KR100416364B1 - N,P,VOC removal and disinfection of microorganism using ultrasonic system in wastewater treament system - Google Patents
N,P,VOC removal and disinfection of microorganism using ultrasonic system in wastewater treament system Download PDFInfo
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- KR100416364B1 KR100416364B1 KR10-2000-0072591A KR20000072591A KR100416364B1 KR 100416364 B1 KR100416364 B1 KR 100416364B1 KR 20000072591 A KR20000072591 A KR 20000072591A KR 100416364 B1 KR100416364 B1 KR 100416364B1
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- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/34—Treatment of water, waste water, or sewage with mechanical oscillations
- C02F1/36—Treatment of water, waste water, or sewage with mechanical oscillations ultrasonic vibrations
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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Abstract
본 발명은 초음파를 이용하여 중수, 하수나 오폐수의 질소, 인, 휘발성유기화합물(VOC)을 제거하거나 혐기성소화조에 사용하여 슬러지를 감량하거나 중수나 하수 및 폐수처리장의 최종 침전조에서 방류되는 처리수나 정수장의 미생물 소독에 이용되는 초음파공법에 관한 것이다. 초음파를 이용하여 하수나 폐수처리과정에서 슬러지의 미생물을 파괴하여 미생물내의 유기물을 용출시키는 방법 또는 상수, 중수, 하수의 처리수 또는 처리과정중에 사용하여 휘발성유기물질(VOC)를 분해하거나 미생물을 소독할 목적으로 이용하는 기술이다. 이에 따른 구성은 초음파발생장치를 하수나 폐수처리공정의 슬러지 반송관에 부착하거나 반송관에 삽입하여 초음파를 발생시키고, 초음파 조사된 슬러지를 혐기조나 무산소조 또는 호기조에 넣어 질소, 인, 휘발성유기물질(VOC)를 제거하는 방법과 장치에 관한 것이다.The present invention removes nitrogen, phosphorus, and volatile organic compounds (VOC) from heavy water, sewage and wastewater using ultrasonic waves, or reduces sludge by using an anaerobic digestion tank or discharged water from a final sedimentation tank of heavy water, sewage, and wastewater treatment plants. It is related with the ultrasonic method used for microbial disinfection. Ultrasonic wave is used to destroy sludge microorganisms in sewage or wastewater treatment, and to dissolve organic matter in microorganisms, or to disinfect volatile organic substances (VOC) or disinfect microorganisms by treating water, water, and sewage. It is a technique used for the purpose. According to the configuration, the ultrasonic generator is attached to the sludge conveying pipe of the sewage or wastewater treatment process or inserted into the conveying pipe to generate ultrasonic waves, and the ultrasonically-treated sludge is placed in an anaerobic tank, an anaerobic tank or an aerobic tank to provide nitrogen, phosphorus, and volatile organic substances ( A method and apparatus for removing VOC).
