KR101818808B1 - A cosmetic composition for anti-wrinkle and skin whitening effect - Google Patents

A cosmetic composition for anti-wrinkle and skin whitening effect Download PDF

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KR101818808B1
KR101818808B1 KR1020150095247A KR20150095247A KR101818808B1 KR 101818808 B1 KR101818808 B1 KR 101818808B1 KR 1020150095247 A KR1020150095247 A KR 1020150095247A KR 20150095247 A KR20150095247 A KR 20150095247A KR 101818808 B1 KR101818808 B1 KR 101818808B1
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oil
cosmetic composition
extract
whitening
acid
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KR20170004631A (en
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김혜정
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김혜정
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41Particular ingredients further characterized by their size
    • A61K2800/413Nanosized, i.e. having sizes below 100 nm

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Abstract

The present invention relates to a cosmetic composition for improving whitening and wrinkles, and more particularly, to a cosmetic composition for improving whitening and wrinkles, which comprises 1 to 2: 1 to 2: 1 to 1: 2, 2. ≪ / RTI > The present invention relates to a cosmetic composition for whitening and wrinkle improvement.
According to the present invention, the cosmetic composition for whitening and wrinkling improves whitening action of the skin and improves wrinkles. The cosmetic composition of the present invention improves the appearance of the skin exposed to an unfavorable external environment and irritant chemicals, There is an effect to protect. In addition, the compositions derived from natural products are significantly effective for skin whitening and wrinkle-reducing cosmetic products because skin irritation is much lower.

Description

A cosmetic composition for anti-wrinkle and skin whitening effect,

The present invention relates to a cosmetic composition for whitening and wrinkle improvement.

Hyperpigmentation of the skin can be caused by various factors such as endocrine disorders, genetic diseases, and ultraviolet irradiation after the inflammation reaction of the skin. The main factor is the melanin pigment synthesis abnormality and distribution.

The main function of melanin is to protect the skin from damage by removing oxygen radicals. Therefore, a large number of melanins means that they have an effective countermeasure to protect the skin from physical and chemical toxicants. The production of melanin is accomplished by the action of tyrosine (tyrosinase) in melanocytes and then by the action of enzymes and the spontaneous oxidation reaction of tyrosinase (Dopaquinone). Therefore, the method of inhibiting melanin production to prevent the skin from becoming dark can be largely divided as follows. First, by blocking ultraviolet rays to remove the main cause of melanin production, this method can be expected to have good results by allowing the cosmetic composition to contain a light scattering agent or a light blocking agent.

Second, tyrosinase, such as glucosamine, inhibits the production of melanin by inhibiting the synthesis of core carbohydrates required for activity.

Third, there is a way to interfere with the function of tyrosinase, an enzyme involved in melanin production, such as kojic acid or arbutin.

Fourth, there is a method of inhibiting cell division because it has specific toxicity to melanocytes, such as hydroquinone, which produces melanin.

In addition, there is a method of decolorizing the produced melanin.

In order to suppress the production process of melanin as described above, conventionally, ascorbic acid, kojic acid, arbutin, hydroquinone, and extracts of natural plant have been used as whitening raw materials come. However, kojic acid or arbutin, which is a representative whitening raw material, is poor in product safety despite its strong whitening effect, and is problematic due to decomposition, coloring, occurrence of odor, efficacy at a living body level, The use thereof is limited.

In recent years, whitening raw materials using natural plant extracts, which have been used for a long time as folk remedies, are recognized as safe for human body, and they are attracting attention as a raw material for whitening coating agents.

Therefore, it is necessary to study the whitening raw material using the extract of natural plant which is excellent in whitening action and safe to human body.

As related prior arts, Korean Patent No. 10-1136822 entitled " Antioxidant or Whitening Composition Comprising Fruit Extract Extract "includes 4-n-butylresorcinol, 4-n-butylresorcinol, Discloses an antioxidant or whitening composition containing quercetin and camphorol as an active ingredient. Korean Patent No. 10-1050237 entitled "Functional Cosmetic Composition Using Pine Bark Extract" contains proanthocyanidin as an active ingredient to cause skin whitening, improve wrinkles, maintain adequate moisture and elasticity To a functional cosmetic composition.

