KR20030062262A - 적층형 압전 세라믹 소자의 제조방법 - Google Patents
적층형 압전 세라믹 소자의 제조방법 Download PDFInfo
- Publication number
- KR20030062262A KR20030062262A KR10-2003-0002048A KR20030002048A KR20030062262A KR 20030062262 A KR20030062262 A KR 20030062262A KR 20030002048 A KR20030002048 A KR 20030002048A KR 20030062262 A KR20030062262 A KR 20030062262A
- Authority
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- South Korea
- Prior art keywords
- piezoelectric
- oxygen concentration
- piezoelectric ceramic
- ceramic
- vol
- Prior art date
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- 239000000919 ceramic Substances 0.000 title claims abstract description 73
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 51
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 51
- 239000001301 oxygen Substances 0.000 claims abstract description 51
- 238000010304 firing Methods 0.000 claims abstract description 28
- 150000001875 compounds Chemical class 0.000 claims abstract description 9
- 239000004020 conductor Substances 0.000 claims abstract description 7
- 238000001354 calcination Methods 0.000 claims abstract description 5
- 229910010293 ceramic material Inorganic materials 0.000 claims abstract description 5
- 238000010438 heat treatment Methods 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 abstract description 44
- 239000011148 porous material Substances 0.000 description 14
- 229910052451 lead zirconate titanate Inorganic materials 0.000 description 6
- 239000000203 mixture Substances 0.000 description 4
- 230000010287 polarization Effects 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 230000000630 rising effect Effects 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 239000011230 binding agent Substances 0.000 description 3
- HFGPZNIAWCZYJU-UHFFFAOYSA-N lead zirconate titanate Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Ti+4].[Zr+4].[Pb+2] HFGPZNIAWCZYJU-UHFFFAOYSA-N 0.000 description 3
- 238000012423 maintenance Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000007650 screen-printing Methods 0.000 description 3
- 230000007847 structural defect Effects 0.000 description 3
- 229910010413 TiO 2 Inorganic materials 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000007606 doctor blade method Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000005684 electric field Effects 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000004014 plasticizer Substances 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 101100513612 Microdochium nivale MnCO gene Proteins 0.000 description 1
- 229910006404 SnO 2 Inorganic materials 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- NKZSPGSOXYXWQA-UHFFFAOYSA-N dioxido(oxo)titanium;lead(2+) Chemical compound [Pb+2].[O-][Ti]([O-])=O NKZSPGSOXYXWQA-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/01—Manufacture or treatment
- H10N30/05—Manufacture of multilayered piezoelectric or electrostrictive devices, or parts thereof, e.g. by stacking piezoelectric bodies and electrodes
- H10N30/053—Manufacture of multilayered piezoelectric or electrostrictive devices, or parts thereof, e.g. by stacking piezoelectric bodies and electrodes by integrally sintering piezoelectric or electrostrictive bodies and electrodes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/48—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
