KR102627686B1 - Liquid crystal cream cosmetic composition that looks like snow particles with a gloss improving effect and manufacturing method thereof - Google Patents
Liquid crystal cream cosmetic composition that looks like snow particles with a gloss improving effect and manufacturing method thereof Download PDFInfo
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- KR102627686B1 KR102627686B1 KR1020230107410A KR20230107410A KR102627686B1 KR 102627686 B1 KR102627686 B1 KR 102627686B1 KR 1020230107410 A KR1020230107410 A KR 1020230107410A KR 20230107410 A KR20230107410 A KR 20230107410A KR 102627686 B1 KR102627686 B1 KR 102627686B1
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- 239000000203 mixture Substances 0.000 title claims abstract description 148
- 239000002537 cosmetic Substances 0.000 title claims abstract description 73
- 239000004973 liquid crystal related substance Substances 0.000 title claims abstract description 36
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 14
- 239000006071 cream Substances 0.000 title abstract description 25
- 230000000694 effects Effects 0.000 title abstract description 22
- 239000002245 particle Substances 0.000 title description 6
- -1 starch Chemical class 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 8
- 239000004006 olive oil Substances 0.000 claims description 22
- 235000008390 olive oil Nutrition 0.000 claims description 22
- 229930006000 Sucrose Natural products 0.000 claims description 20
- 239000005720 sucrose Substances 0.000 claims description 20
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 14
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 10
- 229930182478 glucoside Natural products 0.000 claims description 8
- OWPUOLBODXJOKH-UHFFFAOYSA-N 2,3-dihydroxypropyl prop-2-enoate Chemical compound OCC(O)COC(=O)C=C OWPUOLBODXJOKH-UHFFFAOYSA-N 0.000 claims description 7
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 7
- 239000000539 dimer Substances 0.000 claims description 7
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 6
- NKJOXAZJBOMXID-UHFFFAOYSA-N 1,1'-Oxybisoctane Chemical compound CCCCCCCCOCCCCCCCC NKJOXAZJBOMXID-UHFFFAOYSA-N 0.000 claims description 6
- 229940015975 1,2-hexanediol Drugs 0.000 claims description 6
- 229940043375 1,5-pentanediol Drugs 0.000 claims description 6
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 6
- 229920002126 Acrylic acid copolymer Polymers 0.000 claims description 6
- 229920002125 Sokalan® Polymers 0.000 claims description 6
- 229960001631 carbomer Drugs 0.000 claims description 6
- 229940008099 dimethicone Drugs 0.000 claims description 6
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 6
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 6
- 125000005456 glyceride group Chemical group 0.000 claims description 6
- 235000011187 glycerol Nutrition 0.000 claims description 6
- 229940075529 glyceryl stearate Drugs 0.000 claims description 6
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 claims description 6
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 6
- WCVRQHFDJLLWFE-UHFFFAOYSA-N pentane-1,2-diol Chemical compound CCCC(O)CO WCVRQHFDJLLWFE-UHFFFAOYSA-N 0.000 claims description 6
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 6
- 239000008213 purified water Substances 0.000 claims description 6
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 claims description 6
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 claims description 6
- 229960000281 trometamol Drugs 0.000 claims description 6
- 235000013311 vegetables Nutrition 0.000 claims description 6
- FENRSEGZMITUEF-ATTCVCFYSA-E [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].OP(=O)([O-])O[C@@H]1[C@@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H]1OP(=O)([O-])[O-] Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].OP(=O)([O-])O[C@@H]1[C@@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H]1OP(=O)([O-])[O-] FENRSEGZMITUEF-ATTCVCFYSA-E 0.000 claims description 5
- 229940081733 cetearyl alcohol Drugs 0.000 claims description 5
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 5
- 229940083982 sodium phytate Drugs 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims 1
- 229920002472 Starch Polymers 0.000 abstract description 3
- 150000004676 glycans Chemical class 0.000 abstract description 3
- 229920001282 polysaccharide Polymers 0.000 abstract description 3
- 239000005017 polysaccharide Substances 0.000 abstract description 3
- 239000008107 starch Substances 0.000 abstract description 3
- 235000019698 starch Nutrition 0.000 abstract description 3
- 230000000052 comparative effect Effects 0.000 description 16
- HLZKNKRTKFSKGZ-UHFFFAOYSA-N tetradecan-1-ol Chemical compound CCCCCCCCCCCCCCO HLZKNKRTKFSKGZ-UHFFFAOYSA-N 0.000 description 12
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 description 10
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 10
- 238000009472 formulation Methods 0.000 description 8
- 239000004615 ingredient Substances 0.000 description 8
- 229940043348 myristyl alcohol Drugs 0.000 description 6
- 229960000541 cetyl alcohol Drugs 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- 229960000735 docosanol Drugs 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 5
- 229920002554 vinyl polymer Polymers 0.000 description 5
- 239000003995 emulsifying agent Substances 0.000 description 4
- 239000004480 active ingredient Substances 0.000 description 3
- 230000003750 conditioning effect Effects 0.000 description 3
- 229920005862 polyol Polymers 0.000 description 3
- 150000003077 polyols Chemical class 0.000 description 3
- 239000003755 preservative agent Substances 0.000 description 3
- 230000002335 preservative effect Effects 0.000 description 3
- 230000008591 skin barrier function Effects 0.000 description 3
- 239000002562 thickening agent Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000012790 confirmation Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 230000003472 neutralizing effect Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000019198 oils Nutrition 0.000 description 2
- 125000000185 sucrose group Chemical group 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- WTXXSZUATXIAJO-OWBHPGMISA-N (Z)-14-methylpentadec-2-enoic acid Chemical compound CC(CCCCCCCCCC\C=C/C(=O)O)C WTXXSZUATXIAJO-OWBHPGMISA-N 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 230000010287 polarization Effects 0.000 description 1
- 230000037307 sensitive skin Effects 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 description 1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0295—Liquid crystals
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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Abstract
본 발명은 윤기 개선 효과가 우수한 액정(Liquid Crystal) 크림 화장료 조성물 및 이의 제조 방법에 관한 것으로서, 더욱 상세하게는, 일반적인 액정 화장료 조성물과 달리 스타치(starch)와 같은 다당류 사용 없이도 눈과 같은 외관을 띠며 윤기 개선 효과가 매우 우수하여, 이를 효과적으로 피부 외용 제품으로 사용될 수 있다.The present invention relates to a liquid crystal cream cosmetic composition with excellent gloss-improving effect and a method for manufacturing the same. More specifically, the present invention relates to a liquid crystal cream cosmetic composition that has an excellent gloss-improving effect and, more specifically, to a liquid crystal cream cosmetic composition that provides a snow-like appearance without the use of polysaccharides such as starch, unlike general liquid crystal cosmetic compositions. It has a very excellent shine-improving effect, so it can be effectively used as an external skin product.