Description
본 발명은 초음파를 이용하여 중수, 하수나 폐수의 질소, 인, 휘발성유기물질(VOC)를 제거하거나 혐기성소화조에 사용하여 슬러지를 감량할 목적으로 사용하거나 중수나 하·폐수처리장의 최종침전조로부터 방류되는 처리수 또는 정수장 미생물의 소독에 초음파를 활용하는 방법과 장치에 관한 것이다.구체적으로 설명하면, 초음파를 이용하여 하수나 폐수처리공정중 외부반송슬러지의 미생물을 파괴하여 미생물내의 유기물을 용출시키는 방법 또는 상수, 중수, 하수의 처리수 또는 처리과정중에 초음파를 사용하여 휘발성유기물질(VOC)를 분해하거나 미생물을 소독하는 방법이다. 본 발명의 구성은 초음파발생장치를 하·폐수공정의 반송슬러지관에 부착하거나 반송관에 넣어서 초음파를 발생시키고, 초음파 조사된 슬러지를 혐기조나 무산소조 또는 호기조에 넣어 질소와 인, VOC를 제거하는데 사용하는 기술이다.액체매질에 초음파를 조사하면 수없이 많은 공동이 발생하며 공동화 기포들은 부압이 걸려 깨지면서 수천기압에 달하는 충격파를 발생시키고 이때 높은 온도와 파열압력이 발생되면서 높은 에너지에 의해 화학반응이 촉진되어 휘발성유기화합물을 분해제거하거나 미생물을 살균하거나 미생물을 파괴하여 유기물, 인 질소 등을 용출시키게 된다.본 발명의 목적은 하수나 폐수처리공정중 내,외부반송슬러지의 미생물을 파괴하여 미생물내의 유기물을 용출시켜 유입원수의 탄소원을 충분히 사용토록해 오염물질 제거효율을 높이고자 함이다.본 발명의 또다른 목적은 상수, 중수, 하수의 처리수 또는 처리과정중에 초음파를 사용하여 휘발성유기물질(VOC)를 분해하거나 미생물을 효과적으로 소독하는 방법을 제공하고자 함이다.The present invention is to remove the nitrogen, phosphorus, volatile organic substances (VOC) of heavy water, sewage or wastewater by using ultrasonic waves or to reduce sludge by using in an anaerobic digestion tank or discharged from the final sedimentation tank of heavy water or sewage and wastewater treatment plant The present invention relates to a method and apparatus for utilizing ultrasonic waves for disinfection of treated microorganisms or water purification plants. Specifically, a method for dissolving microorganisms in external transport sludge during the sewage or wastewater treatment process using ultrasonic waves to elute organic matter in microorganisms. Alternatively, it is a method of decomposing volatile organic substances (VOC) or disinfecting microorganisms using ultrasonic waves during treatment of water, heavy water and sewage, or during treatment. The configuration of the present invention is used to remove the nitrogen, phosphorus and VOC by attaching the ultrasonic generator to the conveying sludge tube of the sewage and wastewater process or by putting the ultrasonic wave in the anaerobic tank, anoxic tank or an aerobic tank. When ultrasonic waves are irradiated to a liquid medium, numerous cavities are generated, and cavitation bubbles are broken under negative pressure, generating shock waves reaching thousands of atmospheres, and high temperatures and burst pressures generate chemical energy by high energy. The organic matter, phosphorus nitrogen, and the like are eluted by decomposing and removing volatile organic compounds, sterilizing microorganisms or destroying microorganisms. An object of the present invention is to destroy organic matters in internal and external transport sludge during sewage or wastewater treatment processes. To remove the pollutants by making full use of the carbon source of the influent. It is another object of the present invention to provide a method for decomposing volatile organic substances (VOC) or effectively disinfecting microorganisms using ultrasonic waves during treatment of water, heavy water and sewage, or during treatment. .
