KR102003278B1 - Cosmetic composition containing silicon elasticity powder with temporary anti-wrinkles, and manufacturing method thereof - Google Patents
Cosmetic composition containing silicon elasticity powder with temporary anti-wrinkles, and manufacturing method thereof Download PDFInfo
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Abstract
Description
본 발명은 인체의 피부주름을 일시적으로 개선해 주는 화장료 조성물 및 이의 제조방법에 관한 발명이다. The present invention relates to a cosmetic composition for temporarily improving skin wrinkles of a human body and a method for manufacturing the same.
피부의 주름은 여러 가지 요인이 있는 것으로 알려져 있다. 가장 잘 알려진 요인으로는 햇빛을 들 수 있다. 지속적으로 햇빛에 노출되면 진피의 콜라겐 섬유, 탄력 섬유 등의 변성이 초래되고, 피부가 건조해지면서 피부 노화가 일어난다. 그 결과로 주름살이 생길 수 있다.The wrinkles of the skin are known to have various factors. The best known factor is sunshine. Continuous exposure to sunlight causes degeneration of collagen fibers and elastic fibers of the dermis and aging of the skin as the skin becomes dry. As a result, wrinkles can occur.
얼굴표정 또한 주름 생성에 영향을 준다. 근육이 계속 수축하면 피부 주름살이 발생하는데, 이때 발생하는 주름은 일반적으로 다른 원인에 의해 발생한 주름보다 깊다. 중력 또한 영향을 주는데, 중력은 피부를 아래쪽으로 지속적으로 잡아 당겨 늘어지게 만든다.Facial expression also affects wrinkle formation. When the muscles continue to contract, the skin wrinkles develop, and the wrinkles that develop are generally deeper than those caused by other causes. Gravity also affects gravity, which pulls the skin down continuously.
피부의 건조함도 주름에 영향을 주는데, 나이가 들면서 피부의 수분을 유지시켜 주는 샘 기능이 떨어지면서 피부가 건조해지고, 건조해진 피부는 거칠어지고 탄력이 떨어져 주름진다.The dryness of the skin also affects the wrinkles. As the skin ages, the skin becomes dry as the age of the spleen functioning to maintain the moisture of the skin falls, and the dry skin becomes rough and elastic and wrinkles.
그 외에도 담배, 유전적인 소인, 피부 색깔(하얀 피부를 가진 사람들은 쉽게 햇빛 화상을 입게 되므로 주름이 더 생기는 경향이 있다) 등도 주름살 형성에 영향을 준다.In addition, tobacco, genetic scales, and skin color (people with white skin tend to have more wrinkles because they are easily sunburned) also affect the formation of wrinkles.
본 발명은 실리콘탄성분말을 이용하여 일시적으로 피부주름을 개선하는 화장료 조성물에 관한 것이다. 본 발명은 주름의 일시적인 개선을 가능하게 하며, 연속상을 수용성 물질로 감싸주어 피부모공을 막지않아 피부염증을 유발하지 않는다. The present invention relates to a cosmetic composition which improves skin wrinkles temporarily using a silicone elastic powder. The present invention enables temporary improvement of the wrinkles, and the continuous phase is wrapped with a water-soluble substance so as not to block the pores of the skin, thus causing no inflammation of the skin.
선행기술문헌으로는 대한민국 공개특허공보 10-2011-0101237에 발수성 실리콘 탄성중합체 파우더를 포함하는 파운데이션 조성물이, 대한민국 공개특허공보 10-2014-0132371에 피부 케어 조성물에서 사용하기 위한 초흡수성 중합체 및 실리콘 탄성 중합체가, 대한민국 공개특허공보 10-2006-0009904에 실리콘 탄성중합체를 함유하는 개인 케어 조성물이, 대한민국 공개특허공보 10-2016-0096701에 실리콘 미세입자 및 비휘발성 오일을 포함하는 피니셔 조성물이 각각 기재되어 있다. As a prior art document, Korean Patent Laid-Open Publication No. 10-2011-0101237 discloses a foundation composition comprising a water-repellent silicone elastomer powder, which is disclosed in Korean Patent Laid-Open Publication No. 10-2014-0132371 as a superabsorbent polymer for use in a skin care composition, A personal care composition containing a silicone elastomer is disclosed in Korean Patent Laid-Open Publication No. 10-2006-0009904, and a finishing composition comprising silicone microparticles and a nonvolatile oil is disclosed in Korean Patent Laid-Open Publication No. 10-2016-0096701 have.
