KR101066184B1 - Bubble bath composition comprising for mandarin and carrot macerate and preparing method thereof - Google Patents
Bubble bath composition comprising for mandarin and carrot macerate and preparing method thereof Download PDFInfo
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Abstract
본 발명은 천연물을 함유하는 거품 입욕제 조성물에 관한 것으로, 더욱 상세하게는 감귤 또는 당근을 포함하는 거품 입욕제 조성물 및 그 제조방법에 관한 것이다.The present invention relates to a foam bath composition containing a natural product, and more particularly, to a foam bath composition comprising a tangerine or carrot and a method of manufacturing the same.
제주산 감귤, 당근, 거품 입욕제 Jeju tangerines, carrots, foam bath
Description
도 1은 본 발명의 조성물의 제조 공정도를 나타낸다.1 shows a manufacturing process diagram of the composition of the present invention.
본 발명은 천연물을 함유하는 거품 입욕제 조성물에 관한 것으로, 더욱 상세하게는 감귤 또는 당근을 포함하는 거품 입욕제 조성물 및 그 제조방법에 관한 것이다.The present invention relates to a foam bath composition containing a natural product, and more particularly, to a foam bath composition comprising a tangerine or carrot and a method of manufacturing the same.
일반적으로 입욕제라 함은 천연 또는 합성 성분으로 이루어진 조성물로서, 목욕 시에 탕 속의 물에 투입하여 입욕에 의한 피부 미용 및 건강 증진 효과를 극대화시키기 위한 목욕 보조제를 말하며, 현재 시중에는 다양한 종류의 천연 및 합성 입욕제가 시판되고 있다.Generally, a bathing agent is a composition composed of natural or synthetic ingredients, and refers to a bath aid for maximizing skin beauty and health promotion effect by bathing in water in a bath when bathing. Currently, various kinds of natural and Synthetic baths are commercially available.
입욕제의 개발에 있어서는, 입욕제가 기본적으로 구비하여야 하는 피부 미용의 기능 이외에도, 입욕제의 다양한 성분들이 민감한 피부에 미치는 영향을 고려하여 피부 장애를 야기하는 각종의 부작용들에 대하여 고려하여야 하며, 또한 현재는In the development of bathing agents, in addition to the functions of skin care that the bathing agents should be basically provided, various side effects that cause skin disorders should be considered in consideration of the effects of various components of the bathing agents on sensitive skin.
이러한 입욕제의 기본적 기능에 더하여, 피로 회복 및 각종의 질병 예방 등에 있어서도 긍정적으로 기능을 하는 기능성 입욕제에 대한 연구 개발이 활발히 이루어지고 있다.In addition to the basic functions of these bathing agents, research and development are being actively conducted on functional bathing agents that function positively in fatigue recovery and prevention of various diseases.
기능성 입욕제에 대한 연구 개발은 크게 인위적으로 합성한 성분들을 함유하는 합성 화학물질 입욕제와 자연식물 등으로부터 유래한 성분들을 함유하는 천연물질 입욕제에 대한 연구 개발로 분류된다.Research and development of functional baths are classified into research and development of synthetic chemical baths containing artificially synthesized ingredients and natural baths containing ingredients derived from natural plants.
전자에 해당하는 국내외 특허 문헌들로는 아래와 같은 것들이 있다.The domestic and foreign patent documents corresponding to the former are as follows.
대한민국 특허공고 94-7919호는 탄산염 5 내지 80중량%, 산 10 내지 80중량% 및 보습제 0.001 내지 10중량%를 함유하는 약산성 입욕제에 관하여 개시하고 있다.Korean Patent Publication No. 94-7919 discloses a weakly acidic bath containing 5 to 80% by weight carbonate, 10 to 80% by weight acid and 0.001 to 10% by weight moisturizer.