It is a technical object of the present invention to provide a cosmetic composition which is stable and has an effect of whitening and wrinkle improvement.

According to an aspect of the present invention,

Characterized in that it contains a complex mixture of Rhodiola extract, Rhodiola extract, Pine bark extract, and gum marinolenic acid-4-n-butyl resorcinol emulsion in a weight ratio of 1: 2: 1 to 2: 1 to 2 Thereby providing a cosmetic composition for improvement.

In the present invention, the gammerminolenic acid-4-n-butylresorcinol emulsion comprises 4-n-butylresorcinol, gum marinolanic acid, an emulsifier, amino acid and dextrin.

In the present invention, the gamma-marinolenic acid-4-n-butylresorcinol emulsion is characterized by containing gamma-linolenic acid-4-n-butylresorcinol nanoliposome having a particle size of 10 to 100 nm.

In the present invention, the composite is contained in an amount of 45 to 90% by weight based on the total weight of the cosmetic composition.

Further, in the present invention,

1 to 5% by weight of at least one herbal essential oil selected from lavender essential oil, jasmine essential oil, rosemary essential oil, chamomile essential oil, position hazel essential oil and ylang ylang essential oil; 9 to 25% by weight of at least one moisturizing oil selected from olive oil, argan oil, avocado oil, jojoba oil, camellia oil, grape seed oil and evening primrose oil; 5 to 15% by weight of at least one moisturizer selected from glycerin, honey and aloe vera gel; And 10-15 wt% of an emulsifier selected from olive oil wax and shea butter.

In the present invention, the composition may further comprise at least one additive selected from vitamin E, alginic acid, and grapefruit seed extract.

In the present invention, the cosmetic composition may be formulated into a lotion, essence, lotion, cream, pack, gel, ointment, patch, spray, mask sheet and detergent.

The cosmetic composition for whitening and wrinkle improvement of the present invention causes whitening action of the skin and improves wrinkles and protects skin exposed to an unfavorable external environment and irritant chemicals such as yellow sand by the heavy metal adsorption function It is effective. In addition, the compositions derived from natural products are significantly effective for skin whitening and wrinkle-reducing cosmetic products because skin irritation is much lower.

Hereinafter, the present invention will be described in more detail.

The present invention relates to a cosmetic composition for skin whitening and wrinkle improvement. More specifically, the present invention relates to a cosmetic composition for skin whitening and wrinkle improvement, which comprises 1 to 2: 1 to 2: 1 to 1: 2, 2. ≪ / RTI > The present invention relates to a cosmetic composition for whitening and wrinkle improvement.

The cosmetic composition of the present invention can exhibit hydrogen peroxide-induced cytotoxicity, tyrosinase activity, and melanin synthesis inhibitory function by including the Rhodiola extract. In particular, the cosmetic composition of the present invention comprising a water-soluble red ginseng extract has excellent tyrosinase activity inhibiting action.

Rhodiola Sachalinensis A. Bor (Rhodiola Sachalinensis A. Bor) is a perennial herbaceous plant inhabiting a high mountainous region of about 2000 to 5000 meters above sea level. Hong Kyung Chun has a special adaptability that can survive even in high altitude area where sunshine is large and dry, oxygen is lean and ultraviolet ray is strong, and it is also called alias such as alpine lake or alpine lake. The major components of Hong Kyung Chun include salicyloids, tyrosol, and glycosides as well as starch, proteins, fats, sugars, flavones, amino acids, inorganic elements, and minor essential oils.

The Rhodiola extract used in the present invention can be obtained by a conventional extraction method. Specifically, the dried Rhodiola can be sufficiently dried in the shade, and then cut into a cutter or pulverized by a crusher to make a starting material of the extract. Thereafter, an extraction solvent is added to the starting material, the active ingredient is extracted at room temperature, and the solid material is removed by filtration, and the filtrate can be concentrated under reduced pressure.

The extraction solvent for extracting the active ingredient from the above-mentioned Hong-Kyung Stream is not limited thereto, but ethanol, petroleum ether, chloroform, ethylacetate and butanol are added successively to obtain a non-aqueous precipitate, a petroleum ether extract , Chloroform extract, ethyl acetate extract, butanol extract, and water-soluble extract.

