KR102234375B1 - Deodorant composition containing the natural plant extracts - Google Patents
Deodorant composition containing the natural plant extracts Download PDFInfo
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- A61L9/00—Disinfection, sterilisation or deodorisation of air
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- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
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Abstract
Description
본 발명은 천연 식물추출물을 함유하는 탈취제 조성물에 관한 것으로, 보다 구체적으로는 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일로 이루어진 혼합물을 함유하여 악취를 유발하는 주요성분인 암모니아, 초산, 포름알데히드, 황화수소, 트리메틸아민의 취를 감소/제거시켜 불쾌함을 개선하는 탈취제 조성물에 관한 것이다.The present invention relates to a deodorant composition containing natural plant extracts, and more specifically, contains a mixture consisting of Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, Nahanbaek branch extract, and secretory tree oil to reduce odor. It relates to a deodorant composition that improves discomfort by reducing/removing the odor of ammonia, acetic acid, formaldehyde, hydrogen sulfide, and trimethylamine, which are the main ingredients that cause.
일상 생활환경에서 발생하는 악취의 원인은 다양하다. 대부분의 악취는 주로 황화수소, 황화메틸, 메틸머캅탄 등의 유황계 화합물 또는 암모니아, 트리메틸아민 등의 질소계 화합물로 인해 발생한다. 이러한 악취에 지속적으로 노출되면 식욕 감퇴, 구토, 불면, 알레르기 증상, 작업능률의 저하 등이 유발될 수 있다.There are many causes of odor in everyday life. Most odors are mainly caused by sulfur-based compounds such as hydrogen sulfide, methyl sulfide, and methyl mercaptan, or nitrogen-based compounds such as ammonia and trimethylamine. Continuous exposure to these odors can cause loss of appetite, vomiting, insomnia, allergic symptoms, and decrease in work efficiency.
현재까지 알려진 탈취 또는 소취 방법은 활성탄, 실리카겔, 알루미나 또는 제올라이트 등의 다공질 소재를 이용하여 악취성분을 흡착 또는 흡수하는 물리적 흡착법, 계면활성제, 에틸렌글리콜, 미생물 또는 효소 등을 이용하여 악취발생의 원인이 되는 세균이나 박테리아를 살균하거나 부패를 방지함으로써 소취하는 생물학적 방법, 악취성분에 대하여 반응성이 높은 물질 또는 악취성분과 반응하여 착물을 형성하는 물질을 소취제로 사용하는 화학적 방법, 향료와 같은 방향성 물질에 의해 악취자극을 치환 또는 중화시키는 감각적 방법 등이 있다.Deodorization or deodorization methods known to date are physical adsorption methods in which odor components are adsorbed or absorbed by using porous materials such as activated carbon, silica gel, alumina or zeolite, and the cause of odor is generated by using surfactants, ethylene glycol, microorganisms, or enzymes. By sterilizing bacteria or bacteria or preventing spoilage, a biological method of deodorizing, a chemical method of using a substance highly reactive to odor components or a substance that forms a complex by reacting with odor components as a deodorant, and aromatic substances such as fragrances. There are sensory methods of substituting or neutralizing the odor stimulus.
탈취제는 악취의 제거능력이 우수하고, 환경에 영향을 주지 않아야 할 뿐 아니라, 사용 시 인체의 호흡기를 통하여 흡수되거나 피부에 접촉되는 경우에도 자극을 주거나 만성적인 영향을 끼치지 않아야 한다.The deodorant should not only have excellent odor removal ability and should not affect the environment, but also should not cause irritation or chronic effect when it is absorbed through the respiratory tract of the human body or when it comes into contact with the skin during use.
