KR100739347B1 - Sodium Silicate use product growth a plant and manufacture a method. - Google Patents

Sodium Silicate use product growth a plant and manufacture a method. Download PDF

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KR100739347B1
KR100739347B1 KR1020050039145A KR20050039145A KR100739347B1 KR 100739347 B1 KR100739347 B1 KR 100739347B1 KR 1020050039145 A KR1020050039145 A KR 1020050039145A KR 20050039145 A KR20050039145 A KR 20050039145A KR 100739347 B1 KR100739347 B1 KR 100739347B1
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plant growth
sodium
sodium silicate
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carbonate
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KR20060116636A (en
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장정만
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장정만
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/12—Powders or granules
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/14—Boron; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/26—Phosphorus; Compounds thereof
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture

Abstract

본 발명은 규산소다를 이용한 식물성장제의 조성물 및 제조방법으로 규산소다의 알칼리성분과 규산의 효능을 이용하여 원예작물(채소, 과수) 및 화본과 (禾本科: 벼, 보리, 밀,옥수수, 사탕수수)작물의 병충해 및 내도복성을 강화시키고 화학비료의 과다시비로 산성화된 토양과 오염된 토양을 중성으로 개량시키며, 옆면 시비를 통한 식물의 줄기와 잎을 강건케 하여 내병성을 높여 우수품질과 수확증대로 친환경적이며 규산소다를 이용한 저렴한 식물성장제를 개발한 것이다. 그 조성물의 구성은 규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 51∼65wt％, 무수탄산나트륨(Na2CO3) 26.45∼34.7wt％, 붕사(Na2B4O7) 2∼3wt％, 헥사메타인산소다((NaPO3)6) 1∼3wt％, 탄산카리(K2CO3) 0.5∼1wt％, 피로인산나트륨(Na4P2O7) 4∼5wt％, 탄산칼슘(CaCO3) 0.5∼1wt％, 산화마그네슘(MgO)0.5∼1wt％, 몰리브덴산 소오다(Na2MoO4) 0.05∼0.3wt％로 이루어지며, 이를 고루 혼합하여 연속제조 용해로에 스크류식 투입기(FEED MACHINE)로 연속 투입, 연속적으로 로 내에서 자동온도 센서(SENSER)를 통한 용해점인 1,150℃∼1,250℃ 온도의 축합용융으로 유리상으로 제조된다. 이를 입상, 분상, 액상으로 분류하여 저렴한 식물성장제로 생산 공급하는 것이다.

Figure 112005505790915-pat00001

식물성장제, 규산소다, 커렛트, 용해로, 입상, 분상, 액상

The present invention is a composition and manufacturing method of a plant growth agent using soda silicate, using the alkaline component of sodium silicate and the efficacy of silicic acid horticultural crops (vegetables, fruit trees) and flower plants (禾本科: rice, barley, wheat, corn, sugar cane) Enhance the pest and coat resistance of crops, improve acidified and contaminated soils due to excessive fertilization of chemical fertilizers to neutrality, and strengthen the stem and leaves of plants through side fertilization to increase the disease resistance to improve quality and harvest It is an eco-friendly and inexpensive plant growth agent using sodium silicate. The composition of the composition is 51 to 65 wt% of Curlet, the base of sodium silicate (Na 2 SiO 3 ), 26.45 to 34.7 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), and borax (Na 2 B 4 O 7 ) 2 ~ 3wt%, hexametaphosphate ((NaPO 3 ) 6 ) 1-3wt%, carbonic carbonate (K 2 CO 3 ) 0.5-1wt%, sodium pyrophosphate (Na 4 P 2 O 7 ) 4-5wt%, carbonic acid It consists of 0.5 ~ 1wt% of calcium (CaCO 3 ), 0.5 ~ 1wt% of magnesium oxide (MgO), and 0.05 ~ 0.3wt% of soda molybdate (Na 2 MoO 4 ). Continuous feeding into (FEED MACHINE), continuous melting in the furnace through a temperature sensor (SENSER) is produced in the glass phase by condensation melting at a temperature of 1,150 ℃ to 1,250 ℃. It is classified into granular, powdery, and liquid phase to produce and supply inexpensive plant growth agents.

Figure 112005505790915-pat00001

Plant Growth Agent, Sodium Silicate, Curette, Melting Furnace, Granular, Powdery, Liquid

Description

규산소다를 이용한 식물성장제의 조성물 및 제조제법{Sodium Silicate use product growth a plant and manufacture a method.}Sodium Silicate use product growth a plant and manufacture a method.

도1은 본 발명의 제조 시 규산소다(Na2SiO3)의 커렛트(Cullet)규격 도표1 is a cutlet specification chart of sodium silicate (Na 2 SiO 3 ) in the manufacture of the present invention

도2는 본 발명의 제조 공정도2 is a manufacturing process diagram of the present invention

본 발명은 규산소다의 알칼리성분과 규산의 효능을 이용하여 원예작물 및 화본과(禾本科)작물의 병충해 및 내도복성을 강화시키고 화학비료의 과다시비로 산성화된 토양과 오염된 토양을 중성으로 개량시키며, 옆면 시비를 통한 식물의 줄기와 잎을 강건케 하여 내병성을 높여 우수품질과 수확증대로 친환경적이며 규산소다를 이용한 저렴한 식물성장제를 개발한 것이다.The present invention utilizes the alkaline component of sodium silicate and the efficacy of silicic acid to enhance the pest and tolerability of horticultural crops and flowering plants, and to neutralize the acid and soil contaminated by excessive fertilization of chemical fertilizers. It has developed environmentally-friendly, low-cost plant growth agents using soda silicate with excellent quality and increased yield by strengthening the stem and leaves of plants through side fertilization.

본 발명은 규산소다(Na2SiO3)를 이용한 식물성장제조성물 및 제조방법에 관한 것이다.The present invention relates to a plant growth composition and production method using sodium silicate (Na 2 SiO 3 ).