The cosmetic composition of the present invention contains a pine bark extract to lower the melanin and erythema index of the skin to have a whitening effect and to maintain moisturizing and elasticity of the skin to prevent wrinkles.

The proanthocyanidins contained in the pine bark bark extract are a kind of plant polyphenols and have a strong antioxidant ability. They are present in many kinds of plant leaves, fruit peels, seeds and the like, and have a synergistic effect, antioxidant effect, Effect.

In one embodiment of the present invention, when the pine bark is subjected to hot water extraction, the pine bark is pulverized to obtain a hot water extract of pine bark. At this time, the pine bark can be used for hot water extraction with a powder of 10-300 mesh and a powder of 80-200 mesh.

In order to lower the content of neutral sugar in the pine bark extract and to increase the content of proanthocyanidin as a functional ingredient, a part of the filtered hot water extract was concentrated again, and anhydrous alcohol Can be processed.

In addition, when the precipitate formed on the pine bark extract is filtered and removed, the filtration can be performed at least once using at least one selected from a filter paper, a filter cloth, and a filter.

Examples of the pine bark include Pinus densiflora, Pinus thunbergii, Pinus contorta, Pinus rigida, Pinus taeda, Pinusradiata, Pine bark (Pinus rigitaeda), Pinus banksiana (Pinus banksiana), Pinus serotina (Pinus serotina).

It is preferable that the pine bark is obtained from bark of pine tree having an age of 20 years or more, preferably 20 to 100 years from the viewpoint of obtaining proanthocyanidin.

In addition, the pine bark extract has a function of adsorbing heavy metals, and thus can be used in anti-yellowing cosmetics. In particular, the pine bark extract can adsorb cadmium ions in an aqueous solution state.

In addition, the cosmetic composition of the present invention is excellent in whitening effect due to its low skin irritation and extremely excellent melanin synthesis inhibitory action, by containing a water-soluble sodium persimmono-4-n-butylresorcinol emulsion as an active ingredient.

The water-soluble citrus marinolenic acid-4-n-butylresorcinol emulsion is prepared by liposomalization of 4-n-butylresorcinol and gum marinolenic acid with a phospholipid by a conventional method and then converting the unsaturated lipid to a water- Method. ≪ / RTI > 4-n-butylresorcinol emulsion, specifically comprising emulsifying 4-n-butylresorcinol and 4-n-butylresorcinol by mixing them with an emulsifier, amino acid and dextrin . The thus prepared gum marinolenic acid-4-n-butyl resorcinol emulsion contains gum marinolenic acid-4-n-butyl resorcinol nanoliposome.

The particle size of the gum marinolenic acid-4-n-butylresorcinol nanoliposome prepared by the above method is 10 to 100 nm, more preferably 50 nm or less, and most preferably 33 to 49 nm have.

By using amino acids together in the preparation of the gastrin marinolenic acid-4-n-butylresorcinol nanoliposome of the present invention, liposomes can be rendered water-soluble to use liposomes in water-soluble products. At this time, amino acid is used as a very useful material which greatly increases the solubility of liposome in water, and can be selected from all essential amino acids such as methionine, phenylalanine, and arginine.

The cosmetic composition containing the sodium persimmonolen-4-n-butylresorcinol emulsion of the present invention is easily browsed and increases the stability of 4-n-butylresorcinol, which is irritating to the skin, And it is safe for human skin by reducing inflammation. In addition, gamma-marinolic acid nanoliposome containing 4-n-butylenesinol has an effect of greatly increasing melanin production inhibitory effect, and thus has an effect of greatly increasing the efficacy of 4-n-butylresorcinol relative to the content thereof.

In addition, the cosmetic composition of the present invention can be prepared by mixing the above-mentioned Rhodiola extract, pine bark extract, and gamma-marinolanic acid-4-n-butylresorcinol emulsion at a specific ratio, thereby improving skin whitening, wrinkles, And the effect of protecting the skin exposed to the environment and the irritating chemicals can be increased by synergistic action. The above-mentioned effects can be attained by using the above-mentioned Rhodiola extract, pine bark extract, persimmonolenic acid-4-n- Nol emulsion is mixed in a weight ratio of 1: 2: 1 to 2: 1: 2. When mixed at the above ratios, skin whitening, wrinkle improvement and skin protection effect by the heavy metal adsorption function can be maximized by the Rhodiola extract, pine bark extract, and gum marinolan-4-n-butyl resorcinol emulsion. More preferably, the composite is prepared by mixing in a weight ratio of 1: 1: 2.