이와 관련하여 대한민국 공개특허 제10-2016-0007336호 "고도 분지된 사이클릭 덱스트린 및 식물 추출물을 포함하는 탈취제 조성물"에는 '고도 분지된 사이클릭 덱스트린과 함께 녹차, 감잎, 진피, 및 팔각향을 포함하는 식물 추출물을 포함하여 탈취 효과가 시너지적으로 상승된 탈취제 조성물'이 개시되어 있고, 대한민국 공개특허 제10-2015-0043694호 "친환경 실내용 탈취제 조성물 및 이를 포함하는 친환경 실내용 탈취제"에는 '산화방지성분 55~75 중량%, 식물성오일 10~35 중량%, 솔잎추출물 3~15 중량%, 라임추출물 1~5 중량% 및 아스코르빅산 0.1~5 중량%를 포함하는 탈취제 조성물'이 개시되어 있다.In this regard, Korean Patent Application Publication No. 10-2016-0007336 "Deodorant composition comprising highly branched cyclic dextrin and plant extract" includes green tea, persimmon leaves, dermis, and octagonal flavor together with highly branched cyclic dextrin. A deodorant composition with synergistically increased deodorant effect, including plant extracts, has been disclosed, and Korean Patent Laid-Open No. 10-2015-0043694 "Eco-friendly indoor deodorant composition and eco-friendly indoor deodorant containing the same" discloses'oxidation. A deodorant composition comprising 55 to 75% by weight of prevention component, 10 to 35% by weight of vegetable oil, 3 to 15% by weight of pine needle extract, 1 to 5% by weight of lime extract, and 0.1 to 5% by weight of ascorbic acid is disclosed. .
본 발명자들은 천연 식물추출물을 이용하여 인체에 안전한 탈취제를 제조하고자 연구하였으며, 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일로 이루어진 혼합물을 함유하는 탈취제 조성물이 인체에 안전하면서, 그 상승효과에 의하여 우수한 소취효과를 나타내는 것을 확인하여 본 발명을 완성하였다.The present inventors have studied to prepare a deodorant that is safe for the human body using natural plant extracts, and a deodorant composition containing a mixture consisting of Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, Hanbaek branch extract and secretory tree oil The present invention was completed by confirming that it is safe for the human body and exhibits an excellent deodorizing effect by its synergistic effect.
본 발명은 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일로 이루어진 혼합물을 함유하여 우수한 소취효과를 나타내는 탈취제 조성물을 제공하는 것을 목적으로 한다.It is an object of the present invention to provide a deodorant composition showing excellent deodorant effect by containing a mixture consisting of Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, nahanbaek branch extract, and secretory tree oil.
상기 목적을 달성하기 위하여 본 발명에 따르면 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일로 이루어진 혼합물을 함유하는 탈취제 조성물이 제공된다.In order to achieve the above object, according to the present invention, there is provided a deodorant composition containing a mixture consisting of a Bambusa bulgaris leaf/stem extract, a cedar leaf extract, a cypress leaf extract, a white branch extract and a secretory tree oil.
활성성분으로서의 상기 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일로 이루어진 혼합물은 전체 중량에 대하여 1.0~5.0중량% 함유된다.The mixture consisting of the Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, Hanbaek branch extract, and secretory tree oil as active ingredients is contained in an amount of 1.0 to 5.0% by weight based on the total weight.
상기 조성물에 있어서, 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일은 각각 0.2~1.0중량부, 0.2~1.0중량부, 0.2~1.0중량부, 0.2~1.0중량부, 0.2~1.0중량부의 비율로 포함되는 것이 바람직하다.In the composition, Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, nahanbaek branch extract, and secretory tree oil are respectively 0.2 to 1.0 parts by weight, 0.2 to 1.0 parts by weight, 0.2 to 1.0 parts by weight, 0.2 to It is preferably contained in a ratio of 1.0 parts by weight and 0.2 to 1.0 parts by weight.
상기 탈취제 조성물은 암모니아, 초산, 포름알데히드, 황화수소, 트리메틸아민에 대한 소취효과가 우수한 것을 특징으로 한다.The deodorant composition is characterized in that it has excellent deodorizing effect against ammonia, acetic acid, formaldehyde, hydrogen sulfide, and trimethylamine.
상기 탈취제 조성물에는 부형제, 보존제, 향료, 다가알코올 등이 더욱 포함될 수 있다.The deodorant composition may further include excipients, preservatives, fragrances, polyhydric alcohols, and the like.
본 발명 탈취제 조성물은 천연 소재를 이용하여 안전하며, 생활 속 악취를 유발하는 주요성분인 암모니아, 초산, 포름알데히드, 황화수소, 트리메틸아민에 대한 소취효과가 우수하므로 탈취제로 유용하게 사용될 수 있다. The deodorant composition of the present invention is safe using natural materials, and has excellent deodorizing effects for ammonia, acetic acid, formaldehyde, hydrogen sulfide, and trimethylamine, which are the main components that cause odor in life, so it can be usefully used as a deodorant.
