KR101222743B1 - Method for manufacturing leaf mustard soap and manufactured leaf mustard soap by that method - Google Patents

Method for manufacturing leaf mustard soap and manufactured leaf mustard soap by that method Download PDF

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KR101222743B1
KR101222743B1 KR1020110103365A KR20110103365A KR101222743B1 KR 101222743 B1 KR101222743 B1 KR 101222743B1 KR 1020110103365 A KR1020110103365 A KR 1020110103365A KR 20110103365 A KR20110103365 A KR 20110103365A KR 101222743 B1 KR101222743 B1 KR 101222743B1
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soap
natural
freshly
less
fresh
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KR1020110103365A
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Korean (ko)
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송미정
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송미정
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/10Mixing; Kneading
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14Shaping
    • C11D13/16Shaping in moulds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/442Perfumes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients

Abstract

PURPOSE: A manufacturing method of leaf mustard soap is provided to manufacture leaf mustard soak with high pore-minimizing effect by uniformly dispersing unique components of mustard soap into a natural soap base. CONSTITUTION: A manufacturing method of leaf mustard soap comprises: a step of preparing a natural soap base; a step of powderizing leaf mustard; a step of melting the natural soap base, injecting the leaf mustard powder into the melted natural soap for low-speed stirring; a step of mixing a jojoba or vitamin E into the mixture; a step of mixing an essential oil into the mixture at 40 °C or less; a step of adding perfumes into the mixture and injecting the mixture into a silicon mold; and a step of demolding solidified soap form the silicon mold.

Description

갓 비누 제조방법 및 그 방법에 의해 제조된 갓 비누{METHOD FOR MANUFACTURING LEAF MUSTARD SOAP AND MANUFACTURED LEAF MUSTARD SOAP BY THAT METHOD}METHOD FOR MANUFACTURING LEAF MUSTARD SOAP AND MANUFACTURED LEAF MUSTARD SOAP BY THAT METHOD}

본 발명은 갓 비누 제조방법 및 그 방법에 의해 제조된 갓 비누에 관한 것으로, 보다 상세하게는 천연성분이라 피부트러블이 없고, 특히 모공수렴 효과를 유도하여 탈모를 방지하며, 가려움증, 피부염증 진정효과를 극대화시킨 갓 비누 제조방법 및 그 방법에 의해 제조된 갓 비누에 관한 것이다.
The present invention relates to a fresh soap production method and a fresh soap produced by the method, more specifically because it is a natural ingredient, there is no skin trouble, in particular to induce pores convergence effect to prevent hair loss, itching, skin inflammation calming effect The present invention relates to a freshly prepared soap and a freshly prepared soap.

일반적으로, 비누는 수용액 중에서 가수분해되어 표면활성을 나타내며 표면장력을 강하시켜 안정된 거품 생성을 가능하게 하고 그에 따라 강한 세정력을 갖춘 것으로서, 주로 유지를 수산화알칼리로 끓이고 에스테르가 알칼리의 작용에 의해 가수분해되면서 비누화된 것에 소정의 향료 및 색소를 첨가하여 건조 고형화시킴으로써 제조된다.In general, soaps are hydrolyzed in aqueous solution to show surface activity and lower surface tension to enable stable foam generation and thus have strong detergency. The soap is mainly boiled fat or oil with alkali hydroxide and ester is hydrolyzed by the action of alkali. It is prepared by adding a predetermined flavor and pigment to the saponified and dry solidified.

이러한 비누는 근래 미용, 세정관련 기술의 급속한 발전과 소비자들의 다양한 요구에 기반하여 무수히 많은 기능성 비누들이 제품화되어 시판되고 있다.These soaps have recently been commercialized in the form of a myriad of functional soaps based on the rapid development of beauty and cleaning technologies and various needs of consumers.

예컨대, 원적외선ㆍ음이온 발산기능을 갖는 미백비누로부터 미용비누, 칼라비누, 투명비누를 비롯한 온열, 진정, 항염, 항균 등의 약리용 비누까지 그 종류와 다양한 형상의 비누들이 셀 수 없을 정도로 넘쳐나고 있다.For example, soaps of various types and types are overflowing from whitening soaps having far-infrared rays and anion dissipation functions to pharmacological soaps such as heat soaps, color soaps, and transparent soaps, and heat, soothing, anti-inflammatory and antibacterial agents.

그런데, 이와 같은 비누 대부분은 인공계면활성제나 인공경화제를 사용하고 있어 피부에 유해할 뿐만 아니라, 수질오염의 원인이 되기도 한다.However, most of these soaps use artificial surfactants or artificial hardeners, which are not only harmful to the skin, but also cause water pollution.

이에, 최근에는 천연비누들이 등장하기 시작했으며, 이들또한 다양한 기능성 비누들로 제조 판매되고 있다.Recently, natural soaps have begun to appear, and these are also manufactured and sold as various functional soaps.

하지만, 대부분의 천연비누들은 효능이 크지 않음에도 불구하고 허위 과장로 인해 소비자들의 피해가 커지고 있다.However, even though most natural soaps are not effective, false exaggeration is causing more damage to consumers.

특히, 스트레스성 탈모나 지성, 건성 피부로 인해 생기는 피부염, 세균성 가려움증 등의 경우 약리용 비누를 사용할 경우 비용부담이 크고, 약리용 비누들의 경우 대부분 인공계면활성제를 사용하는 비누들이 대다수이기 때문에 피부트러블이 많고, 피부 표피의 박리현상 등을 초래하는 문제가 있다.In particular, in case of stress hair loss, oily skin, dry skin dermatitis, bacterial itch, etc., pharmacological soap is expensive, and most of pharmacological soaps use artificial surfactants. There are many problems, such as peeling phenomenon of the skin epidermis.

