KR101298078B1 - A composition and a making method of non-explosive reactive material for non-explosive reactive armor - Google Patents
A composition and a making method of non-explosive reactive material for non-explosive reactive armor Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
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- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0008—Compounding the ingredient
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- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
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- C06B45/00—Compositions or products which are defined by structure or arrangement of component of product
- C06B45/04—Compositions or products which are defined by structure or arrangement of component of product comprising solid particles dispersed in solid solution or matrix not used for explosives where the matrix consists essentially of nitrated carbohydrates or a low molecular organic explosive
- C06B45/06—Compositions or products which are defined by structure or arrangement of component of product comprising solid particles dispersed in solid solution or matrix not used for explosives where the matrix consists essentially of nitrated carbohydrates or a low molecular organic explosive the solid solution or matrix containing an organic component
- C06B45/10—Compositions or products which are defined by structure or arrangement of component of product comprising solid particles dispersed in solid solution or matrix not used for explosives where the matrix consists essentially of nitrated carbohydrates or a low molecular organic explosive the solid solution or matrix containing an organic component the organic component containing a resin
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F41—WEAPONS
- F41H—ARMOUR; ARMOURED TURRETS; ARMOURED OR ARMED VEHICLES; MEANS OF ATTACK OR DEFENCE, e.g. CAMOUFLAGE, IN GENERAL
- F41H5/00—Armour; Armour plates
- F41H5/007—Reactive armour; Dynamic armour
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Abstract
Description
본 발명은 비활성 반응장갑용 비활성 반응물질의 조성물 및 그 제조방법에 관한 것으로서, 좀더 상세하게는 에너지 물질, 결합제, 산화제, 가소제 및 첨가제를 포함하여 이루어지는 것을 특징으로 하는 비활성 반응장갑용 비활성 반응물질의 조성물 및 그 제조방법에 관한 것이다.The present invention relates to a composition of an inert reactant for inert reaction gloves and a method of manufacturing the same, and more particularly, to a composition of an inert reactant for inert reaction gloves, comprising an energy material, a binder, an oxidizing agent, a plasticizer and an additive. It relates to a manufacturing method.
기존의 폭발형 반응장갑에서는 반응물질로서 화약을 적용하여, 반응장갑에 탄이 피탄되면 반응물질인 화약이 폭발하고, 화약의 폭발에너지에 의해 전/후면 비행판이 비행하면서 제트와 상호작용을 발생시켜 제트를 파쇄 및 교란시킴으로써 방호 효과를 얻는다. 이러한 폭발형 반응장갑은 높은 폭발 압력과 넓은 폭발 범위, 그리고 파편의 비산 등으로 인해 2차 피해를 발생시키며, 경장갑 차량과 같이 차체구조물의 강도가 약한 차량에 적용하기에는 어려움이 따른다. 따라서 폭발형 반응장갑보다 폭발 속도와 압력 및 폭발 범위를 줄여 방호력은 다소 감소하나 주변 영향이 적은 부가형 반응장갑의 적용이 필요하게 되었다. 이에 비활성 반응장갑의 개발 필요성이 대두되고, 그에 적용가능한 비활성 반응물질(non-explosive reactive material)의 개발이 요구되고 있다.In the existing explosive reaction gloves, gunpowder is applied as a reactant. When the bullets are fired on the reaction gloves, the explosives, which are reactants, explode, and the front and rear flight boards fly by the explosive energy of the gunpowder, causing interaction with the jet. A protective effect is obtained by crushing and disturbing the jets. Such explosion type reaction gloves cause secondary damage due to high explosion pressure, wide explosion range, and scattering of debris, and it is difficult to be applied to vehicles with weak structural strength such as light armored vehicles. Therefore, it is necessary to apply additional reaction gloves that have less protection but less surrounding force by reducing explosion speed, pressure and explosion range than explosion reaction gloves. Therefore, there is a need for the development of inert reactive gloves, and the development of non-explosive reactive materials applicable thereto is required.