총괄하여 보면, 실리콘 중합체를 이용한 화장료 조성물이라는 점에서는 일부 유사하나, 상기 선행기술문헌들에는 연속상을 수용성 물질로 감싸주어 주름의 일시적인 개선이 가능하고 피부모공을 막지않는 제조방법에 대해서는 기재되어 있지 않음을 알 수 있다. As a whole, they are similar to each other in that they are cosmetic compositions using a silicone polymer. However, the above prior art documents describe a manufacturing method in which a continuous phase is wrapped with a water-soluble substance to temporarily improve wrinkles and does not block skin pores .
본 발명은 실리콘탄성분말을 이용하여 일시적으로 피부주름을 개선하는 화장료 조성물 및 이의 제조방법을 해결과제로 한다.The present invention provides a cosmetic composition which improves skin wrinkles temporarily using silicone elastic powder and a method for producing the same.
본 발명은 연속상을 수용성 물질로 감싸주어 피부모공을 막지않아 피부염증을 유발하지 않는 화장료 조성물 및 이의 제조방법을 해결과제로 한다. Disclosed is a cosmetic composition which does not block skin pores by wrapping a continuous phase with a water-soluble substance and does not cause skin inflammation, and a manufacturing method thereof.
본 발명에 따르는 과제 해결수단은,According to the present invention,
정제수 82.75중량% 및 부틸렌글라이콜 5중량%를 균질기로 2500rpm으로 5분간 교반하는 제1단계; 82.75% by weight of purified water and 5% by weight of butyleneglycol with a homogenizer at 2500 rpm for 5 minutes;
상기 제1단계 결과물에 실리콘 탄성분말 조성물 10중량%를 투입한 후 균질기로 3000rpm으로 5분간 교반하는 제2단계; A second step of adding 10 wt% of the silicone elastomer powder composition to the result of the first step and stirring the mixture at 3000 rpm for 5 minutes with a homogenizer;
상기 제2단계 결과물에 하이드록시에틸아크릴레이트/소듐아크릴로일다이메틸타우레이트코폴리머를 0.25중량%를 투입한 뒤 균질기로 4000rpm으로 5분간 교반하는 제3단계; 및Adding 0.25% by weight of hydroxyethyl acrylate / sodium acryloyldimethyltaurate copolymer to the result of the second step and stirring the mixture at 4000 rpm for 5 minutes with a homogenizer; And
상기 제3단계 결과물을 45~50℃까지 냉각 시킨 후 1,2-헥산다이올 2중량%를 투입하여 균질기를 이용하여 2500RPM으로 1분간 교반한 뒤, 30℃이하로 냉각하는 제4단계;를 포함하는 것을 특징을로 하는, 화장료 조성물의 제조방법이다.Cooling the resultant of the third step to 45 to 50 ° C, adding 2% by weight of 1,2-hexanediol, stirring the mixture at 2500 RPM for 1 minute using a homogenizer, and cooling to 30 ° C or less; Or a pharmaceutically acceptable salt thereof.
상기에서, 실리콘 탄성분말 조성물은,In the above, the silicone elastic powder composition comprises
다이메티콘/비닐다이메티콘크로스폴리머 분말의 직경이 1~10㎛이며 비중이 1.01이하인 분말 40중량부와 페닐트라이메티콘 20중량부를 균질기를 이용하여 2000RPM으로 5분간 교반시키는 제1단계;A first step of stirring 40 parts by weight of a dimethicone / vinyl dimethicone crosspolymer powder having a diameter of 1 to 10 탆 and a specific gravity of 1.01 or less and 20 parts by weight of phenyl trimethicone using a homogenizer at 2000 RPM for 5 minutes;
상기 제1단계 결과물에 폴리글리세릴-4 올레이트 10중량부를 60℃ 이상에서 투입하여 용해시켜 균질기를 이용하여 2000RPM으로 5분간 교반시키는 제2단계; 및Adding 10 parts by weight of polyglyceryl-4-oleate to the resultant product of the first step at 60 ° C or higher and dissolving the mixture at 2000 RPM for 5 minutes using a homogenizer; And
상기 제2단계 결과물에 유중수형 유화물을 만들기 위해 연속상으로서 글리세린, 말티톨 및 정제수의 4:3:3 중량비율 혼합물 30중량부를 투입하여 균질기를 이용하여 3000RPM으로 5분간 교반시키는 제3단계;를 포함하는 방법으로 제조된다.And 30 parts by weight of a 4: 3: 3 by weight mixture of glycerin, maltitol and purified water as a continuous phase to prepare a water-in-oil emulsion in the second step, and stirring the mixture at 3000 RPM for 5 minutes using a homogenizer .
