JPS6485265A - Production of colorless rosin - Google Patents
Production of colorless rosinInfo
- Publication number
- JPS6485265A JPS6485265A JP24224187A JP24224187A JPS6485265A JP S6485265 A JPS6485265 A JP S6485265A JP 24224187 A JP24224187 A JP 24224187A JP 24224187 A JP24224187 A JP 24224187A JP S6485265 A JPS6485265 A JP S6485265A
- Authority
- JP
- Japan
- Prior art keywords
- rosin
- production
- purified
- palladium carbon
- colorless
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 title abstract 7
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 title abstract 7
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 title abstract 7
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000000306 component Substances 0.000 abstract 2
- UKVIEHSSVKSQBA-UHFFFAOYSA-N methane;palladium Chemical compound C.[Pd] UKVIEHSSVKSQBA-UHFFFAOYSA-N 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 238000007323 disproportionation reaction Methods 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 230000009965 odorless effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; OIL DRYING AGENTS, i.e. SICCATIVES; TURPENTINE
- C09F1/00—Obtaining purification, or chemical modification of natural resins, e.g. oleo-resins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Developing Agents For Electrophotography (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Color Printing (AREA)
Abstract
PURPOSE:To obtain rosin which is colorless and odorless and excels in thermal stability, by hydrogenating a purified disproportionated rosin. CONSTITUTION:Rosin (a) (e.g., gum rosin) is reacted by heating at 100-300 deg.C for 1-8hr in the presence of 0.01-3wt.%, based on component (a), a disproportiona tion catalyst (e.g., palladium carbon) (b) to obtain disproportionated rosin. The rosin is purified by, for example, distillation at 200-300 deg.C in a vacuum of 1-10mmHg, and then hydrogenated at 100-300 deg.C at an initial pressure of hydrogen of 50-200kg/cm<2> in the presence of 0.01-3wt.%, based on compo nent A, hydrogenation catalyst (B) (e.g., palladium carbon).
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62242241A JP2539851B2 (en) | 1987-09-26 | 1987-09-26 | Method for producing colorless rosin |
US07/248,704 US4906733A (en) | 1987-01-29 | 1988-09-23 | Process for preparing colorless rosin |
DE19883832639 DE3832639C2 (en) | 1987-09-26 | 1988-09-26 | Process for producing a colorless rosin |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP62242241A JP2539851B2 (en) | 1987-09-26 | 1987-09-26 | Method for producing colorless rosin |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS6485265A true JPS6485265A (en) | 1989-03-30 |
JP2539851B2 JP2539851B2 (en) | 1996-10-02 |
Family
ID=17086340
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP62242241A Expired - Lifetime JP2539851B2 (en) | 1987-01-29 | 1987-09-26 | Method for producing colorless rosin |
Country Status (2)
Country | Link |
---|---|
JP (1) | JP2539851B2 (en) |
DE (1) | DE3832639C2 (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH02145668A (en) * | 1988-11-28 | 1990-06-05 | Harima Chem Inc | Production of hydrogenated rosin |
JPH03115480A (en) * | 1989-09-29 | 1991-05-16 | Arakawa Chem Ind Co Ltd | Manufacture of colorless glycidyl ester of rosin |
WO1994026833A1 (en) * | 1993-05-18 | 1994-11-24 | Arakawa Kagaku Kogyo Kabushiki Kaisha | Process for producing colorless rosin |
JPH08259897A (en) * | 1995-03-22 | 1996-10-08 | Arakawa Chem Ind Co Ltd | Production of light-color rosin metal salt |
JPH10219227A (en) * | 1997-01-31 | 1998-08-18 | Arakawa Chem Ind Co Ltd | Tack-imparting resin emulsion and aqueous tacky agent composition |
JP2009191182A (en) * | 2008-02-15 | 2009-08-27 | Denki Kagaku Kogyo Kk | Chloroprene-based polymer composition, adhesive composition and method for producing the chloroprene-based polymer composition |
CN111825846A (en) * | 2020-08-12 | 2020-10-27 | 广西壮族自治区林业科学研究院 | Light-colored high-stability water-soluble rosin resin and preparation method thereof |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2011090061A1 (en) * | 2010-01-22 | 2011-07-28 | 荒川化学工業株式会社 | Easily thermally decomposable binder resin, binder resin composition and use of said composition |
KR101991355B1 (en) * | 2012-05-18 | 2019-06-20 | 아라까와 가가꾸 고교 가부시끼가이샤 | Base resin for soldering flux, soldering flux and solder paste |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58106231A (en) * | 1981-12-18 | 1983-06-24 | Nissan Motor Co Ltd | Drum brake device |
-
1987
- 1987-09-26 JP JP62242241A patent/JP2539851B2/en not_active Expired - Lifetime
-
1988
- 1988-09-26 DE DE19883832639 patent/DE3832639C2/en not_active Expired - Lifetime
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58106231A (en) * | 1981-12-18 | 1983-06-24 | Nissan Motor Co Ltd | Drum brake device |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH02145668A (en) * | 1988-11-28 | 1990-06-05 | Harima Chem Inc | Production of hydrogenated rosin |
JPH03115480A (en) * | 1989-09-29 | 1991-05-16 | Arakawa Chem Ind Co Ltd | Manufacture of colorless glycidyl ester of rosin |
WO1994026833A1 (en) * | 1993-05-18 | 1994-11-24 | Arakawa Kagaku Kogyo Kabushiki Kaisha | Process for producing colorless rosin |
US5606016A (en) * | 1993-05-18 | 1997-02-25 | Arakawa Kagaku Kogyo Kabushiki Kaisha | Process for preparing colorless rosins |
JPH08259897A (en) * | 1995-03-22 | 1996-10-08 | Arakawa Chem Ind Co Ltd | Production of light-color rosin metal salt |
JPH10219227A (en) * | 1997-01-31 | 1998-08-18 | Arakawa Chem Ind Co Ltd | Tack-imparting resin emulsion and aqueous tacky agent composition |
JP2009191182A (en) * | 2008-02-15 | 2009-08-27 | Denki Kagaku Kogyo Kk | Chloroprene-based polymer composition, adhesive composition and method for producing the chloroprene-based polymer composition |
CN111825846A (en) * | 2020-08-12 | 2020-10-27 | 广西壮族自治区林业科学研究院 | Light-colored high-stability water-soluble rosin resin and preparation method thereof |
CN111825846B (en) * | 2020-08-12 | 2021-10-22 | 广西壮族自治区林业科学研究院 | Light-colored high-stability water-soluble rosin resin and preparation method thereof |
Also Published As
Publication number | Publication date |
---|---|
JP2539851B2 (en) | 1996-10-02 |
DE3832639A1 (en) | 1989-04-06 |
DE3832639C2 (en) | 1997-05-22 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
EXPY | Cancellation because of completion of term | ||
FPAY | Renewal fee payment (prs date is renewal date of database) |
Year of fee payment: 12 Free format text: PAYMENT UNTIL: 20080708 |