JPWO2019088186A1 - 粉末状組成物 - Google Patents
粉末状組成物 Download PDFInfo
- Publication number
- JPWO2019088186A1 JPWO2019088186A1 JP2019550464A JP2019550464A JPWO2019088186A1 JP WO2019088186 A1 JPWO2019088186 A1 JP WO2019088186A1 JP 2019550464 A JP2019550464 A JP 2019550464A JP 2019550464 A JP2019550464 A JP 2019550464A JP WO2019088186 A1 JPWO2019088186 A1 JP WO2019088186A1
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- powder
- powdery composition
- present
- oil
- Prior art date
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- UKMWFJSTYVOROV-UHFFFAOYSA-N bis(2,2-dimethylpropyl) butanedioate Chemical compound CC(C)(C)COC(=O)CCC(=O)OCC(C)(C)C UKMWFJSTYVOROV-UHFFFAOYSA-N 0.000 description 1
- BXRHTJSJAFIFSR-UHFFFAOYSA-N bis(2,2-dimethylpropyl) pentanedioate Chemical compound CC(C)(C)COC(=O)CCCC(=O)OCC(C)(C)C BXRHTJSJAFIFSR-UHFFFAOYSA-N 0.000 description 1
- SWQUTKGVXGTROS-UHFFFAOYSA-N bis(2-ethoxyethyl) butanedioate Chemical compound CCOCCOC(=O)CCC(=O)OCCOCC SWQUTKGVXGTROS-UHFFFAOYSA-N 0.000 description 1
- 235000019437 butane-1,3-diol Nutrition 0.000 description 1
- 150000007942 carboxylates Chemical class 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 229940082500 cetostearyl alcohol Drugs 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- SASYSVUEVMOWPL-NXVVXOECSA-N decyl oleate Chemical compound CCCCCCCCCCOC(=O)CCCCCCC\C=C/CCCCCCCC SASYSVUEVMOWPL-NXVVXOECSA-N 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 125000004386 diacrylate group Chemical group 0.000 description 1
- 150000008050 dialkyl sulfates Chemical class 0.000 description 1
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical class OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 1
- 229940119676 diethoxyethyl succinate Drugs 0.000 description 1
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 1
- 229940031578 diisopropyl adipate Drugs 0.000 description 1
- 229940031569 diisopropyl sebacate Drugs 0.000 description 1
- XFKBBSZEQRFVSL-UHFFFAOYSA-N dipropan-2-yl decanedioate Chemical compound CC(C)OC(=O)CCCCCCCCC(=O)OC(C)C XFKBBSZEQRFVSL-UHFFFAOYSA-N 0.000 description 1
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 229960000735 docosanol Drugs 0.000 description 1
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- 150000002148 esters Chemical class 0.000 description 1
- VYYBMZHORYWQJZ-UHFFFAOYSA-N ethyl 2,2-diethylhexanoate Chemical compound CCCCC(CC)(CC)C(=O)OCC VYYBMZHORYWQJZ-UHFFFAOYSA-N 0.000 description 1
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- 238000000227 grinding Methods 0.000 description 1
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- MNWFXJYAOYHMED-UHFFFAOYSA-M heptanoate Chemical compound CCCCCCC([O-])=O MNWFXJYAOYHMED-UHFFFAOYSA-M 0.000 description 1
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- IPCSVZSSVZVIGE-UHFFFAOYSA-M hexadecanoate Chemical compound CCCCCCCCCCCCCCCC([O-])=O IPCSVZSSVZVIGE-UHFFFAOYSA-M 0.000 description 1
- XJNUECKWDBNFJV-UHFFFAOYSA-N hexadecyl 2-ethylhexanoate Chemical compound CCCCCCCCCCCCCCCCOC(=O)C(CC)CCCC XJNUECKWDBNFJV-UHFFFAOYSA-N 0.000 description 1
- DWMMZQMXUWUJME-UHFFFAOYSA-N hexadecyl octanoate Chemical compound CCCCCCCCCCCCCCCCOC(=O)CCCCCCC DWMMZQMXUWUJME-UHFFFAOYSA-N 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
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- 239000007791 liquid phase Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