본 발명은 천연소재 유래의 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일의 혼합물은 그 상승작용에 의하여 우수한 소취활성을 나타낸다는 것을 특징으로 한다.The present invention is characterized in that a mixture of Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, nahanbaek branch extract and secretory tree oil derived from natural materials exhibits excellent deodorizing activity by synergistic action.
대나무는 외떡잎식물 벼목 화본과 대나무아과에 속하는 상록성 여러해살이 식물의 총칭으로, 세계적으로 종류는 매우 많으며 120속 1,250종이 분포한다. 대나무는 습기가 많은 열대지방에서 잘 자라기 때문에 우리나라에서는 중부 이남과 제주도에 많이 분포하고 있다. 본 발명의 활성성분 중 하나로 사용되는 밤부사 불가리스 추출물은 대나무(bambusa vulgaris)의 전초를 추출하여 얻은 성분으로서, 보습, 피부탄력개선 성분 등으로 사용되어 왔다.Bamboo is a collective term for evergreen perennial plants belonging to the monocotyledonous plant and the subfamily Bamboo. There are many types worldwide, and 1,250 species in 120 genera are distributed. Because bamboo grows well in tropical regions with high humidity, it is widely distributed in the south of the central region and Jeju Island in Korea. Bambusa vulgaris extract used as one of the active ingredients of the present invention is a component obtained by extracting the outpost of bamboo (bambusa vulgaris), and has been used as a moisturizing, skin elasticity improvement component, and the like.
삼나무(Cryptomeria japonica)는 겉씨식물 구과목 낙우송과의 상록교목이다. 연평균기온 12∼14℃, 강우량 3,000mm 이상 되는 계곡에서 잘 자라며, 높이 40m, 지름 1∼2m에 달한다. 수피는 붉은빛을 띤 갈색이고 세로로 갈라지며 가지와 잎이 빽빽이 나서 원뿔 모양의 수형이 된다. 잎은 굽어진 바늘 모양이고 나선 모양으로 배열하며 말라도 떨어지지 않는다. 삼나무 흑심재 추출물의 피부사상균에 대한 항진균 활성, 삼나무 잎 추출물의 항산화 활성 등이 알려져 있다.Cedar (Cryptomeria japonica) is an evergreen tree of the coniferous family Larch family. It grows well in valleys with annual average temperature of 12-14℃ and rainfall of 3,000mm or more, reaching 40m in height and 1 to 2m in diameter. The bark is reddish brown, split vertically, and the branches and leaves are dense, forming a cone-shaped tree. The leaves are curved needle-shaped, arranged in a spiral shape, and do not fall off even when dried. The antifungal activity of cedar black heartwood extract against dermatophytes, and the antioxidant activity of cedar leaf extract are known.
편백나무(Chamaecyparis obtusa)는 겉씨식물 구과목 측백나무과의 상록교목이다. 높이 40m, 지름 2m에 달하며, 가지는 수평으로 퍼져서 원뿔형의 수관을 하고 있다. 수피는 적갈색이고 섬유성이며 세로로 얇게 벗겨진다. 잎은 마주나고 두꺼우며 길이 1~1.5mm로 비늘같이 작고 뒷면의 기공조선(氣孔條線)은 Y자형이다. 또한 잎 표면에 1개의 선(腺)이 있으며 뒷면에 흰 점이 있다. 편백나무 잎 추출물의 항산화, 항염 효과 등이 알려져 있다.Cypress tree (Chamaecyparis obtusa) is an evergreen arboreous tree of the coniferous cypress family. It reaches 40m in height and 2m in diameter, and branches spread horizontally to form a conical crown. The bark is reddish brown, fibrous, and thinly peeled vertically. The leaves are opposite, thick, 1~1.5mm long, small like scales, and the Qigong Chosun on the back side is Y-shaped. In addition, there is one line on the surface of the leaf and white spots on the back side. Antioxidant and anti-inflammatory effects of cypress leaf extract are known.