The composite is contained in an amount of 45 to 90% by weight based on the total weight of the cosmetic composition.

In the cosmetic composition of the present invention, preferably 1 to 5% by weight of at least one herbal essential oil selected from the group consisting of lavender essential oil, jasmine essential oil, rosemary essential oil, chamomile essential oil, position hazel essential oil and ylang ylang essential oil; 9 to 25% by weight of at least one moisturizing oil selected from olive oil, argan oil, avocado oil, jojoba oil, camellia oil, grape seed oil and evening primrose oil; 5 to 15% by weight of at least one moisturizer selected from glycerin, honey and aloe vera gel; And 10-15 wt% of an emulsifier selected from olive oil wax and shea butter.

In the cosmetic composition of the present invention, the lavender essential oil of the herbal essential oil is effective for skin cleansing and wounds treatment, and jasmine essential oil is effective for all skin and is effective for calming and restoring dry and damaged skin and sensitive skin, Rosemary essential oil is known to be effective when there is skin trouble such as facial or body rash or itching. In addition, chamomile essential oil has anti-allergy, skin soothing, anti-inflammation and anti-cancer effects, and position hazel essential oil and ylang ylang essential oil provide nutrient and moisture to rough skin and dry skin, , It is good for dry skin and is known to have a soothing effect on the skin. Therefore, the cosmetic composition of the present invention contains the herbal essential oil, thereby controlling the viscosity of the composition and improving the effect of soothing, anti-inflammation, moisturizing, etc. of the essential oil of the herb, thereby improving the relieving and improving effect of the atopic symptoms. At this time, if the herbal essential oil is contained in an amount of less than 1% by weight, the effect of the essential oil of the herb may not be exhibited. If it exceeds 5% by weight, the viscosity of the herbal essential oil may be lowered. By weight based on the total weight of the composition.

In addition, in the cosmetic composition of the present invention, the moisturizing oil is a substance that imparts viscous and oily properties to the cosmetic composition. It enhances the moisture retention of the cosmetic composition, protects the skin by forming an oil film on the skin, . In particular, the olive oil provides excellent moisture resistance, and it contains vitamin A and vitamin E, so it has excellent antioxidative effect, so that it calms the skin and maintains a healthy and healthy skin. In addition, the argan oil is effective for preventing aging / wrinkles, atopic skin, skin elasticity, and skin inflammation. The avocado oil has an effect of skin moisturizing and skin regeneration. Jojoba oil promotes the spreading and lubrication of the skin, It absorbs quickly through the skin. It contains a complex of minerals and vitamins that softens the skin and is effective in moisturizing and cleansing. Camellia oil, grape seed oil, and evening primrose oil also protect the skin's lipid layer against atopic dermatitis patients. At this time, when the moisturizing oil is contained in an amount of less than 9% by weight, viscosity and oiliness are insufficient to exhibit the effect. When the amount of the moisturizing oil is more than 25% by weight, the viscosity is lowered, Preferably from 9 to 25% by weight.

Also, in the cosmetic composition of the present invention, the moisturizing agent is a substance that prevents evaporation of oil / water in the skin and improves the moisturizing power. The moisturizing agent is used in an amount of 5 to 15% by weight As shown in Fig.

In addition, in the cosmetic composition of the present invention, the emulsifier is used as an additive of the cosmetic composition. If the emulsifier is less than 10% by weight, the effect is insufficient and is not preferable. There is a fear that the spreadability may be lowered.

As described above, the cosmetic composition of the present invention contains herbal essential oil, moisturizing oil, moisturizing agent, and emulsifier while containing the Rhodiola extract, pine bark extract, and gum marinolan-4-n-butylresorcinol emulsion as an active ingredient, The present invention relates to a cosmetic composition comprising a cosmetic composition and a cosmetic composition. The cosmetic composition of the present invention can be used as a cosmetic composition, Skin whitening, antioxidant ability, etc., while improving the preference, moisturizing power and the like.