규산(Si)은 기초 광물을 형성하는 요소로서 산소에 이어 지각의 28%를 차지하는 성분이다. 규산은 기상, 토양 물리·화학성의 상호작용으로 용해되며, 토양의 pH에 따라서 분자상(H4SiO4, H3SiO4 -, H2SiO4 2-, HSO4 3- 및 SiO4 4-)으로 변화되는 monosilicic acid와 이들의 복합체인 polysilicic acid(n(SiOH4)), Al, Fe, Ca, Na, MgSO4 등과 무기화합물로 된 복합물, 그리고 유기 규산 복합체로서 존재한다. 식물에는 주로 H4SiO4 형이 잘 흡수되고 이온형은 다른 무기이온과 길항으로 흡수가 억제된다. 식물이 주로 흡수하는 monosilicic acid와 polysilicic acid는 양자의 상호작용으로 토양 pH에 영향을 준다.Silicate (Si) is an element that forms the basic mineral and occupies 28% of the earth's crust following oxygen. Silicic acid is dissolved by the interaction of weather, soil physical and chemical resistance, the molecules according to the soil pH (H 4 SiO 4, H 3 SiO 4 -, H 2 SiO 4 2-, HSO 4 3- and SiO 4 4- ) And polysilicic acid (n (SiOH 4 )), Al, Fe, Ca, Na, MgSO 4 and other inorganic compounds, and organic silicic acid complexes. Plants are mainly absorbed by H 4 SiO 4 form, the ionic form is inhibited by other ions and antagonists. Monosilicic acid and polysilicic acid, which plants mainly absorb, affect soil pH through the interaction of both.

논토양의 규산함량은 130∼180(mg/kg)이 적당하나 우리나라 논의 규산함량은 평균 86(mg/kg)으로 84.4%의 논이 규산이 부족한 실정이며. 벼농사를 짓는데 벼는 규산을 질소의 8배이상 흡수하며 자란다. 규산은 벼의 도열병, 백엽고병, 문고병의 발병을 억제하는 효과가 있으며 각종 채소류 및 과수 화훼류에 충해방지 효과도 겸하고 있으며, 토양오염 경감효과가 있다. 특히 도열병에 대해서는 많은 연구자에 의해 규산시용의 효과가 인정되고 있고, 한랭지에서는 유수형성기 잎의 규산농도를 5%이상으로 하면 잎도열, 출수기의 농도를 8%이상으로 하면 이삭도열을 현저하게 억제할 수 있게 된다고 한다. 이러한 병해저항성은 작물의 표피조직에 침적된 규산이 병원균의 침입을 물리적으로 저지하기 때문이라고 해왔는데 최근의 연구에 의하면 규산은 도열병균의 침입부위에 집적(集積)한다고 하며 다른 양분에서는 볼 수 없는 성질이 있고 활성산소의 생성을 촉진하는 것으로 식물성장에 필수적임을 밝혀내었다. 그리고 줄기와 잎에 규산이 축적되면 조직이 강건하여 도복저항성은 물론 병해충에 대한 내성을 갖게 되므로 양호한 등숙과 품질 향상으로 수량에 기여하게 된다.The amount of silicic acid in paddy soil is 130 ~ 180 (mg / kg), but the silicic acid content in Korea is 86 (mg / kg), which is 84.4% of rice paddy. In rice farming, rice grows by absorbing more than eight times the amount of silicic acid. Silicate has the effect of suppressing the onset of rice blast, white leaf disease, and paperback disease, and also serves as a preventive effect on various vegetables and fruit trees, and also reduces soil pollution. In particular, the effects of silicic acid application have been recognized by many researchers about blasting disease.In the cold districts, if the silicic acid concentration of the oil-forming leaves is 5% or higher, the leaf heating and the extractor concentration of 8% or more are significantly suppressed. It is said to be possible. This disease resistance has been attributed to the silicic acid deposited on the epidermal tissue of crops to physically prevent the invasion of pathogens. Recent studies suggest that silicic acid accumulates at the invasion site of blast germs and is not found in other nutrients. It has been found to be essential for plant growth by having properties and promoting the production of free radicals. When silicic acid accumulates on stems and leaves, the tissues are robust, and thus the resistance to doping and resistance to pests is contributed to the yield by good ripening and quality improvement.

가용성의 규산소다(Na2SiO3)는 뿌리에서 흡수되어 식물체내에 상승하며, 엽면에서의 증발에 따라 경엽의 규소는 그의 표피세포막 중에 침적하여 규질화세포로 되며 식물체를 강인하게 한다. 이 때문에 식물체에 붙었던 도열병균을 비롯하여 여러 병균은 식물체의 내부로 쉽게 침입치 못하고 침입한 것이라도 대게는 발육이 억제되어 병반은 커지지 못하고 또한 그 수효는 적어진다.Soluble sodium silicate (Na 2 SiO 3 ) is absorbed by the roots and rises in the plant. As the leaf evaporates, the silicon of the foliage is deposited in its epidermal cell membrane to become siliceous cells, making the plant robust. Because of this, many germs, such as heat pathogens attached to the plant, are not easily invaded into the inside of the plant, but even if they are invaded, the development of the crab is usually suppressed, and the lesions do not grow and the number thereof decreases.

이러므로 본 발명의 식물성장제는 식물의 세포에 규산을 축적시켜 잎의 물리적 강도를 높이고 식물의 줄기와 잎을 굳세게 하여 직립 하도록 하여 잎의 빛 흡수로 인한 광합성 효율을 높여 도복과 병균의 감염이 방지되고 충해에 대한 내병성을 높이며 한해, 동해에 강하여 잘 쓰러지지 않게 해준다.Therefore, the plant growth agent of the present invention accumulates silicic acid in the cells of the plant to increase the physical strength of the leaves and to stiffen the stems and leaves of the plants so as to stand upright, thereby increasing the photosynthetic efficiency due to light absorption of the leaves and preventing infection of dobok and germs. It increases the disease resistance to impairment and makes it hard to fall down because it is strong in the East Sea.