나한백(Thujopsis dolabrata)은 겉씨식물 구과목 측백나무과의 상록침엽 교목이다. 높이 10∼30m, 지름 약 90cm이다. 나무껍질은 자줏빛이나 잿빛을 띤 갈색이다. 가지와 작은가지는 어긋난다. 잎은 윤이 나고 짙은 녹색이며 뒷면에 흰 기공선이 있고, 편백에 비하여 크고 둥글다. 옆에 달린 잎은 비스듬히 퍼지고 달걀을 반으로 나눈 모양이며 길이 4∼6mm이고 끝이 둔하다. 앞 뒤로 달린 잎은 넓은 달걀 모양이고 납작하며 여러 해 동안 달려 있다. 나한백 가지 추출물은 피부컨디셔닝제로 사용되고 있다.Nahanbaek (Thujopsis dolabrata) is an evergreen coniferous arboreous tree of the coniferous family Cypressaceae family. It is 10-30m in height and about 90cm in diameter. The bark is purplish or grayish brown. Branches and small branches are misaligned. The leaves are shiny and dark green, with white pore lines on the back side, and larger and rounder than cypress. The leaves on the side spread obliquely, the egg is divided in half, and the length is 4~6mm, and the end is dull. The leaves on the front and back are broad egg-shaped, flat, and hang for many years. Nahanbaek eggplant extract is used as a skin conditioning agent.
본 발명 탈취제 조성물의 활성성분 중의 하나인 분비나무 오일(Abies Sibirica Oil)은 분비나무(Abies Sibirica)의 바늘잎과 가지를 스팀 증류하여 얻은 휘발성 오일이다. 방향제, 목욕용품의 향료로 사용된다.One of the active ingredients of the deodorant composition of the present invention, Abies Sibirica Oil, is a volatile oil obtained by steam distillation of needle leaves and branches of Abies Sibirica. It is used as an air freshener and fragrance for bath products.
본 발명에 따르면, 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일을 함유하는 탈취제 조성물이 제공된다.According to the present invention, there is provided a deodorant composition containing Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, Hanbaek branch extract, and secretory tree oil.
상기 추출물은 열수추출, 용매추출, 증류추출 또는 아임계 추출법에 의하여 제조될 수 있으며, 아임계 추출법에 의하여 제조되는 것이 더욱 바람직하다. 본 발명의 바람직한 일 구체예에 따르면 추출원물을 물을 추출용매로 하여 아임계추출 조건인 120~380℃, 압력 0.1~10MPa에서 추출하여 제조한다.The extract may be prepared by hot water extraction, solvent extraction, distillation extraction or subcritical extraction method, and more preferably prepared by subcritical extraction method. According to a preferred embodiment of the present invention, the extract is prepared by extracting the raw material using water as an extraction solvent under subcritical extraction conditions of 120 to 380°C and a pressure of 0.1 to 10 MPa.
용매추출인 경우에는 물, 탄소수 1 내지 4의 무수 또는 함수알코올, 에틸아세테이트, 아세톤, 글리세린, 에틸렌글리콜, 프로필렌글리콜 및 부틸렌글리콜로 이루어지는 군으로부터 선택되는 적어도 하나의 용매로 추출하여 제조될 수 있다.In the case of solvent extraction, it can be prepared by extraction with at least one solvent selected from the group consisting of water, anhydrous or hydrous alcohol having 1 to 4 carbon atoms, ethyl acetate, acetone, glycerin, ethylene glycol, propylene glycol, and butylene glycol. .
밤부사 불가리스 추출물은 밤부사 불가리스 잎/줄기 추출물인 경우에 더 우수한 소취활성을 나타내므로 바람직하다. Bambusa vulgaris extract is preferable because it exhibits more excellent deodorizing activity when it is a leaf/stem extract of Bambusa vulgaris.
활성성분으로서의 상기 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일로 구성된 혼합물은 조성물 전체 중량에 대하여 1.0~5.0중량% 함유된다. 1중량% 미만을 함유하는 경우에는 소취효과가 크지 않고, 5.0중량%를 초과하는 경우에는 효과대비 경제성 측면에서 바람직하지 않다.The mixture consisting of the Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, Hanbaek branch extract, and secretory tree oil as active ingredients is contained in an amount of 1.0 to 5.0% by weight based on the total weight of the composition. When it contains less than 1% by weight, the deodorizing effect is not large, and when it exceeds 5.0% by weight, it is not preferable from the viewpoint of economic efficiency compared to the effect.