Description
본 발명은 윤기 개선 효과가 우수한 액정(Liquid Crystal) 크림 화장료 조성물 및 이의 제조 방법에 관한 것으로서, 더욱 상세하게는, 일반적인 액정 화장료 조성물과 달리 스타치(starch)와 같은 다당류 사용 없이도 눈과 같은 외관을 띠며 윤기 개선 효과가 매우 우수한 액정 크림 화장료 조성물 및 이의 제조 방법에 관한 것이다.The present invention relates to a liquid crystal cream cosmetic composition with excellent gloss-improving effect and a method for manufacturing the same. More specifically, the present invention relates to a liquid crystal cream cosmetic composition that has an excellent gloss-improving effect and, more specifically, to a liquid crystal cream cosmetic composition that provides a snow-like appearance without the use of polysaccharides such as starch, unlike general liquid crystal cosmetic compositions. It relates to a liquid crystal cream cosmetic composition that has excellent gloss improving effect and a method of manufacturing the same.
유화제를 사용하여 유상부와 수상부를 인위적으로 혼합시키는 일반적인 유화 크림과 달리 액정(Liquid Crystal) 크림은 지방족 알코올을 배합하여 피부 라멜라(lamellar) 구조와 유사한 액정(Liquid Crystal) 구조를 형성하여 피부 장벽 개선 및 피부 보습에 매우 효과가 있는 크림으로 알려져 있다.Unlike typical emulsifying creams that artificially mix the oil phase and water phase using an emulsifier, Liquid Crystal cream combines aliphatic alcohol to form a liquid crystal structure similar to the lamellar structure of the skin, improving the skin barrier and improving the skin barrier. It is known as a cream that is very effective in moisturizing the skin.
일반적으로 액정(Liquid Crystal)이라 함은 고체와 액체의 중간적 상태로서, 이는 대개 친수성 부분과 친유성 부분을 동시에 갖고 있는 유기 분자들이 친수성 부분은 친수성 부분끼리 친유성 부분은 친유성 부분끼리 일정하게 배열하여 여러 층을 이루고 있는 라멜라(lamellar) 구조가 생성되는 것을 말한다.In general, liquid crystal is an intermediate state between a solid and a liquid. It is usually an organic molecule that has both hydrophilic and lipophilic parts. The hydrophilic part is connected to the hydrophilic part, and the lipophilic part is connected to the lipophilic part. This refers to the creation of a lamellar structure that is arranged to form multiple layers.
액정은 점도 및 유동성 면에서는 액체처럼 행동하나, 빛의 산란과 반사 같은 물성에 있어서는 고체의 물성을 나타내는 등 독특한 성질을 나타내므로, 화장품, 의약품, 식품 등 여러 분야에서 그 응용범위가 넓다.Liquid crystals behave like liquids in terms of viscosity and fluidity, but exhibit unique properties such as solid properties in terms of light scattering and reflection, so their application range is wide in various fields such as cosmetics, medicine, and food.
다만, 현재 시중에 나와있는 액정 크림의 경우 라멜라 구조에 기인한 피부 윤기 효과가 더 높게 나타나는 충분한 데이터를 제시하지 못하고 있는 실정이다. 이에 본 발명에서는 수크로오스폴리스테아레이트 및 올리브오일불검화물을 유효 성분으로 포함하며, 기존의 액정 크림과 다르게 눈 입자의 외관을 갖고, 우수한 윤기 개선 효과를 나타내는 화장료 조성물을 개시한다.However, liquid crystal creams currently on the market do not provide sufficient data showing a higher skin gloss effect due to the lamellar structure. Accordingly, the present invention discloses a cosmetic composition that contains sucrose polystearate and unsaponifiable olive oil as active ingredients, has the appearance of eye particles unlike existing liquid crystal creams, and exhibits an excellent gloss improvement effect.
이러한 배경 하에, 본 발명자들은 차별화된 제형을 가진 액정 크림 화장료 조성물에 대하여 연구 노력한 끝에, 수크로오스폴리스테아레이트 및 올리브오일불검화물을 유효 성분으로 포함하는 액정 크림 화장료 조성물로서, 본 발명에 따른 화장료 조성물은 눈 입자와 같은 외관을 가지고 윤기 개선 효과와 부드러운 사용감을 나타내는 것을 확인하였다.Against this background, the present inventors have researched a liquid crystal cream cosmetic composition with a differentiated formulation and have developed a liquid crystal cream cosmetic composition containing sucrose polystearate and unsaponifiable olive oil as active ingredients. The cosmetic composition according to the present invention is It was confirmed that it has an appearance similar to snow particles and has a gloss-improving effect and a soft feel.
이에, 본 발명의 목적은, 수크로오스폴리스테아레이트 및 올리브오일불검화물을 포함하는 라멜라 액정 화장료 조성물을 제공하는 것이다.Accordingly, the purpose of the present invention is to provide a lamellar liquid crystal cosmetic composition containing sucrose polystearate and unsaponifiable olive oil.
본 발명의 다른 목적은, 제1혼합물, 제2혼합물 및 제3혼합물의 제조 단계로서, 상기 제2혼합물은 수크로오스폴리스테아레이트 및 올리브오일불검화물을 포함하고;Another object of the present invention is to prepare a first mixture, a second mixture, and a third mixture, wherein the second mixture includes sucrose polystearate and unsaponifiable olive oil;
상기 제1혼합물 및 상기 제2혼합물을 혼합한 후 상기 제3혼합물을 혼합하여 혼합 조성물을 만드는 혼합 단계; 및A mixing step of mixing the first mixture and the second mixture and then mixing the third mixture to form a mixed composition; and
상기 혼합 조성물을 냉각하는 냉각 단계;를 포함하는 라멜라 액정 화장료 조성물의 제조 방법을 제공하는 것이다.A method for producing a lamellar liquid crystal cosmetic composition comprising a cooling step of cooling the mixed composition is provided.
본 발명은 수크로오스폴리스테아레이트 및 올리브오일불검화물을 유효 성분으로 포함하는 액정 크림 화장료 조성물에 관한 것으로서, 본 발명에 따른 화장료 조성물은 눈 입자와 같은 외관을 가지고 윤기 개선 효과와 부드러운 사용감을 나타낸다.The present invention relates to a liquid crystal cream cosmetic composition containing sucrose polystearate and unsaponifiable olive oil as active ingredients. The cosmetic composition according to the present invention has an appearance similar to snow particles and exhibits a gloss improvement effect and a smooth feeling of use.