본 발명과 대치되는 선 등록(특허 등록번호 제0020217호)된 '식물성장촉진제' 는 본 발명과는 판이하며, 특허 등록 제0057402호의 '식물성장촉진, 항균제 조성물' 의 규산소다의 혼합물은 무기 괴상 고체의 표면에 도포하고 가온 경화시켜 제조 된다고 하였으나, 본 발명의 조성물의 구성 및 제조방법은 규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 51∼65wt％, 무수탄산나트륨(Na2CO3) 26.45∼34.7wt％, 붕사(Na2B4O7) 2∼3wt％, 헥사메타인산소다((NaPO3)6) 1∼3wt％, 탄산카리(K2CO3) 0.5∼1wt％, 피로인산나트륨(Na4P2O7) 4∼5wt％, 탄산칼슘(CaCO3) 0.5∼1wt％, 산화마그네슘(MgO)0.5∼1wt％, 몰리브덴산 소오다(Na2MoO4) 0.05∼0.3wt％ 조성물로 이루어지며, 이를 고루 혼합하여 연속제조 용융로에 스크류식 투입기(FEED MACHINE)로 연속 투입, 연속적으로 로 내에서 자동온도 센서(SENSER)를 통한 용융점인 1,150℃∼1,250℃ 온도의 축합용융으로 유리상의 고체로 제조된다. 다시 이것을 입상, 분상으로 분쇄하여 포장하고, 유리상의 고체를 고온반응장치(AUTOCLAVE)에 넣어 5∼6기압의 가압증기로 용해하여 액상으로 분류, 저렴한 식물성장제로 생산 공급하는 것이다.In contrast to the present invention, the 'plant growth promoter', which is registered in advance of the present invention (Patent Registration No. 0020217), is different from the present invention, and the mixture of sodium silicate of 'plant growth promotion and antimicrobial composition' in Patent Registration No. 0057402 is an inorganic block. Although it is said that it is prepared by coating on the surface of the solid and heating and curing, the composition and method of preparing the composition of the present invention are 51 to 65 wt% of a curd, which is a base of sodium silicate (Na 2 SiO 3 ), and anhydrous sodium carbonate (Na 2 CO). 3 ) 26.45 to 34.7 wt%, borax (Na 2 B 4 O 7 ) 2-3 wt%, hexametaphosphate ((NaPO 3 ) 6 ) 1-3 wt%, carbonic carbonate (K 2 CO 3 ) 0.5-1 wt% , Sodium pyrophosphate (Na 4 P 2 O 7 ) 4-5 wt%, calcium carbonate (CaCO 3 ) 0.5-1 wt%, magnesium oxide (MgO) 0.5-1 wt%, sodium molybdate (Na 2 MoO 4 ) 0.05- It is composed of 0.3wt% composition, mixed evenly and continuously put into a continuous production melting furnace with a screw feeder (FEED MACHINE), continuously automatic temperature in the furnace Condensation melting at a temperature of 1,150 ° C. to 1,250 ° C., which is a melting point through a sensor, is made of a glassy solid. It is then crushed and packaged into granular and powdery form, and the glassy solid is dissolved in a pressurized steam of 5 to 6 atm in an autoclave, which is classified as a liquid and produced and supplied as an inexpensive plant growth agent.

본 발명의 목적은 규산소다를 이용한 식물성장제를 저렴하게 농가에 공급함으로서 산성의 토양을 개량하여 주며, 뿌리를 강하게 신장시켜 작물을 강건하게 하며, 식물의 줄기와 잎을 튼튼히 하며 질소과잉흡수를 억제하고, 도열병, 냉해 등 병균저항성으로 수확증대에 기여하는 입상, 분상, 액상의 식물성장제를 제공하는 것이다.It is an object of the present invention to improve the acidic soil by supplying a plant growth agent using sodium silicate at low cost to the farm, strengthening the crops by strengthening the roots, strengthening the stems and leaves of the plant and suppressing the excess absorption of nitrogen. In addition, it provides a granular, powdery, liquid plant growth agent that contributes to the increase of the harvest with resistance to germs, such as blast and cold.

규산소다(Na2SiO3)는 Na2O와 SiO2의 결합비율에 따라 여러 가지 형태로 존재하나 여러 가지 용도에 따라서 상품화 되고 있는 규산소다는 40종 이상이 된다. Na2O : SiO2의 비가 1 : 1.6∼1 : 4까지의 규산염을 Colloidal Silicate라 부르고, Na2O : SiO2의 비가 1 : 1인 것을 Sodium metasilicate라 부르고, Na2O : SiO2의 비가 1.5 : 1의 것을 Sesqui Silicate라 부르고 있다. 본 발명에 쓰이는 규산소다(Na2SiO3)는 SiO2 74∼77%, Na2O 23∼25%, WEIGHT RATIO 3.10∼3.35, MOLAR RATIO 3.10-3.50 규격의 사용함으로서 제품의 균일성을 확보하였고, 규사(SiO2)를 사용하지 않으므로 제조과정에서 생기는 공해적인 분진의 우려도 없어 작업의 난제가 없는 작업공정이 이루어졌다.Sodium silicate (Na 2 SiO 3 ) exists in various forms according to the bonding ratio of Na 2 O and SiO 2 , but more than 40 kinds of sodium silicate commercialized according to various uses. Silicates with a ratio of Na 2 O: SiO 2 from 1: 1.6 to 1: 4 are called colloidal Silicate, a ratio of Na 2 O: SiO 2 is 1: 1 called sodium metasilicate, and the ratio of Na 2 O: SiO 2 is The 1.5: 1 one is called Sesqui Silicate. Sodium silicate (Na 2 SiO 3 ) used in the present invention secured uniformity of the product by using 74 to 77% of SiO 2, 23 to 25% of Na 2 O, 3.10 to 3.35 of WEIGHT RATIO, and 3.10 to 3.50 of MOLAR RATIO. Since it does not use silica sand (SiO 2 ), there is no fear of pollution during the manufacturing process.

본 발명의 목적으로 하는 규사(SiO2)와 탄산나트륨(Na2CO3)의 혼합물로 용융 냉각된 컬리트(Cullet)를 규산소다(Na2SiO3)로 사용함으로서 규사(SiO2)를 용융 하는 것 보다 더 많은 에너지 절감효과 및 원가절감과 함께 시장성의 확보도 유리해 졌다.Melt the silica sand (SiO 2 ) by using a melt-cooled collet (Cullet) with a mixture of silica sand (SiO 2 ) and sodium carbonate (Na 2 CO 3 ) for the purpose of the present invention as sodium silicate (Na 2 SiO 3 ). In addition to more energy savings and cost savings than in the past, securing marketability is also beneficial.

본 발명의 식물성장제는 광합성 알칼리 성분으로 수분과 접촉하여 산성토양을 개량하며 작물의 생육을 촉진 시키고, 동식물 생체에 가장 유익한 5∼20미크론 대의 파장대 방사율이 92%영역의 원적외선의 방사효과로 작물의 대사작용을 원활하게 하며 작물의 생장을 촉진 시킨다.The plant growth agent of the present invention is a photosynthetic alkaline component that improves acid soil by contact with moisture and promotes crop growth, and the far-infrared radiation effect of far infrared rays in the range of 92% of 5 ~ 20 microns, which is most beneficial for animal and plant living, It facilitates metabolism and promotes crop growth.