본 발명의 일 구체예에 따르면, 상기 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일은 각각 0.2~1.0중량부, 0.2~1.0중량부, 0.2~1.0중량부, 0.2~1.0중량부, 0.2~1.0중량부의 비율로 함유될 때 보다 우수한 탈취효과를 나타내므로 더욱 바람직하다. According to an embodiment of the present invention, the Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, nahanbaek branch extract, and secretory tree oil are 0.2 to 1.0 parts by weight, 0.2 to 1.0 parts by weight, 0.2 to 1.0, respectively. When contained in a proportion of parts by weight, 0.2 to 1.0 parts by weight, and 0.2 to 1.0 parts by weight, it exhibits a more excellent deodorizing effect, so it is more preferable.
상기 탈취제 조성물에는 통상적으로 사용되는 부형제, 보존제, 향료, 다가알코올 등이 추가적으로 포함될 수 있다.The deodorant composition may additionally include commonly used excipients, preservatives, flavors, polyhydric alcohols, and the like.
상기 탈취제 조성물은 악취 원인 물질, 그 중에서도 암모니아, 초산, 포름알데히드, 황화수소, 트리메틸아민에 대한 소취 효과가 우수한 것을 확인하였다(시험예).It was confirmed that the deodorant composition has excellent deodorizing effects on odor-causing substances, among others, ammonia, acetic acid, formaldehyde, hydrogen sulfide, and trimethylamine (Test Example).
본 발명의 탈취제 조성물은 세탁 세제, 섬유유연제, 표면 세정제, 주방 세제, 탈취제, 손 세정제 등의 용도로 사용될 수 있으나, 이에 한정되는 것은 아니다. 제형에는 제한이 없으며 통상적으로 제조되는 어떠한 제형으로도 제조될 수 있다. 예를 들어 에멀젼, 마이크로에멀젼, 젤, 스프레이 등의 형태로 제조될 수 있다.The deodorant composition of the present invention may be used for laundry detergents, fabric softeners, surface cleaners, kitchen detergents, deodorants, hand cleaners, and the like, but is not limited thereto. There is no limitation on the dosage form, and it may be prepared in any conventionally prepared dosage form. For example, it can be prepared in the form of an emulsion, microemulsion, gel, spray, or the like.
[실시예][Example]
이하, 실시예 및 시험예를 통하여 본 발명을 더욱 구체적으로 설명한다.Hereinafter, the present invention will be described in more detail through Examples and Test Examples.
실시예 1 ~ 3: 탈취제 조성물의 제조Examples 1 to 3: Preparation of deodorant composition
탈취제 조성물을 제조하기 위하여 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물, 분비나무 오일을 구입(일본 아이재팬社)하여 사용하였다.In order to prepare a deodorant composition, Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, nahanbaek branch extract, and secretory tree oil were purchased (I Japan Co., Ltd.) and used.
상기 추출물들을 동일중량비로 혼합한 혼합물을 함유하는 탈취제 조성물을 하기 표 1의 조성에 따라 통상의 방법으로 제조하였다. 상기 추출물 중 일부만을 포함하는 조성물을 비교예로 하였다.A deodorant composition containing a mixture obtained by mixing the extracts at the same weight ratio was prepared by a conventional method according to the composition of Table 1 below. A composition containing only some of the extracts was used as a comparative example.
시험예 1: 암모니아 소취 테스트(관능평가)Test Example 1: Ammonia deodorant test (sensory evaluation)
상기 실시예 및 비교예 조성물의 소취 효과를 확인하기 위하여 다음과 같은 방법으로 시험하였다. In order to confirm the deodorizing effect of the compositions of Examples and Comparative Examples, the following methods were used.
암모니아(0.05%)용액 0.5g을 함침시킨 섬유조각을 용기에 넣고, 상기 실시예 및 비교예의 조성물이 담긴 분사용기를 1번씩 분사한 후 용기를 밀폐하였다. 밀폐시킨 후 10분, 20분, 30분, 60분 간격으로 암모니아 냄새 감소 정도를 평가하였다.Fiber fragments impregnated with 0.5 g of ammonia (0.05%) solution were put into a container, and the sprayer containing the compositions of Examples and Comparative Examples was sprayed once, and then the container was sealed. After sealing, the degree of ammonia odor reduction was evaluated at intervals of 10 minutes, 20 minutes, 30 minutes, and 60 minutes.
그 결과를 하기 표 2에 나타내었다.The results are shown in Table 2 below.
