KR20010018325A - Synthetic Fibre with the Properties of Antibiotics, Deorderising and Far-infrared Ray Emmision - Google Patents

Synthetic Fibre with the Properties of Antibiotics, Deorderising and Far-infrared Ray Emmision Download PDF

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Publication number
KR20010018325A
KR20010018325A KR1019990034233A KR19990034233A KR20010018325A KR 20010018325 A KR20010018325 A KR 20010018325A KR 1019990034233 A KR1019990034233 A KR 1019990034233A KR 19990034233 A KR19990034233 A KR 19990034233A KR 20010018325 A KR20010018325 A KR 20010018325A
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fiber
charcoal
far
antibacterial
antibiotics
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KR1019990034233A
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Korean (ko)
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KR100311832B1 (en
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최장호
김윤성
이건직
전용진
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김용배
너와나의 주식회사
최장호
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    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D01F1/103—Agents inhibiting growth of microorganisms
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00—Formation of filaments, threads, or the like
    • D01D5/08—Melt spinning methods
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Artificial Filaments (AREA)

Abstract

PURPOSE: Provided is a synthetic fiber obtained by mixing charcoal, inorganic antibiotics containing silver and fiber material, therefore having an antibacterial, deodorizing and far infrared radiating effect. CONSTITUTION: This synthetic fiber having antibacterial, deodorizing and far infrared radiating effect is prepared by adding 1 to 15wt.% of charcoal having a specific surface area of 300 to 1,000m¬2/g and inorganic antibiotics having a silver content of 2 to 10% based on the charcoal powder to fiber material such as polyester fiber, acrylic fiber, nylon fiber and polypropylene fiber.

Description

숯을 함유한 항균성, 소취성 및 원적외선 방사율이 우수한 합성섬유{Synthetic Fibre with the Properties of Antibiotics, Deorderising and Far-infrared Ray Emmision}Synthetic Fiber with the Properties of Antibiotics, Deorderising and Far-infrared Ray Emmision

각종 섬유제품에 숯을 첨가함으로서 숯이 갖는 항균, 소취 및 원적외선 효과 등에 의해 인체에 유해한 주위 환경으로부터 인체를 보호하고 활성화시켜 건강한 삶을 영위할 수 있게 하도록 함을 목적으로 한다.By adding charcoal to various textile products, it aims to enable healthy life by protecting and activating the human body from the surrounding environment harmful to human body by the antibacterial, deodorant and far infrared effect of charcoal.

본 발명은 다공성 구조에 의한 세균 및 악취 등의 흡착기능과 원적외선 방사기능 등 숯의 우수한 기능을 활용하여 인체에 유익한 기능성 섬유제품을 만들고자 하는 것이다.The present invention is to create a functional fiber product beneficial to the human body by utilizing the excellent function of charcoal, such as adsorption function of bacteria and odor and porous infrared radiation function by the porous structure.

항균, 탈취 및 원적외선과 관련된 섬유를 제조한 기존의 것들로는 국내에도 출원번호 1988-016225, 1996-018297, 1998-007433, 1998-012949, 1998-012950, 1997-012986, 1997-017804, 1995-031856 등이 있으나, 이들은 원적외선을 방출하는 광물이나 합성세라믹들을 주원료로 하는 것들로 본 발명에서 사용하는 숯에 비하여 다공성이나 흡착능력이 낮아서 항균 및 탈취 등의 기능이 현저히 낮다.Existing ones that produce fibers related to antibacterial, deodorant and far infrared rays are also applied to domestic applications No. 1988-016225, 1996-018297, 1998-007433, 1998-012949, 1998-012950, 1997-012986, 1997-017804, 1995- 031856 and the like, these are the main raw materials that emit minerals or synthetic ceramics that emit far-infrared rays, the porosity and adsorption capacity is low compared to the char used in the present invention, the antibacterial and deodorizing function is significantly lower.

따라서 본 발명에서는 동일한 목적으로 기존에 사용되는 광물이나 합성세라믹에 비해 뛰어난 다공성과 흡착능력에 따라, 항균 및 탈취능력 등이 훨씬 우수한 숯을 섬유 및 섬유제품에 적용하여 항균, 탈취 및 원적외선 특성이 우수한 섬유 및 섬유제품을 만들고자 한다.Therefore, according to the present invention, charcoal having much superior antibacterial and deodorizing ability is applied to fibers and textile products according to excellent porosity and adsorption capacity compared to minerals or synthetic ceramics used for the same purpose. To make textiles and textile products.

본 발명의 상세한 내용은 다음과 같다.Details of the present invention are as follows.