본 발명에 따르는 과제 해결수단은,According to the present invention,
상기 제조방법으로 제조된 화장료 조성물이다.Is a cosmetic composition prepared by the above production method.
본 발명을 통해, 주름의 일시적인 개선이 가능하며, 연속상을 수용성 물질로 감싸주어 피부모공을 막지않아 피부염증을 유발하지 않는다. Through the present invention, it is possible to temporarily improve the wrinkles, and the continuous phase is wrapped with a water-soluble substance so as not to block the pores of the skin, thus causing no inflammation of the skin.
도 1A 및 도 1B는 실험예 1의 입자관찰 사진이다.
도 2는 본 발명에 따른 조성물의 기능원리를 도시화한 것이다.Figs. 1A and 1B are photographs of particles observed in Experimental Example 1. Fig.
Figure 2 illustrates the functional principle of the composition according to the invention.
이하에서는 본 발명의 이해를 돕기 위하여 실시예 등을 들어 상세히 설명하기로 한다. 그러나, 본 발명에 따른 실시예들은 여러 가지 다른 형태로 변형될 수 있으며, 본 발명의 범위가 하기 실시예들에 한정되는 것으로 해석되어서는 안 된다. 본 발명의 실시예들은 당업계에서 평균적인 지식을 가진 자에게 본 발명을 보다 완전하게 설명하기 위해 제공되는 것이다.Hereinafter, embodiments of the present invention will be described in detail to facilitate understanding of the present invention. However, the embodiments according to the present invention can be modified into various other forms, and the scope of the present invention should not be construed as being limited to the following embodiments. Embodiments of the invention are provided to more fully describe the present invention to those skilled in the art.
제조예 1. 실리콘 탄성분말 조성물Production Example 1. Silicone elastic powder composition
본 발명에 따른 실리콘 탄성분말 조성물은, The silicone elastomer powder composition according to the present invention,
다이메티콘/비닐다이메티콘크로스폴리머 및 비닐다이메티콘/메티콘실세스퀴옥산크로스폴리머 중 한가지 이상이 조합된 실리콘탄성분말;A silicone elastic powder in which one or more of dimethicone / vinyl dimethicone crosspolymer and vinyl dimethicone / methicone silsesquioxane crosspolymer are combined;
페닐트라이메티콘, 다이페닐다이메티콘, 페닐 트리메틸실록시 디페닐실록산, 디페닐 디메티콘 및 디페닐 메틸디페닐 트리실록산 중 한가지 이상의 성분; One or more of the following components: phenyl trimethicone, diphenyl dimethicone, phenyl trimethylsiloxy diphenyl siloxane, diphenyl dimethicone, and diphenyl methyl diphenyl trisiloxane;
흡착력을 증대시키기 위해 폴리글리세릴 유화제중 HLB값이 10이상인 성분 중에서 반고체의 상태인 폴리글리세릴-4 스테아레이트, 폴리글리세릴-4 올레이트, 폴리글리세릴-6미리스테이트, 폴리글리세린-10아이소스테아레이트 및 폴리글리세릴-10 스테아레이트 중 한가지 이상의 성분; 및 Among the polyglyceryl emulsifiers having an HLB value of 10 or more, polyglyceryl-4 stearate, polyglyceryl-4 oleate, polyglyceryl-6 myristate, polyglycerin-10 iso One or more of stearate and polyglyceryl-10 stearate; And
실리콘탄성분말의 모공막힘방지를 낮추기 위한 연속상으로서 글리세린, 말티톨 및 정제수의 적량 혼합물;을 포함하여 구성된다.A suitable mixture of glycerin, maltitol and purified water as a continuous phase for lowering the pore blocking prevention of the silicone elastic powder.