종래의 기술은 인을 제거하기 위하여 유입원수를 혐기조에 넣고 인을 용출시킴으로써 무산소조에서 충분한 탄소원으로 작용하지 못하였으며 슬러지나 방류수중의 휘발성유기물질을 제거하기 위하여 분말활성탄등을 사용하였으나 이는 비용이 많이 들고 분말활성탄에 의한 탁도저하, 운전이 용이하지 못한 문제점이 있다.그리고 하·폐수의 질소와 인을 제거하기 위하여 사용되는 A2O공정은 혐기조에서 인을 용출시켜 호기조에서 인을 과잉섭취하여 인이 흡수된 슬러지를 제거함으로써 인을 제거하는 공정이다. 그러나 상기 공정의 혐기조에 원수가 유입될 경우 원수중의 탄소원이 반송슬러지중에 함유된 질산성질소를 제거하거나 인을 용출시키는데 사용되어 무산소조의 탄소원으로 작용하지 못하게 되는 문제점이 있다.한편, 하·폐수의 처리수를 방류할 경우 휘발성유기물질(VOC)이 그대로 배출되며 소독과정을 거치지 않아 하천에 악영향을 미치고 있다. 중수처리 또는 정수장의 소독과정에서 사용하는 염소소독의 경우 발암성물질인 트리할로메탄(THM)이나 유기염소계 화합물을 발생시켜 인체에 해를 끼치고 있다.본 발명은 하·폐수처리과정의 외부반송슬러지나 내부반송슬러지의 미생물을 파괴하여 질산성질소와 인을 용출시키고, 휘발성유기물질을 제거함으로써 처리장으로 유입되는 유입원수가 충분한 탄소원으로 활용될 수 있도록 한다, 아울러 본 발명이 혐기조나 혐기성소화조에 활용되어 슬러지를 파괴하고 휘발성유기물질을 제거하고 슬러지를 감량시키는데 이용된다.또한 하·폐수처리의 최종침전지나 처리수관에 사용하거나 중수, 정수장의 처리수에 사용되어 처리수중의 휘발정유기물을 분해하고 미생물을 소독하는 과정에 사용되어 유해성을 예방할 수 있다.Conventional techniques have not used sufficient carbon source in an anoxic tank by inflowing inlet water into an anaerobic tank to remove phosphorus and using powdered activated carbon to remove volatile organic substances in sludge or effluent. In addition, the turbidity decrease due to the activated activated carbon powder and the operation is not easy.The A2O process, which is used to remove nitrogen and phosphorus from sewage and wastewater, elutes phosphorus in an anaerobic tank and overtakes phosphorus in an aerobic tank to absorb phosphorus. It is a process of removing phosphorus by removing the sludge. However, when the raw water is introduced into the anaerobic tank of the process, there is a problem that the carbon source in the raw water is used to remove nitrate nitrogen contained in the conveying sludge or elute phosphorus, so that it does not act as a carbon source of the anoxic tank. When the treated water is discharged, volatile organic substance (VOC) is discharged as it is, and it does not go through the sterilization process, which adversely affects the stream. In the case of chlorine disinfection used in the treatment of heavy water treatment or water purification plant, trihalomethane (THM) or organic chlorine compounds, which are carcinogenic substances, are generated to harm the human body. By destroying sludge or internal transport sludge, eluting nitrogen nitrate and phosphorus, and removing volatile organic substances, the inflow water flowing into the treatment plant can be utilized as a sufficient carbon source, and the present invention can be used for anaerobic or anaerobic digestion tanks. It is used to destroy sludge, remove volatile organic substances and reduce sludge.It is also used for final sedimentation or treatment water pipe of sewage and wastewater treatment, or for treatment water of heavy water and water purification plant to decompose volatile organic matter in treated water. It can be used in the process of disinfecting microorganisms to prevent the harmful effects.
본 발명은 상기한 종래의 문제점을 해결하기 위하여 초음파발생장치를 혐기조에 넣거나 반송슬러지관에 부착 또는 반송관에 넣어서 초음파를 발생시켜 반송슬러지의 미생물을 파괴하여 유기물, 질산성질소, 인을 용출시키거나 휘발성유기물질(VOC)를 제거함으로써 슬러지 감량에 활용하고, 처리장에 유입되는 원수가 충분한 탄소원으로 사용될 수 있도록 하여 질소제거효과를 증진시킨다. 또한 중수 및 정수장이나 하수나 폐수처리공정의 최종침전지나 처리수관에 본 발명 기술이 사용되어 휘발성유기물질(VOC)을 분해제거하고 미생물 소독에 효과적으로 사용될 수 있다.The present invention, in order to solve the above-mentioned problems, by putting the ultrasonic generator in the anaerobic tank or attached to the conveying sludge tube or put into the conveying tube to generate ultrasonic waves to destroy the microorganism of the conveying sludge to elute organic matter, nitrate nitrogen, phosphorus. Or volatile organic substances (VOC) to reduce sludge and increase the nitrogen removal effect by ensuring that raw water entering the treatment plant can be used as a sufficient carbon source. In addition, the present invention is used in the final sedimentation or treated water pipe of the heavy water and water purification plant or sewage or wastewater treatment process can be effectively used to decompose and remove volatile organic substances (VOC) and microbial disinfection.
