KR101272792B1 - Moisturizing cream with high water retention effect - Google Patents
Moisturizing cream with high water retention effect Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
Description
본 발명은 수분크림에 관한 것으로, 더욱 상세하게는 보습성이 우수한 수분크림에 관한 것이다.
The present invention relates to a moisture cream, and more particularly to a moisture cream excellent in moisture retention.
화장품 시장은 단순 미용 산업이라는 패러다임을 넘어 최근 기술과 효능을 결합한 하이테크 산업으로 인식되고 있다. 고성장 중인 화장품 산업은 과거 유행 중심의 경쟁 산업이었는데, 최근 다양한 첨단기술과 접목되면서 기술효능 중심의 산업으로 변화하고 있다. 그동안 국내 화장품 시장은 2006년, 5조 6,000억 원에서, 2011년, 8조 9,000억 원으로, 연평균 10.4% 성장하며, 고성장세를 유지했다. 특히 사회 전반에 걸쳐 웰빙안티에이징 열풍이 불면서 화장품 산업의 성장은 당분간 지속할 것으로 전망되고 있다. The cosmetics market is recognized as a high-tech industry that combines technology and efficacy in recent years beyond the paradigm of the beauty industry. The cosmetics industry, which has been growing rapidly, has been a competitive industry focused on fashion in the past. The domestic cosmetics market has been growing at an annual average of 10.4% from 2006 to KRW 5.60 trillion in 2006 and KRW 8.9 trillion in 2011. In particular, the growth of the well-being anti-aging boom across society is expected to continue the growth of the cosmetics industry for the time being.
피부는 온도 및 습도 변화, 자외선 및 공해물질 등의 외부환경자극으로부터 인체를 보호해 주는 기능을 가진다. 사람의 피부는 나이를 먹으면서 피부노화에 의해 끊임없이 변한다. The skin has a function of protecting the human body from external environmental stimuli such as temperature and humidity changes, ultraviolet rays and pollutants. Human skin is constantly changed by skin aging as it ages.
피부노화는 내인성 노화로 불리는 자연 노화와 외적 노화로 구분되는데, 자연 노화는 유전적인 요인에 의해 영향을 받기 때문에 인위적인 조절이 어렵다. 하지만, 외적 노화는 환경적인 요소에 영향을 받기 때문에 인위적인 조절이 비교적 용이하다. Skin aging is divided into natural aging and external aging, called endogenous aging. Since natural aging is influenced by genetic factors, artificial control is difficult. However, since external aging is influenced by environmental factors, artificial control is relatively easy.
대표적인 외적 노화 인자로는 중금속, 황사, 오존, 자외선, 화학물질 등이 있다. 외적 자극인자들은 자유 라디칼 경로를 경유하는데, 자유 라디칼들은 피부세포의 활성을 억제하고, 피부세포의 괴사와 변성을 유도하여, 피부 콜라겐 등의 결합조직을 파괴하고, 세포막 기능저해, DNA 변이촉진, 단백질 작용 변형, 세포 간 에너지 전이, 신진대사와 관련된 분자들의 변형 등을 유발하는 것으로 알려져 있다. 이러한 내적·외적 요인에 의한 피부 노화 및 손상을 방지하여 아름다운 피부를 유지하기 위하여, 다양한 동물, 식물 및 미생물 등에서 얻어진 생리 활성 물질들이 화장품에 사용되고 있다. Representative external aging factors include heavy metals, yellow sand, ozone, ultraviolet rays, and chemicals. External stimulators pass through the free radical pathway, which inhibits the activity of skin cells, induces necrosis and degeneration of skin cells, destroys connective tissues such as skin collagen, inhibits cell membrane function, promotes DNA mutation, It is known to cause protein action alteration, intercellular energy transfer, metabolism related metabolism. In order to maintain beautiful skin by preventing skin aging and damage caused by such internal and external factors, physiologically active substances obtained from various animals, plants and microorganisms are used in cosmetics.