이하, 본 발명을 더욱 자세히 설명하고자 한다.Hereinafter, the present invention will be described in more detail.
본 발명의 일 양태는, 수크로오스폴리스테아레이트 및 올리브오일불검화물을 포함하는 라멜라 액정 화장료 조성물에 관한 것이다.One aspect of the present invention relates to a lamellar liquid crystal cosmetic composition containing sucrose polystearate and unsaponifiable olive oil.
본 발명의 일 구현예에 따라, 라멜라 구조를 형성하는 액정 화장료 조성물을 제조하여 사용할 경우, 이러한 조성물은 피부 보습 및 피부 장벽 기능에 중요한 역할을 할 수 있다. 이것은 인지질로 구성된 일종의 판막 구조의 유화 형태로서, 오일층과 수상층이 차례로 블록을 쌓아놓은 형태인 라멜라 구조가 갖는 구조적인 특징으로 인한 것일 수 있다.According to one embodiment of the present invention, when a liquid crystal cosmetic composition forming a lamellar structure is manufactured and used, this composition can play an important role in skin moisturization and skin barrier function. This is a kind of emulsified form of a valve structure composed of phospholipids, and may be due to the structural characteristics of the lamellar structure, in which the oil layer and the water layer are sequentially stacked in blocks.
본 발명에 있어서, 상기 수크로오스폴리스테아레이트의 함량은 상기 화장료 조성물 총 중량에 대하여 0.2 내지 10 중량%, 0.2 내지 8 중량%, 0.2 내지 6 중량%, 0.2 내지 4 중량%, 0.4 내지 10 중량%, 0.4 내지 8 중량%, 0.4 내지 6 중량%, 0.4 내지 4 중량%, 0.6 내지 10 중량%, 0.6 내지 8 중량%, 0.6 내지 6 중량%, 0.6 내지 4 중량%, 0.8 내지 10 중량%, 0.8 내지 8 중량%, 0.8 내지 6 중량%, 0.8 내지 4 중량%, 1 내지 10 중량%, 1 내지 8 중량%, 1 내지 6 중량%, 예를 들어, 1 내지 4 중량% 포함된 것일 수 있으나, 이에 한정되는 것은 아니다.In the present invention, the content of the sucrose polystearate is 0.2 to 10% by weight, 0.2 to 8% by weight, 0.2 to 6% by weight, 0.2 to 4% by weight, 0.4 to 10% by weight, based on the total weight of the cosmetic composition. 0.4 to 8% by weight, 0.4 to 6% by weight, 0.4 to 4% by weight, 0.6 to 10% by weight, 0.6 to 8% by weight, 0.6 to 6% by weight, 0.6 to 4% by weight, 0.8 to 10% by weight, 0.8 to It may contain 8% by weight, 0.8 to 6% by weight, 0.8 to 4% by weight, 1 to 10% by weight, 1 to 8% by weight, 1 to 6% by weight, for example, 1 to 4% by weight. It is not limited.
본 발명에 있어서, 상기 올리브오일불검화물의 함량은 상기 화장료 조성물 총 중량에 대하여 0.02 내지 6 중량%, 0.02 내지 5 중량%, 0.02 내지 4 중량%, 0.02 내지 3 중량%, 0.02 내지 2 중량%, 0.04 내지 6 중량%, 0.04 내지 5 중량%, 0.04 내지 4 중량%, 0.04 내지 3 중량%, 0.04 내지 2 중량%, 0.06 내지 6 중량%, 0.06 내지 5 중량%, 0.06 내지 4 중량%, 0.06 내지 3 중량%, 0.06 내지 2 중량%, 0.08 내지 6 중량%, 0.08 내지 5 중량%, 0.08 내지 4 중량%, 0.08 내지 3 중량%, 0.08 내지 2 중량%, 0.1 내지 6 중량%, 0.1 내지 5 중량%, 0.1 내지 4 중량%, 0.1 내지 3 중량%, 예를 들어, 0.1 내지 2 중량% 포함된 것일 수 있으나, 이에 한정되는 것은 아니다.In the present invention, the content of the unsaponifiable olive oil is 0.02 to 6% by weight, 0.02 to 5% by weight, 0.02 to 4% by weight, 0.02 to 3% by weight, 0.02 to 2% by weight, based on the total weight of the cosmetic composition. 0.04 to 6% by weight, 0.04 to 5% by weight, 0.04 to 4% by weight, 0.04 to 3% by weight, 0.04 to 2% by weight, 0.06 to 6% by weight, 0.06 to 5% by weight, 0.06 to 4% by weight, 0.06 to 3% by weight, 0.06 to 2% by weight, 0.08 to 6% by weight, 0.08 to 5% by weight, 0.08 to 4% by weight, 0.08 to 3% by weight, 0.08 to 2% by weight, 0.1 to 6% by weight, 0.1 to 5% by weight %, 0.1 to 4% by weight, 0.1 to 3% by weight, for example, 0.1 to 2% by weight, but is not limited thereto.
본 발명의 일 구현예에서, 화장료 조성물 총 중량에 대하여 수크로오스폴리스테아레이트(sucrose polystearate)의 함량이 1 내지 4 중량% 및 올리브오일불검화물(olive oil unsaponifiables)의 함량이 0.1 내지 2 중량% 포함된 화장료 조성물의 경우, 액정(Liquid Crystal) 구조가 잘 형성될 뿐만 아니라, 윤기 개선 효과가 우수한 것을 확인하였다.In one embodiment of the present invention, the cosmetic composition contains 1 to 4% by weight of sucrose polystearate and 0.1 to 2% by weight of olive oil unsaponifiables based on the total weight of the cosmetic composition. In the case of the cosmetic composition, it was confirmed that not only the liquid crystal structure was well formed, but also the gloss improvement effect was excellent.