도 1은 본 발명에 따른 초음파를 이용한 질소, 인, 휘발성유기화합물(VOC) 제거시스템(UNR시스템)의 개략적인 구성도이다.1 is a schematic diagram of a nitrogen, phosphorus, volatile organic compound (VOC) removal system (UNR system) using ultrasonic waves according to the present invention.
도 2는 본 발명에 따른 초음파를 이용한 질소, 인, 휘발성유기화합물(VOC) 제거시스템(UNR시스템)의 변형예를 도시한 개략적인 구성도이다.Figure 2 is a schematic diagram showing a modification of the nitrogen, phosphorus, volatile organic compound (VOC) removal system (UNR system) using ultrasonic waves according to the present invention.
본 발명은 상기 목적을 달성하기 위하여 음행주파수는 20㎑이상, 음향강도는 1kW/㎡이상인 초음파발생장치를 사용하여 하·폐수처리장의 혐기조나 혐기성소화조에 넣거나 하·폐수처리과정의 반송슬러지관에 부착하거나 관에 넣어서 초음파를 발생시킨다.상기 장치에서 발생된 초음파에 의해 공동화 기포들의 충격파에 의해 발생되는 높은 온도와 에너지를 이용하여 외부 및 내부반송슬러지의 미생물을 파괴하여 질산성질소와 인을 용출시키고, 유기물용출 및 유기산반응을 촉진시키고, 휘발성유기물질(VOC)을 제거한다.상기 장치를 혐기성소화조에 사용하는 경우에는 슬러지내 미생물을 파괴하여 슬러지의 감량 또는 유기산을 촉진하는 것으로 사용된다. 유입원수는 무산소조에 넣어 호기조에서 유입된 내부반송수를 탈질시키는 탄소원으로 사용하거나 일부를 혐기조에 넣어 외부반송슬러지의 미생물의 인 용출을 돕는 탄소원으로 사용하도록 한다.한편, 초음파장치를 하수처리장이나 폐수처리장의 최종침전지 유출관이나 상부에 설치하여 처리수의 휘발성유기물질(VOC)를 제거하거나 미생물을 살균하는 장치로 사용한다. 또한 중수도나 정수장의 처리수조나 처리수관에 사용하여 처리수의 휘발성유기물질(VOC)를 분해제거하고 미생물을 소독하는 공정으로 사용한다.In order to achieve the above object, the present invention uses an ultrasonic wave generator having a sound frequency of 20 kHz or more and an acoustic intensity of 1 kW / m 2 or more into an anaerobic tank or an anaerobic digestion tank of a sewage and wastewater treatment plant or into a conveying sludge tube of a wastewater treatment process. Ultrasonic waves are generated by attaching them to a tube or by placing them in a tube. The ultrasonic waves generated by the device use high temperature and energy generated by shock waves of cavitation bubbles to destroy microorganisms in external and internal transport sludge to elute nitrate nitrogen and phosphorus. And promote organic elution and organic acid reactions and remove volatile organic matter (VOC). When the device is used in an anaerobic digestion tank, it is used to destroy sludge microorganisms and to promote sludge reduction or organic acid. Inflow water is used as a carbon source to denitrate the internal transport water introduced from an aerobic tank, or a part is put in an anaerobic tank as a carbon source to help withdraw microorganisms from external transport sludge. Installed in the final sedimentation outlet or upper part of the treatment plant, it is used as a device to remove volatile organic substances (VOC) from treated water or to sterilize microorganisms. In addition, it is used in the treatment water tank or treatment water pipe of heavy water or water treatment plant to decompose and remove volatile organic substances (VOC) of treated water and to disinfect microorganism.