(--:소취 거의 안됨 / -:소취 약간 됨 / +:소취 적당히 됨 / ++:소취 거의 됨 / +++: 냄새없음)(--: Almost no deodorant / -: Slightly deodorant / +: Moderately deodorant / ++: Almost no deodorant / +++: No odor)
상기 표 2에 나타낸 바와 같이 상기 실시예의 탈취제 조성물을 적용한 결과, 악취의 주된 원인 성분인 암모니아의 농도가 시간이 경과함에 따라 현저하게 감소되어 소취 효과가 우수한 것을 확인할 수 있다. 또한 상기 실시예의 탈취제 조성물은 일부 성분을 포함하지 않은 비교예의 조성물에 비하여 더욱 우수한 소취활성을 나타내었다.As shown in Table 2, as a result of applying the deodorant composition of the above example, it can be seen that the concentration of ammonia, which is the main cause of odor, is significantly reduced as time passes, so that the deodorizing effect is excellent. In addition, the deodorant composition of the above example exhibited more excellent deodorizing activity compared to the composition of the comparative example that did not contain some components.
시험예 2: 트리메틸아민 소취 테스트(관능평가)Test Example 2: Trimethylamine deodorization test (sensory evaluation)
상기 실시예 및 비교예 조성물의 소취 효과를 확인하기 위하여 다음과 같은 방법으로 시험하였다.In order to confirm the deodorizing effect of the compositions of Examples and Comparative Examples, the following methods were used.
트리메틸아민(0.005%)용액 0.5g을 함침시킨 섬유조각을 용기에 넣고, 상기 실시예 및 비교예의 조성물이 담긴 분사용기를 1번씩 분사한 후 용기를 밀폐하였다. 밀폐시킨 후 30분, 1시간, 3시간, 15시간, 24시간 간격으로 트리메틸아민 냄새 감소 정도를 평가하였다.A piece of fiber impregnated with 0.5 g of a trimethylamine (0.005%) solution was put into a container, and a sprayer containing the compositions of the Examples and Comparative Examples was sprayed once, and the container was sealed. After sealing, the degree of reduction of trimethylamine odor was evaluated at intervals of 30 minutes, 1 hour, 3 hours, 15 hours, and 24 hours.
그 결과를 하기 표 3에 나타내었다.The results are shown in Table 3 below.
(--:소취 거의 안됨 / -:소취 약간 됨 / +:소취 적당히 됨 / ++:소취 거의 됨 / +++:냄새없음) (--: Almost no deodorant / -: Slightly deodorant / +: Moderately deodorant / ++: Almost no deodorant / +++: No odor)
상기 표 3에 나타낸 바와 같이 상기 실시예의 탈취제 조성물을 적용한 결과, 악취의 주된 원인 성분인 트리메틸아민의 농도가 시간이 경과함에 따라 현저하게 감소되어 소취 효과가 우수한 것을 확인할 수 있다. 또한 상기 실시예의 탈취제 조성물은 일부 성분을 포함하지 않은 비교예의 조성물에 비하여 더욱 우수한 소취활성을 나타내었다.As shown in Table 3, as a result of applying the deodorant composition of the above example, it can be seen that the concentration of trimethylamine, which is the main cause of odor, is remarkably reduced as time elapses, so that the deodorizing effect is excellent. In addition, the deodorant composition of the above example exhibited more excellent deodorizing activity compared to the composition of the comparative example that did not contain some components.
시험예 3: 소취성능 시험Test Example 3: Deodorization performance test
본 발명에 따른 밤부사 불가리스잎/줄기 추출물, 삼나무잎 추출물, 편백잎 추출물, 나한백가지 추출물 및 분비나무 오일로 구성된 혼합물을 전체 중량에 대하여 2.0중량%을 적용한 탈취제 조성물(실시예 2)을 가스검지관법을 사용하여 포름알데히드(HCHO), 황화수소(H2S), 암모니아(NH3), 초산(CH3COOH), 트리메틸아민(C3H9N)에 대한 소취성능 시험을 각각 실시하였다. 탈취율은 다음과 같은 식에 의하여 계산하였고, 결과를 하기의 표 4에 나타내었다.Gas detection of a deodorant composition (Example 2) in which 2.0% by weight of a mixture consisting of Bambusa bulgaris leaf/stem extract, cedar leaf extract, cypress leaf extract, Nahanbaek branch extract, and secretory tree oil according to the present invention was applied to the total weight. Formaldehyde (HCHO), hydrogen sulfide (H 2 S), ammonia (NH 3 ), acetic acid (CH 3 COOH), and trimethylamine (C 3 H 9 N) were tested for deodorizing performance, respectively. The deodorization rate was calculated by the following equation, and the results are shown in Table 4 below.