이하 본 발명의 첨부된 도표를 참조하여 상세히 설명한다.Reference will now be made in detail to the accompanying drawings of the present invention.

도1은 본 발명의 제조 시 규산소다(Na2SiO3)의 커렛트(Cullet)규격 도표이다.1 is a cutlet specification chart of sodium silicate (Na 2 SiO 3 ) in the manufacture of the present invention.

도2는 본 발명의 제조공정도이며 제품의 완성단계까지의 공정은 연속적인 자동화 공정으로 이루어져 대량생산에 따른 국제경쟁력으로 생산원가에 반영될 수 있다.2 is a manufacturing process diagram of the present invention, the process up to the completion of the product is made of a continuous automated process can be reflected in the production cost as an international competitiveness according to mass production.

도1의 규산소다(Na2SiO3)는 규사와 소다회를 분쇄 혼합하여 용융로에 넣어서 가열하여 완전 용해한 후, 투명체가 되었을 때 쏟아내어 냉각고화 시키는데 이것을 커렛트(Cullet)라 부르며 이것을 진공증발로 농축한 진한 수용액을 물유리(Water glass)라고 한다.Sodium silicate (Na 2 SiO 3 ) of FIG. 1 is pulverized and mixed with silica sand and soda ash in a melting furnace, heated to completely dissolve, then poured into a transparent body to cool and solidify this is called a Curlet (Cullet) and concentrated by vacuum evaporation One concentrated aqueous solution is called water glass.

Na2CO3 + nSiO2 = Na2O · nSiO2 + CO2↑Na 2 CO 3 + nSiO 2 = Na 2 O · nSiO 2 + CO 2 ↑

본 발명의 제조 원료로 규산소다(Na 2 SiO 3 )의 SiO2규격이 72∼76% 기조물인 커렛트(Cullet)는 적정 배합된 무수탄산나트륨(Na 2 CO 3 )과 축합 용융되므로 Na함량이 높을수록 용해온도가 1,150℃∼1,250℃로 낮아지고 축합 용융됨으로서 물에 잘 녹는 성질을 가지므로 토양에 뿌려질 시에는 녹아서 산성토양을 중화 시키고 뿌리에서 흡수된 가용성 규산은 식물체 내를 상승하여 엽면에서의 표피세포막 중에 침적하며 식물체를 강인하게 한다. 질소과잉흡수를 억제하고 병충해에 강건하게 하며 과수의 경우 생장이 촉진되고 과색이 좋아지며 낙과 및 병과를 방지한다. 붕사(Na 2 B 4 O 7 )는 작물의 초기 발육에는 절대로 필요한 원소(B)를 함유하고 있으며, 탄수화물의 이동, 세포막 형성에 관여되며, 헥사메타인산소다((NaPO 3 ) 6 )는 식물체에 있어서 열의 이동과 탄수화물의 분해 및 식물세포가 엽록소와 일광에 의해서 탄산가스와 물에서 당분을 만드는 작용을 하며, 단맛을 많게 하고 뿌리의 발육을 촉진시키고 가지와 잎의 생장을 증가시킴으로 수확의 증가를 가져온다. 탄산카리(K 2 CO 3 )는 광합성 작용과 수분의 증발작용 및 수분의 공급조절을 원활히 하여 한해에 대한 저 항력을 증가시키고, 식물의 섬유소를 만드는데 기여하며, 식물의 세포조성을 증진 시킨다. 피로인산나트륨(Na 4 P 2 O 7 )은 영양제로서 발아를 왕성하게 하며 식물의 성숙을 촉진시키고 전분을 만드는 능력을 왕성하게 한다.As a raw material of the present invention, a curlet having a SiO 2 specification of 72 to 76% as a raw material of sodium silicate (Na 2 SiO 3 ) is condensed and melted with an appropriately formulated anhydrous sodium carbonate (Na 2 CO 3 ) to increase Na content. As the melting temperature is lowered from 1,150 ℃ to 1,250 ℃ and it is condensed and melted, it dissolves well in water. So when it is sprayed on soil, it dissolves to neutralize acidic soils, and the soluble silicic acid absorbed from the roots rises in the leaf surface. It deposits in the epidermal cell membrane and makes the plant strong. It suppresses the excess absorption of nitrogen, makes it robust against pests, and in the case of fruit trees, it promotes growth, improves color, and prevents fruits and vegetables. Borax (Na 2 B 4 O 7 ) contains element (B) which is absolutely necessary for the early development of crops, is involved in carbohydrate migration and cell membrane formation, and hexametaphosphate ((NaPO 3 ) 6 ) Heat transfer, carbohydrate breakdown, and plant cells produce sugar in carbon dioxide and water by chlorophyll and sunlight, increase sweetness, promote root development, and increase eggplant and leaf growth. Bring. Carbo carbonate (K 2 CO 3 ) increases photosynthesis, evaporation of water and regulation of water supply to increase resistance to the year, contribute to the production of plant fiber, and enhance the cell composition of plants. Sodium pyrophosphate (Na 4 P 2 O 7 ) is a nutritious fertilizer that promotes plant maturation and the ability to make starch.

탄산칼슘(CaCO 3 )은 세포막의 구성요소이고 산성토양을 중화시켜 토양반응을 교정시켜 줌으로서 토양미생물의 활동을 촉진시키고 식물성장에 알맞은 토양환경개량에 지대한 역할을 한다. 질소동화, 마그네슘, 가리, 나트륨의 과잉흡수를 억제하는 길항작용 역할을 하며 토양중의 공기와 수분의 유통을 좋게 한다. 산화마그네슘(MgO)은 엽록소와 형성성분이며 녹색식물에 있어서는 없어서는 안 될 원소이며 특히 인산대사나 광합성에 관여하는 효소의 활성을 높인다. 몰리브덴산 소오다(Na 2 MoO 4 )는 식물의 아미노산과 단백질 생성에 중요한 미량원소역할을 하며 질소환원 효소의 구성성분이다. Calcium carbonate (CaCO 3 ) is a component of cell membranes and neutralizes acidic soils to correct soil reactions, thereby promoting soil microbial activity and playing a significant role in improving soil environment suitable for plant growth. It acts as an antagonist that inhibits the over-absorption of nitrogen assimilation, magnesium, girly and sodium, and improves the circulation of air and water in the soil. Magnesium oxide (MgO) is a constituent with chlorophyll, an indispensable element for green plants, and especially enhances the activity of enzymes involved in phosphate metabolism or photosynthesis. Sodium molybdate (Na 2 MoO 4 ) plays an important trace element in the production of amino acids and proteins in plants and is a component of nitrogen-reducing enzymes.