<실시예 1>초음파발생장치를 혐기조에 유입되는 반송관에 부착하여 외부반송슬러지를 음향주파수 20㎑, 음향강도 4kW/㎡이상인 초음파를 발생하여 1분당 520㎖와 1분당 2000㎖이 흐르는 외부반송슬러지에 초음파를 조사하였다. 초음파를 조사하지 않은 슬러지와 흐르는 관의 슬러지에 초음파를 발생시켜 슬러지의 온도와 pH를 조사하고 슬러지의 미생물파괴정도와 미생물의 파괴에 의한 COD, PO4-P, NO3-N, NH3-N, 총질소, 총인을 파악하였다. 초음파를 조사한 경우 미생물이 파괴되고 휘발성유기화합물이 제거되었으며 PO4-P의 용출현상이 나타났다.<Example 1> An ultrasonic wave generator was attached to a conveying pipe flowing into an anaerobic tank, and the external conveying sludge generated ultrasonic waves having an acoustic frequency of 20 Hz and an acoustic intensity of 4 kW / m 2 or more, and the external conveying stream flowed at 520 ml per minute and 2000 ml per minute. The sludge was irradiated with ultrasound. Ultrasonic waves are generated in the sludge and the sludge of the flowing tube to investigate the temperature and pH of the sludge, and COD, PO 4 -P, NO 3 -N, NH 3- N, total nitrogen and total phosphorus were identified. Ultrasonic irradiation resulted in the destruction of microorganisms, the removal of volatile organic compounds and the dissolution of PO 4 -P.
<실시예 2>초음파를 혐기조에 부착하여 외부반송슬러지를 음향주파수 20㎑, 음향강도 4kW/㎡이상인 초음파를 발생하여 5분, 10분, 20분, 30분을 조사하였다. 초음파를 조사하지 않은 슬러지와 혐기조의 슬러지에 초음파를 발생시켜 슬러지의 온도와 pH를 조사하고 슬러지의 미생물파괴정도와 미생물의 파괴에 의한 COD, PO4-P, NO3-N, NH3-N, 총질소, 총인을 파악하였다. 초음파를 조사한 경우 휘발성유기화합물이 제거되었으며 PO4-P의 용출현상이 나타났다.<Example 2> Ultrasonic waves were attached to an anaerobic tank, and the external conveying sludge generated ultrasonic waves having an acoustic frequency of 20 Hz and an acoustic intensity of 4 kW / m 2 or more, and irradiated for 5 minutes, 10 minutes, 20 minutes, and 30 minutes. Ultrasonic wave is generated in the sludge and anaerobic sludge which do not irradiate the ultrasonic wave to investigate the temperature and pH of the sludge, and COD, PO 4 -P, NO 3 -N, NH 3 -N , Total nitrogen and total phosphorus were identified. Ultrasonic irradiation removed volatile organic compounds and showed the dissolution of PO 4 -P.
<실시예 3>초음파를 침전지에 부착하여 음향주파수 20㎑, 음향강도 4kW/㎡이상인 초음파를 발생하여 처리수에 5분, 10분, 20분, 30분을 조사하였다. 초음파를 조사하지 않은 처리수와 최종침전지의 처리수에 초음파를 발생시킨 처리수의 온도와 pH를 조사하고 처리수의 미생물파괴정도와 미생물의 파괴에 의한 COD, PO4-P, NO3-N, NH3-N, 총질소, 총인을 파악하였다. 초음파를 조사한 경우 미생물이 살균되었으며 휘발성유기화합물이 제거되었으며 PO4-P의 용출현상이 나타났다.<Example 3> Ultrasonic waves were attached to the sedimentation basin to generate ultrasonic waves having an acoustic frequency of 20 Hz and an acoustic intensity of 4 kW / m 2 or more, and the treated water was irradiated for 5 minutes, 10 minutes, 20 minutes, and 30 minutes. Investigate the temperature and pH of the treated water without ultrasonication and the treated water of the final settler with the ultrasonication and the COD, PO 4 -P, NO 3 -N , NH 3 -N, total nitrogen and total phosphorus were identified. Ultrasonic irradiation showed microorganisms sterilized, volatile organic compounds were removed and PO 4 -P dissolution was observed.