또한, 본 발명에 따른 실리콘 탄성분말 조성물은,Further, the silicone elastomer powder composition according to the present invention,
다이메티콘/비닐다이메티콘크로스폴리머 및 비닐다이메티콘/메티콘실세스퀴옥산크로스폴리머 중 한가지 이상의 것에서 40 내지 80중량부;40 to 80 parts by weight of at least one of dimethicone / vinyl dimethicone crosspolymer and vinyl dimethicone / methicone silsesquioxane crosspolymer;
페닐트라이메티콘, 다이페닐다이메티콘, 페닐 트리메틸실록시 디페닐실록산, 디페닐 디메티콘 및 디페닐 메틸디페닐 트리실록산 중 한가지 이상의 성분 10 내지 50중량부;10 to 50 parts by weight of at least one component of phenyl trimethicone, diphenyl dimethicone, phenyl trimethylsiloxy diphenyl siloxane, diphenyl dimethicone and diphenyl methyl diphenyl trisiloxane;
폴리글리세릴-4 스테아레이트, 폴리글리세릴-4 올레이트, 폴리글리세릴-6 미리스테이트, 폴리글리세린-10 아이소스테아레이트 및 폴리글리세릴-10 스테아레이트 중 한가지 이상의 성분 10중량부; 및 10 parts by weight of at least one component of polyglyceryl-4 stearate, polyglyceryl-4 oleate, polyglyceryl-6 myristate, polyglycerin-10 isostearate and polyglyceryl-10 stearate; And
실리콘탄성분말의 모공막힘방지현상을 저해시키기위해 연속상으로서 글리세린, 말티톨, 정제수의 40:30:30의 중량비율로 혼합한 혼합물을 30 내지 40 중량부;가 포함된다.30 to 40 parts by weight of a mixture of glycerin, maltitol and purified water at a weight ratio of 40:30:30 as a continuous phase in order to inhibit the pore blocking effect of the silicone elastic powder.
제조예 2. 실리콘 탄성분말 조성물의 제조방법 Production Example 2. Production method of silicone elastic powder composition
제조예 1에 따르는 실리콘 탄성분말 조성물의 제조방법의 일예는 다음과 같다. 설계조건에 따라, 하기 수치는 다소간 적절한 범위내에서 조절될 수 있다.An example of a method for producing a silicone elastic powder composition according to Production Example 1 is as follows. Depending on the design conditions, the following values may be adjusted somewhat within a suitable range.
다이메티콘/비닐다이메티콘크로스폴리머 분말의 직경이 1~10㎛이며 비중이 1.01이하인 분말 40중량부와 페닐트라이메티콘 20중량부를 균질기를 이용하여 2000RPM으로 5분간 교반시키는 제1단계;A first step of stirring 40 parts by weight of a dimethicone / vinyl dimethicone crosspolymer powder having a diameter of 1 to 10 탆 and a specific gravity of 1.01 or less and 20 parts by weight of phenyl trimethicone using a homogenizer at 2000 RPM for 5 minutes;
상기 제1단계 결과물에 폴리글리세릴-4 올레이트 10중량부를 60℃ 이상에서 투입하여 용해시켜 균질기를 이용하여 2000RPM으로 5분간 교반시키는 제2단계; 및Adding 10 parts by weight of polyglyceryl-4-oleate to the resultant product of the first step at 60 ° C or higher and dissolving the mixture at 2000 RPM for 5 minutes using a homogenizer; And
상기 제2단계 결과물에 유중수형 유화물을 만들기 위해 연속상으로서 글리세린, 말티톨 및 정제수의 4:3:3 중량비율 혼합물 30중량부를 투입하여 균질기를 이용하여 3000RPM으로 5분간 교반시키는 제3단계;를 포함한다.And 30 parts by weight of a 4: 3: 3 by weight mixture of glycerin, maltitol and purified water as a continuous phase to prepare a water-in-oil emulsion in the second step, and stirring the mixture at 3000 RPM for 5 minutes using a homogenizer do.
제조예 3. 실리콘 탄성분말 조성물을 적용한 화장료 조성물Production Example 3. Cosmetic composition to which silicone elastic powder composition was applied
제조예 1에 따르는 실리콘 탄성분말 조성물을 적용한 화장료 조성물의 조성예는 다음과 같다.An example of the composition of the cosmetic composition to which the silicone elastic powder composition according to Production Example 1 is applied is as follows.
실리콘 탄성분말 조성물; 부틸렌글라이콜; 하이드록시에틸아크릴레이트/소듐아크릴로일다이메틸타우레이트코폴리머; 및 1,2-헥산다이올;을 포함하여 구성한다.Silicone elastic powder composition; Butyleneglycol; Hydroxyethyl acrylate / sodium acryloyl dimethyl taurate copolymer; And 1,2-hexanediol.
