 : 회전식 열교환기 70,71 : 여과기60: rotary heat exchanger 70, 71: filter

80 : 히터 90 : 분사 파이프80: heater 90: injection pipe

본 고안의 상기 목적은 고정된 외부통, 이 외부통으로부터 배출되는 수증기를 재압축시키는 증기재압축기, 외부통 내부에서 회전하며 증기재압축기에서 발생된 압축수증기에 의하여 가열되어 표면에 분사된 원료를 증발시키는 회전식 증발기, 회전식 증발기를 경유하고 응축수 배출펌프를 통해 이송된 응축수의 열에 의하여 원료저장조로부터 여과기를 통과한 원료를 가열시키는 회전식 열교환기 및 열교환기를 통하여 100 ℃에 근접한 온도로 가열되고, 펌프에 의하여 외부통으로 압송되는 원료와 외부통 하부에 모인 잔여물을 여과기로 여과한 원료를 함께 상기 회전식 증발기 표면으로 분사시키는 분사 파이프 및 초기 수증기 공급과 운전중 손실된 열에너지 보충을 위한 히터로 이루어진 유동 세정구를 가진 다관(多管) 회전식 증발 농축 장치에 의해 달성된다.The object of the present invention is a fixed outer cylinder, a steam recompressor for recompressing water vapor discharged from the outer cylinder, the raw material sprayed on the surface heated by the compressed steam generated in the outer cylinder steam recompressor Heated to a temperature close to 100 ° C through a rotary heat exchanger and a heat exchanger for heating the raw material passed through the filter from the raw material storage tank by the heat of the condensate passed through the rotary evaporator, the rotary evaporator and the condensate discharge pump. A flow washing device consisting of a spray pipe for injecting the raw material that is conveyed to the outer cylinder and the residue collected in the lower part of the outer cylinder by a filter together to the surface of the rotary evaporator, and a heater for supplying initial steam supply and heat energy lost during operation. By multi-pipe rotary evaporative concentrator with It is achieved.

본 고안의 상기 목적과 기술적 구성 및 그에 따른 작용효과에 관한 자세한 사항은 본 고안의 바람직한 실시예를 도시하고 있는 도면을 참조한 이하 상세한 설명에 의해 보다 명확하게 이해될 것이다.Details of the above object and technical configuration of the present invention and the effects thereof according to the present invention will be more clearly understood by the following detailed description with reference to the drawings showing preferred embodiments of the present invention.

먼저, 도 1은 본 고안에 따른 유동 세정구를 가진 다관 회전식 증발 농축 장치를 나타낸 개략적인 전체 구성도에 관한 것이다. 도시된 바와 같이 초기에 히터(80)에서 발생된 수증기는 증기재압축기(20)를 통해 모터(100)에 의하여 외부통(10) 내부에서 서서히 회전하는 회전식 증발기(30)로 압송되며, 다수개의 증발관 내부를 따라 이동하며 증발관을 가열시키고, 분사 파이프(90)를 통해 분사되는 원료를 증발시킨 후, 응축배출수펌프(40)에 의하여 회전식 열교환기(60)로 압송되어 원료저장조(50)로부터 여과기(70)를 통과한 상온의 원료를 100 ℃ 부근까지 승온시킨 뒤 방출된다.First, Figure 1 relates to a schematic overall configuration showing a multi-tube rotary evaporation concentrator having a flow cleaning device according to the present invention. As shown in the drawing, the water vapor initially generated by the heater 80 is pumped to the rotary evaporator 30 which is gradually rotated inside the outer cylinder 10 by the motor 100 through the steam recompressor 20, After moving along the evaporation tube to heat the evaporation tube, and after evaporating the raw material injected through the injection pipe 90, it is pumped to the rotary heat exchanger (60) by the condensate discharge water pump (40) raw material storage tank (50) It is discharged after raising the raw material of normal temperature which passed the filter 70 from the temperature to near 100 degreeC.

응축배출수에 의하여 승온된 원료는 원료압송펌프(42)에 의하여 외부통(10) 내부에 위치한 분사파이프(10)로 압송된 후 회전식 증발기(30)의 표면에 고속으로 분사되어 증발된다. 이 때 외부통(10) 하부에 증발되지 않은 잔여물은 여과기(71)로 여과된 후 원료순환펌프(41)에 의하여 리사이클(recycle)된다. 한편, 상기 외부통(10) 내부에서 증발된 수증기는 히터(80)와 증기재압축기(20)에 의하여 회전식 증발기(30) 내부로 압송되어 재활용된다.The raw material heated up by the condensate discharge water is injected into the injection pipe 10 located inside the outer cylinder 10 by the raw material pressure pump 42 and then sprayed at high speed on the surface of the rotary evaporator 30 to be evaporated. At this time, the residue not evaporated in the lower portion of the outer cylinder 10 is filtered by the filter 71 and recycled by the raw material circulation pump 41. On the other hand, the water vapor evaporated in the outer cylinder 10 is recycled by being pumped into the rotary evaporator 30 by the heater 80 and the steam recompressor 20.