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- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
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- 150000002736 metal compounds Chemical class 0.000 description 1
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
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- 229940105132 myristate Drugs 0.000 description 1
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- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
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- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
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- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
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- XOJVVFBFDXDTEG-UHFFFAOYSA-N pristane Chemical compound CC(C)CCCC(C)CCCC(C)CCCC(C)C XOJVVFBFDXDTEG-UHFFFAOYSA-N 0.000 description 1
- WHMQHKUIPUYTKP-UHFFFAOYSA-N propane-1,2,3-triol;propanoic acid Chemical compound CCC(O)=O.OCC(O)CO WHMQHKUIPUYTKP-UHFFFAOYSA-N 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
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- 229910001388 sodium aluminate Inorganic materials 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
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- 150000003432 sterols Chemical class 0.000 description 1
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- 238000003756 stirring Methods 0.000 description 1
- 230000000475 sunscreen effect Effects 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 description 1
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- DZKXJUASMGQEMA-UHFFFAOYSA-N tetradecyl tetradecanoate Chemical compound CCCCCCCCCCCCCCOC(=O)CCCCCCCCCCCCC DZKXJUASMGQEMA-UHFFFAOYSA-N 0.000 description 1
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- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 description 1
- 235000013769 triethyl citrate Nutrition 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- DUXYWXYOBMKGIN-UHFFFAOYSA-N trimyristin Chemical compound CCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCC DUXYWXYOBMKGIN-UHFFFAOYSA-N 0.000 description 1
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 1
- 229940099259 vaseline Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
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- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
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- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
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- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 229960001763 zinc sulfate Drugs 0.000 description 1
- 229910000368 zinc sulfate Inorganic materials 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
Description
(a)フッ素処理粉体
本発明に用いられる(a)フッ素処理粉体(以下、単に「(a)成分」と称する場合がある)は、粉体表面にフッ素基を付与して撥水性・撥油性をもたせるようにしたものや、粉体自身がフッ素基を有して撥水性・撥油性をもつものなどを広く包含する。具体的には、(i)フッ素基を有する分子で粉体表面の一部〜全部を処理した処理粉体、(ii)フッ素基を含む高分子粉体、等が例示されるが、これら例示に限定されるものでない。
本発明の(b)常温で液状の油性成分(以下、単に「(b)成分」と称する場合がある)は、特に限定されるものではなく、化粧品、医薬部外品又は医薬品等に用いられる物であれば何ら問題なく使用でき、1種または2種以上の油性成分の混合であってよい。