피부 노화의 가장 큰 지표는 피부주름과 피부탄력 감소인데, 콜라겐 함유량 및 외부 환경에 대한 면역작용능력 등의 여러 가지 요소들이 영향을 미치는 것으로 알려져 있다. 그 중 가장 큰 영향을 미치는 것이 피부 수분 함유량이다. 따라서, 보습력이 우수한 보습제가 많이 개발되고 있는 실정이다.
The biggest indicators of skin aging are skin wrinkles and reduced skin elasticity. Several factors, such as collagen content and the ability to act on the environment, are known. One of the biggest influences is the skin moisture content. Accordingly, many moisturizers having excellent moisturizing power have been developed.
본 발명에서는 피부 보습성이 우수한 보습크림을 개발하여 제공하고자 한다.
In the present invention, it is intended to develop and provide a moisturizing cream having excellent skin moisturizing properties.
본 발명은 유화크림과 젤리크림을 혼합하여 제조되되, 상기 유화크림은, 세틸알코올 스테아레스-2, 스테아레스-21 , 피이지-30디폴리하이드록시스테아레이트, 세틸에칠헥사노에이트, 스테아릭애씨드, 카프릴릭/카프릭 트리글리세라이드, 디메치콘을 혼합하여 제조된 유상파트와, 글리세린, 트리에탄올아민, 아크릴레이트/C10-30알킬아크릴레이트크로스폴리머를 정제수에 혼합하여 제조된 수상파트가 혼합되어 제조된 것임을 특징으로 하고, 상기 젤리크림은, 디소듐이디티에이, 글리세린, 피이지-32, 카보머, 폴리소르베이트 80 , 부틸렌글라이콜, 트리에탄올아민을 정제수에 혼합하여 제조된 것임을 특징으로 하는 수분크림을 제공한다. The present invention is prepared by mixing an emulsified cream and jelly cream, the emulsified cream, cetyl alcohol steares-2, steares-21, Fiji-30 dipolyhydroxystearate, cetylethylhexanoate, stearate Oil phase parts prepared by mixing ric acid, caprylic / capric triglyceride, and dimethicone, and water phase parts prepared by mixing glycerin, triethanolamine and acrylate / C10-30 alkyl acrylate crosspolymer in purified water are mixed. It is characterized in that the jelly cream, Disodium ethane, Glycerin, Fiji-32, Carbomer, Polysorbate 80, Butylene glycol, Triethanolamine characterized in that it is prepared by mixing in purified water It provides a moisture cream.
한편, 본 발명의 수분크림은 상기에 기재된 성분 외에 다른 성분을 포함할 수도 있다. 다른 성분으로는 피부 주름 개선 등을 부여하는 기능성 성분, 부패를 막는 방부제, 제형의 안정성을 유지시키는 안정제 등이 있다.On the other hand, the moisture cream of the present invention may contain other components in addition to the components described above. Other ingredients include functional ingredients that impart skin wrinkle improvement and the like, preservatives to prevent rot, stabilizers to maintain the stability of the formulation, and the like.
한편, 본 발명의 수분크림에 있어서, 상기 유화크림은, 바람직하게 상기 유상파트와 수상파트를 혼합하고, 가온하여 균질화한 후 냉각하여 제조되는 것이 좋다. On the other hand, in the water cream of the present invention, the emulsified cream is preferably prepared by mixing, heating and homogenizing the oil phase part and the water phase part.
한편, 본 발명의 수분크림에 있어서, 상기 젤리크림은, 바람직하게 상기 젤리크림의 구성성분 중 트리에탄올아민을 제외한 성분을 가온하여 완전용해한 후, 냉각하고, 트리에탄올아민을 투입하여 혼합함으로써 제조되는 것이 좋다. On the other hand, in the moisture cream of the present invention, the jelly cream is preferably prepared by heating and completely dissolving the components except the triethanolamine in the constituents of the jelly cream, and then cooling and adding and mixing the triethanolamine. .
한편, 본 발명의 수분크림에 있어서, 상기 수분크림은, 바람직하게 유화크림과 젤리크림이 무게비로 1:2 내지 1:3의 비율로 혼합되는 것이 좋다.