In addition, the cosmetic composition of the present invention may further comprise at least one additive selected from vitamin E, alginic acid, and grapefruit seed extract. Such an additive acts as a preservative of the cosmetic composition, more preferably 1 to 5% by weight based on the total weight of the cosmetic composition. When the content is less than 1% by weight, the effect is insignificant. When the content is more than 5% by weight, the preservation effect is not remarkable, which is not preferable.

The cosmetic composition for whitening and wrinkle improvement according to the present invention can be manufactured into various cosmetics such as lotion, essence, lotion, cream, pack, gel, ointment, patch, spray, mask sheet and detergent. At this time, it may further include a chemically acceptable additive.

Hereinafter, the constitution and effects of the present invention will be described in more detail with reference to examples, comparative examples and test examples. However, these examples, comparative examples and test examples are provided for illustrative purposes only in order to facilitate understanding of the present invention, and the scope and scope of the present invention are not limited thereto.

≪ Example 1 > Production of Hongikong Stream Extract

Hong Kyung Chun was washed with purified water, dried and pulverized to obtain a Hong Kyung Stream fine powder. 1 kg of the above-mentioned Hongryeocheon fine powder was mixed with 5 L of a 70% aqueous ethanol solution as an extract solvent, and reacted at room temperature for 5 days. The precipitate of the mixed solution was filtered with Watman filter paper, and the filtrate was concentrated in a rotary vacuum evaporator at 65 ° C to remove ethanol. Distilled water was mixed with the concentrate to obtain a non-aqueous precipitate and a supernatant. At this time, the non-aqueous precipitate may be dissolved in a DMSO solution or a 50% ethanol aqueous solution to be used as an aqueous non-aqueous precipitate solution. Petroleum ether was added to the supernatant to separate the upper and lower layers, and the upper layer was obtained by calling it as a petroleum ether extract. After obtaining the lower layer, chloroform was added to separate the upper and lower layers, and then the upper layer was obtained as a chloroform-extracted fraction. The lower layer was again separated into upper and lower layers by adding ethyl acetate, and the upper layer was obtained as an ethylacetate extract. Butanol was added to the lower layer in the same manner to obtain a butanol extract, and the fraction not extracted in the butanol was obtained by calling it as a water-soluble red ginseng extract.

Example 2: Preparation of bark extract of pine bark

In order to prepare pine extract, 30kg (base weight) of Radiata pine bark powder was used. Radiata pine bark powder was extracted at 100 캜 for 1 hour under the condition of liquid 10. The extract was filtered with a 200 mesh filter and concentrated under reduced pressure at 50 ° C or lower. The precipitate formed upon concentration was filtered off with a 10 탆 stick-shaped cartridge. In order to lower the content of neutral sugar in the extract and to increase the content of proanthocyanidin as a functional ingredient, a part of the filtered hot water extract was concentrated again, and anhydrous alcohol was treated to remove neutral sugars and the like. The resulting precipitate was filtered through a 10 탆 stick-shaped cartridge.

≪ Example 3 > Preparation of emulsified tonmarinolenic acid-4-n-butylresorcinol

To make 4-n-butylresorcinol into nanoliposome, 100 g of L-arginine was completely dissolved in 1 kg of tertiary distilled water at a temperature of 55 DEG C, 200 g of borax oil was slowly added thereto, and the mixture was stirred at 2500 rpm Lt; / RTI > Then, 3 g of soybean lecithin (for food) and 70 g of 4-n-butylresorcinol, which were emulsifiers, were slowly added thereto, followed by cooling to 4 ° C and stirring at a stirring speed of 5000 rpm. 100 g of dextrin was added at 4 캜 to the uniformity, fineness and stabilization of the particle size of the liposome thus formed, and the mixture was vigorously stirred at a stirring speed of 10000 rpm to obtain 33 mg to 49 nM gum marinolenic acid-4-n- An emulsion containing a nanol nanoliposome was prepared.