바람직하게는, 실리콘 탄성분말 조성물 10중량부; 부틸렌글라이콜 5중량부; 하이드록시에틸아크릴레이트/소듐아크릴로일다이메틸타우레이트코폴리머 0.25중량부; 및 1,2-헥산다이올 2중량부;를 포함하여 구성한다.Preferably, 10 parts by weight of the silicone elastic powder composition; 5 parts by weight of butyleneglycol; 0.25 part by weight of hydroxyethyl acrylate / sodium acryloyldimethyltaurate copolymer; And 2 parts by weight of 1,2-hexanediol.
제조예 4. 실리콘 탄성분말 조성물을 적용한 화장료 조성물의 제조방법Production Example 4. Manufacturing method of cosmetic composition using silicone elastic powder composition
제조예 3에 따르는 화장료 조성물의 제조방법의 일예는 다음과 같다. 설계조건에 따라, 하기 수치는 다소간 적절한 범위내에서 조절될 수 있다.An example of the method for producing the cosmetic composition according to Production Example 3 is as follows. Depending on the design conditions, the following values may be adjusted somewhat within a suitable range.
정제수 82.75중량% 및 부틸렌글라이콜 5중량%를 균질기로 2500rpm으로 5분간 교반하는 제1단계; 82.75% by weight of purified water and 5% by weight of butyleneglycol with a homogenizer at 2500 rpm for 5 minutes;
상기 제1단계 결과물에 실리콘 탄성분말 조성물 10중량%를 투입한 후 균질기로 3000rpm으로 5분간 교반하는 제2단계; A second step of adding 10 wt% of the silicone elastomer powder composition to the result of the first step and stirring the mixture at 3000 rpm for 5 minutes with a homogenizer;
상기 제2단계 결과물에 하이드록시에틸아크릴레이트/소듐아크릴로일다이메틸타우레이트코폴리머를 0.25중량%를 투입한 뒤 균질기로 4000rpm으로 5분간 교반하는 제3단계; 및Adding 0.25% by weight of hydroxyethyl acrylate / sodium acryloyldimethyltaurate copolymer to the result of the second step and stirring the mixture at 4000 rpm for 5 minutes with a homogenizer; And
상기 제3단계 결과물을 45~50℃까지 냉각 시킨 후 1,2-헥산다이올 2중량%를 투입하여 균질기를 이용하여 2500RPM으로 1분간 교반한 뒤, 30℃이하로 냉각하는 제4단계;를 포함한다. Cooling the resultant of the third step to 45 to 50 ° C, adding 2% by weight of 1,2-hexanediol, stirring the mixture at 2500 RPM for 1 minute using a homogenizer, and cooling to 30 ° C or less; .
실험예 1. 제조예 1의 조성 및 제조예 2의 방법 검증Experimental Example 1. Composition of Production Example 1 and Method Validation of Production Example 2
[실험방법][Experimental Method]
하기와 같이 표 1에 기재된 것과 같은 성분 및 함량으로 구성된 실시예의 실리콘 탄성분말 조성물을 제조하였다.Silicone elastic powder compositions of the examples constituted by ingredients and contents as shown in Table 1 were prepared as follows.
A상을 균질기(Homogenizer)를 이용하여 2000RPM으로 5분간 교반 후 B상을 A상에 투입한 후 60℃ 까지 용해하여 5분간 같은 RPM으로 교반하였다. 다음 C상을 투입하여 균질기(Homogenizer) 3000RPM으로 5분간 교반한다.The A phase was agitated for 5 minutes at 2000 RPM using a homogenizer, then the phase B was added to the phase A, and the mixture was dissolved at 60 ° C. and stirred for 5 minutes at the same RPM. Add the following C phase and stir with homogenizer 3000 RPM for 5 minutes.
1Example
One
2Example
2
3Example
3
4Example
4
5Example
5
6Example
6
7Example
7
1Comparative Example
One
40:30:30 중량대비 혼합물Glycerin, maltitol, purified water
40:30:30 Weight to weight mixture
[성능 평가 1][Performance evaluation 1]
하기 표 2와 같이, 실시예 및 비교예의 도포시 주름사이의 부착성을 측정하기 위해 Brookfield CT3 TA-SF를 이용하여 부착력을 측정하였다. 측정조건은, Target Value: 10.0mm, Trigger Load: 1.0g, Test Speed: 1.0mm/s, Sample Temperature: 25±3℃As shown in the following Table 2, the adhesion was measured using Brookfield CT3 TA-SF in order to measure the adhesion between the wrinkles at the time of application of the examples and the comparative examples. The measurement conditions were: Target Value: 10.0 mm, Trigger Load: 1.0 g, Test Speed: 1.0 mm / s, Sample Temperature: 25 3
또한 도 1A, 도 1B와 같이 실시예 및 비교예의 실리콘탄성분말의 응집도를 측정하기 위해 입자관찰을 실시하였다. 입자관찰은 Olympus社의 BX43을 이용하여 400배율, 편광모드로 촬영하였다.1A and 1B, particle observations were made to measure the cohesion degree of the silicone elastic powder of the examples and comparative examples. Particle observations were taken using a BX43 from Olympus at 400 magnification and polarization mode.