본 발명은 기존의 폭발형 반응장갑의 반응물질과 조성을 달리하여 폭발 속도와 압력을 현저히 감소시키고, 반응물질의 반응 범위를 축소시킴으로써, 경장갑 차량과 같은 차제가 약한 차량에 적용하여 부가적인 방호력 증대에 기여할 수 있는 비활성 반응장갑용 비활성 반응물질의 조성물 및 그 제조방법을 제공하는 것이다.The present invention significantly reduces the explosion speed and pressure by changing the composition and the reactant of the conventional explosive reaction gloves, and by reducing the reaction range of the reactant, it is applied to a vehicle with a weak vehicle, such as a light armored vehicle to increase the additional protection It is to provide a composition of the inert reactant for inert reaction gloves that can contribute to and a method for producing the same.
본 발명의 비활성 반응장갑용 비활성 반응물질의 조성물은 에너지 물질, 결합제, 산화제, 가소제 및 첨가제를 포함하여 이루어지는 것을 특징으로 한다.The composition of the inert reactant for inert reaction gloves of the present invention is characterized in that it comprises an energy substance, a binder, an oxidizing agent, a plasticizer and an additive.
본 발명에서 사용되는 에너지 물질은 그 종류에 특별히 한정이 없으며, 바람직한 예로는 시클로트리메틸렌트리니트라민(RDX; Research Department Explosive: Cyclotrimethylenetrinitramine; C3H6N6O6), 테트라니트로테트라조칸(HMX; High-Molecular-weight RDX: Tetranitrotetrazocane; C4H8N8O8) 등으로부터 선택되는 1종 이상을 들 수 있다. 상기 에너지 물질의 함량은 15~50중량%인 것이 바람직한데, 15중량% 미만 사용되는 경우에는 방호성능이 저하하여 바람직하지 않고, 50중량%를 초과하여 사용되는 경우에는 폭발 현상으로 인하여 차체에 손상을 유발할 수 있어 바람직하지 않다.The energy substance used in the present invention is not particularly limited in kind, and preferred examples thereof include cyclotrimethylenetrinitramine (RDX; Research Department Explosive: Cyclotrimethylenetrinitramine; C 3 H 6 N 6 O 6 ), tetranitrotetrazocan (HMX High-Molecular-weight RDX: Tetranitrotetrazocane; C 4 H 8 N 8 O 8 ) and the like. It is preferable that the content of the energy substance is 15 to 50% by weight, when less than 15% by weight of the protection performance is not preferable, and when used in excess of 50% by weight damage to the vehicle body due to the explosion phenomenon It is not preferable because it can cause.
본 발명에서 사용되는 결합제는 그 종류에 특별히 한정이 없으며, 바람직한 예로는 히드록실 터미네이티드 폴리부타디엔(HTPB; Hydroxyl Terminated Polybutadiene), 히드록실 터미네이티드 폴리에테르(HTPE; Hydroxyl Terminated Polyether) 및 히드록실 터미네이티드 카프로락톤 에테르(HTCE; Hydroxyl Terminated Caprolactone Ether) 등으로부터 선택되는 1종 이상을 들 수 있다. 상기 결합제의 함량은 5~30중량%인 것이 바람직한데, 5중량% 미만 사용되는 경우에는 에너지 물질을 결합시킬 수 없어서 바람직하지 않고, 30중량%을 초과하여 사용되는 경우에는 방호성능이 저하하여 바람직하지 않다.The binder used in the present invention is not particularly limited in its kind, and preferred examples thereof include hydroxyl terminated polybutadiene (HTPB), hydroxyl terminated polyether (HTPE) and hydroxyl terminated polyether (HTPE). And at least one selected from Terminated Caprolactone Ether (HTCE; Hydroxyl Terminated Caprolactone Ether). It is preferable that the content of the binder is 5 to 30% by weight, but less than 5% by weight is not preferable because it is not able to bind the energy material, when used in excess of 30% by weight is lowered the protective performance is preferred. Not.