대한민국 공개특허 92-14465호는 산과 탄산염 및 0.1 내지 50중량%의 콜로이달 물질을 함유하는 입욕제에 관하여 개시하고 있다.Korean Patent Laid-Open Publication No. 92-14465 discloses a bath containing acid and carbonate and 0.1 to 50% by weight of colloidal material.
일본특허 평7-91180호는 유기산과 탄산염을 함유하는 입욕제로서 유기산의 70중량% 이상을 아데닌산으로 하고, 향료성분으로서 탄소수 10의 터핀계 탄화수소 또는 탄소수 5 내지 10의 알코올의 개미산 에스테르, 초산 에스테르, 또는 프로Japanese Patent No. Hei 7-91180 is a bathing agent containing an organic acid and a carbonate, wherein at least 70% by weight of an organic acid is adenic acid, and formic acid esters and acetic acid esters of terpene hydrocarbons having 10 or more carbon atoms or alcohols having 5 to 10 carbon atoms as perfume components. , Or pro
피온산 에스테르의 1종 또는 2종 이상을 함유하는 것을 특징으로 하는 입욕제에 관하여 개시하고 있다.It discloses about the bath agent characterized by containing 1 type (s) or 2 or more types of a ionic acid ester.
상기 특허 문헌들은 모두 유기산, 탄산염, 이온성 계면활성제 및 각종의 폴리머 등의 인위적으로 합성한 합성 화학물질들을 입욕제의 주성분으로 함유하고 있는 관계로, 제조 공정이 복잡하고, 함께 첨가된 유화제, 방부제 등으로 인한 피부장애 유발의 문제가 있을 수 있으며, 천연의 향을 얻기가 어려울 뿐 아니라, 천연 입욕제에 포함된 각종의 건강증진 천연 추출물질을 함유하지 않는 관계로 상대적으로 건강증진 효과가 낮다는 문제점이 있다.All of the above patent documents contain artificial synthetic synthetic chemicals such as organic acids, carbonates, ionic surfactants, and various polymers as main components of the bath, and thus, the manufacturing process is complicated, and emulsifiers, preservatives, etc. added together There may be a problem of causing skin disorders, and it is difficult to obtain a natural aroma, and relatively low health promotion effect because it does not contain a variety of health-promoting natural extracts contained in natural baths. have.
또한, 통상적으로 종래 자연식물 등으로부터 추출한 성분들을 함유하는 천연추출물질 입욕제는 녹차 및 외국에서 생산되는 허브 식물을 이용한 목욕용 백의 형태로 시판되거나, 분말 형태의 입욕제는 우유 성분과 무기염 등을 함유한 제품들이In addition, conventionally, a natural extract material bath containing components extracted from natural plants, etc. are commercially available in the form of a bath bag using green tea and foreign herbal plants, or powdered baths contain milk components and inorganic salts. Products
시판되어 왔다. 그러나, 녹차 목욕용 팩은 침출이 용이하지 않은 문제점이 있으며, 허브식물의 목욕용 백 또한 침출이 용이하지 않고, 소비자에게 입수되기까지의 유통기간이 장기간이 될 수밖에 없는 외국에서 생산되어 수입된 인공적인 향을 첨가함으로써 천연의 향을 느끼기 어려우며, 피부 미용 및 건강 증진에 있어서 그 효과가 뛰어나지 못하다는 문제점이 있었다.It has been commercially available. However, the green tea bath pack has a problem that it is not easy to leach, the herbal bag of the herbal plant is also not easy to leach, and the artificial fragrance produced and imported from abroad, which has a long shelf life until it is available to consumers. It is difficult to feel the natural aroma by the addition, there was a problem that the effect is not excellent in skin beauty and health promotion.
일반적인 샤워와는 달리 입욕(욕조목욕)은 혈액순환을 도와 피로회복과 각질층을 부드럽게 해주는 것은 물론 우울증과 긴장 완화 등의 효과를 줄 수 있고 입욕할 때 특히 거품목욕을 하면 노폐물 제거에 효과적이고, 목욕시 상쾌한 기분으로 목욕을 즐길 수 있는 효과가 있다.Unlike general showers, bathing helps to circulate blood, soothing tiredness and stratum corneum, as well as relieving depression and tension, and is especially effective for removing waste when bathing. It is effective to enjoy bathing in fresh feeling.