도 2의 증발관(31) 내측으로 고온 압축 수증기가 흐르면서 증발관 표면에 분사되는 원료는 수증기의 에너지를 전달받아 증발된다. 기존의 단순한 증발관은 열전달 면적이 작아 원료를 효과적으로 증발시키는 데 어려움이 있다. 따라서, 본 고안에서는 도 3과 같이 증발관의 외표면에 다수의 돌출부(32)를 형성하고, 내표면에는 복수의 핀(33)을 부착시켜 열전달 면적을 넓히고, 압축 수증기의 증발관내 체류 시간을 연장시켜 열전달 효율을 극대화한 특징이 있다.The raw material injected onto the surface of the evaporation tube while the hot compressed steam flows into the evaporation tube 31 of FIG. 2 is evaporated by the energy of the water vapor. The existing simple evaporation tube has a small heat transfer area, which makes it difficult to effectively evaporate raw materials. Therefore, in the present invention, as shown in FIG. 3, a plurality of protrusions 32 are formed on the outer surface of the evaporation tube, and a plurality of fins 33 are attached to the inner surface to increase the heat transfer area, and the residence time of the compressed steam in the evaporation tube is increased. It extends heat transfer efficiency.

도 3 내지 도 5의 회전식 증발기(30)의 내부를 살펴보면 다수개의 상기 증발관(31)이 가상의 원의 원주상에 위치하여 단일 증발관의 열전달 면적보다 더 큰 열전달 면적을 형성하며 회전축을 중심으로 회전한다. 증발관 표면에서 원료가 연속적으로 증발되면서 증발관 외표면에는 스케일이 형성되어, 압축 수증기와 원료간의 열교환을 방해한다. 따라서, 본 고안에서는 회전식 증발기(30)에 그물망(34)을 부착하고 그 내부에 유동 세정구(35)가 증발기가 회전함에 따라 움직이도록 하였다. 복수의 유동 세정구는 그물망(34) 내부에서 자유롭게 유동하면서 증발관 표면에 스케일이 생성되는 것을 방지하거나 이미 생성된 스케일을 제거하여 기존의 문제점을 개선한 특징이 있다.Looking at the interior of the rotary evaporator 30 of Figures 3 to 5 a plurality of the evaporation tube 31 is located on the circumference of the virtual circle to form a heat transfer area larger than the heat transfer area of a single evaporation tube centered on the axis of rotation Rotate As the raw material is continuously evaporated from the surface of the evaporator tube, a scale is formed on the outer surface of the evaporator tube, thereby preventing heat exchange between the compressed steam and the raw material. Therefore, in the present invention, the net 34 is attached to the rotary evaporator 30, and the flow washing hole 35 moves therein as the evaporator rotates. The plurality of flow scrubbers may freely flow in the mesh 34 to prevent generation of scale on the surface of the evaporator tube or to remove existing scales, thereby improving existing problems.

본 고안은 이상에서 살펴본 바와 같이 바람직한 실시 예를 들어 도시하고 설명하였으나, 상기한 실시 예에 한정되지 아니하며 본 고안의 정신을 벗어나지 않는 범위 내에서 당해 고안이 속하는 기술분야에서 통상의 지식을 가진 자에 의해 다양한 변경과 수정이 가능할 것이다.The present invention has been shown and described with reference to the preferred embodiment as described above, but is not limited to the above-described embodiment without departing from the spirit of the present invention to those of ordinary skill in the art Various changes and modifications will be possible.

따라서, 본 고안의 유동 세정구를 가진 다관(多管) 회전식 증발 농축 장치는 다각적인 요소에서 증발 농축 장치의 효율을 극대화시킴으로써 원료처리에 필요한 에너지를 최소화시켜 경제적인 효과를 거둘 수 있으며, 화학 처리용 약품을 사용하지 않고도 스케일을 제거하여 안정적인 장치 운용을 할 수 있는 기술적인 효과도 거둘 수 있다.Therefore, the multi-pipe rotary evaporation concentrator with the flow cleaning device of the present invention can maximize the efficiency of the evaporation concentrator in various factors, thereby minimizing the energy required for raw material treatment, and achieving economical effects. There is also a technical effect of stable scale operation by removing the scale without the use of chemicals.