이에, 본 발명자는 전라남도 여수지방의 특산품인 갓, 특히 돌산갓에 주목하였고, 이를 비누와 접목시켜 천연비누로 활용할 수 있는 길은 없는지 고심하게 되었다.Therefore, the present inventors paid attention to the specialty of the specialty of Yeosu, Jeollanam-do, especially Dolsan gat, and worries whether there is no way to utilize it as a natural soap by combining it with soap.

이러한 연구가 수행되는 동안 전남대학교 산학협력단에서 출원 공개한 공개특허 제10-2011-0076470호 '갓과 유자를 이용한 천연식물 비누 제조방법 및 조성물'이 개시되어 있음을 확인하였고, 이를 분석하게 되었다.While the research was conducted, it was confirmed that the Patent Application Publication No. 10-2011-0076470 published by Chonnam National University Industry-Academic Cooperation Foundation discloses a method and composition for preparing natural plant soap using fresh fruit and citron.

그런데, 본 발명자가 생각하고 있는 것과 개시된 선행기술의 내용은 많이 달랐는데, 이를 테면 개시된 기술에서는 갓 자체를 분말화하여 사용하지 않고, 갓으로부터 추출된 추출물을 사용하고 있을 뿐만 아니라 그외 유자 추출물도 함께 사용하고 있어 소비자가 손쉽게 만들거나 혹은 저렴하게 구매하여 사용하기 어렵다고 판단되었다.By the way, the present inventors think that the contents of the disclosed prior art were much different, for example, the disclosed technology does not use the powdered itself of the gat, not only using the extract extracted from the gat but also other citron extract It was judged that it is difficult for consumers to make it easily or buy it at low cost.

특히, 개시된 특허 기술에서는 갓과 유자 추출액을 어떠한 방식으로 추출하는지 정확하게 개시하지 않고 있어 갓을 활용한다는 측면에서는 유사성이 없지 않지만, 후술될 본 발명자의 기술 사상과 많은 차이가 있고, 상호 인용가능성이 거의 없는 것으로 판단되었고, 따라서 갓 분말을 이용한 약리성과 기능성을 모두 갖춘 천연 갓 비누를 개발할 필요가 있었다.
In particular, the disclosed patent technology does not disclose exactly how to extract the mustard and citron extract, there is no similarity in terms of utilizing the lampshade, but there are many differences from the technical spirit of the present inventors to be described later, and there is almost no mutual citation Therefore, it was necessary to develop a natural fresh soap with both pharmacological and functional properties.

본 발명은 상술한 바와 같은 종래 기술상의 제반 문제점을 감안하여 이를 해결하고자 창출된 것으로, 천연 비누베이스(비누소지)를 녹인 후 천연 갓 분말과 에센셜오일 등을 혼합하여 탈모를 예방하고, 가려움증이나 피부염증에 우수한 효능을 갖는 갓 성분이 함유된 천연 갓비누 제조방법 및 그 방법에 의해 제조된 천연 갓 비누를 제공함에 그 주된 목적이 있다.
The present invention was created in view of the above-mentioned problems in the prior art as described above, and after melting a natural soap base (soap), natural freshly mixed with powder and essential oils to prevent hair loss, itching and skin Its main purpose is to provide a method for producing a natural fresh soap containing fresh ingredients having excellent efficacy against inflammation and a natural fresh soap prepared by the method.

본 발명은 상기한 목적을 달성하기 위한 수단으로, 공지의 천연 비누베이스를 준비하는 단계; 생 갓을 수거한 후 불순물을 제거한 다음 수분 5% 미만이 되게 건조하고, 분쇄기로 분쇄하여 입도 0.05mm 미만이 되도록 미분화시키는 생 갓 분말화단계; 준비된 고체 상태의 천연 비누베이스를 85~95℃의 온도로 서서히 가열하여 용융시키고, 천연 비누베이스가 완전히 용융되면 천연 비누베이스 100g 대비 1~1.5g의 갓 분말을 투입한 후 교반기로 10~20분간 저속 교반(100rpm 이하)하여 투입된 갓 분말을 균일하게 혼합하는 혼합단계; 상기 혼합단계의 말기에 방부성을 제공하는 호호바오일 또는 비타민E를 천연 비누베이스 100g 대비 5~10g의 범위로 투입하여 5~10분간 교반하는 방부처리단계; 상기 방부처리단계 후 교반액의 온도가 40℃ 미만으로 떨어졌을 때 천연 비누베이스 100g 대비 1.5~2g의 비율로 에센셜오일을 투입하여 5~10분간 교반하는 에센셜오일 첨가단계; 교반이 완료되면 향료를 천연 비누베이스 100g 대비 1g 미만으로 첨가하여 교반한 후 교반액을 실리콘몰드에 주입하고 1~3시간 동안 방치하여 비누 형태로 고형화시키는 비누 고형화단계; 비누 고형화단계가 완료되면 실리콘몰드로부터 고형화된 비누를 꺼내 포장하는 탈형 및 포장단계;로 구성된 것을 특징으로 하는 갓 비누 제조방법을 제공한다.The present invention as a means for achieving the above object, preparing a known natural soap base; After collecting the fresh shade, the impurities are removed and then dried to less than 5% moisture, and pulverized with a grinder to finely powder the freshness to less than 0.05mm; The prepared natural soap base is slowly heated to a temperature of 85-95 ° C. and melted, and when the natural soap base is completely melted, 1 ~ 1.5 g of freshly prepared powder is added to 100g of natural soap base, followed by 10-20 minutes with a stirrer. A mixing step of uniformly mixing the freshly added powder by slow stirring (100 rpm or less); Preservative treatment step of adding 5 to 10g of jojoba oil or vitamin E which provides antiseptic at the end of the mixing step in a range of 5 to 10 g compared to 100 g of a natural soap base; When the temperature of the stirring solution after the antiseptic treatment step falls below 40 ℃ essential oil addition step of stirring for 5 to 10 minutes by putting the essential oil in a ratio of 1.5 ~ 2g compared to 100g of natural soap base; When the stirring is completed, the fragrance is added to less than 1g compared to the natural soap base 100g, the soap solidification step of injecting the stirring solution into the silicone mold and left for 1 to 3 hours to solidify in the form of a soap; When the soap solidification step is completed, demolding and packaging step of taking out the solidified soap from the silicone mold and packaging; provides a fresh soap manufacturing method comprising a.