한편 제주산 감귤 및 당근의 경우, 유기산 및 비타민 등의 인체에 이로운 물질이 다량 함유되어 있어 식용으로 상용되고 있는 농작물로 알려져 있으나, 수요량 대비 생산량이 과하여 농가 소득 증대와는 거리가 먼 실정이다. 한편, 최근 국민 생활 수준이 높아짐에 따라 웰빙 경향이 두드러지고 있어 입욕 문화 역시 단순한 몸 씻기 수준을 넘어 다양한 소비자의 욕구를 충족시킬 필요성이 절실히 요구되고 있다.On the other hand, citrus fruits and carrots from Jeju are known to be commercially available crops because they contain a large amount of beneficial substances such as organic acids and vitamins, but they are far from increasing farm incomes due to their excessive production. On the other hand, as the standard of living in recent years has increased, well-being tendency has become more prominent, so the bathing culture is also urgently required to satisfy the needs of various consumers beyond simple body washing.
따라서, 제주산 감귤 및 당근의 과생산량을 해소할 수 있는 다양한 소비 전략의 수립이 필요한 시점으로 이러한 관점에서 입욕 첨가제로서의 개발 등은 바람직한 소비 전략중의 하나로 생각된다. Therefore, the development of bathing additives is considered to be one of the preferred consumption strategies in view of the need to establish various consumption strategies to overcome the overproduction of Jeju citrus fruits and carrots.
본 발명은 상기의 문제점을 해결하고, 상기의 필요성에 의하여 안출된 것으로서 본 발명의 목적은 천연물을 함유하는 버블 입욕제 조성물을 제공하는 것이다.The present invention solves the above problems, and the object of the present invention as devised by the above necessity is to provide a bubble bath composition containing natural products.
본 발명의 다른 목적은 상기 버블 입욕제 조성물의 제조방법을 제공하는 것이다.Another object of the present invention is to provide a method for producing the bubble bath composition.
상기의 목적을 달성하기 위하여, 본 발명은 감귤 또는 당근 마쇄액 30∼50 중량부, 탄산수소 나트륨 15∼25 중량부, 탄산나트륨 7∼12 중량부, 카제인 나트륨 2∼5 중량부, 콜로이드 오트 밀 2∼5 중량부, 미코린 S430 0.5∼1.5 중량부, 폴리에틸렌 글리콜 1.5∼3 중량부, 솔비톨 15∼25 중량부 및 산화마그네슘 0.1∼0.5 중량부를 포함하는 거품 입욕제 조성물을 제공한다.In order to achieve the above object, the present invention, citrus or carrot grinding liquid 30-30 parts by weight, sodium bicarbonate 15-25 parts by weight, sodium carbonate 7-12 parts by weight, casein sodium 2-5 parts by weight, colloidal oatmeal 2 It provides a foam bath composition comprising -5 parts by weight, mycorin S430 0.5-1.5 parts by weight, polyethylene glycol 1.5-3 parts by weight, sorbitol 15-25 parts by weight and magnesium oxide 0.1-0.5 parts by weight.