Claims (6)

증발 농축 장치에 있어서,In the evaporation concentrator, 고정된 외부통;Fixed outer cylinder; 상기 외부통으로부터 배출되는 수증기를 재압축시키는 증기재압축기;A steam recompressor for recompressing water vapor discharged from the outer cylinder; 상기 외부통 내부에서 회전하며 상기 증기재압축기에서 발생된 압축수증기에 의하여 가열되어 표면에 분사된 원료를 증발시키는 회전식 증발기;A rotary evaporator rotating inside the outer cylinder and evaporating the raw material sprayed on the surface by heating by compressed steam generated by the steam recompressor; 상기 회전식 증발기를 경유하고 응축수 배출펌프를 통해 이송된 응축수의 열에 의하여 원료저장조로부터 여과기를 통과한 원료를 가열시키는 회전식 열교환기;A rotary heat exchanger for heating the raw material passing through the filter from the raw material storage tank by the heat of the condensate transferred through the rotary evaporator to the condensate discharge pump; 상기 회전식 열교환기를 통하여 가열되고, 펌프에 의하여 상기 외부통으로 압송되는 원료와 상기 외부통 하부에 모인 잔여물을 여과기로 여과한 원료를 함께 상기 회전식 증발기 표면으로 분사시키는 분사 파이프; 및An injection pipe heated through the rotary heat exchanger and injecting the raw material fed into the outer cylinder by a pump and the residue collected in the lower portion of the outer cylinder together with a filter to the surface of the rotary evaporator; And 초기 수증기 공급과 운전중 손실된 열에너지 보충을 위한 히터Heater for initial steam supply and replenishment of heat energy lost during operation 를 포함하는 것을 특징으로 하는 유동 세정구를 가진 다관 회전식 증발 농축 장치.A multi-tube rotary evaporation concentrator having a flow scrubber comprising a. 제 1 항에 있어서,The method of claim 1, 상기 회전식 증발기는 열전달 효과를 극대화하기 위하여 직선 증발관이 복수로 설치된 것을 특징으로 하는 유동 세정구를 가진 다관 회전식 증발 농축 장치.The rotary evaporator is a multi-tube rotary evaporator with a flow scrubber, characterized in that a plurality of linear evaporator is installed in order to maximize the heat transfer effect. 제 2 항에 있어서,The method of claim 2, 상기 직선 증발관의 외표면에는 열전달을 위하여 다수개의 돌출부를 형성함을 특징으로 하는 유동 세정구를 가진 다관 회전식 증발 농축 장치.A multi-tube rotary evaporation concentrator with a flow scrubber, characterized in that the outer surface of the linear evaporation tube to form a plurality of protrusions for heat transfer. 제 2 항에 있어서,The method of claim 2, 상기 직선 증발관의 내표면에는 열전달을 위하여 다수개의 핀을 형성함을 특징으로 하는 유동 세정구를 가진 다관 회전식 증발 농축 장치.A multi-tube rotary evaporation concentrator having a flow scrubber, characterized in that a plurality of fins are formed on the inner surface of the linear evaporation tube for heat transfer. 제 1 항 또는 제 2 항에 있어서,The method according to claim 1 or 2, 상기 복수의 직선 증발관으로 구성된 상기 회전식 증발기는 그물망에 둘러싸여 있음을 특징으로 하는 유동 세정구를 가진 다관 회전식 증발 농축 장치.And said rotary evaporator composed of said plurality of straight evaporator tubes is surrounded by a mesh. 제 1 항 또는 제 2 항에 있어서,The method according to claim 1 or 2, 상기 그물망 내에는 상기 회전식 증발기가 회전함에 따라 함께 유동하며 상기 직선 증발관의 표면에 스케일 방지나 이미 형성된 스케일 제거를 목적으로 하는세정구들을 포함하는 것을 특징으로 하는 유동 세정구를 가진 다관 회전식 증발 농축 장치.In the mesh, the rotary evaporator flows together as the rotary evaporator rotates and includes: tubing rotary evaporation concentrators with flow scrubbers for the purpose of preventing scale or removing already formed scales on the surface of the linear evaporator. Device.
KR20-2004-0024030U 2004-08-23 2004-08-23 Apparatus for multi-tube rotary evaporator with movable balls KR200367389Y1 (en)

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