이때, 상기 생 갓 분말화단계는 생 갓의 뿌리, 잎, 줄기를 수분 5% 미만으로 건조시킨 다음 각각을 분쇄한 후 1:1:1의 중량비로 혼합한 형태로 미분화되는 것에도 그 특징이 있다.At this time, the raw fresh powder powdering step is characterized in that the root, leaves, stems of the fresh freshly dried to less than 5% moisture and then pulverized each and then finely divided into a mixed form in a weight ratio of 1: 1: 1. have.

또한, 상기 비누 고형화단계에서, 향료를 투입하기 전에 진정작용을 강화하기 위해 건조후 입도 0.05mm 이하로 분말화한 산해박(Cynanchum paniculatum) 미분을 천연 비누베이스 100g 대비 0.5g 이하로 더 첨가하는 것에도 그 특징이 있다.In addition, in the solidifying step of the soap, in order to enhance the sedation before the fragrance is added, the powdered seaweed (Cynanchum paniculatum) powdered to a particle size of 0.05mm or less after drying to 0.5g or less compared to 100g of a natural soap base. It also has its features.

나아가, 상기에 기재된 갓 비누 제조방법으로 제조된 갓 비누 자체를 제공함에도 그 특징이 있다.
Furthermore, there is a feature in providing the freshly soap itself prepared by the freshly soap manufacturing method described above.

본 발명에 따르면, 갓이 함유한 특유의 성분이 천연 비누베이스에 균일하게 분포되어 있어 세안이나 세발시 모공수렴 효과를 높여 탈모를 예방하고, 피부 가려움증이나 피부염증을 진정시켜 주며, 무엇보다로 저렴하게 제조할 수 있는 장점이 있다.
According to the present invention, the unique ingredients contained in the freshly distributed evenly in the natural soap base to increase the pore-converging effect when washing or washing hair to prevent hair loss, soothing skin itching or skin inflammation, and most of all, it is inexpensive There is an advantage that can be manufactured.

이하에서는, 본 발명에 따른 바람직한 실시예를 보다 상세하게 설명하기로 한다.Hereinafter, preferred embodiments according to the present invention will be described in detail.

본 발명은 천연 비누베이스와 갓 분말을 이용하여 천연 갓 비누를 제조하는 방법을 제공한다.The present invention provides a method for producing a natural fresh soap using a natural soap base and freshly powdered.

이를 위해, 천연 비누베이스는 공지된 것이기는 하지만, 좀더 구체적으로 설명하면 천연 오일과 가성소다(NaOH)를 혼합하여 만들어진 고체상태로서, 본 발명에서를 이를 가열하여 녹인 다음 사용한다.To this end, the natural soap base is known, but in more detail, as a solid state made by mixing natural oil and caustic soda (NaOH), in the present invention is used after melting it by heating it.

특히, 가성소다는 상술한 선행 기술에도 개시되어 있듯이, 대표적인 강염기이기 때문에 취급시 주의하여야 한다.In particular, caustic soda, as disclosed in the above prior art, is a representative strong base and should be handled with care.

아울러, 천연 오일은 여러가지 종류가 있을 수 있다.In addition, there may be various kinds of natural oils.

대표적인 천연 오일로는 올리브오일, 코코넛오일, 팜오일, 포도씨오일, 피마자오일, 해바라기오일 등 다양한 종류가 될 수 있고, 종래 기술에서 언급한 선행기술에 개시된 비율로 혼합하여 천연 비누베이스를 만들 수도 있고, 혹은 그외 지금까지 공개된 모든 방식으로 천연 비누베이스를 만들 수 있다.Representative natural oils may be a variety of olive oil, coconut oil, palm oil, grape seed oil, castor oil, sunflower oil, etc., may be mixed in the ratio disclosed in the prior art mentioned in the prior art to make a natural soap base You can make a natural soap base in any of the ways that have been published.

본 발명은 천연 비누베이스를 만드는 것이 특징이 아니라, 공지된 천연 비누 베이스에 갓 분말을 첨가하는 것에 특징이 있는 것으로, 단순히 갓 분말만 첨가한다고 해서 효능과 특성을 갖는 것이 아니므로 거기에 기술적 특징이 있는 것이다.The present invention is not characterized by making a natural soap base, but is characterized by adding a fresh powder to a known natural soap base, and simply adding fresh powder does not have efficacy and characteristics, so the technical features therein It is.

덧붙여, 본 발명에서 사용되는 갓(leaf mustard)은 선행 기술에도 잘 나타나 있듯이, 독특한 자극성 매운맛을 갖는데 이는 갓에 함유되어 있는 glucosinolate류의 일종인 sinigrin에 효소 myrosinase(thioglucoside glucohydrolase)가 작용하여 생성되는 것으로 알려져 있다.In addition, the mustard used in the present invention (leaf mustard) has a unique irritant pungent, as well shown in the prior art, which is produced by the action of the enzyme myrosinase (thioglucoside glucohydrolase) to sinigrin, a kind of glucosinolates contained in the Known.