본 발명의 식물성장제는 인체 및 동식물에 전혀 무해, 무독, 무취하며 폐수 시 강이나 바다로 흘러갔을 시 공해문제를 일으키지 않으며 독성의 염려가 없고 환경적 측면에서 볼 때 환경친화적 식물성장제이다.The plant growth agent of the present invention is harmless to humans and animals and plants, harmless and odorless and does not cause pollution problems when it flows into rivers or seas during wastewater, and is an environmentally friendly plant growth agent from an environmental point of view.

도2의 제조공정은 조성물을 믹서기로 고루 혼합하여 스크류식 투입기(FEED MACHINE)로 전기로나 가스용해로에 연속 투입되며, 용해온도는 상기의 규산소다(Na2SiO3)와 탄산나트륨(Na2CO3)의 적정배합으로 1,250℃이하의 온도로 4∼5시간에 충분히 용해되며, 로 내에서 자동온도 센서(SENSER)를 통한 용해점인 1,150℃∼1,250℃ 온도의 축합용융으로 출탕된 용융물을 주물밧드에 담아 서냉장치를 통하여 냉각시켜 유리상의 결정물을 얻는데, 이를 입상, 분상으로 분쇄하여 포장하고, 유리상의 결정물을 고온반응장치(AUTOCLAVE)에 넣어 5∼6기압의 가압증기로 용해하여 액상으로 분류되어 계량, 포장, 검사과정을 거쳐 출고되는 것이다.In the manufacturing process of FIG. 2, the composition is evenly mixed with a blender and continuously fed into an electric furnace or a gas melting furnace with a screw feeder (FEED MACHINE), and the dissolution temperature is sodium silicate (Na 2 SiO 3 ) and sodium carbonate (Na 2 CO 3). The melted mixture melted by condensation melting of 1,150 ℃ ~ 1,250 ℃ which is the melting point through the automatic temperature sensor (SENSER) in the furnace. It is cooled in a slow cooling apparatus to obtain glassy crystals, which are pulverized into granular and powdery phases. The glassy crystals are placed in a high temperature reactor (AUTOCLAVE) and dissolved in a pressurized steam of 5 to 6 atm to give a liquid phase. They are sorted, weighed, packaged and inspected and shipped.

다음은 본 발명의 실시에 따른 예를 들어 설명하기로 한다.Next will be described with an example according to the embodiment of the present invention.

(실시 예 1)(Example 1)

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 55wt%, 무수탄산나트륨(Na2CO3) 35wt%, 붕사(Na2B4O7) 2wt%, 헥사메타인산소다((NaPO3)6) 2wt%, 탄산카리(K2CO3) 0.5 wt%, 피로인산나트륨(Na4P2O7) 4wt%, 탄산칼슘(CaCO3) 0.9wt%, 산화마그네슘(MgO)1wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 식물성장제를 10kg용 PP 2중 지대포장 한다.Sodium silicate (Na 2 SiO 3 ) is the base of the curlet (Cullet) 55wt%, anhydrous sodium carbonate (Na 2 CO 3 ) 35wt%, borax (Na 2 B 4 O 7 ) 2wt%, sodium hexametaphosphate ((NaPO 3 ) 6 ) 2 wt%, carbonic carbonate (K 2 CO 3 ) 0.5 wt%, sodium pyrophosphate (Na 4 P 2 O 7 ) 4 wt%, calcium carbonate (CaCO 3 ) 0.9 wt%, magnesium oxide (MgO) 1 wt%, Sodium molybdate (Na 2 MoO 4 ) 0.1wt% was mixed in a mixer, put into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C, melted and cooled, and then pulverized into 3 to 5 mm coarse particles using a plant growth agent. Pack 10 kg of PP double bags.

(실시 예2)Example 2

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 55wt%, 무수탄산나트륨(Na2CO3) 35wt%, 붕사(Na2B4O7) 2wt%, 헥사메타인산소다((NaPO3)6) 2wt%, 탄산카리(K2CO3) 0.5 wt%, 피로인산나트륨(Na4P2O7) 4wt%, 탄산칼슘(CaCO3) 0.9wt%, 산화마그네슘(MgO)1wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 고온반응장치(AUTOCLAVE)에 넣어 5∼6기압의 가압증기로 용 해하여 액상식물성장제로 제조한다.Sodium silicate (Na 2 SiO 3 ) is the base of the curlet (Cullet) 55wt%, anhydrous sodium carbonate (Na 2 CO 3 ) 35wt%, borax (Na 2 B 4 O 7 ) 2wt%, sodium hexametaphosphate ((NaPO 3 ) 6 ) 2 wt%, carbonic carbonate (K 2 CO 3 ) 0.5 wt%, sodium pyrophosphate (Na 4 P 2 O 7 ) 4 wt%, calcium carbonate (CaCO 3 ) 0.9 wt%, magnesium oxide (MgO) 1 wt%, 0.1 wt% of sodium molybdate (Na 2 MoO 4 ) was mixed with a mixer and introduced into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C., melted and cooled, and then pulverized into 3 to 5 mm thick particles by a grinder to react with high temperature. It is put into the apparatus (AUTOCLAVE) and dissolved in a pressurized steam of 5 to 6 atm to prepare a liquid plant growth agent.

(실시 예3)Example 3

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 60wt%, 무수탄산나트륨(Na2CO3) 30wt%, 붕사(Na2B4O7) 2wt%, 헥사메타인산소다((NaPO3)6) 2wt%, 탄산카리(K2CO3) 0.5 wt%, 피로인산나트륨(Na4P2O7) 4wt%, 탄산칼슘(CaCO3) 0.9wt%, 산화마그네슘(MgO)1wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 입상 식물성장제를 제조한다.60 wt% of Curlet, the base of sodium silicate (Na 2 SiO 3 ), 30 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 2 wt% of borax (Na 2 B 4 O 7 ), hexametaphosphate ((NaPO 3 ) 6 ) 2 wt%, carbonic carbonate (K 2 CO 3 ) 0.5 wt%, sodium pyrophosphate (Na 4 P 2 O 7 ) 4 wt%, calcium carbonate (CaCO 3 ) 0.9 wt%, magnesium oxide (MgO) 1 wt%, Sodium molybdate (Na 2 MoO 4 ) 0.1wt% was mixed in a mixer, put into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C, melted and cooled, and then pulverized into 3 to 5 mm coarse particles with a granular vegetable Prepare enteric.