또 본 발명은 a) 물 500 중량부에 감귤 또는 당근 마쇄액 30∼50 중량부, 탄산수소 나트륨 15∼25 중량부, 탄산나트륨 7∼12 중량부, 카제인 나트륨 2∼5 중량부, 콜로이드 오트 밀 2∼5 중량부, 미코린 S430 0.5∼1.5 중량부, 폴리에틸렌 글리콜 1.5∼3 중량부, 솔비톨 15∼25 중량부 및 산화마그네슘 0.1∼0.5 중량부를 혼합하는 단계; b) 상기 혼합한 수용액을 교반기를 이용하여 균질하게 녹이는 단계; c) 상기 균질화된 수용액을 초저온 냉동고에서 전-냉동(pre-freezing)하는 단계; d) 상기의 냉동한 시료를 동결건조하는 단계; 및 e) 상기 동결건조 시료를 회수하여 분쇄기를 미세하게 분말화하는 단계를 포함하는 거품 입욕제 조성물의 제조 방법을 제공한다.In addition, the present invention is a) 500 parts by weight of citrus or carrot grinding liquid 30-50 parts by weight, sodium bicarbonate 15-25 parts by weight, sodium carbonate 7-12 parts by weight, casein sodium 2-5 parts by weight, colloidal oatmeal 2 -5 parts by weight, 0.5 to 1.5 parts by weight of Mycoline S430, 1.5 to 3 parts by weight of polyethylene glycol, 15 to 25 parts by weight of sorbitol and 0.1 to 0.5 parts by weight of magnesium oxide; b) homogeneously dissolving the mixed aqueous solution using a stirrer; c) pre-freezing the homogenized aqueous solution in a cryogenic freezer; d) lyophilizing the frozen sample; And e) recovering the lyophilized sample to finely powder the grinder to provide a method for producing a foam bath composition.
본 발명의 조성물의 제조방법에 있어서, 상기 c)단계의 냉동 온도는 -20∼-70℃, d)단계의 동결 건조 시간은 12∼36시간인 것이 바람직하나 이에 한정되지 아니한다.In the preparation method of the composition of the present invention, the freezing temperature of the step c) is -20 ~ -70 ℃, the freeze drying time of step d) is preferably 12 to 36 hours, but is not limited thereto.
이하 본 발명을 설명한다. Hereinafter, the present invention will be described.
본 발명은 원재료로 제주산 감귤 및 당근과 이산화탄소를 발생하는 유기 탄산염, 피부염 치료 효과를 지니는 오트밀, 옥수수, 밀, 대두, 쌀, 보리로부터 유도된 콜로이드 분말을 적절하게 조합하여 피부 염증 치료 및 보습 효과를 가지는 발포성 입욕제를 제조한 후, 소비톨, 폴리에틸렌글리콜 등의 결합안정제와 조합하여 분말 또는 정제 상태로 제제화하였다. 또한, 상기한 제조 공법을 최적화하여 제제 제조 공정을 개발하였다.The present invention is a combination of oatmeal, corn, wheat, soybean, rice, barley, colloidal powder derived from citrus and carrots and carbon dioxide to produce carbon dioxide and dermatitis treatment as a raw material to treat skin inflammation and moisturizing effect After preparing a foaming bath having a, it was formulated in powder or tablet form in combination with a binding stabilizer such as sorbitol, polyethylene glycol. In addition, the formulation manufacturing process was developed by optimizing the above manufacturing process.
본 발명에 사용된 탄산수소나트륨, 탄산나트륨, 탄산암모늄 등의 탄산염은 물에 용해되어 콜로이드 물질의 분산성을 개선하고, 이산화탄소 발생에 의한 발포성을 가지므로 피부에 상쾌한 자극을 부여하여 피로 회복에 도움을 주는 것으로 알려져 있다. 이들 탄산염과 조합되는 상으로서는 아세트산, 프로피온산, 부티르산 등의 직쇄 지방산, 옥살산, 글루타르산, 푸말산, 말레인산 등의 카르복실산, 글루타민산, 아스파라긴산 등의 산성 아미노산, 젖산, 말레인산, 타르타르산, 히드록시벤조산, 시트르산, 살리실산, 아스코르빈산 등의 히드록시산과 이들 유기산의 산성 염을 들 수 있다. 특히, 탄산염과 산의 바람직한 조합으로서는 탄산나트륨 및(또는) 탄산수소나트륨과 숙신산 및(또는) 푸말산, 구연산 등의 조합이 알려져 있다.Carbonate salts such as sodium bicarbonate, sodium carbonate and ammonium carbonate used in the present invention are dissolved in water to improve the dispersibility of colloidal substances, and have a foaming property due to the generation of carbon dioxide to give a refreshing stimulus to the skin to help to recover from fatigue It is known to give. Examples of phases combined with these carbonates include straight-chain fatty acids such as acetic acid, propionic acid and butyric acid, carboxylic acids such as oxalic acid, glutaric acid, fumaric acid and maleic acid, acidic amino acids such as glutamic acid and aspartic acid, lactic acid, maleic acid, tartaric acid and hydroxybenzoic acid. And acid salts of hydroxy acids such as citric acid, salicylic acid and ascorbic acid and these organic acids. In particular, as a preferable combination of carbonate and acid, a combination of sodium carbonate and / or sodium bicarbonate and succinic acid and / or fumaric acid, citric acid and the like are known.