On the other hand, in the moisture cream of the present invention, the moisture cream, preferably emulsified cream and jelly cream is preferably mixed in a ratio of 1: 2 to 1: 3 by weight ratio.
본 발명에서 개발한 보습크림은 하기 실험에 의할 경우, 우수한 피부 보습성을 발휘하였다. 본 발명의 보습크림을 도포한 직후에는 도포전과 비교하여 거의 2~6배 가량의 높은 수분함량을 나타내었다. 시간이 경과하면서 지속적으로 서서히 감소하였지만 도포전과 비교하면 유의적으로 높은 수분 함량을 유지하고 있음을 확인할 수 있었다.
The moisturizing cream developed in the present invention exhibited excellent skin moisturizing properties by the following experiment. Immediately after applying the moisturizing cream of the present invention, the moisture content was about 2 to 6 times higher than before application. Although it gradually decreased over time, it was confirmed that the water content was maintained significantly higher than before application.
도 1은 하기 실험예에 기재된 실험에 따른 피부 수분 함량 변화를 보여준다. 도 1에서, "(a) 20대 중반 여성, (b) 20대 중반 남성, (c) 20대 초반 여성, (d) 20대 초반 여성, (e) 20대 후반 여성, (f) 20대 후반 여성, (g) 20대 후반 여성, (h) 30대 초반 여성, (i) 30대 초반 여성, (j) 30대 초반 여성"이다. 도 1에서 "CONTROL"은 대조군이고, "GEL"은 ALOE VERA 98% MOISTURE GEL이며, "CREAM"은 본 발명의 수분 크림이다.
도 2는 대조군, ALOE VERA 98% MOISTURE GEL과 본 발명의 수분 크림 간의 피부 수분 함량 변화를 보여준다. 도 2에서 "CONTROL"은 대조군이고, "GEL"은 ALOE VERA 98% MOISTURE GEL이며, "CREAM"은 본 발명의 수분 크림이다. Figure 1 shows the skin moisture content change according to the experiment described in the following experimental example. In Figure 1, "(a) mid 20s, (b) mid 20s, (c) early 20s, (d) early 20s, (e) late 20s, (f) 20s Late women, (g) late 20s, (h) early 30s, (i) early 30s, (j) early 30s ". In Figure 1 "CONTROL" is a control, "GEL" is ALOE VERA 98% MOISTURE GEL, "CREAM" is the moisture cream of the present invention.
Figure 2 shows the skin moisture content change between the control, ALOE VERA 98% MOISTURE GEL and the moisture cream of the present invention. In Figure 2 "CONTROL" is a control, "GEL" is ALOE VERA 98% MOISTURE GEL, "CREAM" is the moisture cream of the present invention.
이하, 본 발명의 내용을 하기 실시예 및 실험예를 통해 더욱 상세히 설명하고자 한다. 다만, 본 발명의 권리범위가 하기 실시에에만 한정되는 것은 아니고, 그와 등가의 기술적 사상의 변형까지를 포함한다.
Hereinafter, the present invention will be described in more detail with reference to the following Examples and Experimental Examples. However, the scope of the present invention is not limited to the following embodiments, but includes modifications of equivalent technical ideas.
[[ 실시예Example 1: 본 발명의 1: 수분크림Moisture cream 제조] Produce]
본 발명의 수분크림은 하기와 같이 제조한 유화크림과 젤리크림을 혼합하여 제조되었다. 유화크림과 젤리크림을 하기와 같이 제조 완료한 후, 유화크림 30 g과 젤리크림 70 g을 각각 칭량하여 전량을 100그램으로 한 후, 메인 믹서에 투입하여 "HOMO : 3600 rpm, AGI : 26 rpm"의 조건으로 5분간 균일 교반하여 최종 제조하였다.
Moisture cream of the present invention was prepared by mixing the emulsion cream and jelly cream prepared as follows. After the emulsion cream and jelly cream were prepared as follows, 30 g of emulsion cream and 70 g of jelly cream were weighed to 100 grams, respectively, and then put into a main mixer, followed by "HOMO: 3600 rpm, AGI: 26 rpm". The final production was carried out by uniform stirring for 5 minutes under the condition of ".