또한, 갓에 관한 연구로 갓의 항산화 활성을 측정한 결과 시금치보다 활성이 강하였으며, 유효성분 중의 하나로 sinapine을 분리하였다고 보고되고 있으며, 갓의 항산화작용이 있음도 확인되었다.In addition, the studies on the gat showed that the antioxidant activity of the gat was stronger than that of spinach, and it was reported that sinapine was isolated as one of the active ingredients.

뿐만 아니라, 갓의 생리활성 성분으로 대표적인 것은 십자화과 식물 특유의 isothiocyanate인데, 주성분인 allylisothiocyanate 뿐만 아니라, 2-phenyl ethyl isothiocyanate, 5-methyl thiopentyl isothiocyanate, benzyl isothiocyanate 등의 유도체에도 강력한 항균작용이 있음으로 확인하였고, isothiocyanate 종류에 따라 항균spectrum 항균활성 등에 있어서 차이를 나타낸다고 보고되어 있다.In addition, the most representative of the physiologically active components of gat is isothiocyanate, which is unique to cruciferous plants. In addition, it is reported that the antimicrobial specrum exhibits a difference in antimicrobial activity according to isothiocyanate type.

특히, 갓에는 isothiocyanate 이외의 항균성분도 확인되고 있는데 갓의 추출물 중 항균작용이 가장 강한 fraction에서 flavonoid인 isorhamnetin-3-o-β-glucopyrano-side를 분리하여 항균활성을 확인하였다.In particular, the antimicrobial component of isothiocyanate was also identified in the gat. Isolation of flavonoid isorhamnetin-3-o-β-glucopyrano-side from the strongest antimicrobial activity of gat extract confirmed the antimicrobial activity.

갓은 항균작용 뿐만 아니라 항진균작용도 있는 것으로 연구되었으며, 특히, 돌산 갓의 항암성은 뿌리에서, 항산화성과 ACE 저해율은 잎에서 활성이 높게 나타났다고 보고되어 있다.Gad has been studied to have antifungal activity as well as antimicrobial activity. In particular, the anticancer activity of Dolsan gat has been reported to have high activity in roots, and antioxidant and ACE inhibition rates in leaves.

본 발명은 이러한 갓의 효능을 고려하여 연구 완성되었다.The present invention has been studied in consideration of the efficacy of these lampshade.

이하, 본 발명에 따른 갓 비누 제조방법에 대하여 설명한다.Hereinafter, a method for preparing a fresh soap according to the present invention will be described.

먼저, 공지의 천연 비누베이스를 준비하는 단계가 수행된다.First, a step of preparing a known natural soap base is performed.

천연 비누베이스는 앞서 설명한 바와 같이, 공지된 것을 사용하기 때문에 특별히 한정할 필요는 없다.As described above, the natural soap base does not need to be particularly limited because it uses known materials.

이어, 생 갓 분말화 단계가 수행된다.Subsequently, a fresh fresh powdering step is performed.

생 갓을 분말화하는 단계는 생 갓을 수거한 후 불순물을 제거한 다음 수분 5% 미만이 되게 건조기 또는 자연상태에서 말린 다음 분쇄기로 분쇄하여 입도 0.05mm미만이 되도록 미분화시키는 단계이다.The step of pulverizing the fresh shade is a step of collecting the fresh shade, removing impurities, and drying it in a dryer or natural state to less than 5% moisture, and then pulverizing with a pulverizer to finely reduce the particle size to less than 0.05 mm.

이때, 앞서 설명하였듯이 생 갓의 뿌리 부분이 가장 효과 있으므로 이 부분을 전량 사용하면 좋겠지만, 효과의 평준화를 위해 뿌리, 잎, 줄기를 수분 5% 미만으로 충분히 건조시킨 다음 각각을 분쇄한 후 1:1:1의 중량비로 혼합하여 사용하면 더욱 좋다.At this time, as described above, the root portion of the fresh mustard is the most effective, so you may use the whole amount, but for leveling the effect, dry the roots, leaves, and stems to less than 5% of moisture, and then grind each 1: It is better to mix and use at a weight ratio of 1: 1.

여기에서, 생 갓의 수분을 5%로 미만으로 건조해야 하는 이유는 생 갓의 경우 엽산이 풍부하게 함유되어 있고, 또 카로틴, 비타민C, 철분이 함유되어 있으며, 독특한 매운 맛을 내는 시니그린이 들어 있는데, 특히 매운맛을 내는 시니그린은 건조시 약해지며, 5% 미만의 수분을 갖게 되면 매운맛이 85~90% 정도 경감되기 때문에 상기 범위의 수분함량을 갖도록 고르고 균일하게 건조하여야 한다.Here, the reason why the fresh mustard should be dried to less than 5% is that the fresh mustard contains rich in folic acid, carotene, vitamin C and iron, and a unique spicy flavor In particular, the spicy flavor of shinny green is weak when drying, and if the moisture of less than 5% is reduced to about 85 to 90% of the spicy taste should be evenly and uniformly dried to have a water content in the above range.

건조방식은 열풍 건조가 바람직하나, 필요에 따라 마이크로트론, 즉 전자렌지에 사용되는 원리를 이용하여 급속 건조도 가능하다.The drying method is preferably hot air drying, but if necessary, rapid drying is also possible by using a principle used in a microtron, that is, a microwave oven.