또한, 오트밀, 소수성 전분 등은 물에 분산되어 입욕시 피부의 불쾌감을 해소시켜 일시적인 치유 효과를 가지고 있는 것으로 알려져 있다.In addition, oatmeal and hydrophobic starch are known to have a temporary healing effect by dispersing in water to relieve skin discomfort during bathing.
본 발명에서는 제주산 감귤 및 당근의 과생산량을 해소할 수 있는 다양한 소비 전략의 일환으로 상기한 몇 가지 효능성 제제를 조합한 피부염증 치료 및 보습 효과를 가지는 발포성 입욕제를 개발하여 건강 뿐 아니라 농가 소득 증대에 기여할 수 있는 효과를 가진다.In the present invention, as a part of various consumption strategies that can eliminate the over-production of citrus fruits and carrots of Jeju produced by developing a foaming bath having a skin inflammation treatment and moisturizing effect of the combination of several of the above-mentioned efficacy agents, as well as farmhouse income It has the effect of contributing to the increase.
이하, 비한정적인 실시예를 통하여 본 발명을 더욱 상세하게 설명한다.Hereinafter, the present invention will be described in more detail with reference to non-limiting examples.
실시예Example 1: 감귤을 원료로 포함한 발포성 거품 입욕제의 제조 방법 1: Manufacturing method of foam foam bath containing citrus as raw material
제주산 감귤 또는 당근 100g을 homogenizer로 마쇄하였다. 이 마쇄액 41.8g을 취하여 colloidal oat meal 3%를 첨가하고, sodium caseinate 3g을 첨가하고, sodium bicarbonate 18.5g과 sodium carbonate 9.1g을 각각 첨가하였다.100 g of tangerine or carrot from Jeju was ground with a homogenizer. 41.8 g of this grinding solution was taken, 3% colloidal oat meal was added, 3 g of sodium caseinate was added, and 18.5 g of sodium bicarbonate and 9.1 g of sodium carbonate were added, respectively.
여기에 계면활성제인 Micolin S430 1%와 polyethylene glycol (분자량 600) 2.2g을 첨가하고, 결합안정제인 sorbitol 18.2g과 magnesium oxide 0.2g을 각각 첨가하였다. 이 들 혼합물을 증류수를 이용하여 총 500ml로 보정하였다.To this were added 1% Micolin S430 surfactant and 2.2 g polyethylene glycol (molecular weight 600), and 18.2 g binding stabilizer sorbitol and 0.2 g magnesium oxide, respectively. These mixtures were corrected to 500 ml in total with distilled water.