본 발명에서 사용되는 산화제는 그 종류에 특별히 한정이 없으며, 바람직한 예로는 암모늄 퍼클로레이트(AP; Ammonium Perchlorate), 암모늄 니트레이트(AN; Ammonium Nitrate) 등으로부터 선택되는 1종 이상을 들 수 있다. 상기 산화제의 사용량은 10~50중량%인 것이 바람직한데, 10중량% 미만 사용되는 경우에는 연소가 불완전하게 되어 바람직하지 않고, 50중량%를 초과하여 사용되는 경우에는 에너지 물질의 부족으로 인해 방호성능이 저하되거나 연소속도가 과하게 되어 바람직하지 않다.The type of oxidizing agent used in the present invention is not particularly limited, and preferred examples thereof include at least one selected from ammonium perchlorate (AP), ammonium nitrate (AN) and the like. The amount of the oxidizing agent is preferably 10 to 50% by weight, but less than 10% by weight of the combustion is incomplete, and when used in excess of 50% by weight of the protective material due to the lack of energy materials This is undesirable because it is lowered or the combustion rate is excessive.
본 발명에서 사용되는 가소제의 예로는 그 종류에 특별히 한정이 없으며, 바람직한 예로는 디옥틸 아디페이트(DOA; dioctyl adipate), 디옥틸 아질레이트(DOZ; dioctyl azelate), 디옥틸 세바케이트(DOS; dioctyl sebacate), 이소데실 펠라고네이트(IDP; isodecyl pelagonate), 부탄트리올 트리니트레이트(BTTN; butanetriol trinitrate), 트리메틸올에탄 트리니트레이트(TMETN; Trimethylolethane Trinitrate) 등으로부터 선택되는 1종 이상을 들 수 있고, 상기 가소제의 사용량은 2~15중량%인 것이 바람직한데, 2중량% 미만 사용되는 경우에는 판상의 성형체로 성형하기 어려워 바람직하지 않고, 15중량%를 초과하는 경우에는 치수 안정성 유지가 어려우며, 장기간 보관시 가소제의 누출현상이 발생할 수 있어 바람직하지 않다.Examples of the plasticizer used in the present invention are not particularly limited in kind, preferred examples thereof are dioctyl adipate (DOA), dioctyl azelate (DOZ; dioctyl azelate), dioctyl sebacate (DOS; dioctyl sebacate), isodecyl pelagonate (IDP; isodecyl pelagonate), butanetriol trinitrate (BTTN; butanetriol trinitrate), and at least one selected from trimethylol ethane trinitrate (TMETN). It is preferable that the amount of the plasticizer used is 2 to 15% by weight, but when used less than 2% by weight, it is difficult to mold into a plate-shaped molded body, and when it exceeds 15% by weight, it is difficult to maintain dimensional stability, It is not preferable because long term storage may cause plasticizer leakage.
본 발명에서 사용되는 첨가제로는 부석을 사용할 수 있는데, 부석은 입자속에 다량의 미세한 기공들을 포함하고 있어 고온에서 팽창하여 에너지 물질의 팽창과 함께 방호 효과를 나타낸다. 부석의 사용량이 10중량% 미만이면 에너지 물질의 상대적인 증가로 폭발 현상을 유발할 수 있음으로 바람직하지 않고, 30중량%를 초과하는 경우에는 에너지 물질의 첨가량 저하로 인해 급격한 팽창을 유발하는 에너지 물질의 공급이 적어짐으로 인해 저팽창이 발생하므로 바람직하지 않다.As an additive used in the present invention, pumice may be used, and pumice contains a large amount of fine pores in the particle and expands at high temperature to exhibit a protective effect with expansion of an energy material. If the amount of pumice stone is less than 10% by weight, it is not preferable to cause an explosion phenomenon due to the relative increase of the energy material.If the amount of pumice stone is more than 30% by weight, the supply of energy material causing rapid expansion due to the decrease in the amount of energy material added. This decrease is undesirable because low expansion occurs.