본 발명의 일 구현예에서, 화장료 조성물 총 중량에 대하여 베헤닐알코올(behenyl alcohol)을 1 내지 4 중량% 포함하는 경우보다, 수크로오스폴리스테아레이트(sucrose polystearate)를 1 내지 4 중량% 및 올리브오일불검화물(olive oil unsaponifiables)을 0.1 내지 2 중량% 포함하는 경우에 제형 표면에 눈과 같은 특징적인 외관이 형성될 뿐만 아니라, 피부 윤기 개선 효과가 더 우수한 것을 확인하였다.In one embodiment of the present invention, 1 to 4% by weight of sucrose polystearate and olive oil are used compared to the case where the cosmetic composition contains 1 to 4% by weight of behenyl alcohol based on the total weight of the cosmetic composition. It was confirmed that when 0.1 to 2% by weight of olive oil unsaponifiables was included, not only a characteristic snow-like appearance was formed on the surface of the formulation, but also the effect of improving skin gloss was more excellent.
본 발명의 일 구현예에서, 화장료 조성물 총 중량에 대하여 미리스틸알코올(myristyl alcohol)을 1 내지 4 중량% 포함하는 경우보다, 수크로오스폴리스테아레이트(sucrose polystearate)를 1 내지 4 중량% 및 올리브오일불검화물(olive oil unsaponifiables)을 0.1 내지 2 중량% 포함하는 경우에 제형 표면에 눈과 같은 특징적인 외관이 형성될 뿐만 아니라, 피부 윤기 개선 효과가 더 우수한 것을 확인하였다.In one embodiment of the present invention, 1 to 4% by weight of sucrose polystearate and olive oil are used compared to the case where the cosmetic composition contains 1 to 4% by weight of myristyl alcohol based on the total weight of the cosmetic composition. It was confirmed that when 0.1 to 2% by weight of olive oil unsaponifiables was included, not only a characteristic snow-like appearance was formed on the surface of the formulation, but also the effect of improving skin gloss was more excellent.
본 발명의 일 구현예에서, 화장료 조성물 총 중량에 대하여 세틸알코올(cetyl alcohol)을 1 내지 4 중량% 포함하는 경우보다, 수크로오스폴리스테아레이트(sucrose polystearate)를 1 내지 4 중량% 및 올리브오일불검화물(olive oil unsaponifiables)을 0.1 내지 2 중량% 포함하는 경우에 제형 표면에 눈과 같은 특징적인 외관이 형성될 뿐만 아니라, 피부 윤기 개선 효과가 더 우수한 것을 확인하였다.In one embodiment of the present invention, 1 to 4% by weight of sucrose polystearate and unsaponifiable olive oil are used compared to the case where the cosmetic composition contains 1 to 4% by weight of cetyl alcohol based on the total weight of the cosmetic composition. It was confirmed that when 0.1 to 2% by weight of (olive oil unsaponifiables) was included, not only a characteristic snow-like appearance was formed on the surface of the formulation, but also the effect of improving skin gloss was more excellent.
본 발명에 있어서, 상기 화장료 조성물은 폴리올, 점증제, 스킨컨디셔닝제, 방부제, 정제수, 유화제 및 중화제로 이루어진 그룹에서 선택되는 1종 이상을 추가로 포함하는 것일 수 있으나, 이에 한정되는 것은 아니다.In the present invention, the cosmetic composition may further include one or more selected from the group consisting of polyol, thickener, skin conditioning agent, preservative, purified water, emulsifier and neutralizer, but is not limited thereto.
본 명세서 상의 용어 “폴리올(polyol)”은 여러 수산기(-OH)를 포함하는 화합물을 의미하며, 화장료 조성물의 성분으로 사용되는 경우 피부에 막을 형성하여 수분이 증발하는 것을 막아주어 보습에 중요한 역할을 할 수 있으며, 본 발명에서 상기 폴리올(polyol)은 글리세린(glycerin) 및 부틸렌글라이콜(butylene glycol)로 이루어진 그룹에서 선택되는 1종 이상인 것일 수 있으나, 이에 한정되는 것은 아니다.The term “polyol” in this specification refers to a compound containing several hydroxyl groups (-OH), and when used as an ingredient in a cosmetic composition, it plays an important role in moisturizing by forming a film on the skin and preventing moisture from evaporating. In the present invention, the polyol may be one or more selected from the group consisting of glycerin and butylene glycol, but is not limited thereto.
본 명세서 상의 용어 “점증제”는 화장료 조성물의 점도 및 안정성 유지를 위해 사용되는 성분을 의미하는 것일 수 있으며, 본 발명에서 상기 점증제는 글리세릴아크릴레이트/아크릴릭애씨드코폴리머(glyceryl acrylate/acrylic acid copolymer) 및 카보머(carbomer)로 이루어진 그룹에서 선택되는 1종 이상인 것일 수 있으나, 이에 한정되는 것은 아니다.The term “thickener” in this specification may refer to an ingredient used to maintain the viscosity and stability of a cosmetic composition, and in the present invention, the thickener is glyceryl acrylate/acrylic acid copolymer (glyceryl acrylate/acrylic acid). It may be one or more types selected from the group consisting of copolymer and carbomer, but is not limited thereto.
본 명세서 상의 용어 “스킨컨디셔닝제”는 화장료 조성물의 성분으로 사용되는 경우 피부를 부드럽고 유연하게 유지하는 역할을 할 수 있으며, 본 발명에서 상기 스킨컨디셔닝제는 카프릴릭/카프릭트라이글리세라이드(caprylic/capric triglyceride), 아세틸레이티드하이드로제네이티드식물성글리세라이드(acetylated hydrogenated vegetable glyceride), 피토스테릴이소스테아릴다이머디리놀리에이트(phytosteryl isostearyl dimer dilinoleate), 다이카프릴릴에터(dicaprylyl ether) 및 비닐다이메티콘(vinyldimethicone)으로 이루어진 그룹에서 선택되는 1종 이상인 것일 수 있으나, 이에 한정되는 것은 아니다.The term “skin conditioning agent” in this specification can play a role in keeping the skin soft and flexible when used as an ingredient in a cosmetic composition. In the present invention, the skin conditioning agent is caprylic/capric triglyceride (caprylic triglyceride). /capric triglyceride), acetylated hydrogenated vegetable glyceride, phytosteryl isostearyl dimer dilinoleate, dicaprylyl ether and vinyl It may be one or more types selected from the group consisting of dimethicone (vinyldimethicone), but is not limited thereto.
본 명세서 상의 용어 “방부제”는 화장료 조성물의 변질을 막고 순도를 유지하기 위해 사용되는 성분을 의미하는 것일 수 있으며, 본 발명에서 상기 방부제는 펜틸렌글라이콜(pentylene glycol) 및 1,2-헥산다이올(1,2-hexanediol)로 이루어진 그룹에서 선택되는 1종 이상인 것일 수 있으나, 이에 한정되는 것은 아니다.The term “preservative” in this specification may refer to an ingredient used to prevent deterioration of a cosmetic composition and maintain its purity. In the present invention, the preservative is pentylene glycol and 1,2-hexanedihydrogen. It may be one or more types selected from the group consisting of all (1,2-hexanediol), but is not limited thereto.