(실시 예4)Example 4

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 60wt%, 무수탄산나트륨(Na2CO3) 30wt%, 붕사(Na2B4O7) 2wt%, 헥사메타인산소다((NaPO3)6) 2wt%, 탄산카리(K2CO3) 0.5 wt%, 피로인산나트륨(Na4P2O7) 4wt%, 탄산칼슘(CaCO3) 0.9wt%, 산화마그네슘(MgO)1wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 고온반응장치(AUTOCLAVE)에 넣어 5∼6기압의 가압증기로 용해하여 액상식물성장제로 제조한다.60 wt% of Curlet, the base of sodium silicate (Na 2 SiO 3 ), 30 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 2 wt% of borax (Na 2 B 4 O 7 ), hexametaphosphate ((NaPO 3 ) 6 ) 2 wt%, carbonic carbonate (K 2 CO 3 ) 0.5 wt%, sodium pyrophosphate (Na 4 P 2 O 7 ) 4 wt%, calcium carbonate (CaCO 3 ) 0.9 wt%, magnesium oxide (MgO) 1 wt%, 0.1 wt% of sodium molybdate (Na 2 MoO 4 ) was mixed with a mixer and introduced into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C., melted and cooled, and then pulverized into 3 to 5 mm thick particles by a grinder to react with high temperature. It is put into an apparatus (AUTOCLAVE) and dissolved in a pressurized steam of 5 to 6 atm to prepare a liquid plant growth agent.

(실시 예5)Example 5

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 65wt%, 무수탄산나트륨(Na2CO3) 21wt%, 붕사(Na2B4O7) 3wt%, 헥사메타인산소다((NaPO3)6) 2.7wt%, 탄산카리(K2CO3) 1wt%, 피로인산나트륨(Na4P2O7) 5wt%, 탄산칼슘(CaCO3) 1wt%, 산화마그네슘(MgO)1wt%, 몰리브덴산 소오다(Na2MoO4) 0.3wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 30∼50메쉬(目)의 작은 입자로 분쇄하여 분상 식물성장제를 제조한다.65 wt% of a pellet of sodium silicate (Na 2 SiO 3 ), 21 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 3 wt% of borax (Na 2 B 4 O 7 ), and hexamethaphosphate ((NaPO 3) ) 6 ) 2.7 wt%, Carritic Carbonate (K 2 CO 3 ) 1 wt%, Sodium Pyrophosphate (Na 4 P 2 O 7 ) 5 wt%, Calcium Carbonate (CaCO 3 ) 1 wt%, Magnesium Oxide (MgO) 1 wt%, Molybdenum 0.3 wt% of acid soda (Na 2 MoO 4 ) is mixed with a mixer, put into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C., melted and cooled, and then ground into small particles of 30 to 50 mesh using a grinder. Powder plant growth agents are prepared.

(실시 예6)Example 6

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 65wt%, 무수탄산나트륨(Na2CO3) 21wt%, 붕사(Na2B4O7) 3wt%, 헥사메타인산소다((NaPO3)6) 2.7wt%, 탄산카리(K2CO3) 1wt%, 피로인산나트륨(Na4P2O7) 5wt%, 탄산칼슘(CaCO3) 1wt%, 산화마그네슘(MgO)1wt%, 몰리브덴산 소오다(Na2MoO4) 0.3wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 고온반응장치(AUTOCLAVE)에 넣어 5∼6기압의 가압증기로 용해하여 액상식물성장제로 제조한다.65 wt% of a pellet of sodium silicate (Na 2 SiO 3 ), 21 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 3 wt% of borax (Na 2 B 4 O 7 ), and hexamethaphosphate ((NaPO 3) ) 6 ) 2.7 wt%, Carritic Carbonate (K 2 CO 3 ) 1 wt%, Sodium Pyrophosphate (Na 4 P 2 O 7 ) 5 wt%, Calcium Carbonate (CaCO 3 ) 1 wt%, Magnesium Oxide (MgO) 1 wt%, Molybdenum 0.3 wt% of acid soda (Na 2 MoO 4 ) was mixed with a mixer, put into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C., melted and cooled, and then pulverized into 3 to 5 mm coarse particles using a high temperature reactor. It is put into (AUTOCLAVE) and dissolved in a pressurized steam of 5 to 6 atm to prepare a liquid plant growth agent.

(실시 예7)Example 7

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 58wt%, 무수탄산나트륨(Na2CO3) 30wt%, 붕사(Na2B4O7) 2wt%, 헥사메타인산소다((NaPO3)6) 3wt%, 탄산카리 (K2CO3) 1wt%, 피로인산나트륨(Na4P2O7) 5wt%, 탄산칼슘(CaCO3) 0.5wt%, 산화마그네슘(MgO)0.4wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 입상 식물성장제를 제조한다.58 wt% of a pellet of sodium silicate (Na 2 SiO 3 ), 30 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 2 wt% of borax (Na 2 B 4 O 7 ), hexamethaphosphate ((NaPO 3 ) 6 ) 3wt%, carbonic carbonate (K 2 CO 3 ) 1wt%, sodium pyrophosphate (Na 4 P 2 O 7 ) 5wt%, calcium carbonate (CaCO 3 ) 0.5wt%, magnesium oxide (MgO) 0.4wt%, Sodium molybdate (Na 2 MoO 4 ) 0.1wt% was mixed in a mixer, put into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C, melted and cooled, and then pulverized into 3 to 5 mm coarse particles with a granular vegetable Prepare enteric.

(실시 예8)Example 8

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 58wt%, 무수탄산나트륨(Na2CO3) 30wt%, 붕사(Na2B4O7) 2wt%, 헥사메타인산소다((NaPO3)6) 3wt%, 탄산카리(K2CO3) 1wt%, 피로인산나트륨(Na4P2O7) 5wt%, 탄산칼슘(CaCO3) 0.5wt%, 산화마그네슘(MgO)0.4wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 고온반응장치(AUTOCLAVE)에 넣어 5∼6기압의 가압증기로 용해하여 액상식물성장제로 제조한다.58 wt% of a pellet of sodium silicate (Na 2 SiO 3 ), 30 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 2 wt% of borax (Na 2 B 4 O 7 ), hexamethaphosphate ((NaPO 3 ) 6 ) 3wt%, carbonic carbonate (K 2 CO 3 ) 1wt%, sodium pyrophosphate (Na 4 P 2 O 7 ) 5wt%, calcium carbonate (CaCO 3 ) 0.5wt%, magnesium oxide (MgO) 0.4wt%, 0.1 wt% of sodium molybdate (Na 2 MoO 4 ) was mixed with a mixer and introduced into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C., melted and cooled, and then pulverized into 3 to 5 mm thick particles by a grinder to react with high temperature. It is put into an apparatus (AUTOCLAVE) and dissolved in a pressurized steam of 5 to 6 atm to prepare a liquid plant growth agent.