본 발명에 따른 비활성 반응물질의 제조방법은 다음의 단계들을 포함하여 이루어진다 :The method for preparing an inert reactant according to the present invention comprises the following steps:
(1) 결합제와 가소제를 균일하게 혼합하는 단계;(1) uniformly mixing the binder and the plasticizer;
(2) 상기 (1)단계에서 얻어진 혼합물에 에너지 물질, 산화제 및 첨가제를 투입하여 혼합하는 단계;(2) mixing the energy material, the oxidizing agent and the additive by adding the mixture obtained in the step (1);
(3) 상기 (2)단계에서 얻어진 혼합물을 용기에 담고 진공을 가하여 기공을 제거하는 단계; 및(3) removing the pores by placing the mixture obtained in step (2) in a container and applying a vacuum; And
(4) 기공이 제거된 혼합물을 경화시키는 단계.(4) curing the mixture from which the pores have been removed.
본 발명의 비활성 반응물질의 제조방법에 있어서, 상기 (4)단계에서의 경화는 50~75℃에서 48~120시간 동안 5~20mm의 두께로 경화시키는 것이 바람직한데, 경화시 온도가 50℃ 미만이거나 경화시간이 48시간 미만이면 충분한 경화가 진행되지 않아 바람직하지 않고, 75℃를 초과하면 경화 후 상온에서 부피 수축이 많아지며, 경화시간이 120시간을 초과하는 경우에는 경화 진행이 극히 미미함으로 에너지 낭비를 초래하여 바람직하지 않다. 그리고, 경화 후 두께가 5mm 미만인 경우에는 얇은 두께로 인하여 성형작약탄과의 반응에 필요한 시간이 부족하여 방호성능이 저하하여 바람직하지 않고, 20mm를 초과하는 경우에는 필요 이상의 두께로 인한 에너지 물질의 과다로 인해 차체 손상이 유발되므로 바람직하지 않다.In the preparation method of the inert reactant of the present invention, the curing in the step (4) is preferably cured to a thickness of 5 ~ 20mm for 48 to 120 hours at 50 ~ 75 ℃, the temperature at the time of curing less than 50 ℃ If the curing time is less than 48 hours or not enough curing does not proceed, it is not preferable, if it exceeds 75 ℃, the volume shrinkage at room temperature after curing increases, if the curing time exceeds 120 hours, the progress of curing is extremely small It is undesirable because it causes waste. In addition, when the thickness after curing is less than 5 mm, the thin film thickness is insufficient for the reaction with the molding peony, and thus the protection performance is not preferable. When the thickness exceeds 20 mm, the excess of energy material due to the thickness more than necessary is exceeded. This is undesirable because it causes body damage.
본 발명의 비활성 반응장갑용 비활성 반응물질의 조성물 및 제조방법에 따르면 최적화된 비활성 반응물질을 설계할 수 있으며, 피탄시 반응 후 장갑 차량 및 주변에 압력과 영향을 미치는 범위를 줄이는 효과가 있다. 또한 차체가 약한 장갑 차량에 적용하여 부가적인 방호력 증대를 가지게 할 수 있다.According to the composition and method of preparing the inert reactant for inert reaction gloves of the present invention, it is possible to design an optimized inert reactant, and it is effective to reduce the range of pressure and influence on the armored vehicle and surroundings after the reaction. It can also be applied to weak armored vehicles to have additional protection.
도 1은 본 발명의 비활성 반응물질의 제조 공정도를 나타낸 도면이다.1 is a view showing a manufacturing process of the inert reactant of the present invention.
이하, 본 발명을 하기 실시예 및 비교예에 의하여 보다 구체적으로 설명한다. 하기의 실시예는 본 발명을 실시하기 위한 예에 지나지 않으며, 본 발명의 보호범위를 제한하고자 하는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to the following examples and comparative examples. The following examples are merely examples for carrying out the present invention and are not intended to limit the scope of protection of the present invention.