먼저 숯을 분쇄하여 섬유에 넣어 용융방사할 수 있는 크기로 제조한다. 숯은 비표면적이 300㎡/g - 1000㎡/g범위의 것을 사용하여야 소취, 흡착 및 항균 특성이 우수하다.First, charcoal is pulverized and prepared into a size that can be melt-spun into fibers. Charcoal has a specific surface area of 300㎡ / g-1000㎡ / g, so it has excellent deodorization, adsorption and antibacterial properties.

그리고 숯 자체가 갖는 항균, 소취 등의 특성을 더욱 향상시키기 위해서는 숯과 함께 은(Ag) 성분이 2% - 10% 함유된 무기계 항균제를 숯 분말대비 무게비로 20% - 50%를 혼합하여 사용하면 보다 우수한 항균 및 소취기능을 얻을 수 있다.In order to further improve the antibacterial and deodorant properties of the charcoal itself, if the inorganic antimicrobial agent containing 2% to 10% of silver (Ag) is mixed with the charcoal in a weight ratio of 20% to 50% Better antibacterial and deodorant function can be obtained.

은(Ag)이 함유된 무기계 항균제의 담체로는 인산칼슘, 인산지르코늄, 제올라이트, 이산화티탄, 견운모, 맥반석, 황산바륨, 유리 등을 사용할 수 있다.As a carrier of the inorganic antimicrobial agent containing silver (Ag), calcium phosphate, zirconium phosphate, zeolite, titanium dioxide, mica, elvan, barium sulfate, glass and the like can be used.

본 발명에서는 숯에 대해 무게비로 20 - 50%의 비율로 무기계 항균제가 혼합된 상기 분말과 폴리에스터, 나일론, 아크릴, 폴리프로필렌 등의 수지성분으로 이루어진 섬유를 제조할 때 최종섬유에서 상기 분말의 함유량이 무게로 최소 1%에서 15%까지의 범위가 되도록 본 발명의 숯함유 섬유를 제조한다.In the present invention, the content of the powder in the final fiber when producing a fiber made of a resin component such as polyester, nylon, acrylic, polypropylene and the powder mixed with an inorganic antibacterial agent in a ratio of 20 to 50% by weight relative to charcoal At this weight, the charcoal-containing fibers of the present invention are produced so that they range from at least 1% to 15%.

더 자세히 설명하면 상기 분말의 입자크기 면에서는 섬유의 굵기가 3데니어 이하일 경우에는 평균입자크기 1㎛이하와 최대입자크기 4㎛이하면 섬유의 제조가 가능하나 섬유제조시의 작업성 및 섬유제조 후의 후가공 및 제직 등의 공정에서의 장치 마모문제 등을 고려할 때 평균입자크기 0.7㎛ 이하 및 최대입자크기 2㎛ 이하로 입자를 제조하는 것이 바람직하다. 섬유 굵기 7데니어의 경우 평균 입자크기 1.5㎛ 이하 최대 입자크기 7㎛ 이하, 섬유굵기 15데니어의 경우 평균 입자크기 2㎛ 이하 최대 입자크기 10㎛ 이하의 입자가 바람직하다.More specifically, in terms of the particle size of the powder, when the thickness of the fiber is 3 denier or less, the fiber can be manufactured when the average particle size is 1 μm or less and the maximum particle size is 4 μm or less. In consideration of device wear problems in processes such as post-processing and weaving, it is preferable to produce particles with an average particle size of 0.7 μm or less and a maximum particle size of 2 μm or less. In the case of 7 denier, the average particle size is 1.5 mu m or less, and in the case of fiber denier 15 denier, the average particle size is 2 mu m or less.

또한, 섬유에 상기 분말을 혼합하고자 할 때는 섬유용 폴리머의 중합과정에서부터 상기 분말을 첨가, 중합하여 혼합 원료칩을 만들고 이를 다시 용융방사하여 섬유를 제조하는 방법과 미리 중합된 수지를 상기 분말과 혼합하여 분말의 함량이 놓은 마스터배치를 만들고 이를 다시 수지와 혼합하여 용융방사함으로서 원하는 함량의 상기 분말을 함유하는 섬유를 만드는 방법이 있다. 이밖에도 아크릴 섬유 등의 경우에는 폴리머와 분말을 슬러리 상태로 만들어 혼합방사하는 방법으로도 섬유를 제조할 수 있다.In addition, when the powder is to be mixed with the fiber, the powder is added and polymerized from the polymerization process of the fiber polymer to produce a mixed raw material chip and melt-spun again to manufacture the fiber, and the prepolymerized resin is mixed with the powder. There is a method of making a fiber containing the powder of the desired content by making a master batch with a powder content and mixing it with a resin to melt spinning. In addition, in the case of acrylic fibers or the like, the fibers may be produced by mixing and spinning a polymer and powder in a slurry state.

본 발명의 실시 예는 다음 표1과 같다.An embodiment of the present invention is shown in Table 1 below.