(실시 예9)Example 9

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 62wt%, 무수탄산나트륨(Na2CO3) 25wt%, 붕사(Na2B4O7) 2.3wt%, 헥사메타인산소다((NaPO3)6) 3wt%, 탄산카리(K2CO3) 1wt%, 피로인산나트륨(Na4P2O7) 5wt%, 탄산칼슘(CaCO3) 1wt%, 산화마그네슘(MgO)0.5wt%, 몰리브덴산 소오다(Na2MoO4) 0.2wt%를 믹서기로 혼합하여 전기로에 투 입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 입상 식물성장제를 제조한다.62 wt% of Curlet, the base of sodium silicate (Na 2 SiO 3 ), 25 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 2.3 wt% of borax (Na 2 B 4 O 7 ), hexametaphosphate ((NaPO 3 ) 6 ) 3wt%, 1% by weight of carbonic acid (K 2 CO 3 ), 5wt% of sodium pyrophosphate (Na 4 P 2 O 7 ), 1wt% of calcium carbonate (CaCO 3 ), 0.5wt% of magnesium oxide (MgO), 0.2 wt% of sodium molybdate (Na 2 MoO 4 ) was mixed with a mixer and introduced into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C., melted and cooled, and then pulverized into 3 to 5 mm thick particles by a grinder. Prepare plant growth agents.

(실시 예10)Example 10

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 58wt%, 무수탄산나트륨(Na2CO3) 30wt%, 붕사(Na2B4O7) 1.9wt%, 헥사메타인산소다((NaPO3)6) 3wt%, 탄산카리(K2CO3) 1wt%, 피로인산나트륨(Na4P2O7) 5wt%, 탄산칼슘(CaCO3) 0.5wt%, 산화마그네슘(MgO)0.5wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 입상 식물성장제를 제조한다.58 wt% of Curlet, the base of sodium silicate (Na 2 SiO 3 ), 30 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 1.9 wt% of borax (Na 2 B 4 O 7 ), hexametaphosphate ((NaPO 3 ) 6 ) 3wt%, 1% by weight of carbonic acid (K 2 CO 3 ), 5% by weight of sodium pyrophosphate (Na 4 P 2 O 7 ), 0.5% by weight of calcium carbonate (CaCO 3 ), 0.5% by weight of magnesium oxide (MgO) , 0.1 mol% of sodium molybdate (Na 2 MoO 4 ) was mixed with a mixer and introduced into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C., melted and cooled, and then pulverized into 3 to 5 mm thick particles by a pulverizer. Prepare plant growth agents.

(실시 예11)Example 11

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 58wt%, 무수탄산나트륨(Na2CO3) 30wt%, 붕사(Na2B4O7) 1.9wt%, 헥사메타인산소다((NaPO3)6) 3wt%, 탄산카리(K2CO3) 1wt%, 피로인산나트륨(Na4P2O7) 5wt%, 탄산칼슘(CaCO3) 0.5wt%, 산화마그네슘(MgO)0.5wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 분쇄기로 30∼50메쉬(目)의 작은 입자로 분쇄하여 분상 식물성장제를 제조한다.58 wt% of Curlet, the base of sodium silicate (Na 2 SiO 3 ), 30 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 1.9 wt% of borax (Na 2 B 4 O 7 ), hexametaphosphate ((NaPO 3 ) 6 ) 3wt%, 1% by weight of carbonic acid (K 2 CO 3 ), 5% by weight of sodium pyrophosphate (Na 4 P 2 O 7 ), 0.5% by weight of calcium carbonate (CaCO 3 ), 0.5% by weight of magnesium oxide (MgO) , Sodium molybdate (Na 2 MoO 4 ) 0.1wt% was mixed in a blender, put into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C, melted and cooled, and then pulverized into 3 to 5 mm thick particles with a grinder. A powdery plant growth agent is prepared by pulverizing into small particles of 30 to 50 mesh.

(실시 예12)(Example 12)

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 58wt%, 무수탄산나트륨(Na2CO3) 30wt%, 붕사(Na2B4O7) 1.9wt%, 헥사메타인산소다((NaPO3)6) 3wt%, 탄산카리(K2CO3) 1wt%, 피로인산나트륨(Na4P2O7) 5wt%, 탄산칼슘(CaCO3) 0.5wt%, 산화마그네슘(MgO)0.5wt%, 몰리브덴산 소오다(Na2MoO4) 0.1wt%를 믹서기로 혼합하여 전기로에 투입하고 1,200℃의 온도로 4시간 용융하여 출탕, 냉각시킨 후, 분쇄기로 3∼5mm의 굵은 입자로 분쇄하여 고온반응장치(AUTOCLAVE)에 넣어 5∼6기압의 가압증기로 용해하여 액상식물성장제로 제조한다.58 wt% of Curlet, the base of sodium silicate (Na 2 SiO 3 ), 30 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 1.9 wt% of borax (Na 2 B 4 O 7 ), hexametaphosphate ((NaPO 3 ) 6 ) 3wt%, 1% by weight of carbonic acid (K 2 CO 3 ), 5% by weight of sodium pyrophosphate (Na 4 P 2 O 7 ), 0.5% by weight of calcium carbonate (CaCO 3 ), 0.5% by weight of magnesium oxide (MgO) , 0.1% by weight of sodium molybdate (Na 2 MoO 4 ) was mixed with a mixer, put into an electric furnace, melted for 4 hours at a temperature of 1,200 ° C., melted and cooled, and then pulverized into 3 to 5 mm thick particles by a grinder to obtain a high temperature. It is put into the reactor (AUTOCLAVE) and dissolved in a pressurized steam of 5 to 6 atm to prepare a liquid plant growth agent.