결과를 검토하여 보면, 다이메티콘/비닐다이메티콘크로스폴리머가 50중량% 이상 함유될 경우 응집되어 분산성이 우수하지 못함을 알 수 있고, 다이메티콘/비닐다이메티콘크로스폴리머가 20 ~ 30중량% 에서는 대체적으로 양호해 보이지만 구형실리콘파우더의 분포가 적거나 복합물의 입자사이즈가 커짐을 알 수 있다.As a result, it can be seen that when the dimethicone / vinyl dimethicone crosspolymer is contained in an amount of 50 wt% or more, it is aggregated and the dispersibility is not excellent, and the dimethicone / vinyl dimethicone crosspolymer is 20 ~ 30% by weight, it is seen that the distribution of the spherical silicone powder is small or the particle size of the composite is large.
점착력에서, 실시예 3, 실시예 5가 점착력이 가장 우수함을 알 수 있다.From the adhesive force, it can be seen that the adhesive force of Examples 3 and 5 is the most excellent.
따라서 다이메티콘/비닐다이메티콘크로스폴리머가 40중량% 함유된 실시예 5가 점착력이 뛰어나며 입자가 상당히 안정하게 분포하고, 사이즈가 고른것으로 판단할 수 있다.Therefore, it can be judged that Example 5 containing 40% by weight of dimethicone / vinyl dimethicone crosspolymer is excellent in adhesion, particles are distributed fairly stably, and the size is uniform.
[성능평가 2][Performance evaluation 2]
실리콘탄성분말은 흡유하는 성질을 지니고 있어 피부에 도포시 인체에서 나오는 유분에 의해 피부에 흡착되어 고정되어 있다. 그래서 일반적인 세정법으로는 좀처럼 제거가 힘들거나 꼼꼼한 세정이 필요하며 잘 씻겨나가지 않은 물질들이 모공이나 주름등에 존재하여 피부염증을 일으키거나 Comedogenic을 발생시키는 원인이 된다.Silicone elastic powder has the property of oil absorption, and is adsorbed on the skin by the oil coming from the human body when it is applied to the skin and fixed. Therefore, it is difficult to remove by ordinary cleaning method, or it needs to be thoroughly cleaned and materials which are not washed well are present in the pores or wrinkles, causing skin irritation or causing comedogenic.
그리하여 모공을 막지 않게하기 위해 연속상이 수계인 것을 확인하기 위해 표3 과 같이 실시예 및 비교예의 수용화도를 평가하였다. 도 2를 참조하여 보면 조성물이 도포되기 전과 후에는 연속상이 수계인 경우 일시적인 주름 완화효과가 발생됨을 알 수 있다.The degree of water solubility of the examples and comparative examples was evaluated as shown in Table 3 to confirm that the continuous phase was a water system so as not to block the pores. Referring to FIG. 2, it can be seen that a temporary wrinkle relaxation effect occurs when the continuous phase is water-based before and after the composition is applied.
수용화도의 측정방법은 10% 함량의 실시예 및 비교예에 정제수 95% 함량을 투입하여 디스퍼믹서 1000rpm으로 5분 교반 후 수용화도를 측정한다.For the measurement of the degree of water-solubility, 95% of purified water is added to 10% of the Example and Comparative Example, and the degree of water-solubility is measured after stirring for 5 minutes at 1000 rpm in a Dispermixer.
◎ : 매우안정 ○ : 안정 △ : 보통 Ｘ : 불안정?: Very stable?: Stable?: Normal X: unstable
실시예 5의 수용화도가 매우 우수한 것으로 평가되었다. The degree of water-solubility of Example 5 was evaluated to be very good.