섬유 종류별로 본 발명의 분말을 적용해 본 결과 우수한 원적외선 방사율, 항균성 및 소취성을 얻을 수 있었다.As a result of applying the powder of the present invention for each fiber type, excellent far-infrared emissivity, antimicrobial activity and deodorization were obtained.

본 실시예 및 비교예에서 사용한 분말은 무게로 숯 80%와 인산칼슘계 무기항균제 20%의 혼합분말이며, 무기항균제중의 은(Ag) 함량은 4%이었다.The powders used in this example and the comparative example were a mixed powder of charcoal 80% and calcium phosphate inorganic antibacterial agent by weight of 20%, and the silver (Ag) content in the inorganic antimicrobial agent was 4%.

항균성은 대장균을 사용하여 KS규격에 의해 시험하였으며 소취 성 평가는 KICM-FIR-1004 방법에 의해 암모니아(NH3) 가스에 대해 측정하였다. 원적외선 방사율은 FT-IR을 이용하여 5㎛ - 20㎛ 영역에서의 평균 방사율을 측정하였다.Antimicrobial activity was tested by KS standard using Escherichia coli and deodorant evaluation was measured for ammonia (NH 3 ) gas by KICM-FIR-1004 method. Far-infrared emissivity was measured using FT-IR to measure the average emissivity in the region of 5 μm-20 μm.

[ 표1 ]Table 1

..

Claims (2)

항균성, 소취성 및 원적외선 방사성을 갖는 합성섬유를 제조함에 있어 숯 분말을 폴리에스테르 섬유, 아크릴 섬유, 나일론 섬유 및 폴리프로필렌 섬유 등에 무게로 1% - 15%를 첨가하는 방법Method of adding 1% to 15% by weight of charcoal powder to polyester fiber, acrylic fiber, nylon fiber and polypropylene fiber in preparing synthetic fiber having antimicrobial, deodorant and far infrared radiation 제 1항에 있어서 숯 분말의 항균성 및 소취성 등을 보완하기 위해 은(Ag) 성분이 2% - 10% 함유된 무기계 항균제를 숯 분말 대비 무게비로 20% - 50%를 첨가하는 합성섬유 제조 방법The method of preparing synthetic fibers according to claim 1, wherein an inorganic antimicrobial agent containing 2% to 10% of silver (Ag) is added in a weight ratio of charcoal powder to supplement the antibacterial and deodorizing properties of the charcoal powder.
KR1019990034233A 1999-08-18 1999-08-18 Synthetic Fibre with the Properties of Antibiotics, Deorderising and Far-infrared Ray Emmision KR100311832B1 (en)

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KR20020060654A (en) * 2002-06-14 2002-07-18 김제하 Health functional artificial fiber in which silver powder is synthesized, and a manufacturing method thereof.
KR20030062600A (en) * 2002-01-17 2003-07-28 최명부 Production of Cotton Preventing Ticks and Viruses
KR20030064020A (en) * 2002-01-25 2003-07-31 김상년 manufacture method of charcoal powder be contain composition cotton
KR100399108B1 (en) * 2001-03-12 2003-09-22 제이티엘주식회사 Method of manufacturing a activated synthetic cottonwool
KR20040014105A (en) * 2002-08-09 2004-02-14 최명부 The Manufacture of PP silk using charcoal and silver
KR100776533B1 (en) * 2006-04-25 2007-12-12 조인술 Manufacturing method of polyester yarn
KR100839467B1 (en) * 2007-06-08 2008-06-19 권정순 A polypropylene complex resin and thread manufactured the same
CN103668538A (en) * 2012-09-13 2014-03-26 东华大学 Uvioresistant type biomass polyester fiber and preparation method thereof
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KR20030062600A (en) * 2002-01-17 2003-07-28 최명부 Production of Cotton Preventing Ticks and Viruses
KR20030064020A (en) * 2002-01-25 2003-07-31 김상년 manufacture method of charcoal powder be contain composition cotton
KR20020060654A (en) * 2002-06-14 2002-07-18 김제하 Health functional artificial fiber in which silver powder is synthesized, and a manufacturing method thereof.
KR20040014105A (en) * 2002-08-09 2004-02-14 최명부 The Manufacture of PP silk using charcoal and silver
KR100776533B1 (en) * 2006-04-25 2007-12-12 조인술 Manufacturing method of polyester yarn
KR100839467B1 (en) * 2007-06-08 2008-06-19 권정순 A polypropylene complex resin and thread manufactured the same
CN103668538A (en) * 2012-09-13 2014-03-26 东华大学 Uvioresistant type biomass polyester fiber and preparation method thereof
CN103668538B (en) * 2012-09-13 2016-01-20 东华大学 A kind of ultraviolet-resisting biomass polyester fiber and preparation method thereof
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