상기와 같이 농작물에 대하여 (실시 예1)로 제조된 입상과 분상 식물성장제 1kg을 적당량의 비료와 함께 섞어서 200평의 비닐하우스에 산포 하여 개량된 토양효과를 얻어 방울토마토의 과육이 두껍고 크기가 배가 되며 30％증수효과의 양질의 방울토마토를 수확 하였다.As mentioned above, 1 kg of granular and powdery plant growth agents prepared in Example 1 are mixed with an appropriate amount of fertilizer and dispersed in a plastic house of 200 pyeong to obtain an improved soil effect. The flesh of the cherry tomatoes is thick and doubled in size. A high quality cherry tomato of 30% evaporation effect was harvested.

또한 (실시 예2)로 제조된 액상 식물성장제 1ℓ를 물 500ℓ에 희석하여 옆면시비용으로 1,000평의 고추 밭작물에 살포하여 고추탄저병을 예방하였고 20％의 증수효과를 보았으며, 과수원에 동일한 방법으로 산포한 결과 병충해 발생이 없어 사과잎의 낙엽지는 현상이 없어지고 사과에 윤기가 있으며 당도가 높고 신선도가 오래가서 저장이 용이하며 낙과현상이 없어져 20％의 증수효과를 보았다.In addition, 1 liter of the liquid plant growth agent prepared in Example 2 was diluted in 500 liters of water, and then sprayed on a 1,000-pound red pepper field crop at a side cost to prevent pepper anthrax, and a 20% increase effect was observed. As a result, there were no pests, and the deciduous area of the apple leaves disappeared, the apples were glossy, the sugar content was high, the freshness was long, so it was easy to store, and there was no fallout phenomenon.

본 발명의 식물성장제를 규사(SiO2)를 용융할시 높은 고온(1,600℃이상)이 필요하여 높은 제조원가가 형성되나, 규산소다(Na2SiO3)의 커렛트(Cullet)를 사용함으로서 저렴한 제품경쟁력을 갖게 되어 대량생산이 가능하게 되었고, 본 발명의 규산소다를 이용한 식물성장제는 산성의 토양을 개량하며 엽면시비를 통하여 병충해, 풍수해 및 기상장애 등으로 작물체가 쇠약해 졌을 때와 미량요소의 결핍 증세에 속히 회복시킬 수 있으며, 특히 원예시설채소나 과수재배에 품질향상과 높은 당도를 유지하고 빠른 성장과 함께 증수효과를 가져온다. 최근까지 국내외에서 연구된 작물별 규산 시용에 따른 증수효과로는 기상과 토양 환경을 고려하여 국가별, 작물별로 보면 세계적으로 벼에서는 10∼46%의 효과가 인정되는데 특히 미국에서 21∼46%의 가장 높은 효과를 내었다. 밀, 보리, 옥수수에서는 10∼15%의 증수를, 사탕수수에서(브라질)는 5∼13%, 땅콩은 15∼25%(중국), 오이에서는 3∼10%, 토마토에서는 8∼9%, 장미는 4∼8%의 증수를 가져왔다는 학계의 연구발표대로 규산의 식물성장제는 농업에 크게 이바지 할 것이다.When the plant growth agent of the present invention melts silica sand (SiO 2 ), a high temperature is required (1,600 ° C. or more), so a high manufacturing cost is formed, but a cheap product is made by using a silicate of sodium silicate (Na 2 SiO 3 ). Being competitive, mass production was possible, and the plant growth agent using sodium silicate of the present invention improves acidic soils, and when crops are deteriorated due to insect pests, feng shui and weather disorders through foliar fertilization and lack of trace elements. It can recover quickly, especially in horticultural plant or fruit cultivation, maintaining quality improvement, high sugar content, and rapid growth. The effects of silicic acid application by crops studied domestically and internationally until recently are considered to be 10 to 46% in rice, by country and crop, taking into account the weather and soil environment, especially in the United States. Had the highest effect. 10 to 15% increase in wheat, barley and corn, 5 to 13% in sugarcane (Brazil), 15 to 25% in peanuts (China), 3 to 10% in cucumbers, 8 to 9% in tomatoes, As the academic research indicates that roses have produced a 4-8% increase, silicic acid plant growth agents will greatly contribute to agriculture.

Claims (2)

규산소다(Na2SiO3)의 기조물인 커렛트(Cullet) 51∼65wt％, 무수탄산나트륨(Na2CO3) 26.45∼34.7wt％, 붕사(Na2B4O7) 2∼3wt％, 헥사메타인산소다((NaPO3)6) 1∼3wt％, 탄산카리(K2CO3) 0.5∼1wt％, 피로인산나트륨(Na4P2O7) 4∼5wt％, 탄산칼슘(CaCO3) 0.5∼1wt％, 산화마그네슘(MgO)0.5∼1wt％, 몰리브덴산 소오다(Na2MoO4) 0.05∼0.3wt％ 조성물로 이루어지며, 이를 고루 혼합하여 용융로 내에서 1,150℃∼1,250℃ 온도의 축합용융으로 출탕, 서냉, 냉각과정을 거쳐 제조되는 유리상의 고체를 얻는데, 이 유리상의 고체를 분쇄하여 입상, 분상의 식물성장제로 제조하는 식물성장제의 제조제법.51 to 65 wt% of a pellet of sodium silicate (Na 2 SiO 3 ), 26.45 to 34.7 wt% of anhydrous sodium carbonate (Na 2 CO 3 ), 2 to 3 wt% of borax (Na 2 B 4 O 7 ), hexa Sodium metaphosphate ((NaPO 3 ) 6 ) 1 to 3 wt%, Carri carbonate (K 2 CO 3 ) 0.5 to 1 wt%, Sodium pyrophosphate (Na 4 P 2 O 7 ) 4 to 5 wt%, calcium carbonate (CaCO 3 ) 0.5 to 1 wt%, magnesium oxide (MgO) 0.5 to 1 wt%, sodium molybdate (Na 2 MoO 4 ) 0.05 to 0.3 wt% composition, and evenly mixed to condense at a temperature of 1,150 ℃ to 1,250 ℃ in the furnace A method for producing a plant growth agent, which is obtained by melting, tapping, slow cooling, or cooling a glassy solid, which is pulverized to produce a granular or powdery plant growth agent. 제1항에 있어서 유리상의 냉각된 화합물을 고온반응장치(AUTOCLAVE)에 넣어 5∼6기압의 가압증기로 용해하여 액상으로 분류 제조하는 식물성장제 제조제법.The method for producing a plant growth agent according to claim 1, wherein the cooled compound in glass phase is dissolved in a pressurized steam of 5 to 6 atm in an autoclave.
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