본 명세서 상의 용어 “유화제”는 화장료 조성물의 친유성을 가진 성분과 친수성을 가진 성분이 서로 잘 섞이도록 도와주는 역할을 하는 성분을 의미하는 것일 수 있으며, 본 발명에서 상기 유화제는 수크로오스폴리스테아레이트(sucrose polystearate), 올리브오일불검화물(olive oil unsaponifiables), 세테아릴알코올(cetearyl alcohol), C14-22알코올(C14-22 alcohol), 글리세릴스테아레이트(glyceryl stearate) 및 C12-20알킬글루코사이드(C12-20 alkyl glucoside)로 이루어진 그룹에서 선택되는 1종 이상인 것일 수 있으나, 이에 한정되는 것은 아니다.The term “emulsifier” in this specification may refer to a component that helps the lipophilic component and the hydrophilic component of the cosmetic composition to mix well with each other. In the present invention, the emulsifier is sucrose polystearate ( sucrose polystearate, olive oil unsaponifiables, cetearyl alcohol, C14-22 alcohol, glyceryl stearate and C12-20 alkyl glucoside (C12 It may be one or more types selected from the group consisting of -20 alkyl glucoside), but is not limited thereto.
본 명세서 상의 용어 “중화제”는 화장료 조성물의 pH(산도)를 조절하기 위해 필요한 성분을 의미하는 것일 수 있으며, 본 발명에서 상기 중화제는 트로메타민(tromethamine)일 수 있으나, 이에 한정되는 것은 아니다.The term “neutralizing agent” in this specification may refer to an ingredient necessary to adjust the pH (acidity) of a cosmetic composition. In the present invention, the neutralizing agent may be tromethamine, but is not limited thereto.
본 발명의 다른 일 양태는, 제1혼합물, 제2혼합물 및 제3혼합물의 제조 단계로서, 상기 제2혼합물은 수크로오스폴리스테아레이트 및 올리브오일불검화물을 포함하고;Another aspect of the present invention is a step of preparing a first mixture, a second mixture, and a third mixture, wherein the second mixture includes sucrose polystearate and unsaponifiable olive oil;
상기 제1혼합물 및 상기 제2혼합물을 혼합한 후 상기 제3혼합물을 혼합하여 혼합 조성물을 만드는 혼합 단계; 및A mixing step of mixing the first mixture and the second mixture and then mixing the third mixture to form a mixed composition; and
상기 혼합 조성물을 냉각하는 냉각 단계;를 포함하는 라멜라 액정 화장료 조성물의 제조 방법에 관한 것이다.It relates to a method of producing a lamellar liquid crystal cosmetic composition comprising a cooling step of cooling the mixed composition.
본 발명에서 상기 혼합 단계는 제조된 제1혼합물과 제2혼합물을 혼합하여 크림 조성물을 만드는 단계 이후, 혼합된 크림 조성물에 제조된 제3혼합물을 혼합하여 점도를 형성하는 단계를 포함하는 것일 수 있으나, 이에 한정되는 것은 아니다.In the present invention, the mixing step may include forming a viscosity by mixing the prepared third mixture into the mixed cream composition after making a cream composition by mixing the prepared first mixture and the second mixture. , but is not limited to this.
본 발명의 일 구현예에서, 제1혼합물과 제2혼합물을 혼합하여 크림 조성물을 만든 후, 크림 조성물과 제3혼합물을 혼합하여 점도가 형성되도록 화장료 조성물을 제조하였다.In one embodiment of the present invention, a cream composition was prepared by mixing the first mixture and the second mixture, and then the cream composition and the third mixture were mixed to prepare a cosmetic composition to form a viscosity.
본 발명에 있어서, 상기 제1혼합물은 정제수, 글리세린(glycerin), 부틸렌글라이콜(butylene glycol), 펜틸렌글라이콜(pentylene glycol), 1,2-헥산다이올(1,2-hexanediol), 트로메타민(tromethamine), 소듐파이테이트(sodium phytate) 및 글리세릴아크릴레이트/아크릴릭애씨드코폴리머(glyceryl acrylate/acrylic acid copolymer)로 이루어진 그룹에서 선택되는 1종 이상을 포함하고, 상기 제1혼합물의 제조 단계는 60 내지 80℃ 온도에서 교반 및 용해하는 것일 수 있으나, 이에 한정되는 것은 아니다.In the present invention, the first mixture includes purified water, glycerin, butylene glycol, pentylene glycol, 1,2-hexanediol, Contains at least one member selected from the group consisting of tromethamine, sodium phytate, and glyceryl acrylate/acrylic acid copolymer, and the first mixture The manufacturing step may include stirring and dissolving at a temperature of 60 to 80° C., but is not limited thereto.
본 발명에서 상기 제1혼합물의 제조 단계는 60 내지 80℃, 60 내지 75℃, 65 내지 80℃ 또는 65 내지 75℃ 온도에서 교반 및 용해하여 제조할 수 있으며, 예를 들어, 70℃ 온도에서 교반 및 용해하여 제조하는 것일 수 있다.In the present invention, the first mixture preparation step can be prepared by stirring and dissolving at a temperature of 60 to 80 ℃, 60 to 75 ℃, 65 to 80 ℃ or 65 to 75 ℃, for example, stirring at 70 ℃ And it may be prepared by dissolving.
본 발명에 있어서, 상기 제2혼합물은 카프릴릭/카프릭트라이글리세라이드(caprylic/capric tryglycerides), 아세틸레이티드하이드로제네이티드식물성글리세라이드(acetylated hydrogenated vegetable glyceride), 피토스테릴이소스테아릴다이머디리놀리에이트(phytosteryl isostearyl dimer dilinoleate), 다이카프릴릴에터(dicaprylyl ether), 비닐다이메티콘(vinyl dimethicone), C14-22알코올(C14-22 alcohol), 글리세릴스테아레이트(glyceryl stearate) 및 C12-20알킬글루코사이드(C12-20 alkyl glucoside)로 이루어진 그룹에서 선택되는 1종 이상을 추가로 포함하고, 상기 제2혼합물의 제조 단계는 60 내지 80℃ 온도에서 가온 용해하는 것일 수 있으나, 이에 한정되는 것은 아니다.In the present invention, the second mixture includes caprylic/capric tryglycerides, acetylated hydrogenated vegetable glyceride, and phytosteryl isostearyl dimer dihydride. phytosteryl isostearyl dimer dilinoleate, dicaprylyl ether, vinyl dimethicone, C14-22 alcohol, glyceryl stearate and C12 -20 alkyl glucoside (C12-20 alkyl glucoside), and the manufacturing step of the second mixture may be dissolving by heating at a temperature of 60 to 80 ℃, but is limited thereto. That is not the case.