< Manufacturing example  1 to 6> Cosmetics  Preparation of composition

4-n-butylresorcinol emulsion was prepared, the temperature of the extract was adjusted to 60 ° C, and the emulsifier was heated at 70 ° C to prepare a solution state , An emulsifier, herbal essential oil, a moisturizing oil and a moisturizing agent were mixed with each of the above extracts, and the mixture was stirred while being maintained at 70 캜. Thereafter, the mixture was gradually cooled to prepare a lotion-type cosmetic composition. Olive oil wax was used as an emulsifying agent used in the preparation. Ylang Ylang essential oil was used as a herbal essential oil, olive oil was used as a moisturizing oil, and glycerin was used as a moisturizing agent.

The composition according to each example is shown in Table 1 below.

Production Example 1 Production Example 2 Production Example 3 Production Example 4 Production Example 5 Production Example 6 Hong Kyung Chun Extract 40g 30g 30g - 60g 60g Pine bark extract 40g 60g 30g 60g - 60g Gum marinolenic acid-4-n-butyl resorcinol emulsion 40g 30g 60g 60g 60g - Emulsifier 20g 20g 20g 20g 20g 20g Herbal Essential Oil 3g 3g 3g 3g 3g 3g Moisturizing oil 27g 27g 27g 27g 27g 27g Moisturizer 12g 12g 12g 12g 12g 12g

<Test Example> Sensory Evaluation on Cosmetic Composition

The sensory evaluation of the cosmetic compositions prepared in Preparation Examples 1 to 5 was carried out. The cosmetic composition prepared in Preparation Examples 1 to 5 and the commercially available anti-aging lotion A (manufacturer: 00) and the whitening lotion B (manufacturer: 00) were used as Comparative Examples 1 and 2, Respectively.

At this time, the subject was evaluated by subjecting 21 adult women (three per each cosmetic composition) having no skin allergy symptoms of 20 years old or more to the skin at least twice a day for at least one week.

The evaluation score was in the range of 1 to 5, and the best score was 5 points. The results are shown in Table 3 below. (1: very bad, 2: bad, 3: normal, 4: good, 5: very good)

Production Example 1 Production Example 2 Production Example 3 Production Example 4 Production Example 5 Production Example 6 Comparative Example 1 Comparative Example 2 Skin moisturizing 4.7 4.6 4.8 4.4 4.5 4.6 4.6 4.5 wrinkle improvement 4.7 4.7 4.9 4.6 4.5 4.2 4.2 4.4 Skin whitening 4.8 4.7 5.0 4.6 4.6 4.5 4.1 4.2 preference 4.6 4.6 4.7 4.5 4.4 4.3 4.7 4.8

As shown in Table 2 above, the sensory evaluation results showed that the cosmetic composition of the present invention exhibited more excellent effects than the case of Comparative Examples 1 and 2, in which the cosmetic composition of the present invention was marketed as a conventional whitening lotion. Particularly, in Production Example 3, there was an evaluation that the effect of remarkable whitening and wrinkle improvement was shown.

It was evaluated that the cosmetic composition of the present invention exhibits excellent effects because it has a longer maintenance period of moisturizing power than the commercial product.

However, in terms of preference, it was evaluated to be somewhat lower than that of a conventional product, but it was evaluated that it was due to the heterogeneity of the fragrance and the like because additives such as synthetic flavoring agents were not included.

From the results of Table 2, it can be seen that the cosmetic composition of the present invention contains a natural extract having excellent whitening effect as an active ingredient, thereby reducing the content of the chemical composition to improve the moisturizing power while reducing the skin irritation force, It is considered that the effect of maximizing the whitening effect is obtained.

It will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the spirit or scope of the present invention as defined by the following claims. It can be understood that it is possible.