아울러, 생 갓의 분말을 상기의 입도로 한정하는 이유는 0.05mm를 초과하게 되면 알갱이 형태로 남게 되어 피부와 접촉시 피부 표피를 거칠게 하거나 연마시키면서 깍아 내리기 때문에 상기 범위로 한정하여 모공 속으로 침투할 수 있는 크기인 상기 크기로 한정해야 한다.In addition, the reason for limiting the freshness of the powder to the above granularity is that when it exceeds 0.05mm, it remains in the form of granules, and when it comes into contact with the skin, it cuts while roughening or polishing the skin epidermis, so that it can penetrate into the pores. The size should be limited to the above size.

이어, 천연 비누베이스와 생 갓 분말 혼합단계가 수행된다.Subsequently, a natural soap base and freshly ground powder mixing step is performed.

상기 혼합단계는 고체 상태의 천연 비누베이스를 85~95℃의 온도로 서서히 가열하여 용융시키고, 천연 비누베이스가 완전히 용융되면 천연 비누베이스 100g 대비 1~1.5g의 갓 분말을 투입한 후 교반기로 10~20분간 저속 교반(100rpm 이하)하여 투입된 갓 분말이 충분히 그리고 고르고 균일하게 혼합되도록 하여 준다.The mixing step is to slowly melt the natural soap base in the solid state to a temperature of 85 ~ 95 ℃, and when the natural soap base is completely melted 1 ~ 1.5g of freshly prepared powder compared to 100g of natural soap base 10 Slowly stir for 20 minutes (100 rpm or less) to allow the freshly added powder to be mixed sufficiently, evenly and evenly.

이때, 상기 갓 분말을 천연 비누베이스 대비 상기 범위로 한정하여 투입하는 이유는 비록 건조과정에서 갓의 매운 성분이 많이 휘발되었다고 하지만, 그래도 여전히 매운 성분이 남아 있으므로 1.5g을 초과하면 피부 부작용을 야기할 뿐만 아니라 비누 고유의 특징이 거품 발현성이 떨어지고, 1g 미만으로 첨가되면 갓이 갖는 톡특한 특성인 모공수렴과 가려움증 및 피부염증 진정작용이 거의 발현되지 않기 때문에 상기 범위로 한정해야 한다.At this time, the reason why the fresh powder is limited to the range compared to the natural soap base is that although the spicy ingredient of the freshly evaporated during the drying process, the spicy ingredient still remains, so if it exceeds 1.5 g, it may cause skin side effects. In addition, the inherent characteristics of the soap is less foam expression, and when added to less than 1g should be limited to the above range because almost no characteristic pore convergence and itching and skin inflammation sedation is not expressed.

이렇게 하여, 융용된 천연 비누베이스에 생 갓 분말이 완전히 혼합되면, 이후 방부처리단계가 수행된다.In this way, when the raw fresh powder is completely mixed in the molten natural soap base, a preservation step is then performed.

상기 방부처리단계는 본 발명이 천연 비누라는 점을 감안하여 방부성을 제공하는 호호바오일 또는 비타민E를 첨가하는 형태로 이루어지는데, 이들은 상기 천연 비누베이스 100g 대비 5~10g의 범위로 투입되어야 한다.The antiseptic treatment step is made in the form of adding jojoba oil or vitamin E to provide antiseptic in view of the fact that the present invention is a natural soap, these should be added in the range of 5 ~ 10g compared to 100g of the natural soap base.

여기에서, 호호바오일은 피부의 피지와 유사한 성분을 가진 오일로서, 부드럽고 피부에 잘 흡수되므로 아로마테라피 희석용 오일로 가장 많이 애용되며, 주로 비누와 바디 크림, 바디 로션 등을 만드는데 쓰인다.Here, jojoba oil is an oil having an ingredient similar to the sebum of the skin, and is used most frequently as an aromatherapy diluent oil because it is soft and well absorbed by the skin, and is mainly used to make soaps, body creams and body lotions.

특히, 산화방지 성분이 있어 방부성이 뛰어나 오랫동안 보존할 수 있는 것이 장점이며, 비누에 첨가할 때는 전체 비누 용량의 10% 이하로 넣도록 규정되어 있으므로 본 발명에서는 천연 비누베이스 100g 대비 10g 이하로 첨가해야 하고, 5g 미만으로 첨가되면 산화방지 기능이 떨어지므로 상기 범위로 유지하여야 한다.In particular, there is an anti-oxidant component is excellent in preservatives and can be preserved for a long time, and when added to the soap is prescribed to put less than 10% of the total soap capacity in the present invention should be added to 10g or less than 100g of natural soap base If less than 5g is added, the anti-oxidation function is lowered, so it must be maintained in the above range.

또한, 비타민E는 세포를 지켜주는 항산화작용을 하기 때문에 산패를 막는 일종의 방부기능을 가지고 있다.In addition, vitamin E has a kind of antiseptic function to prevent rancidity because it is an antioxidant that protects cells.

본 발명에서는 합성 비타민E는 물론 천연 비타민E 모두 사용할 수 있는데, 천연 비타민E의 경우 토코페롤b-알파, 토코페롤b-베타 모두 사용할 수 있다.In the present invention, both synthetic vitamin E as well as natural vitamin E can be used. For natural vitamin E, both tocopherol b-alpha and tocopherol b-beta can be used.

아울러, 비타민E를 섭취할 경우에는 하루 권장량이 7.5~9mmg으로 한정되어 있지만, 본 발명인 비누는 섭취하는 것이 아니므로 이를 방부제로 사용할 경우 앞서 설명한 범위로 투입 혼합하여야 한다. In addition, when ingesting vitamin E, the recommended daily amount is limited to 7.5 ~ 9mmg, but the present invention soap is not ingested, so when used as a preservative should be mixed in the above-mentioned range.