본 발명에서 상기 제2혼합물의 제조 단계는 60 내지 80℃, 60 내지 75℃, 65 내지 80℃ 또는 65 내지 75℃ 온도에서 가온 용해하여 제조할 수 있으며, 예를 들어, 70℃ 온도에서 가온 용해하여 제조하는 것일 수 있다.In the present invention, the manufacturing step of the second mixture can be prepared by heating and dissolving at a temperature of 60 to 80 ℃, 60 to 75 ℃, 65 to 80 ℃ or 65 to 75 ℃, for example, heating and dissolving at 70 ℃. It may be manufactured by doing so.
본 발명에 있어서, 상기 제3혼합물은 카보머(carbomer)를 포함하고, 상기 제3혼합물의 제조 단계는 60 내지 80℃ 온도에서 가온 용해하는 것일 수 있다.In the present invention, the third mixture includes a carbomer, and the manufacturing step of the third mixture may be dissolving by heating at a temperature of 60 to 80°C.
본 발명에서 상기 제3혼합물의 제조 단계는 60 내지 80℃, 60 내지 75℃, 65 내지 80℃, 65 내지 75℃ 온도에서 가온 용해하여 제조할 수 있으며, 예를 들어, 70℃ 온도에서 가온 용해하여 제조하는 것일 수 있다.In the present invention, the third mixture preparation step can be prepared by heating and dissolving at a temperature of 60 to 80°C, 60 to 75°C, 65 to 80°C, and 65 to 75°C, for example, heating and dissolving at a temperature of 70°C. It may be manufactured by doing so.
본 발명에 있어서, 상기 냉각 단계는 40 내지 50℃ 온도에서 냉각하는 것일 수 있으나, 이에 한정되는 것은 아니다.In the present invention, the cooling step may be cooling at a temperature of 40 to 50° C., but is not limited thereto.
본 발명에서 상기 냉각 단계는 40 내지 50℃, 40 내지 48℃, 40 내지 45℃, 43 내지 50℃ 또는 43 내지 48℃ 온도에서 냉각할 수 있으며, 예를 들어, 45℃ 온도에서 냉각하는 것일 수 있다.In the present invention, the cooling step may be cooling at a temperature of 40 to 50°C, 40 to 48°C, 40 to 45°C, 43 to 50°C, or 43 to 48°C, for example, cooling at a temperature of 45°C. there is.
본 발명은 윤기 개선 효과가 우수한 액정(Liquid Crystal) 크림 화장료 조성물 및 이의 제조 방법에 관한 것으로서, 더욱 상세하게는, 일반적인 액정 화장료 조성물과 달리 스타치(starch)와 같은 다당류 사용 없이도 눈과 같은 외관을 띠며 윤기 개선 효과가 매우 우수하여, 이를 효과적으로 피부 외용 제품으로 사용할 수 있다.The present invention relates to a liquid crystal cream cosmetic composition with excellent gloss-improving effect and a method for manufacturing the same. More specifically, the present invention relates to a liquid crystal cream cosmetic composition that has an excellent gloss-improving effect and, more specifically, to a liquid crystal cream cosmetic composition that provides a snow-like appearance without the use of polysaccharides such as starch, unlike general liquid crystal cosmetic compositions. It has an excellent shine-improving effect, so it can be effectively used as an external skin product.
도 1은 본 발명의 일 실시예에 따라, 제조된 실시예 1 화장료 조성물의 액정 이미지를 촬영하여 나타낸 것이다.
도 2는 본 발명의 일 실시예에 따라, 제조된 실시예 1 화장료 조성물 제형의 외관을 나타낸 것이다.
도 3은 본 발명의 일 실시예에 따라, 제조된 비교예 1 화장료 조성물 제형의 외관을 나타낸 것이다.
도 4는 본 발명의 일 실시예에 따라, 제조된 비교예 2 화장료 조성물 제형의 외관을 나타낸 것이다.
도 5는 본 발명의 일 실시예에 따라, 제조된 비교예 3 화장료 조성물 제형의 외관을 나타낸 것이다.
도 6 및 도 7은 본 발명의 일 실시예에 따라, 제조된 화장료 조성물의 피부 윤기 개선 효과를 평가한 그래프를 나타낸 것이다.Figure 1 shows a liquid crystal image of the cosmetic composition of Example 1 prepared according to an embodiment of the present invention.
Figure 2 shows the appearance of the cosmetic composition formulation of Example 1 prepared according to an embodiment of the present invention.
Figure 3 shows the appearance of the cosmetic composition formulation of Comparative Example 1 prepared according to an embodiment of the present invention.
Figure 4 shows the appearance of the cosmetic composition formulation of Comparative Example 2 prepared according to an embodiment of the present invention.
Figure 5 shows the appearance of the cosmetic composition formulation of Comparative Example 3 prepared according to an embodiment of the present invention.
Figures 6 and 7 show graphs evaluating the skin gloss improvement effect of the cosmetic composition prepared according to an embodiment of the present invention.
이하, 본 발명이 속하는 분야에서 통상의 지식을 가진 자가 용이하게 실시할 수 있도록 본 발명의 실시예에 대하여 도면을 참고하여 구체적으로 설명한다. 본 명세서에서 사용되는 용어는 따로 정의하지 않는 한, 해당 분야에서 통상의 지식을 가진 자가 일반적으로 이해하는 내용으로 해석되어야 할 것이다.Hereinafter, embodiments of the present invention will be described in detail with reference to the drawings so that those skilled in the art can easily practice the present invention. Unless otherwise defined, terms used in this specification should be interpreted as generally understood by those skilled in the art.
본 명세서의 도면 및 실시예는 통상의 기술자가 본 발명을 쉽게 이해하고 실시하기 위한 것으로 도면 및 실시예에서 발명의 요지를 흐릴 수 있는 내용은 생략될 수 있으며, 본 발명이 도면 및 실시예로 한정되는 것은 아니다.The drawings and examples of this specification are intended to enable those skilled in the art to easily understand and practice the present invention. Content that may obscure the gist of the invention may be omitted from the drawings and examples, and the present invention is limited to the drawings and examples. It doesn't work.