Claims (7)

Preparing a Rhodiola extract;
Preparing a pine bark extract;
Preparing a citrus marinolan-4-n-butylresorcinol emulsion;
Adjusting the prepared Rhodiola extract, pine bark extract, and gamma-linolenic acid-4-n-butylresorcinol emulsion to 60 ° C;
Heating the emulsifier at 70 占 폚 to prepare an emulsifier in a solution state; And
After mixing the Rhodiola extract, pine bark extract, gum marinolenic acid-4-n-butylresorcinol emulsion, the emulsifying agent in the solution state, herbal essential oil, moisturizing oil and moisturizing agent, Lt; 0 &gt; C, and then cooling the mixture to prepare a cosmetic composition,
The Rhodiola extract, the pine bark extract and the gum marinolenic acid-4-n-butyl resorcinol emulsion are mixed in a weight ratio of 1: 2: 1 to 2: 1 to 2,
The mixture of the Rhodiola extract, the pine bark extract, and the gum marinolan-4-n-butyl resorcinol emulsion is contained in an amount of 45 to 75% by weight based on the total weight of the cosmetic composition,
Wherein the cosmetic composition comprises 1 to 5% by weight of the herbal essential oil, 9 to 25% by weight of a moisturizing oil, 5 to 15% by weight of a moisturizer, and 10 to 15% by weight of an emulsifier,
The herbal essential oil is at least one selected from the group consisting of lavender essential oil, jasmine essential oil, rosemary essential oil, chamomile essential oil, position hazel essential oil and ylang ylang essential oil,
The moisturizing oil is at least one selected from olive oil, argan oil, avocado oil, jojoba oil, camellia oil, grape seed oil, and evening primrose oil,
The moisturizing agent is at least one selected from glycerin, honey and aloe vera gel,
Wherein the emulsifying agent is selected from olive oil wax and shea butter.
The method according to claim 1,
4. The cosmetic composition for whitening and wrinkle improvement according to claim 1, wherein the gum marinolenic acid-4-n-butylresorcinol emulsion comprises 4-n-butyl resorcinol, gum marinol acid, an emulsifier, amino acid and dextrin &Lt; / RTI &gt;
The method according to claim 1,
The cosmetic composition for whitening and wrinkle improvement according to any one of claims 1 to 4, wherein the gum marinolenic acid-4-n-butylresorcinol emulsion comprises a gum marinolenic acid-4-n-butylresorcinol nanoliposome having a particle size of 10 to 100 nm &Lt; / RTI &gt;
delete A cosmetic composition for whitening and wrinkle improvement, which is produced by the method of any one of claims 1 to 3. delete delete
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101921551B1 (en) 2018-05-15 2018-11-23 주식회사 코드바이오 Enzymatic degradation product of shea butter and method for manufacturing the same
KR20200092495A (en) * 2019-01-11 2020-08-04 농업회사법인(주)제이케이크래프트 Fermented material manufacturing system for beauty products having low irritation function
KR20200122677A (en) 2019-04-18 2020-10-28 구원림 cosmetic composition using pine tree and seaweeds and manufacturing method of it

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107296764B (en) * 2017-06-28 2020-06-26 深圳市永济泰科技有限公司 Cream and preparation method thereof
KR102091142B1 (en) 2017-07-28 2020-03-19 (주)엘에스화장품 A chelating cosmetic composition effective for removing harmful heavy metals among fine dust and yellow dust
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100751883B1 (en) * 2006-09-07 2007-08-23 주식회사 웰스킨 Whitening composition containing gamma linolenic acid and 4-n-butylresorcinol water-soluble nanoliposome
KR101050237B1 (en) * 2008-09-10 2011-07-19 필로스 주식회사 Functional Cosmetic Composition Using Pine Bark Extract

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100751883B1 (en) * 2006-09-07 2007-08-23 주식회사 웰스킨 Whitening composition containing gamma linolenic acid and 4-n-butylresorcinol water-soluble nanoliposome
KR101050237B1 (en) * 2008-09-10 2011-07-19 필로스 주식회사 Functional Cosmetic Composition Using Pine Bark Extract

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101921551B1 (en) 2018-05-15 2018-11-23 주식회사 코드바이오 Enzymatic degradation product of shea butter and method for manufacturing the same
KR20200092495A (en) * 2019-01-11 2020-08-04 농업회사법인(주)제이케이크래프트 Fermented material manufacturing system for beauty products having low irritation function
KR102176901B1 (en) * 2019-01-11 2020-11-10 농업회사법인(주)제이케이크래프트 Fermented material manufacturing system for beauty products having low irritation function
KR20200122677A (en) 2019-04-18 2020-10-28 구원림 cosmetic composition using pine tree and seaweeds and manufacturing method of it

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