1.유화크림 1.Oil Cream
<유상파트> <Paid part>
세틸알코올(Cetyl Alcohol) 2.0 g, 스테아레스-2(Steareth-2) 1.0 g, 스테아레스-21(Steareth-21) 2.0 g, 피이지-30디폴리하이드록시스테아레이트(PEG-30 Dipolyhydroxystearate) 0.5 g, 세틸에칠헥사노에이트(Cetyl Ethylhexanoate) 5.0 g, 스테아릭애씨드(Stearic Acid) 1.0 g, 카프릴릭/카프릭 트리글리세라이드(Caprylic/Capric Triglyceride) 5.0 g, 디메치콘(Dimethicone) 1.5 g을 칭량하여 80℃로 가온하여 완전 용해하였다.2.0 g of Cetyl Alcohol, 1.0 g of Steetheth-2, 2.0 g of Steetheth-21, PEG-30 Dipolyhydroxystearate 0.5 g, Cetyl Ethylhexanoate 5.0 g, Stearic Acid 1.0 g, Caprylic / Capric Triglyceride 5.0 g, Dimethicone 1.5 g Weighed and warmed to 80 ° C. to complete dissolution.
<수상파트> <Water Part>
글리세린(Glycerin) 3.0 g, 트리에탄올아민(Triethanolamine) 0.1 g, 아크릴레이트/C10-30알킬아크릴레이트크로스폴리머(Acrylates/C10-30 Alkyl Acrylate Crosspolymer) 0.1 g에 정제수 잔량을 첨가하여 100 g으로 한 후, 80℃로 가온하여 완전 용해하였다.After adding 3.0 g of glycerin (Glycerin), 0.1 g of Triethanolamine, and 0.1 g of Acrylates / C10-30 Alkyl Acrylate Crosspolymer, the remaining amount of purified water was added to 100 g. Warm to 80 ° C. to complete dissolution.
<제조공정> <Manufacturing process>
상기의 유상파트와 수상파트를 메인 가마에 투입하여 "HOMO : 3600 rpm, AGI : 26 rpm"의 조건으로 5분간 유화한 후 32℃까지 냉각하였다.
The oil and water parts were put in a main kiln, emulsified for 5 minutes under the condition of “HOMO: 3600 rpm, AGI: 26 rpm”, and then cooled to 32 ° C.
2.젤리크림 2.jelly cream
<조성> <Composition>
디소듐이디티에이(Disodium EDTA) 0.02 g, 글리세린 2.0 g, 피이지-32(PEG-32) 2.0 g, 카보머(Carbomer) 0.46 g, 폴리소르베이트 80(Polysorbate) 0.3 g , 부틸렌글라이콜(Butylene Glycol) 2.0 g, 트리에탄올아민 0.46 g에 정제수 잔량을 첨가하여 100 g으로 하였다.0.02 g of disodium EDTA, 2.0 g of glycerin, 2.0 g of PIG-32, 2.06 g of Carbomer, 0.4 g of polysorbate 80, 0.3 g of butylene glycol To 2.0 g of (Butylene Glycol) and 0.46 g of triethanolamine were added the remaining water of purified water to make 100 g.
<제조공정> <Manufacturing process>
위 구성성분 중 트리에탄올아민을 제외한 성분을 혼합한 후 50℃로 가온하여 완전 용해하고, 30℃까지 냉각한 후, 트리에탄올아민을 투입하여 "HOMO : 3600 rpm, AGI : 26 rpm"의 조건으로 5분간 균일 교반하였다.After mixing components other than the triethanolamine of the above components, and then completely dissolved by heating to 50 ℃, cooled to 30 ℃, triethanolamine was added for 5 minutes under the conditions of "HOMO: 3600 rpm, AGI: 26 rpm" Stirred uniformly.