본 명세서 전체에 걸쳐, 특정 물질의 농도를 나타내기 위하여 사용되는 “%”는 별도의 언급이 없는 경우, 고체/고체는 (중량/중량)%, 고체/액체는 (중량/부피)%, 그리고 액체/액체는 (부피/부피)%이다.Throughout this specification, “%” used to indicate the concentration of a specific substance means (weight/weight)% for solid/solid, (weight/volume)% for solid/liquid, and Liquid/liquid is (volume/volume)%.
제조예: 실시예 1 내지 4 및 비교예 1 내지 3 화장료 조성물의 제조Preparation Example: Examples 1 to 4 and Comparative Examples 1 to 3 Preparation of cosmetic compositions
실시예 1 내지 4 및 비교예 1 내지 3의 화장료 조성물을 제조하였으며, 구체적인 제조 방법은 다음과 같다.The cosmetic compositions of Examples 1 to 4 and Comparative Examples 1 to 3 were prepared, and the specific manufacturing method was as follows.
먼저, 제1혼합물은 정제수, 글리세린, 부틸렌글라이콜, 펜틸렌글라이콜, 1,2-헥산다이올, 트로메타민, 소듐파이테이트 및 글리세릴아크릴레이트/아크릴릭애씨드코폴리머를 혼합하였으며, 70℃ 온도에서 교반 및 용해하여 제조하였다.First, the first mixture was a mixture of purified water, glycerin, butylene glycol, pentylene glycol, 1,2-hexanediol, tromethamine, sodium phytate, and glyceryl acrylate/acrylic acid copolymer, 70 It was prepared by stirring and dissolving at a temperature of ℃.
그리고, 제2혼합물은 수크로오스폴리스테아레이트, 올리브오일불검화물, 미리스틸알코올, 세테아릴알코올, 베헤닐알코올, 미리스틸알코올, 세틸알코올, 카프릴릭/카프릭트라이글리세라이드, 아세틸레이티드하이드로제네이티드식물성글리세라이드, 피토스테릴이소스테아릴다이머디리놀리에이트, 다이카프릴릴에터, 비닐다이메티콘, C14-22알코올, 글리세릴스테아레이트 및 C12-20알킬글루코사이드를 혼합하였으며, 70℃ 온도에서 가온 용해하여 제조하였다.And, the second mixture is sucrose polystearate, unsaponifiable olive oil, myristyl alcohol, cetearyl alcohol, behenyl alcohol, myristyl alcohol, cetyl alcohol, caprylic/capric triglyceride, and acetylated hydro. Generated vegetable glyceride, phytosteryl isostearyl dimer dilinoleate, dicaprylyl ether, vinyl dimethicone, C14-22 alcohol, glyceryl stearate, and C12-20 alkyl glucoside were mixed, 70°C. It was prepared by heating and dissolving at temperature.
또한, 제3혼합물은 카보머를 포함하고 70℃ 온도에서 가온 용해하여 제조하였으며, 제1혼합물과 제2혼합물을 혼합하여 크림 조성물을 제조하였다. 그 이후에 크림 조성물과 제3혼합물을 혼합하여 점도가 형성되도록 혼합 조성물을 제조하였다. 이후, 혼합 조성물을 45℃ 온도에서 냉각하여, 하기 표 1 내지 표 2에 기재된 성분으로 구성된 실시예 1 내지 4 및 비교예 1 내지 3의 화장료 조성물을 제조하였다.In addition, the third mixture contained carbomer and was prepared by heating and dissolving at a temperature of 70°C, and a cream composition was prepared by mixing the first mixture and the second mixture. Thereafter, the cream composition and the third mixture were mixed to prepare a mixed composition to form a viscosity. Thereafter, the mixed composition was cooled at a temperature of 45°C to prepare cosmetic compositions of Examples 1 to 4 and Comparative Examples 1 to 3 consisting of the ingredients shown in Tables 1 and 2 below.
1
혼
합
물my
One
soul
bout
water
2
혼
합
물my
2
soul
bout
water
혼합물3rd
mixture
1
혼
합
물my
One
soul
bout
water
2
혼
합
물my
2
soul
bout
water
혼합물3rd
mixture
실험예 1: 액정(Liquid Crystal) 구조 형성 확인Experimental Example 1: Confirmation of liquid crystal structure formation
상기 제조예 1에 따라 제조된 실시예 1 화장료 조성물의 액정(Liquid Crystal) 구조 형성 여부를 광학 현미경을 통해 분석하였다. 액정 입자 이미지는 Olympus사의 olympus bx51 구용 형광/편광/위상차 정립 현미경(400배율)으로 촬영하였으며, 이를 도 1에 나타내었다.The formation of a liquid crystal structure in the cosmetic composition of Example 1 prepared according to Preparation Example 1 was analyzed using an optical microscope. The liquid crystal particle image was taken with an Olympus bx51 fluorescence/polarization/phase-contrast microscope (400x magnification) from Olympus, and is shown in Figure 1.
촬영 결과, 도 1에 제시된 바와 같이, 본 발명에 따라 수크로오스폴리스테아레이트 및 올리브오일불검화물을 포함하는 실시예 1의 화장료 조성물에서 액정(Liquid Crystal) 구조가 잘 형성되는 것을 확인하였다.As a result of the imaging, as shown in FIG. 1, it was confirmed that a liquid crystal structure was well formed in the cosmetic composition of Example 1 containing sucrose polystearate and unsaponifiable olive oil according to the present invention.
실험예 2: 화장료 조성물의 외관 비교Experimental Example 2: Comparison of appearance of cosmetic compositions
상기 제조예 1에 따라 제조된 화장료 조성물의 외관을 비교하였으며, 이를 도 2 내지 도 5에 나타내었다.The appearances of the cosmetic compositions prepared according to Preparation Example 1 were compared, and are shown in Figures 2 to 5.
도 2 내지 도 5에 제시된 바와 같이, 비교예 1 내지 3 화장료 조성물의 외관은 매끈한 반면, 실시예 1 화장료 조성물은 비교예 1 내지 3과 확연히 구별되는 눈 입자와 같이 울퉁불퉁한 외관이 특징적으로 형성되는 것을 확인하였다.As shown in Figures 2 to 5, the cosmetic compositions of Comparative Examples 1 to 3 had a smooth appearance, while the cosmetic composition of Example 1 had a characteristically bumpy appearance like snow particles, which was clearly different from that of Comparative Examples 1 to 3. confirmed.