本発明に用いられる(c)45mN/m以上65mN/m以下の表面張力値を有する水性成分(以下、単に「(c)成分」と称する場合がある)は、化粧料に一般的に配合される品質の蒸留水、イオン交換水、精製水に各種保湿剤や薬剤等を溶解した水性成分であって、表面張力値が45mN/m以上65mN/m以下、好ましくは47mN/m以上65mN/m以下の水性成分を指す。ここで、「(c)成分の表面張力値」とは、液状をなす(c)成分全体の表面張力を、表面張力測定装置DCAT(英弘精機社製)を用いたウィルヘルミプレート法により測定した値をいう。(c)成分全体としての表面張力値が前記範囲を満足する限りにおいて、(c)成分の構成成分としての各水性成分が前記表面張力値の範囲を満たさないものであっても用いることができる。
(c)成分の表面張力値が45mN/mより小さい場合には、衝撃により容易に転相(粉体が液体の中に分散された状態)し、空気を含むペースト状になり、(a)成分で安定に粉末化するのが難しくなる。65mN/mを超える場合には、組成物を肌上に塗擦した際の肌へのなじみが悪くなる。
本発明の粉末状組成物は、(a)成分に油相である(b)成分を噴霧混合したのち、続けて(c)成分(水相)を噴霧する工程により調製される。なお、油相および水相の噴霧はどちらが先でもよい。
各実施例品、比較例品の使用性(きしみ感のなさ)を、パネラー(50名)の実使用試験によって下記の基準に従って判定、評価した。
(判定基準)
著効:きしまない
有効:わずかにきしむが、使用上問題のない程度である
やや有効:ややきしむ
無効:著しくきしむ
(評価)
A:著効、有効、およびやや有効の評価をした被験者が80%以上
B:著効、有効、およびやや有効の評価をした被験者が50〜80%未満
C:著効、有効、およびやや有効の評価をした被験者が30〜50%未満
D:著効、有効、およびやや有効の評価をした被験者が30%未満
各実施例品、比較例品の使用性(なじみのよさ、みずみずしさ)を、パネラー(50名)の実使用試験によって下記の基準に従って判定、評価した。
(判定基準:なじみのよさ)
著効:肌へのなじみがよい
有効:肌へのなじみがややよい
やや有効:あまり肌になじまない
無効:肌へのなじみが悪い
(判定基準:みずみずしさ)
著効:みずみずしい
有効:ややみずみずしい
やや有効:あまりみずみずしくない
無効:全くみずみずしくない
(評価)
A:著効、有効、およびやや有効の評価をした被験者が80%以上
B:著効、有効、およびやや有効の評価をした被験者が50〜80%未満
C:著効、有効、およびやや有効の評価をした被験者が30〜50%未満
D:著効、有効、およびやや有効の評価をした被験者が30%未満
各実施例品、比較例品のかさつき抑制効果を、パネラー(50名)の3日間実使用試験によって下記の基準に従って判定、評価した。
(判定基準)
著効:非常にかさつきが抑制された
有効:ややかさつきが抑制された
やや有効:ややかさつきが抑制されたがあまり変化ない
無効:かさつきが悪化した
(評価)
A:著効、有効、およびやや有効の評価をした被験者が80%以上
B:著効、有効、およびやや有効の評価をした被験者が50〜80%未満
C:著効、有効、およびやや有効の評価をした被験者が30〜50%未満
D:著効、有効、およびやや有効の評価をした被験者が30%未満
紫外線吸収剤を含む基剤を調製し、PMMAプレートに一定量を塗布し、UVスペクトルを測定した。このプレートを水洗し1分後にUVスペクトルを測定し、水洗前を1としたときのスペクトルの積分値の比を算出した。
白金製のウィルヘルミプレートを用い、表面張力測定装置DCAT(英弘精機社製)にて表面張力値を測定した。油相に固形油分を含む場合には80℃で溶解した後に測定した。
調製した基剤1gを30mlの樹脂容器に入れ、ペイントシェーカーで振とうさせ、ペースト状態になるまでの時間を測定した。ペースト状態になるまでの時間が長いほど耐衝撃性が高いことを示す。
調製した基剤3gを30mlの樹脂容器に入れ、約30cm×20cm×10cmのダンボール箱にパッキンなしで10個を入れ、東京−大阪間をトラック便で往復輸送した。1個以上ペースト状になっていた場合には、不合格(不良)とした。
下記表1に示す組成で粉末状化粧料を調製した。前記試験方法により、各化粧料について粉末化の可否、使用性(きしみ感のなさ、みずみずしさ、なじみのよさ)、耐水性、ペーストになるまでの時間(耐衝撃性)、輸送テストを評価した。なお、表1中のフッ素処理マイカは「EPF MICA S」(大東化成工業社製)を用い、フッ素処理合成酸化チタンは「FSA−3 TiO2 CR−50」(大東化成工業社製)を用い、シリコーン処理タルクは「SA−タルク JA−13R」(三好化成工業社製)と「SA−タルク JA−46R」(三好化成工業社製)を混合して用いた。
(4)〜(6)を混合、溶解した油相を(1)〜(3)の粉体にスプレーし、混合、撹拌したのち、(7)〜(9)を混合した水相をさらにスプレーし、混合、攪拌、容器に充填した。
下記表2に示す組成で粉末状化粧料を調製した。前記試験方法により、各化粧料について使用性(きしみ感のなさ、みずみずしさ、なじみのよさ)、かさつき抑制効果、ペーストになるまでの時間(耐衝撃性)、輸送テストを評価した。なお、表2中のフッ素処理セリサイトは、「PF−10 AL−10 セリサイトFSE」(大東化成工業社製)を用いた。
(2)〜(4)を混合し、溶解した油相を(1)の粉体にスプレーし、混合および撹拌したのち、(5)〜(9)を混合した水相をさらにスプレーし、混合および攪拌して、容器に充填した。
下記表3に示す組成を用いて、日焼け止め効果を有するスキンケアパウダー(実施例4)およびデコルテ用ボディーパウダー(実施例5)を調製した。なお、表3中のフッ素処理タルクおよびフッ素処理酸化チタンは、それぞれタルクと微粒子酸化チタンに水酸化アルミニウムを処理した上から、ペルフルオロアルキルリン酸エステルセリサイト表面に処理した、PFX−10シリーズ(いずれも大東化成工業社製)を用いた。
(6)〜(9)を混合し、溶解した水相を(1)および(2)の粉体にスプレーし、混合および撹拌したのち、(3)〜(5)を混合した油相をさらにスプレーし、混合および攪拌して、容器に充填した。
下記表4に示す組成を用いて、パウダリーファンデーションを調製した。なお、表4中のフッ素処理酸化チタンは、水酸化アルミニウムを処理した酸化チタンにペルフルオロアルキルリン酸エステルを表面に処理した「PFX−5酸化チタン」(大東化成工業社製)を用いた。
均一混合した(1)〜(5)に均一溶解した(6)および(7)を噴霧し、混合および攪拌した。さらに均一溶解した(8)〜(11)を噴霧し、混合および攪拌して、容器に充填した。
Claims (7)
- (a)フッ素処理粉体、
(b)1〜50質量%の常温で液状の油性成分、
(c)45mN/m以上65mN/m以下の表面張力値を有する水性成分
を含有し、かつ、(b)成分と(c)成分の配合比が1:10〜3:1であり、塗擦により液化することを特徴とする粉末状組成物。 - (b)成分が固形油分を含まない、請求項1に記載の粉末状組成物。
- 実質的に界面活性剤を含まない、請求項1に記載の粉末状組成物。
- (a)成分の粉体が、タルク、カオリン、無水ケイ酸、サポナイト、セリサイト、マイカの中から選ばれる1種または2種以上である、請求項1から3のいずれか1項に記載の粉末状組成物。
- (a)成分を10〜65質量%含有する、請求項1から4のいずれか1項に記載の粉末状組成物。
- (c)成分を15〜70質量%含有する、請求項1から5のいずれか1項に記載の粉末状組成物。
- (a)成分に(b)成分を噴霧する工程、および、前記工程で調製された粉体に(c)成分を噴霧する工程、あるいは、
(a)成分に(c)成分を噴霧する工程、および、前記工程で調製された粉体に(b)成分を噴霧する工程、
を含む、請求項1に記載の粉末状組成物の製造方法。
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