[[ 실험예Experimental Example 1: One: 실시예Example 1에서 제조한 1 수분크림의Moisture cream 피부보습Skin hydration 효능 검증] Efficacy Verification]
미용 및 의료환경에서 피부 보습도의 측정 방식은 카파시탄스(capacitance) 측정 방식, 컨덕턱스(conductance) 측정 방식, 서스셉탄스(susceptance) 측정 방식 등으로 나눌 수 있는데, 본 발명에서는 각질(corneum) 층의 수분 보유 능력(water binding capacity)을 측정하기 위해 컨덕턴스를 측정하였다. 본 발명에서는 DermaLab USB(Denmark, CORTEX technology) 측정 장비를 가지고 피부 팔 안쪽 부위에 대하여 비교 실험하였다. 이때, 3개의 등심원(최고 직경이 12.5 mm) 전극을 이용하여 약 100kHz의 주파수를 이용하였다. 모든 실험은 3회 반복하여 측정하여 측정치의 평균을 구하여 통계처리 하였다. Skin moisturizing measurement method in the cosmetic and medical environment can be divided into a capacitance measurement method, conductance measurement method, susceptance measurement method, etc. In the present invention, corneum Conductance was measured to determine the water binding capacity of the layer. In the present invention, using the DermaLab USB (Denmark, CORTEX technology) measuring equipment was compared to the inner portion of the skin arm. At this time, a frequency of about 100 kHz was used using three wicks (maximum diameter of 12.5 mm). All experiments were repeated three times, averaged, and statistically processed.
실험은 과거에 알레르기성 질환이나 아토피 피부염 등 질환의 병력이 없는 23~30세의 남성과 여성 10명을 대상으로 항온항습조건(22±2℃, 40~60%)이 유지되는 환경에서 20분간 안정을 취한 후 실험을 진행하였다. The experiment was conducted on 20 men and women aged 23 to 30 years with no history of allergic disease or atopic dermatitis in an environment where constant temperature and humidity conditions (22 ± 2 ℃, 40 to 60%) were maintained. After the stability was conducted, the experiment was conducted.
보습상태의 비교를 위하여 10명을 대상으로 ALOE VERA 98% MOISTURE GEL(도면에서 "GEL"로 표시)과 본 발명의 수분 크림(도면에서 "CREAM"으로 표시)을 직경 1×1 ㎠ 안에 도포하였고, 도포한 직후, 30분, 60분, 90분, 180분 후의 피부수분을 측정하여 제품에 따른 보습상태 변화의 차이를 비교해 보았다. 무도포 상태를 대조군(도면에서 "CONTROL"으로 표시)으로 하여 실험하였다. For comparison of the moisturizing conditions, 10 persons were coated with ALOE VERA 98% MOISTURE GEL (indicated by "GEL" in the figure) and the moisture cream (indicated by "CREAM" in the figure) in a diameter of 1 × 1 cm 2. After the application, skin moisture was measured after 30 minutes, 60 minutes, 90 minutes, and 180 minutes. The uncoated state was tested as a control (labeled "CONTROL" in the figure).
실험 결과는 도 1과 같았다. 도 1은 실험에 따른 피부 수분 함량 변화를 보여준다. (a) 20대 중반 여성, (b) 20대 중반 남성, (c) 20대 초반 여성, (d) 20대 초반 여성, (e) 20대 후반 여성, (f) 20대 후반 여성, (g) 20대 후반 여성, (h) 30대 초반 여성, (i) 30대 초반 여성, (j) 30대 초반 여성이다.Experimental results were as shown in FIG. 1 shows the skin moisture content change according to the experiment. (a) women in their 20s, (b) men in their 20s, (c) women in their 20s, (d) women in their 20s, (e) women in their 20s, (f) women in their 20s, (g ) Women in their late 20s, (h) women in their early 30s, (i) women in their early 30s, and (j) women in their early 30s.