단, 실시예 7 및 비교예 2는 수용화도가 매우 안정함을 알 수 있으나 이는 다이메티콘/비닐다이메티콘이 미투입 또는 10중량% 이하인 것에 기인한다.However, in Example 7 and Comparative Example 2, it can be seen that the degree of water solubility is very stable, but it is due to the fact that dimethicone / vinyl dimethicone is not added or 10 wt% or less.
실험예 2. 제조예 3의 조성 및 제조예 4의 방법 검증Experimental Example 2. Composition of Production Example 3 and Verification of Production Example 4
표 4와 같이 가장 성능이 좋을 것으로 예측되는 것 중 일부인 실시예 1, 3, 5를 이용하여 유중수형 타입의 화장품 실시예 8, 9, 10를 제조하였다. 또 비교를 위해 비교예 1을 이용해 같이 비교예 3을 제조하였다.Examples 8, 9 and 10 of water-in-oil type were prepared using Examples 1, 3 and 5, which are expected to have the best performance as shown in Table 4. For comparison, Comparative Example 3 was also prepared using Comparative Example 1.
그리고 보다 객관적인 평가를 위해 최소한의 원료만을 이용하여 평가하였다.And, for more objective evaluation, only the minimum amount of raw materials was evaluated.
제조방법은 아래와 같다.The manufacturing method is as follows.
A상을 상온에서 균질기(Homogenizer)를 이용하여 2500RPM으로 5분간 교반 후 B상을 A상에 투입하여 균질기를 이용하여 3000RPM으로 5분간 교반한다. 분산이 잘 되었는지 확인 후 C상을 A상에 투입 한 뒤 5분간 균질기를 이용하여 4000RPM으로 교반한다. 그 후 D상을 투입하여 균질기를 이용하여 2500RPM으로 1분간 교반 한 뒤 공정을 종료한다. The A-phase was stirred at room temperature for 5 minutes at 2500 RPM using a homogenizer. The B-phase was added to the A-phase and stirred for 5 minutes at 3000 RPM using a homogenizer. After confirming that the dispersion is good, the C phase is put into the phase A and stirred for 5 minutes at 4000 RPM using a homogenizer. Thereafter, the D phase is added and stirred for 1 minute at 2500 RPM using a homogenizer, and the process is terminated.
[성능평가][Performance evaluation]
표 5와 같이, 구형실리콘분말의 고질적인 문제점인 수계에서의 고온안정성을 평가하기 위해 고온의 50℃ 챔버에서 1달간 제형의 안정도와 제형의 표면 안정도-실리콘탄성분말은 시간이 지날수록 표면에 떠오르려는 성질을 가진다- 를 평가하고 또 피부 도포 후의 발림성 및 주름가림성에 대한 관능평가를 실시하였다.The stability of the formulation and the surface stability of the formulation for one month in a high temperature 50 ° C chamber to evaluate the high temperature stability in the aqueous system, which is a chronic problem of spherical silicon powder, as shown in Table 5 - silicon elastomer powder floats on the surface over time . The sensory evaluations were carried out on the spreadability and wrinkle blocking ability after application of the skin.
주름 가림성Temporary after application
Wrinkle blocking ability
◎ : 양호 ○ : 보통 △ :미흡 Ｘ : 불량?: Good?: Normal?: Poor X: Bad
위에서와 같이 실시예 5를 적용한 실시예 10이 원료안정도, 관능평가 및 휘발도 등 여러 척도에서 현저히 개선된 성능을 나타냄을 알 수 있다. 다시말해, 제조예 1 내지 4를 이용하여 제조된 실시예 5 및 10의 성능이 우수한 것이 검증되었다고 할 수 있겠다.As described above, it can be seen that Example 10 to which Example 5 was applied shows remarkably improved performance on various scales such as raw material stability, sensory evaluation and volatility. In other words, it can be said that the performance of Examples 5 and 10 prepared using Production Examples 1 to 4 was proved to be excellent.
이상의 설명은 본 발명의 기술 사상을 예시적으로 설명한 것에 불과한 것으로서, 본 발명이 속하는 기술 분야에서 통상의 지식을 가진 자라면 본 발명의 본질적인 특성에서 벗어나지 않는 범위에서 다양한 수정 및 변형이 가능할 것이다. The foregoing description is merely illustrative of the technical idea of the present invention, and various changes and modifications may be made by those skilled in the art without departing from the essential characteristics of the present invention.