- C04B35/49—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates containing also titanium oxides or titanates
-
- H—ELECTRICITY
- H04—ELECTRIC COMMUNICATION TECHNIQUE
- H04R—LOUDSPEAKERS, MICROPHONES, GRAMOPHONE PICK-UPS OR LIKE ACOUSTIC ELECTROMECHANICAL TRANSDUCERS; DEAF-AID SETS; PUBLIC ADDRESS SYSTEMS
- H04R17/00—Piezoelectric transducers; Electrostrictive transducers
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/01—Manufacture or treatment
- H10N30/09—Forming piezoelectric or electrostrictive materials
- H10N30/093—Forming inorganic materials
- H10N30/097—Forming inorganic materials by sintering
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/40—Piezoelectric or electrostrictive devices with electrical input and electrical output, e.g. functioning as transformers
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/80—Constructional details
- H10N30/85—Piezoelectric or electrostrictive active materials
- H10N30/853—Ceramic compositions
- H10N30/8548—Lead-based oxides
- H10N30/8554—Lead-zirconium titanate [PZT] based
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/42—Piezoelectric device making
Landscapes
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Chemical & Material Sciences (AREA)
- Signal Processing (AREA)
- Physics & Mathematics (AREA)
- Acoustics & Sound (AREA)
- Ceramic Engineering (AREA)
- Composite Materials (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
Description
소성 분위기 조건 No. | 산소 농도 조건(단위 : 체적%) | ||
승온 과정600℃∼1100℃ | 유지 과정1100℃ | 강온 과정1100℃∼600℃ | |
J1* | 85 | 10 | 10 |
J2 | 90 | 10 | 10 |
J3 | 95 | 10 | 10 |
J4* | 95 | 2 | 10 |
J5 | 95 | 5 | 10 |
J6 | 95 | 15 | 10 |
J7* | 95 | 21 | 10 |
J8* | 95 | 10 | 2 |
J9 | 95 | 10 | 5 |
J10 | 95 | 10 | 15 |
J11* | 95 | 10 | 21 |
J12* | 21 | 21 | 21 |
J13* | 90 | 90 | 90 |
시료 번호 | 소성 분위기조건 No. | 특성 | |||
최대 승압비(dB) | 최대 효율(%) | 포어 점유율(%) | 항절 강도(MPa) | ||
1* | J1* | 31.5 | 94.5 | 1.7 | 115 |
2 | J2 | 31.5 | 95.4 | 0.7 | 125 |
3 | J3 | 31.1 | 95.6 | 0.5 | 130 |
4* | J4* | 28.3 | 88 | 0.6 | 128 |
5 | J5 | 31.8 | 95.6 | 0.7 | 129 |
6 | J6 | 32.0 | 95.1 | 0.6 | 125 |
7* | J7* | 29.4 | 89.5 | 0.5 | 132 |
8* | J8* | 29.5 | 89.7 | 0.8 | 123 |
9 | J9 | 31.3 | 95.2 | 0.6 | 129 |
10 | J10 | 31.4 | 95.4 | 0.6 | 130 |
11* | J11* | 29.8 | 89.8 | 0.6 | 128 |
12* | J12* | 30.8 | 94.5 | 3.2 | 96.8 |
13* | J13* | 28.0 | 88.7 | 0.7 | 126 |
시료 번호 | 소성 분위기조건 No. | 특성 | |||
|d31|(10-12C/N) | ρ(1012Ωㆍ㎝) | 포어 점유율(%) | 항절 강도(MPa) | ||
14* | J1* | 212 | 6.1 | 1.6 | 105 |
15 | J2 | 208 | 6.5 | 0.5 | 118 |
16 | J3 | 210 | 6.0 | 0.6 | 115 |
17* | J4* | 197 | 1.0 | 0.7 | 118 |
18 | J5 | 211 | 6.1 | 0.6 | 120 |
19 | J6 | 210 | 5.7 | 0.6 | 119 |
20* | J7* | 201 | 0.98 | 0.5 | 119 |
21* | J8* | 199 | 2.5 | 0.7 | 120 |
22 | J9 | 208 | 6.2 | 0.7 | 121 |
23 | J10 | 207 | 5.9 | 0.6 | 118 |
24* | J11* | 196 | 1.5 | 0.7 | 119 |
25* | J12* | 206 | 5.9 | 2.6 | 94.5 |
26* | J13* | 190 | 0.56 | 0.7 | 121 |
Claims (1)
- Pb원소의 화합물을 함유하고 있는 압전 세라믹 재료의 세라믹 그린시트상에, Ag를 주성분으로 하는 도체를 포함하는 도전성 페이스트를 도포하고, 상기 세라믹 그린시트를 겹쳐 쌓아서 적층체로 하는 공정과; 상기 적층체를 소성시의 승온 과정에서의 산소 농도가 90체적% 이상이고, 또한 유지 과정과 강온(降溫) 과정에서의 산소 농도가 5체적%∼15체적%가 되는 분위기 중에서 소성하는 공정;을 구비하는 것을 특징으로 하는 적층형 압전 세라믹 소자의 제조방법.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JPJP-P-2002-00007674 | 2002-01-16 | ||