혼합방식은 상기 생 갓 분말이 투입된 후 저속 교반되는 말기에 투입되어 약 5~10분간 혼합 교반됨이 바람직한데, 이는 생 갓 분말이 충분하고 균일하게 분포된 이후에 방부성 물질이 투입되어야 하기 때문이다.The mixing method is preferably added at the end of the low-speed stirring after the freshly prepared powder is mixed and stirred for about 5 to 10 minutes, since the preservative should be added after the freshly prepared fresh powder is sufficiently and uniformly distributed. .

이어, 에센셜오일 첨가단계가 수행된다.Subsequently, the essential oil addition step is performed.

상기 에센셜오일 첨가단계는 방부처리단계 후 교반액의 온도가 40℃ 미만으로 떨어졌을 때 천연 비누베이스 100g 대비 1.5~2g의 비율로 투입된 후 5~10분간 교반하여야 한다.The essential oil addition step should be stirred for 5 to 10 minutes after the antiseptic treatment step is added at a rate of 1.5 ~ 2g compared to 100g of the natural soap base when the temperature of the stirring solution drops below 40 ℃.

이는 에센셜오일 자체가 약간의 휘발성을 가지고 있기 때문에 40℃를 초과한 온도에서는 휘발분이 급격히 증가하여 원하는 효과를 얻을 수 없기 때문에 그 이하의 온도에서 충분히 교반될 수 있도록 하기 위함이다.This is because the essential oil itself has some volatility, so that at a temperature exceeding 40 ° C., the volatilization increases rapidly, and thus, it is possible to sufficiently stir at a temperature lower than the desired effect.

여기에서, 에센셜오일이란 방향 식물에서 추출한 휘발성 있는 고농축 정유로서, 본 발명에서는 소독성과 방부성을 강화시키기 위해 첨가된다.Here, essential oils are volatile highly concentrated essential oils extracted from aromatic plants, and are added in the present invention to enhance disinfection and antiseptic properties.

특히, 가장 바람직한 에센셜오일로는 라벤더 에센셜오일, 티트리 에센셜오일 중 하나이고, 1.5g 미만으로 첨가되면 휘발분 때문에 소독성 및 방부성 강화기능이 거의 없고, 2g을 초과하면 비누화가 지연됨은 거품 발생이 줄어들게 되므로 상기 범위로 첨가하여야 한다.In particular, the most preferable essential oil is one of lavender essential oil and tea tree essential oil, and when it is added below 1.5g, there is little disinfection and antiseptic strengthening function due to volatile matter, and when it exceeds 2g, saponification is delayed to reduce foaming. Therefore, it should be added in the above range.

이러한 과정을 거쳐 충분한 시간 동안 교반이 완료되면 다양한 종류의 향료를 거품 발생을 저해하지 않을 정도의 양인 천연 비누베이스 100g 대비 1g 미만으로 첨가하고, 교반을 완료한다.After the agitation is completed for a sufficient time through this process, various types of fragrances are added to less than 1 g of the natural soap base 100g in an amount that does not inhibit the foaming, and the stirring is completed.

이후, 교반이 완료된 교반액을 실리콘몰드에 주입한 후 약 1~3시간 동안 방치하여 비누 형태로 고형화시키는 단계가 수행된다.Thereafter, after the stirring is completed, the stirring solution is injected into the silicon mold, and then left to stand for about 1 to 3 hours to solidify in a soap form.

이어, 고형화단계가 완료되면 실리콘몰드로부터 고형화된 비누를 꺼내는 탈형 후 포장하여 제품화하게 된다.Subsequently, when the solidification step is completed, the product is packaged after demolding to remove the solidified soap from the silicon mold.

덧붙여, 진정작용을 강화하기 위해 상기 향료를 투입하기 전에 산해박(Cynanchum paniculatum)을 건조시켜 입도 0.05mm 이하의 미분상태로 분말화하여 천연 비누베이스 100g 대비 0.5g 이하로 더 첨가할 수 있다.In addition, before the fragrance is added to enhance the sedation, acid seabac (Cynanchum paniculatum) may be dried and powdered into a fine particle size of 0.05 mm or less, and may be further added to 0.5 g or less than 100 g of a natural soap base.

산해박은 서장경이라고도 하는 박주가리과로 산과 들의 볕이 잘 드는 풀밭에서 자라며, 줄기는 곧게 서고 가늘며 마디 사이가 길고, 개화기는 8~9월경이며 연한 황갈색을 띤다. 이러한 산해박의 뿌리를 한방에서는 서장경(徐長卿)이라는 약재로 쓰는데, 진통·진정·항균 효과가 있는 것으로 알려져 있다.Sanhaebak is also called Seojanggyeong, which grows in the sunny meadows of mountains and fields. The stems stand straight, thin, long nodes, and bloom in August to September, and have a light tan. The root of Sanhaebak is used as a medicine called Seo Jang-kyung in oriental medicine, and it is known to have analgesic, soothing, and antibacterial effects.

본 발명에서는 생 갓 분말과 보강 보조하여 피부진정 효과를 높이게 되며, 투입되는 분말량이 많아질 수록 비누 사용시 거품이 나지 않기 때문에 이를 방지하고자 최대 0.5g까지만 첨가하는 것이 바람직하다. In the present invention, the freshness of the powder and reinforcing aid to increase the skin soothing effect, the amount of powder to be added is preferably added only up to 0.5g to prevent this because the foam does not foam when using the soap.

이하, 실시예에 대하여 설명한다.Hereinafter, examples will be described.

[실시예][Example]

본 발명에 따라 제조된 갓 비누의 효능을 확인하기 위해 다음과 같이 실험하였다.In order to confirm the efficacy of the freshly prepared soap according to the present invention was tested as follows.