실험예 3: 피부 윤기 개선 효과 확인Experimental Example 3: Confirmation of skin radiance improvement effect
상기 제조예 1에 따라 제조된 화장료 조성물의 피부 윤기 개선 효과를 확인하였다.The skin gloss improvement effect of the cosmetic composition prepared according to Preparation Example 1 was confirmed.
구체적으로, 화장료 조성물 도포 후 윤기를 평가하기 위해, 민감성 피부라 생각되는 성인 남, 녀 5명 (평균나이 32.4세)을 선발하여, 상기 제조예 1에 따라 제조된 실시예 1 내지 4 및 비교예 1 내지 3의 화장료 조성물을 안면부에 도포하여 도포 전과, 도포 10분 후 SKIN GLOSS UNIT을 이용하여 측정된 값을 비교 평가하였다. 측정 기기는 Skin Gloss Meter (Delfin, Finland)로 측정하였으며, 이를 하기 도 6 내지 도 7에 나타내었다.Specifically, in order to evaluate the gloss after applying the cosmetic composition, five adult men and women (average age 32.4 years old) who were considered to have sensitive skin were selected and Examples 1 to 4 and Comparative Examples prepared according to Preparation Example 1 above. Cosmetic compositions 1 to 3 were applied to the facial area, and the values measured using the SKIN GLOSS UNIT before and 10 minutes after application were compared and evaluated. The measurement was performed using a Skin Gloss Meter (Delfin, Finland), which is shown in Figures 6 and 7 below.
측정 결과, 도 6 내지 도 7에 제시된 바와 같이, 비교예 1 내지 3 화장료 조성물은 SKIN GLOSS UNIT의 증감률이 모두 10 % 미만으로 측정된 반면, 실시예 1 내지 4 화장료 조성물의 경우 SKIN GLOSS UNIT의 증감률이 모두 12 % 이상으로 측정되었으며, 특히 실시예 1 화장료 조성물은 SKIN GLOSS UNIT의 증감률이 17 %로 측정되었다. 따라서, 본 발명에 따른 화장료 조성물은 현저히 우수한 피부 윤기 개선 효과가 있음을 구체적으로 확인하였다.As a result of the measurement, as shown in Figures 6 and 7, the increase/decrease rate of the SKIN GLOSS UNIT for the cosmetic compositions of Comparative Examples 1 to 3 was measured to be less than 10%, while for the cosmetic compositions of Examples 1 to 4, the increase/decrease rate of the SKIN GLOSS UNIT was measured to be less than 10%. The increase/decrease rates were all measured to be more than 12%, and in particular, the increase/decrease rate of the SKIN GLOSS UNIT for the cosmetic composition of Example 1 was measured to be 17%. Therefore, it was specifically confirmed that the cosmetic composition according to the present invention has a significantly excellent skin gloss improvement effect.
소결sintering
상기 실험예의 결과를 종합하면, 베헤닐알코올을 포함하는 화장료 조성물(비교예1), 미리스틸알코올을 포함하는 화장료 조성물(비교예 2), 및 세틸알코올을 포함하는 화장료 조성물(비교예 3) 대비, 본 발명의 일 양태에 따라 수크로오스폴리스테아레이트 및 올리브오일불검화물을 포함하는 화장료 조성물은 액정(Liquid Crystal) 구조가 잘 형성될 뿐만 아니라, 눈과 같은 특징적인 외관을 갖고, 현저히 우수한 피부 윤기 개선 효과가 있음을 확인할 수 있다.Summarizing the results of the above experimental examples, compared to the cosmetic composition containing behenyl alcohol (Comparative Example 1), the cosmetic composition containing myristyl alcohol (Comparative Example 2), and the cosmetic composition containing cetyl alcohol (Comparative Example 3) According to one aspect of the present invention, the cosmetic composition containing sucrose polystearate and unsaponifiable olive oil not only forms a liquid crystal structure well, but also has a characteristic appearance like snow and significantly improves skin gloss. You can confirm that it is effective.
Claims (9)
제1혼합물, 제2혼합물 및 제3혼합물의 제조 단계로서,
상기 제1혼합물은 정제수, 글리세린, 부틸렌글라이콜, 펜틸렌글라이콜, 1,2-헥산다이올, 트로메타민, 소듐파이테이트 및 글리세릴아크릴레이트/아크릴릭애씨드코폴리머로 이루어진 그룹에서 선택되는 1종 이상을 포함하고,
상기 제2혼합물은 수크로오스폴리스테아레이트 및 올리브오일불검화물을 포함하고,
상기 제3혼합물은 카보머를 포함하고;
상기 제1혼합물 및 상기 제2혼합물을 혼합한 후 상기 제3혼합물을 혼합하여 혼합 조성물을 만드는 혼합 단계; 및
상기 혼합 조성물을 냉각하는 냉각 단계.Method for producing a lamellar liquid crystal cosmetic composition comprising the following steps:
As a manufacturing step of the first mixture, second mixture, and third mixture,
The first mixture is selected from the group consisting of purified water, glycerin, butylene glycol, pentylene glycol, 1,2-hexanediol, tromethamine, sodium phytate, and glyceryl acrylate/acrylic acid copolymer. Contains one or more types,
The second mixture includes sucrose polystearate and unsaponifiable olive oil,
The third mixture includes carbomer;
A mixing step of mixing the first mixture and the second mixture and then mixing the third mixture to form a mixed composition; and
A cooling step of cooling the mixed composition.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101113374B1 (en) | 2008-11-26 | 2012-02-21 | (주)아모레퍼시픽 | Cosmetic composition for improving the skin elasticity |
| KR20180101378A (en) | 2016-01-15 | 2018-09-12 | 독토르. 아우구스트 볼프 게엠베하 운트 코. 카게 아르쯔네이미텔 | Water-in-oil emulsion |
| CN110812273A (en) * | 2019-12-11 | 2020-02-21 | 佛山市顺德区恒杏润医疗科技有限公司 | Skin barrier moisturizing and repairing cream and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101113374B1 (en) | 2008-11-26 | 2012-02-21 | (주)아모레퍼시픽 | Cosmetic composition for improving the skin elasticity |
| KR20180101378A (en) | 2016-01-15 | 2018-09-12 | 독토르. 아우구스트 볼프 게엠베하 운트 코. 카게 아르쯔네이미텔 | Water-in-oil emulsion |
| CN110812273A (en) * | 2019-12-11 | 2020-02-21 | 佛山市顺德区恒杏润医疗科技有限公司 | Skin barrier moisturizing and repairing cream and preparation method thereof |
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