탈취율(감소율)(%)=(공시험의 2시간 후 측정치 - 시료의 2시간 후 측정치)/공시험의 2시간 후 측정치 × 100Deodorization rate (reduction rate) (%) = (Measured value after 2 hours of blank test-Measured value after 2 hours of sample)/Measurement value after 2 hours of blank test × 100
상기 표 4에 나타낸 바와 같이 상기 실시예 2의 탈취제 조성물을 적용한 결과, 악취의 주된 원인 성분인 포름알데히드(HCHO), 황화수소(H2S), 암모니아(NH3), 초산(CH3COOH), 트리메틸아민(C3H9N)의 농도가 시간이 경과함에 따라 현저하게 감소되어 소취 효과가 우수한 것을 확인할 수 있다. 상기 실시예 2의 소취성능 시험결과로 보아 실시예 3의 소취성능은 더욱 우수할 것임을 알 수 있다.As shown in Table 4, as a result of applying the deodorant composition of Example 2, formaldehyde (HCHO), hydrogen sulfide (H 2 S), ammonia (NH 3 ), acetic acid (CH 3 COOH), which are the main causes of odor, It can be seen that the concentration of trimethylamine (C 3 H 9 N) is remarkably reduced with the passage of time, so that the deodorizing effect is excellent. From the results of the deodorization performance test of Example 2, it can be seen that the deodorization performance of Example 3 will be more excellent.
Claims (5)
The deodorant composition according to claim 1, wherein the deodorant composition comprises at least one component of a preservative, fragrance, polyhydric alcohol, and surfactant.
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| KR102665344B1 (en) * | 2023-11-24 | 2024-05-10 | 주식회사 바이오텍 | Liquid type deodorant using minerals and livestock urine and manufacturing method thereof |
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| JPH09202721A (en) * | 1996-01-25 | 1997-08-05 | Ichimaru Pharcos Co Ltd | Deodorant |
| KR20070080437A (en) * | 2006-02-07 | 2007-08-10 | 담양군 | Method of preparing wood vinegar composition and wood vinegar composition prepared using the method |
| KR20130014912A (en) * | 2011-08-01 | 2013-02-12 | 신광섭 | The phytoncide composition and phytoncide composition releasing package |
| JP2014151137A (en) * | 2013-02-14 | 2014-08-25 | Ichimaru Pharcos Co Ltd | Deodorant and uses of the same |
| KR20160042586A (en) * | 2014-10-10 | 2016-04-20 | 박흥순 | Armoma compositon, and aroma products using the same |
| JP6577885B2 (en) * | 2016-02-18 | 2019-09-18 | 夢木香株式会社 | Deodorants |
-
2020
- 2020-07-02 KR KR1020200081542A patent/KR102234375B1/en active IP Right Grant
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09202721A (en) * | 1996-01-25 | 1997-08-05 | Ichimaru Pharcos Co Ltd | Deodorant |
| KR20070080437A (en) * | 2006-02-07 | 2007-08-10 | 담양군 | Method of preparing wood vinegar composition and wood vinegar composition prepared using the method |
| KR20130014912A (en) * | 2011-08-01 | 2013-02-12 | 신광섭 | The phytoncide composition and phytoncide composition releasing package |
| JP2014151137A (en) * | 2013-02-14 | 2014-08-25 | Ichimaru Pharcos Co Ltd | Deodorant and uses of the same |
| KR20160042586A (en) * | 2014-10-10 | 2016-04-20 | 박흥순 | Armoma compositon, and aroma products using the same |
| JP6577885B2 (en) * | 2016-02-18 | 2019-09-18 | 夢木香株式会社 | Deodorants |
Non-Patent Citations (1)
| Title |
|---|
| 인터넷 자료(2019.04.23. 9:18)* * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20230034765A (en) | 2021-09-03 | 2023-03-10 | 동의대학교 산학협력단 | A deodorizing composition comprising an salt sandspurry extract as an active ingredient |
| KR102665344B1 (en) * | 2023-11-24 | 2024-05-10 | 주식회사 바이오텍 | Liquid type deodorant using minerals and livestock urine and manufacturing method thereof |
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