도포 직 후, 아무것도 바르지 않은 대조군(CONTROL)에 비해 GEL과 본 발명의 수분크림(CREAM)을 도포한 부위의 값이 유의하게 더 높음을 확인할 수 있었다. 180분이 경과한 후, 10명의 피시험자 대부분에서 피부 수분함량이 CONTROL에 비해 GEL과 CREAM 모두 높은 것으로 확인되었다. 특히, CREAM 도포 부위의 수분함량이 GEL 도포 부위보다 높게 나타난 것을 확인할 수 있었다. 다만, 도포 직후부터 180분이 경과 후까지 급격한 수분함량 감소현상은 보이지 않았으나, 대체로 시간이 지남에 따라 서서히 수분함량이 줄어드는 결과를 나타내었다. Immediately after the application, it was confirmed that the value of the site where GEL and the moisture cream (CREAM) of the present invention was applied was significantly higher than the control (No control). After 180 minutes, the skin moisture content of most 10 subjects was found to be higher in both GEL and CREAM than in CONTROL. In particular, it was confirmed that the water content of the CREAM application site was higher than the GEL application site. However, a sudden decrease in moisture content was not observed from 180 minutes after application, but the water content gradually decreased over time.
한편, 무도포군 CONTROL을 100% 기준으로 하여 도포군인 GEL과 본 발명 수분크림(CREAM)의 수분 보유력을 상대적으로 비교하여 보았는데, 그 결과는 도 2와 같았다. 도 2는 대조군과 실험 제품들 간 피부 수분 함량 변화를 보여준다. 피시험자 10명의 평균 수분 함량 측정 결과, 도포 0~180분 동안 CONTROL보다 도포군이 평균적으로 높게 나왔고, 도포군 중에서는 GEL보다 본 발명의 CREAM이 더 높은 수분 함량을 보이는 것으로 확인되었다. On the other hand, based on the
Claims (4)
상기 유화크림은,
세틸알코올 스테아레스-2, 스테아레스-21 , 피이지-30디폴리하이드록시스테아레이트, 세틸에칠헥사노에이트, 스테아릭애씨드, 카프릴릭/카프릭 트리글리세라이드, 디메치콘을 혼합하여 제조된 유상파트와, 글리세린, 트리에탄올아민, 아크릴레이트/C10-30알킬아크릴레이트크로스폴리머를 정제수에 혼합하여 제조된 수상파트가 혼합되어 제조된 것임을 특징으로 하고,
상기 젤리크림은,
디소듐이디티에이, 글리세린, 피이지-32, 카보머, 폴리소르베이트 80 , 부틸렌글라이콜, 트리에탄올아민을 정제수에 혼합하여 제조된 것임을 특징으로 하는 수분크림.
It is manufactured by mixing emulsion cream and jelly cream,
The emulsified cream is,
Cetyl Alcohol Steares-2, Steares-21, Fiji-30 Dipolyhydroxystearate, Cetylethylhexanoate, Stearic Acid, Caprylic / Capric Triglyceride, Dimethicone It is characterized in that the oil phase, and the water phase prepared by mixing glycerin, triethanolamine, acrylate / C10-30 alkyl acrylate crosspolymer in purified water,
The jelly cream is,
Moisturizing cream, characterized in that it is prepared by mixing disodium ID, glycerin, Fiji-32, carbomer, polysorbate 80, butylene glycol, triethanolamine in purified water.
상기 유화크림은,
상기 유상파트와 수상파트를 혼합하고, 가온하여 균질화한 후, 냉각하여 제조되는 것을 특징으로 하는 수분크림.
The method of claim 1,
The emulsified cream is,
Water cream, characterized in that the oil phase parts and the water phase parts are mixed, heated and homogenized, and then cooled.
상기 젤리크림은,
상기 젤리크림의 구성성분 중 트리에탄올아민을 제외한 성분을 가온하여 완전용해한 후, 냉각하고, 트리에탄올아민을 투입하여 혼합함으로써 제조되는 것을 특징으로 하는 수분크림.
The method of claim 1,
The jelly cream is,
Moisturizing cream, characterized in that the gel cream is prepared by heating and completely dissolving the components other than triethanolamine of the components of the jelly cream, and then cooled and added to the triethanolamine.
상기 수분크림은,
유화크림과 젤리크림이 무게비로 1:2 내지 1:3의 비율로 혼합되는 것을 특징으로 하는 수분크림.
The method of claim 1,
The moisture cream is,
Moisturizing cream, characterized in that the emulsion cream and jelly cream are mixed in a ratio of 1: 2 to 1: 3 by weight.
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