(1) 세정력 테스트(1) cleaning power test

본 발명에 따른 갓 비누의 세정력을 확인하기 위해 세안 후 피부세정력을 측정하였는데, 측정방법은 온도 20~22℃, 습도 40~60%로 유지되는 실험실에서 선발된 8명의 피실험자(20대~50대 남녀 각 1명씩)로 하여금 세안 후 2시간 간격으로 6시간 동안 피부의 유분제거율을 측정하였는데, 측정도구는 AROMA-TS 유분측정기를 사용하였고, 남자와 여자로 나누어 평균하였다.Skin cleansing power was measured after washing to check the washing power of the freshly soap according to the present invention, and the measuring method was selected from eight test subjects selected from a laboratory maintained at a temperature of 20 to 22 ° C. and a humidity of 40 to 60% (20 to 50 years old). The skin oil removal rate was measured for 6 hours at 2 hour intervals after washing the face. The measurement tool was AROMA-TS oil meter, and the average was divided into male and female.

측정결과, 세안 후 유분량은 세안 전에 비해 표 1과 같이 나타났는데, 비교를 위해 국내 비누제조업체인 L사, D사의 제품에 대해서도 동일하게 테스트하였다.As a result, the amount of oil after cleansing was shown in Table 1 as compared to before cleansing. For comparison, the same test was conducted on the products of domestic soap manufacturers L and D.

구분division 갓 비누Freshly soap L사 비누L company soap A사 비누A company soap 남자man 68→6168 → 61 64→5964 → 59 59→5759 → 57 여자Woman 62→5762 → 57 61→5761 → 57 58→5658 → 56

실험결과, 본 발명에 따른 갓 비누도 충분한 세정력을 가지고 있음이 입증되었고, 적어도 비교되는 L사, A사와 동등이상의 효과를 나타내는 것으로 확인되었다.As a result, it was proved that the fresh soap according to the present invention also had sufficient cleaning power, and had at least the same effect as that of L company and A company to be compared.

(2) 거품성 테스트(2) foam test

본 발명에 따른 갓 비누의 거품성을 테스트하기 위해 500㎖ 플라스크에 갓 비누, L사 비누, A사 비누 각각을 1g씩 투입하고 동일한 방법으로 흔들어 각 비누의 거품성을 육안으로 확인하였다.In order to test the foaming properties of the freshly soaps according to the present invention, 1 g each of freshly soap, L company soap, and A company soap was put in a 500 ml flask and shaken in the same manner to visually check the foaming properties of each soap.

육안으로 확인 결과, 3개 비누 모두 거품성이 우수하였다.As a result of visual observation, all three soaps were excellent in foaming property.

이로써, 본 발명에 따른 갓 비누도 충분한 거품성을 갖는 비누로서 사용할 수 있음을 확인하였다.Thus, it was confirmed that the fresh soap according to the present invention can also be used as a soap having sufficient foamability.

(3) 모공수렴성 테스트(3) pore convergence test

본 발명에 따른 갓 비누의 모공수렴성을 테스트하기 위해 탈모가 진행중인 남성 3명을 선발하여 갓 비누, L사 비누, A사 비누를 각각 나누어 준 후 3일씩 총 9일에 걸쳐 세발하도록 하였다.In order to test the pore astringency of the fresh soap according to the present invention, three males were selected for hair loss, and each was divided into freshly soap, L company soap, and A company soap, and then three days were taken for three days.

이때, 3일 후 비누를 바꿀 때에는 하루 동안 비누를 사용하지 못하게 했으며, 비누를 사용하지 않을 경우에는 동일한 샴푸를 1일 1회만 사용하도록 하였다.At this time, when changing the soap after three days was not allowed to use the soap for a day, when the soap is not used to use the same shampoo only once a day.

아울러, 세발시 빠지는 머리카락의 개수를 세어 보고하도록 하였으며, 이를 취합하였고, 그 결과는 표 2에 나타내었다.In addition, to report the number of hair falls out when the tricycle, it was collected, and the results are shown in Table 2.

구분division 남성1Male 1 남성2Male 2 남성3Male 3 갓 비누Freshly soap 4개4 2개2 3개Three L사 비누L company soap 6개6 5개5 6개6 A사 비누A company soap 5개5 5개5 7개7

상기 표 2의 결과로부터, 본 발명에 따른 갓 비누가 모공을 축소시키는 수렴효과가 뛰어나 세발시 머리카락 보지력이 우수하므로 머리카락이 쉽게 빠지지 않은 것으로 확인되었다.From the results of Table 2, it was confirmed that the freshly soap according to the present invention has excellent converging effect of shrinking pores, and thus hair was not easily pulled out because hair holding power was excellent at trituration.

또한, 가려움증과 피부염증 진정효과의 경우도 임상실험결과, 우수한 것으로 확인되었지만 이를 정량적으로 검증하기 어려워 간략히 언급하는 것으로 대신한다.In addition, itching and skin irritation sedative effects were also confirmed as clinical results, but it is difficult to quantitatively verify it is replaced with a brief description.

이로써, 본 발명에 따른 갓 비누는 기능성 비누로서 충분한 사용가치를 지닌 것으로 확인되었다.Thus, the fresh soap according to the present invention was found to have sufficient value as a functional soap.