<실시예 4>초음파를 폭기조에서 최종침전지에 유입되는 처리관에 부착하여 포기조에서 최종침전지로 유입되는 슬러지를 음향주파수 20㎑, 음향강도 4kW/㎡이상인 초음파를 발생하여 1분당 520㎖와 1분당 2000㎖이 흐르는 외부반송슬러지에 초음파를 조사하였다. 초음파를 조사하지 않은 슬러지와 흐르는 관의 슬러지에 초음파를 발생시켜 슬러지의 온도와 pH를 조사하고 슬러지의 미생물파괴정도와 미생물의 파괴에 의한 COD, PO4-P, NO3-N, NH3-N, 총질소, 총인, 슬러지의 침강성을 파악하였다. 초음파를 조사한 경우 휘발성유기화합물이 제거되었으며 미생물의 살균현상이 나타나고 슬러지의 침강성이 향상되었다.<Example 4> Ultrasonic waves are attached to the processing tube flowing into the final settler in the aeration tank, and sludge flowing into the final settler in the aeration tank generates ultrasonic waves with an acoustic frequency of 20 kHz and an acoustic intensity of 4 kW / m2 or more. Ultrasonic wave was irradiated to 2000 ml of external transport sludge. Ultrasonic waves are generated in the sludge and the sludge of the flowing tube to investigate the temperature and pH of the sludge, and COD, PO 4 -P, NO 3 -N, NH 3- The sedimentation properties of N, total nitrogen, total phosphorus and sludge were determined. Ultrasonic irradiation removed volatile organic compounds, showed microbial sterilization and improved sludge settling.
본 발명은 하수나 폐수처리과정중 반송슬러지의 미생물을 파괴하여 미생물내의 유기물, 질산성질소, 용존성인, 휘발성유기화합물(VOC)을 용출시키고 분해 제거함으로써 유입원수가 최대한 탄소원으로 활용될 수 있도록 하여 오염물질제거효율을 극대화하는 효과가 있다.또한 본 발명에 따른 초음파장치를 하수처리장이나 폐수처리장의 최종침전지의 유출관이나 상부에 설치하여 최종침전지에서 처리되어 배출되는 처리수의 휘발성유기물질(VOC)을 제거하거나 미생물을 살균하는 장치로 사용하며 중수도나 정수장의 처리수조나 처리수관에 사용하여 처리수의 휘발성유기물질(VOC)을 분해 제거하고 미생물을 소독하는 공정으로 사용하여 기존의 처리수에 있는 휘발성유기화합물을 제거하고 소독을 하여 별도의 처리과정 없이도 처리수를 깨끗이 할 수 있고 경제성을 제고시킬 수 있다.The present invention destroys microorganisms in the return sludge during sewage or wastewater treatment so as to elute and decompose organic matter, nitrate nitrogen, and dissolved volatile organic compounds (VOC) in the microorganisms so that inflow water can be utilized as a carbon source as much as possible. In addition, the ultrasonic device according to the present invention is installed in the outlet pipe or the upper part of the final settler of a sewage treatment plant or a wastewater treatment plant, and the volatile organic matter (VOC) of the treated water discharged from the final settler is discharged. ) Is used to remove microorganisms or sterilize microorganisms, and it is used for treatment tank or treatment water pipe of heavy water or water purification plant to decompose and remove volatile organic substance (VOC) of treated water and to disinfect microorganisms. By removing and disinfecting volatile organic compounds, the treated water can be cleaned without any additional treatment. And it can improve the economy.
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