실시예Example 및 And 비교예Comparative example
하기 표 1에 나타낸 조성으로 이루어진 비활성 반응물질의 조성물을 사용하여 제조된 성형작약탄의 반응성과 파편탄의 안전성을 측정한 결과를 표 1에 나타내었다.Table 1 shows the results of measuring the reactivity and the safety of the fragmentation coal of the molding peony coal prepared using the composition of the inert reactants composed of the composition shown in Table 1.
상기 표 1에서, 에너지 물질은 RDX, 산화제는 AP, 첨가제는 부석, 가소제는 DOA, 결합제는 HTPB이다.In Table 1, the energy material is RDX, the oxidizing agent is AP, the additive is pumice, the plasticizer is DOA, the binder is HTPB.
상기 표 1에 나타낸 바와 같이, 본 발명의 비활성 반응물질의 조성물은 비교예의 폭발형 조성물에 비해 에너지 물질의 비율을 크게 줄임으로써, 성형작약탄 반응성 시험시 폭발 현상이 일어나지 않으므로 파편의 비산 등으로 인한 2차 피해를 유발시키지 않으며, 경장갑 차량과 같이 차체 구조물의 강도가 약한 차량에 적용가능하다. 또한, 20mm 파편탄 안전성 시험에서도 무반응하여 안전한 성능을 나타내므로 취급 및 저장상의 안전성이 입증되었다.As shown in Table 1, the composition of the inert reactant of the present invention by reducing the ratio of the energy material significantly compared to the explosive composition of the comparative example, because the explosion phenomenon does not occur during the molding peony reactivity test due to scattering of debris, etc. It does not cause secondary damage and can be applied to vehicles with weak strength of the body structure, such as light armored vehicles. In addition, the safety of handling and storage has been proved because of the non-responsive and safe performance in the 20mm fragmentation coal safety test.
Claims (7)
(1) 결합제와 가소제를 균일하게 혼합하는 단계;
(2) 상기 (1)단계에서 얻어진 혼합물에 에너지 물질, 산화제 및 첨가제를 투입하여 혼합하는 단계;
(3) 상기 (2)단계에서 얻어진 혼합물을 용기에 담고 진공을 가하여 기공을 제거하는 단계; 및
(4) 기공이 제거된 혼합물을 경화시키는 단계.A method for preparing an inert reactant for inert gloves comprising the composition of the inert reactant according to any one of claims 1 to 5, characterized in that it comprises the following steps:
(1) uniformly mixing the binder and the plasticizer;
(2) mixing the energy material, the oxidizing agent and the additive by adding the mixture obtained in the step (1);
(3) removing the pores by placing the mixture obtained in step (2) in a container and applying a vacuum; And
(4) curing the mixture from which the pores have been removed.
The method according to claim 6, wherein the curing in the step (4) is carried out by curing to a thickness of 5 to 20mm for 48 to 120 hours at 50 ~ 75 ℃ to inert reaction material for inert reaction gloves.
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Citations (3)
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JPH06341792A (en) * | 1993-05-17 | 1994-12-13 | Rockwell Internatl Corp | Non-deflagration type reactive armor |
US7360479B2 (en) | 2004-04-22 | 2008-04-22 | Rafael Advanced Defense Systems Ltd. | Non-explosive energetic material and a reactive armor element using same |
KR20110124827A (en) * | 2010-05-12 | 2011-11-18 | 국방과학연구소 | Reactive material composition for a less sensitive explosive reactive armor and a pressing thereof |
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH06341792A (en) * | 1993-05-17 | 1994-12-13 | Rockwell Internatl Corp | Non-deflagration type reactive armor |
US7360479B2 (en) | 2004-04-22 | 2008-04-22 | Rafael Advanced Defense Systems Ltd. | Non-explosive energetic material and a reactive armor element using same |
KR20110124827A (en) * | 2010-05-12 | 2011-11-18 | 국방과학연구소 | Reactive material composition for a less sensitive explosive reactive armor and a pressing thereof |
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