Claims (4)

공지의 천연 비누베이스를 준비하는 단계;
생 갓을 수거한 후 불순물을 제거한 다음 수분 5% 미만이 되게 건조하고, 분쇄기로 분쇄하여 입도 0.05mm 미만이 되도록 미분화시키는 생 갓 분말화단계;
준비된 고체 상태의 천연 비누베이스를 85~95℃의 온도로 서서히 가열하여 용융시키고, 천연 비누베이스가 완전히 용융되면 천연 비누베이스 100g 대비 1~1.5g의 갓 분말을 투입한 후 교반기로 10~20분간 저속 교반(100rpm 이하)하여 투입된 갓 분말을 균일하게 혼합하는 혼합단계;
상기 혼합단계의 말기에 방부성을 제공하는 호호바오일 또는 비타민E를 천연 비누베이스 100g 대비 5~10g의 범위로 투입하여 5~10분간 교반하는 방부처리단계;
상기 방부처리단계 후 교반액의 온도가 40℃ 미만으로 떨어졌을 때 천연 비누베이스 100g 대비 1.5~2g의 비율로 에센셜오일을 투입하여 5~10분간 교반하는 에센셜오일 첨가단계;
교반이 완료되면 향료를 천연 비누베이스 100g 대비 1g 미만으로 첨가하여 교반한 후 교반액을 실리콘몰드에 주입하고 1~3시간 동안 방치하여 비누 형태로 고형화시키는 비누 고형화단계;
비누 고형화단계가 완료되면 실리콘몰드로부터 고형화된 비누를 꺼내 포장하는 탈형 및 포장단계;로 구성된 것을 특징으로 하는 갓 비누 제조방법.
Preparing a known natural soap base;
After collecting the fresh shade, the impurities are removed and then dried to less than 5% moisture, and pulverized with a grinder to finely powder the freshness to less than 0.05mm;
The prepared natural soap base is slowly heated to a temperature of 85-95 ° C. and melted, and when the natural soap base is completely melted, 1 ~ 1.5 g of freshly prepared powder is added to 100g of natural soap base, followed by 10-20 minutes with a stirrer. A mixing step of uniformly mixing the freshly added powder by slow stirring (100 rpm or less);
Preservative treatment step of adding 5 to 10g of jojoba oil or vitamin E which provides antiseptic at the end of the mixing step in a range of 5 to 10 g compared to 100 g of a natural soap base;
When the temperature of the stirring solution after the antiseptic treatment step falls below 40 ℃ essential oil addition step of stirring for 5 to 10 minutes by putting the essential oil in a ratio of 1.5 ~ 2g compared to 100g of natural soap base;
When the stirring is completed, the fragrance is added to less than 1g compared to the natural soap base 100g, the soap solidification step of injecting the stirring solution into the silicone mold and left for 1 to 3 hours to solidify in the form of a soap;
Fresh soap production method comprising a; demolding and packaging step of taking out the solidified soap from the silicone mold when the soap solidification step is completed.
청구항 1에 있어서;
상기 생 갓 분말화단계는 생 갓의 뿌리, 잎, 줄기를 수분 5% 미만으로 건조시킨 다음 각각을 분쇄한 후 1:1:1의 중량비로 혼합한 형태로 미분화되는 것을 특징으로 하는 갓 비누 제조방법.
The method according to claim 1;
The fresh-fresh powdering step is a freshly prepared soap, characterized in that the roots, leaves, stems of the freshly freshly dried to less than 5% of moisture and then pulverized each of them to be finely divided into a mixed form in a weight ratio of 1: 1: 1. Way.
청구항 1에 있어서;
상기 비누 고형화단계에서, 향료를 투입하기 전에 진정작용을 강화하기 위해 건조후 입도 0.05mm 이하로 분말화한 산해박(Cynanchum paniculatum) 미분을 천연 비누베이스 100g 대비 0.5g 이하로 더 첨가하는 것을 특징으로 하는 갓 비누 제조방법.
The method according to claim 1;
In the soap solidifying step, the powdered acid seaweed (Cynanchum paniculatum) powdered to a particle size of 0.05mm or less after drying to enhance the sedation before the fragrance is added to less than 0.5g compared to 100g of the natural soap base. Freshly soap production method.
청구항 1 내지 청구항 3 중 어느 한 항에 따른 갓 비누 제조방법으로 제조된 갓 비누.Freshly prepared soaps according to any one of claims 1 to 3, freshly soap manufacturing method.
KR1020110103365A 2011-10-11 2011-10-11 Method for manufacturing leaf mustard soap and manufactured leaf mustard soap by that method KR101222743B1 (en)

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Cited By (2)

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KR101804954B1 (en) * 2017-05-30 2018-01-11 문하영 Method for manufacturing natrual rice soap using of rice powder
US11019548B2 (en) 2017-11-24 2021-05-25 Samsung Electronics Co., Ltd. Electronic device and communication method thereof

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JP2006052340A (en) 2004-08-12 2006-02-23 Ttc:Kk Food detergent
KR20090127389A (en) * 2009-07-02 2009-12-11 이정미 Method for manufacturing a soap with gwamegi using natural soap base
KR20110076470A (en) * 2009-12-29 2011-07-06 전남대학교산학협력단 The composition and method manufacture of soap plant function use citron and leaf mustard

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Publication number Priority date Publication date Assignee Title
KR20020095616A (en) * 2001-06-15 2002-12-28 나드리화장품주식회사 Anti-irritant cosmetic composition containing medical plant extracts
JP2006052340A (en) 2004-08-12 2006-02-23 Ttc:Kk Food detergent
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KR20110076470A (en) * 2009-12-29 2011-07-06 전남대학교산학협력단 The composition and method manufacture of soap plant function use citron and leaf mustard

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101804954B1 (en) * 2017-05-30 2018-01-11 문하영 Method for manufacturing natrual rice soap using of rice powder
US11019548B2 (en) 2017-11-24 2021-05-25 Samsung Electronics Co., Ltd. Electronic device and communication method thereof
US11218938B2 (en) 2017-11-24 2022-01-04 Samsung Electronics Co., Ltd. Electronic device and communication method thereof

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