따라서, 본 발명에 개시된 실시 예들은 본 발명의 기술 사상을 한정하기 위한 것이 아니라 설명하기 위한 것이고, 이러한 실시 예에 의하여 본 발명의 기술 사상의 범위가 한정되는 것은 아니다. 본 발명의 보호 범위는 아래의 청구범위에 의하여 해석되어야 하며, 그와 동등한 범위 내에 있는 모든 기술 사상은 본 발명의 권리범위에 포함되는 것으로 해석되어야 할 것이다.Therefore, the embodiments disclosed in the present invention are intended to illustrate rather than limit the scope of the present invention, and the scope of the technical idea of the present invention is not limited by these embodiments. The scope of protection of the present invention should be construed according to the following claims, and all technical ideas within the scope of equivalents should be construed as falling within the scope of the present invention.
Claims (3)
상기 제1단계 결과물에 최종 화장료 조성물의 총 중량을 기준으로 실리콘 탄성분말 조성물 10중량%를 투입한 후 균질기로 3000rpm으로 5분간 교반하는 제2단계;
상기 제2단계 결과물에 최종 화장료 조성물의 총 중량을 기준으로 하이드록시에틸아크릴레이트/소듐아크릴로일다이메틸타우레이트코폴리머를 0.25중량%를 투입한 뒤 균질기로 4000rpm으로 5분간 교반하는 제3단계; 및
상기 제3단계 결과물을 45~50℃까지 냉각 시킨 후 최종 화장료 조성물의 총 중량을 기준으로 1,2-헥산다이올 2중량%를 투입하여 균질기를 이용하여 2500RPM으로 1분간 교반한 뒤, 30℃이하로 냉각하는 제4단계;를 포함하고,
상기 실리콘 탄성분말 조성물은,
다이메티콘/비닐다이메티콘크로스폴리머 분말의 직경이 1~10㎛이며 비중이 1.01이하인 분말 40중량부와 페닐트라이메티콘 20중량부를 균질기를 이용하여 2000RPM으로 5분간 교반시키는 제1단계;
상기 제1단계 결과물에 폴리글리세릴-4 올레이트 10중량부를 60℃ 이상에서 투입하여 용해시켜 균질기를 이용하여 2000RPM으로 5분간 교반시키는 제2단계; 및
상기 제2단계 결과물에 유중수형 유화물을 만들기 위해 연속상으로서 글리세린, 말티톨 및 정제수의 4:3:3 중량비율 혼합물 30중량부를 투입하여 균질기를 이용하여 3000RPM으로 5분간 교반시키는 제3단계;를 포함하는 방법으로 제조되는 것을 특징으로 하는, 화장료 조성물의 제조방법.
82.75% by weight of purified water and 5% by weight of butylene glycol based on the total weight of the final cosmetic composition are stirred with a homogenizer at 2500 rpm for 5 minutes;
Adding 10 wt% of the silicone elastic powder composition to the resultant product of the first stage based on the total weight of the final cosmetic composition, and then stirring the mixture at 3000 rpm for 5 minutes with a homogenizer;
In the second step, 0.25% by weight of hydroxyethyl acrylate / sodium acryloyldimethyltaurate copolymer was added to the final cosmetic composition based on the total weight of the final cosmetic composition, and the mixture was stirred at 4000 rpm for 5 minutes with a homogenizer ; And
After cooling the resultant of the third step to 45 to 50 ° C, 2 wt% of 1,2-hexanediol was added thereto based on the total weight of the final cosmetic composition, stirred at 2500 RPM for 1 minute using a homogenizer, Or less, and the fourth step of cooling
Wherein the silicone elastomer powder composition comprises:
A first step of stirring 40 parts by weight of a dimethicone / vinyl dimethicone crosspolymer powder having a diameter of 1 to 10 탆 and a specific gravity of 1.01 or less and 20 parts by weight of phenyl trimethicone using a homogenizer at 2000 RPM for 5 minutes;
Adding 10 parts by weight of polyglyceryl-4-oleate to the resultant product of the first step at 60 ° C or higher and dissolving the mixture at 2000 RPM for 5 minutes using a homogenizer; And
And 30 parts by weight of a 4: 3: 3 by weight mixture of glycerin, maltitol and purified water as a continuous phase to prepare a water-in-oil emulsion in the second step, and stirring the mixture at 3000 RPM for 5 minutes using a homogenizer Wherein the cosmetic composition is prepared by a method comprising the steps of:
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Cited By (1)
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| KR20220039077A (en) * | 2020-09-21 | 2022-03-29 | 주식회사 투래빗코스메틱 | Sheet type makeup-boosting cosmetics |
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