JP2002007674A JP3982267B2 (ja) | 2002-01-16 | 2002-01-16 | 積層型圧電セラミック素子の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR20030062262A true KR20030062262A (ko) | 2003-07-23 |
KR100492813B1 KR100492813B1 (ko) | 2005-06-02 |
Family
ID=27646132
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR10-2003-0002048A KR100492813B1 (ko) | 2002-01-16 | 2003-01-13 | 적층형 압전 세라믹 소자의 제조방법 |
Country Status (4)
Country | Link |
---|---|
US (1) | US6758927B2 (ko) |
JP (1) | JP3982267B2 (ko) |
KR (1) | KR100492813B1 (ko) |
CN (1) | CN100365842C (ko) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6749706B2 (en) * | 2001-12-26 | 2004-06-15 | Murata Manufacturing Co., Ltd. | Method of manufacturing monolithic piezoelectric ceramic device |
JP2005174974A (ja) * | 2003-12-08 | 2005-06-30 | Matsushita Electric Ind Co Ltd | 積層圧電体部品の製造方法 |
DE112011103776B4 (de) * | 2010-11-15 | 2019-07-04 | Tdk Electronics Ag | Piezoelektrisches Bauelement und Verfahren zu seinem Betrieb |
US8899115B2 (en) * | 2011-04-20 | 2014-12-02 | United Technologies Corporation | Method and system for locating a laser vibrometer during non-contact scanning |
CN103992529A (zh) * | 2014-04-29 | 2014-08-20 | 天长永泰密封材料有限公司 | 一种丁晴橡胶密封胶 |
DE102015202725A1 (de) * | 2015-02-16 | 2016-08-18 | Robert Bosch Gmbh | Kraftstoffinjektor und Verfahren zur Herstellung eines Piezoelements für einen Kraftstoffinjektor |
JP7491713B2 (ja) * | 2020-03-27 | 2024-05-28 | Tdk株式会社 | 圧電素子、圧電アクチュエータ、および圧電トランス |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6022835B2 (ja) * | 1978-08-17 | 1985-06-04 | 株式会社村田製作所 | 圧電性磁器の製造方法 |
JPS6356971A (ja) * | 1986-08-28 | 1988-03-11 | Nippon Soken Inc | 積層形圧電体 |
JP2652425B2 (ja) | 1988-09-10 | 1997-09-10 | 松下電器産業株式会社 | 圧電セラミツクスの製造方法 |
JPH04357164A (ja) | 1991-05-31 | 1992-12-10 | Kyocera Corp | 圧電磁器の製造方法 |
JPH06140279A (ja) * | 1992-09-11 | 1994-05-20 | Murata Mfg Co Ltd | 積層セラミック電子部品の焼成方法 |
JP3577175B2 (ja) | 1996-09-20 | 2004-10-13 | Tdk株式会社 | 圧電磁器組成物及びその製造方法 |
JPH11163433A (ja) * | 1997-11-27 | 1999-06-18 | Hitachi Metals Ltd | 積層型圧電セラミックス振動子および製造方法 |
JPH11171645A (ja) * | 1997-12-09 | 1999-06-29 | Hitachi Metals Ltd | 電子部品 |
JPH11274595A (ja) * | 1998-03-23 | 1999-10-08 | Hitachi Metals Ltd | 圧電セラミックス、積層型圧電セラミックス振動子およびその製造方法 |
AU2002219827A1 (en) * | 2000-11-16 | 2002-05-27 | The Penn State Research Foundation | Cofired multilayered piezoelectric ceramic materials with base metal electrodes |
US6749706B2 (en) * | 2001-12-26 | 2004-06-15 | Murata Manufacturing Co., Ltd. | Method of manufacturing monolithic piezoelectric ceramic device |
-
2002
- 2002-01-16 JP JP2002007674A patent/JP3982267B2/ja not_active Expired - Lifetime
-
2003
- 2003-01-13 KR KR10-2003-0002048A patent/KR100492813B1/ko active IP Right Grant
- 2003-01-16 CN CNB031027520A patent/CN100365842C/zh not_active Expired - Lifetime
- 2003-01-16 US US10/346,603 patent/US6758927B2/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
JP3982267B2 (ja) | 2007-09-26 |
US6758927B2 (en) | 2004-07-06 |
KR100492813B1 (ko) | 2005-06-02 |
CN1433092A (zh) | 2003-07-30 |
US20030163908A1 (en) | 2003-09-04 |
JP2003209304A (ja) | 2003-07-25 |
CN100365842C (zh) | 2008-01-30 |
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