상기의 보정된 수용액을 교반기를 이용하여 균질하게 녹였다. 상기 균질화된 수용액을 -30℃의 초저온 냉동고에서 pre-freezing하였다. 상기의 냉동한 시료를 24시간 동결건조한 후 동결건조 시료를 회수하여 ball miller를 이용하여 미세하게 분말화하였다. 분말화한 후, 용해도, 거품 발생 비율 등의 특성을 토대로 적절한 형태로 성형하여 제품을 제조하였다. 최종적으로 얻어진 분말 시료의 수율은 약 40% 정도로 확인되었다.The calibrated aqueous solution was dissolved homogeneously using a stirrer. The homogenized aqueous solution was pre-freezed in an cryogenic freezer at -30 ° C. After freeze-drying the frozen sample for 24 hours, the freeze-dried sample was collected and finely powdered using a ball miller. After powdering, a product was manufactured by molding into an appropriate form based on the properties such as solubility, foaming rate and the like. The yield of the finally obtained powder sample was confirmed to be about 40%.
실시예Example 2: 감귤을 원료로 포함한 발포성 거품 입욕제의 제조 방법 2: manufacturing method of foam foam bath containing citrus as raw material
상기 실시예의 제조 방법에서 원료를 감귤 대신 당근으로 치환한 것을 제외하곤 실시예1과 동일한 조성과 방법으로 입욕제 조성물을 제조하였다.A bath composition was prepared in the same composition and method as in Example 1, except that the raw material was replaced with carrots instead of citrus fruits in the manufacturing method of the above embodiment.
최종적으로 얻어진 분말 시료의 수율은 약 40% 정도로 확인되었다. The yield of the finally obtained powder sample was confirmed to be about 40%.
본 발명의 제제 제조 공정을 요약하면 도 1과 같다.A summary of the preparation process of the present invention is shown in FIG. 1.
본 발명에서 제조한 제주산 감귤 및 당근을 이용한 발포성 거품 입욕제 조성은 표 1과 2와 같다.Jeju foam citrus and carrot prepared in the present invention foam foam bath composition is shown in Tables 1 and 2.
표 1은 제주산 감귤을 이용한 발포성 거품 입욕제의 조성을 나타내고, 표 2는 제주산 당근을 이용한 발포성 거품 입욕제의 조성을 나타낸다.Table 1 shows the composition of the foam foam bath using Jeju citrus, Table 2 shows the composition of the foam foam bath using Jeju carrot.
상기의 구성에서 알 수 있는 바와 같이 본 발명의 감귤 및 당근을 원재료로 하여 계면활성제, sodium caseinate, 탄산염을 적절하게 배합한 발포성 거품 입욕제 조성물은 감귤의 주성분인 구연산에 의한 피부 피로 회복 효과 및 당근의 주성분인 카로티노이드에 의한 피부 노화 방지 및 억제 효과 및 염증 치료 및 보습 효과를 가진다.As can be seen from the above configuration, the foamable foam bath composition comprising the tangerine and carrot of the present invention as a raw material, and a surfactant, sodium caseinate, and carbonates as appropriate, has a skin fatigue recovery effect due to citric acid, the main component of tangerine, and carrot It has the effect of preventing and inhibiting skin aging and inflammation treatment and moisturizing effect by the main component carotenoid.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH07228522A (en) * | 1994-02-17 | 1995-08-29 | Tsumura & Co | Bathing agent for jet bath |
| JPH0912443A (en) * | 1995-06-30 | 1997-01-14 | Kao Corp | Solid-like bubble bath composition |
| KR0184283B1 (en) * | 1991-01-31 | 1999-05-01 | 도끼와 후미가쯔 | Bathing preparation for colloidal material |
| JP2005194233A (en) | 2004-01-08 | 2005-07-21 | Kansai Koso Kk | Foaming skin cosmetic |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR0184283B1 (en) * | 1991-01-31 | 1999-05-01 | 도끼와 후미가쯔 | Bathing preparation for colloidal material |
| JPH07228522A (en) * | 1994-02-17 | 1995-08-29 | Tsumura & Co | Bathing agent for jet bath |
| JPH0912443A (en) * | 1995-06-30 | 1997-01-14 | Kao Corp | Solid-like bubble bath composition |
| JP2005194233A (en) | 2004-01-08 | 2005-07-21 | Kansai Koso Kk | Foaming skin cosmetic |
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